CN107779275A - A kind of soaping agent and preparation method thereof - Google Patents
A kind of soaping agent and preparation method thereof Download PDFInfo
- Publication number
- CN107779275A CN107779275A CN201710859016.1A CN201710859016A CN107779275A CN 107779275 A CN107779275 A CN 107779275A CN 201710859016 A CN201710859016 A CN 201710859016A CN 107779275 A CN107779275 A CN 107779275A
- Authority
- CN
- China
- Prior art keywords
- parts
- soaping agent
- powder
- ethanol
- olein
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/30—Sulfonation products derived from lignin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/30—Amines; Substituted amines ; Quaternized amines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
- C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of soaping agent and preparation method thereof, the soaping agent is made up of the raw material of following parts by weight：20 30 parts of maleated polypropylene copolymer, 57 parts of ammonium persulfate, 5 10 parts of sodium lignin sulfonate, 5 10 parts of sodium acid carbonate, 35 parts of polymethyl siloxane, 5 10 parts of ammonium chloride, 35 parts of chitosan, 35 parts of olein, 5 10 parts of plant powder, 10 20 parts of ethanol, 35 parts of triethanolamine, 30 50 parts of deionized water.The soaping agent of the present invention is used to remove non-set reactive dye, can reduce temperature of soaping.The soaping agent manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and nontoxic, human body is not stimulated, volatility is low.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of soaping agent and preparation method thereof.
Background technology
Soap be primarily referred to as print and dye postprocessing working procedures, to fabric after dyeing and printing process, for improve its color fastness with
Gorgeous degree, with soap or detergent solution by the dyestuff without fixation, dyeing auxiliaries used, concentrator etc. on its surface in closely boiling bar
The processing technology of washing is carried out under part.
Reactive dye chromatogram is complete, and bright in colour, cost is low, and dyeing is ripe, therefore, more than 80% cellulose fiber
Dimension dyeing and stamp use reactive dye.Reactive dye species is various, and chemical constitution is various, and its reaction efficiency also respectively has difference
It is different, but they can not all react completely with cellulose fibre, in addition, while upper dye fixed fiber, dyestuff also occurs that
Hydrolysis, i.e., the active group in reactive dye is substituted by hydroxyl and forms hydrolised dye.The dyestuff of these non-sets and hydrolysis contaminate
Material, its diffusion and absorption property and original reactive dye are closely similar, therefore are readily adsorbed in fiber surface, and diffuse into
Fiber.In the case of alkaline agent and temperature, pressure, the dyestuff and hydrolised dye (loose colour) of these non-sets and part and fiber knot
Close, easily cause bleeding and recontamination, fastness to wet rubbing, dry fastness, washing fastness fastness, anti-staining performance are paid no attention to
Think.The main purpose soaped is exactly to remove loose colour, improves the quality of product.
Printing and dyeing mill enters to remove the finish applied when institute's pollutant and spinning on textile through conventional washes
Row is scrubbed, and in addition in order to remove the dyestuff contaminated on not after dyeing or stamp, is also necessary that carrying out washes soaps, to ensure to contaminate
Thing arrives at certain dyefastness.Soap all in 95-100 DEG C of progress.Temperature reduces, then dyefastness is unqualified.
Therefore it is current urgent problem to develop a kind of soaping agent of efficient cryogenic.
The content of the invention
It is an object of the invention to provide a kind of soaping agent and preparation method, is asked with solve to propose in above-mentioned background technology
Topic.
To achieve the above object, the present invention provides following technical scheme：
A kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-polypropylene copolymer 20-30 parts, mistake
Ammonium sulfate 5-7 parts, sodium lignin sulfonate 5-10 parts, sodium acid carbonate 5-10 parts, polymethyl siloxane 3-5 parts, ammonium chloride 5-10 parts,
Chitosan 3-5 parts, olein 3-5 parts, plant powder 5-10 parts, ethanol 10-20 parts, triethanolamine 3-5 parts, deionized water
30-50 parts.
Preferably, described ethanol is absolute ethyl alcohol, and purity is pure to analyze.
Preferably, described plant powder is Alose, bracketplant powder, sansevieria trifasciata powder, Aspidlsiraelatior powder, Monstera deliciosa
It is one or more than one kinds of in powder, kaffir lily powder, cactus powder.
Preferably, described a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
20 parts of thing, 5 parts of ammonium persulfate, 5 parts of sodium lignin sulfonate, 5 parts of sodium acid carbonate, 3 parts of polymethyl siloxane, 5 parts of ammonium chloride, shell gather
3 parts of sugar, 3 parts of olein, 5 parts of plant powder, 10 parts of ethanol, 3 parts of triethanolamine, 30 parts of deionized water.
Preferably, described a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
25 parts of thing, 6 parts of ammonium persulfate, 8 parts of sodium lignin sulfonate, 8 parts of sodium acid carbonate, 4 parts of polymethyl siloxane, 8 parts of ammonium chloride, shell gather
4 parts of sugar, 4 parts of olein, 8 parts of plant powder, 15 parts of ethanol, 4 parts of triethanolamine, 40 parts of deionized water.
Preferably, described a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
30 parts of thing, 7 parts of ammonium persulfate, 10 parts of sodium lignin sulfonate, 10 parts of sodium acid carbonate, 5 parts of polymethyl siloxane, 10 parts of ammonium chloride,
5 parts of chitosan, 5 parts of olein, 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, 50 parts of deionized water.
A kind of preparation method of soaping agent, is comprised the following steps that：
Step 1, deionized water 30-50 parts, maleic anhydride-polypropylene copolymer 20-30 parts, over cure are added in a kettle
Sour ammonium 5-7 parts, polymethyl siloxane 3-5 parts, rise temperature nitrogen protection, 500-1000 revs/min, stir to 50-60 DEG C
20-30 minutes；
Step 2, first by plant powder 5-10 parts, ethanol 10-20 parts, triethanolamine 3-5 parts, with ultrasonic disperse, ultrasonic work(
Rate is 500-1000W, and ultrasonic time is 20-30 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 10-20 minutes；
Step 4,30-40 DEG C is cooled to, adds sodium lignin sulfonate 5-10 parts, olein 3-5 parts, 500-1000
Rev/min, stir 20-30 minutes；
Step 5, sodium acid carbonate 5-10 parts, ammonium chloride 5-10 parts, chitosan 3-5 parts are added, 500-1000 revs/min, is stirred
Mix 10-20 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, soaping agent of the invention is used to remove non-set reactive dye, can reduce temperature of soaping,
2nd, soaping agent of the invention complies fully with the following requirement to textile process and environmental standard, is environment-friendly products.
3rd, soaping agent unfading of the invention is excellent, and strength damage is small, and chelating ability is good, does not influence premetallized dye
Metal ion.
4th, soaping agent of the invention can reduce required washing and the number soaped, and can remove the dye of non-set on fabric
Material, dye molecule is retained in dye liquor, prevents it from being deposited on fabric.
5th, soaping agent action effect of the invention is not influenceed by pH, water quality, salinity.
6th, soaping agent of the invention is all effective to all chromophoric groups of reactive dye and reactive group, also has to blend fabric
Effect.
7th, soaping agent manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic, to people
Body does not stimulate, and volatility is low.
8th, mutual compatibility between various raw materials used in soaping agent of the invention, synergy, collectively constitutes excellent performance
Product.
9th, technique is simplified, safe operation is simple, is easy to industrialized production, and use of the invention can receive good economic effect
Benefit.
Example is embodied
The invention discloses a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
Thing 20-30 parts, ammonium persulfate 5-7 parts, sodium lignin sulfonate 5-10 parts, sodium acid carbonate 5-10 parts, polymethyl siloxane 3-5 parts,
Ammonium chloride 5-10 parts, chitosan 3-5 parts, olein 3-5 parts, plant powder 5-10 parts, ethanol 10-20 parts, triethanolamine
3-5 parts, deionized water 30-50 parts.
Present invention also offers a kind of preparation method of soaping agent, comprise the following steps that：
Step 1, deionized water 30-50 parts, maleic anhydride-polypropylene copolymer 20-30 parts, over cure are added in a kettle
Sour ammonium 5-7 parts, polymethyl siloxane 3-5 parts, rise temperature nitrogen protection, 500-1000 revs/min, stir to 50-60 DEG C
20-30 minutes；
Step 2, first by plant powder 5-10 parts, ethanol 10-20 parts, triethanolamine 3-5 parts, with ultrasonic disperse, ultrasonic work(
Rate is 500-1000W, and ultrasonic time is 20-30 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 10-20 minutes；
Step 4,30-40 DEG C is cooled to, adds sodium lignin sulfonate 5-10 parts, olein 3-5 parts, 500-1000
Rev/min, stir 20-30 minutes；
Step 5, sodium acid carbonate 5-10 parts, ammonium chloride 5-10 parts, chitosan 3-5 parts are added, 500-1000 revs/min, is stirred
Mix 10-20 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
20 parts of thing, 5 parts of ammonium persulfate, 5 parts of sodium lignin sulfonate, 5 parts of sodium acid carbonate, 3 parts of polymethyl siloxane, 5 parts of ammonium chloride, shell gather
3 parts of sugar, 3 parts of olein, 5 parts of plant powder, 10 parts of ethanol, 3 parts of triethanolamine, 30 parts of deionized water.
Present invention also offers a kind of preparation method of soaping agent, comprise the following steps that：
Step 1,30 parts of deionized water, 20 parts of maleic anhydride-polypropylene copolymer, ammonium persulfate 5 are added in a kettle
Part, 3 parts of polymethyl siloxane, rise temperature nitrogen protection, 500 revs/min, stir 20 minutes to 50 DEG C；
Step 2, first by 5 parts of plant powder, 10 parts of ethanol, 3 parts of triethanolamine, with ultrasonic disperse, ultrasonic power 500W,
Ultrasonic time is 20 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,500 revs/min, stirred 10 minutes；
Step 4,30 DEG C are cooled to, 5 parts of sodium lignin sulfonate, 3 parts of olein is added, 500 revs/min, stirs 20
Minute；
Step 5,5 parts of sodium acid carbonate, 5 parts of ammonium chloride, 3 parts of chitosan are added, 500 revs/min, is stirred 10 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
25 parts of thing, 6 parts of ammonium persulfate, 8 parts of sodium lignin sulfonate, 8 parts of sodium acid carbonate, 4 parts of polymethyl siloxane, 8 parts of ammonium chloride, shell gather
4 parts of sugar, 4 parts of olein, 8 parts of plant powder, 15 parts of ethanol, 4 parts of triethanolamine, 40 parts of deionized water.
Present invention also offers a kind of preparation method of soaping agent, comprise the following steps that：
Step 1,40 parts of deionized water, 25 parts of maleic anhydride-polypropylene copolymer, ammonium persulfate 6 are added in a kettle
Part, 4 parts of polymethyl siloxane, rise temperature nitrogen protection, 900 revs/min, stir 25 minutes to 55 DEG C；
Step 2, first by 8 parts of plant powder, 15 parts of ethanol, 4 parts of triethanolamine, with ultrasonic disperse, ultrasonic power 800W,
Ultrasonic time is 25 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,900 revs/min, stirred 15 minutes；
Step 4,35 DEG C are cooled to, 8 parts of sodium lignin sulfonate, 4 parts of olein is added, 800 revs/min, stirs 25
Minute；
Step 5,8 parts of sodium acid carbonate, 8 parts of ammonium chloride, 4 parts of chitosan are added, 800 revs/min, is stirred 15 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
30 parts of thing, 7 parts of ammonium persulfate, 10 parts of sodium lignin sulfonate, 10 parts of sodium acid carbonate, 5 parts of polymethyl siloxane, 10 parts of ammonium chloride,
5 parts of chitosan, 5 parts of olein, 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, 50 parts of deionized water.
Present invention also offers a kind of preparation method of soaping agent, comprise the following steps that：
Step 1,50 parts of deionized water, 30 parts of maleic anhydride-polypropylene copolymer, ammonium persulfate 7 are added in a kettle
Part, 5 parts of polymethyl siloxane, rise temperature nitrogen protection, 1000 revs/min, stir 30 minutes to 60 DEG C；
Step 2, first by 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, with ultrasonic disperse, ultrasonic power is
1000W, ultrasonic time are 30 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,1000 revs/min, stirred 20 minutes；
Step 4,40 DEG C are cooled to, 10 parts of sodium lignin sulfonate, 5 parts of olein is added, 1000 revs/min, stirs
30 minutes；
Step 5,10 parts of sodium acid carbonate, 10 parts of ammonium chloride, 5 parts of chitosan are added, 1000 revs/min, is stirred 20 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of soaping agent, according to parts by weight, including following components：Maleic anhydride-Polypropylene copolymer
30 parts of thing, 7 parts of ammonium persulfate, 8 parts of sodium lignin sulfonate, 8 parts of sodium acid carbonate, 5 parts of polymethyl siloxane, 8 parts of ammonium chloride, shell gather
4 parts of sugar, 4 parts of olein, 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, 30 parts of deionized water.
Present invention also offers a kind of preparation method of soaping agent, comprise the following steps that：
Step 1,30 parts of deionized water, 30 parts of maleic anhydride-polypropylene copolymer, ammonium persulfate 7 are added in a kettle
Part, 5 parts of polymethyl siloxane, rise temperature nitrogen protection, 1000 revs/min, stir 30 minutes to 60 DEG C；
Step 2, first by 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, with ultrasonic disperse, ultrasonic power is
1000W, ultrasonic time are 20 minutes；
Step 3, the solution of step 2 is added in the solution of step 1,1000 revs/min, stirred 10 minutes；
Step 4,35 DEG C are cooled to, 8 parts of sodium lignin sulfonate, 4 parts of olein is added, 900 revs/min, stirs 25
Minute；
Step 5,8 parts of sodium acid carbonate, 8 parts of ammonium chloride, 4 parts of chitosan are added, 900 revs/min, is stirred 15 minutes；
Step 6, stirring is closed down, the liquid soaping agent prepared；
Step 7, stand and be cooled in stirred tank liquid soaping agent and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
Soap aftertreatment technology：Dyeing discharge opeing → cold water wash → hot water wash (50~60 DEG C) → soap (60 DEG C × 20min,
Embodiment 1,2,3,4) → peracid 0.3g/L → hot water wash (60 DEG C, 1~2), test result is as follows：
| Embodiment | Washing fastness | Fastness to rubbing | Waterflooding fastness |
| 1 | 4 | 3 | 4-5 |
| 2 | 4-5 | 3-4 | 4-5 |
| 3 | 5 | 4-5 | 4-5 |
| 4 | 4-5 | 4 | 4-5 |
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (7)
- A kind of 1. soaping agent, it is characterised in that：The soaping agent includes the raw material of following parts by weight：Maleic anhydride-polypropylene Copolymer 20-30 parts, ammonium persulfate 5-7 parts, sodium lignin sulfonate 5-10 parts, sodium acid carbonate 5-10 parts, polymethyl siloxane 3-5 Part, ammonium chloride 5-10 parts, chitosan 3-5 parts, olein 3-5 parts, plant powder 5-10 parts, ethanol 10-20 parts, three ethanol Amine 3-5 parts, deionized water 30-50 parts.
- 2. soaping agent according to claim 1, it is characterised in that：The ethanol is absolute ethyl alcohol, and purity is pure to analyze.
- 3. soaping agent according to claim 1, it is characterised in that：Described plant powder be Alose, bracketplant powder, It is one or more than one kinds of in sansevieria trifasciata powder, Aspidlsiraelatior powder, Monstera deliciosa powder, kaffir lily powder, cactus powder.
- 4. soaping agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Maleic acid 20 parts of acid anhydride-polypropylene copolymer, 5 parts of ammonium persulfate, 5 parts of sodium lignin sulfonate, 5 parts of sodium acid carbonate, 3 parts of polymethyl siloxane, 5 parts of ammonium chloride, 3 parts of chitosan, 3 parts of olein, 5 parts of plant powder, 10 parts of ethanol, 3 parts of triethanolamine, deionized water 30 Part.
- 5. soaping agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Maleic acid 25 parts of acid anhydride-polypropylene copolymer, 6 parts of ammonium persulfate, 8 parts of sodium lignin sulfonate, 8 parts of sodium acid carbonate, 4 parts of polymethyl siloxane, 8 parts of ammonium chloride, 4 parts of chitosan, 4 parts of olein, 8 parts of plant powder, 15 parts of ethanol, 4 parts of triethanolamine, deionized water 40 Part.
- 6. soaping agent according to claim 1, it is characterised in that：According to parts by weight, including following components：Maleic acid 30 parts of acid anhydride-polypropylene copolymer, 7 parts of ammonium persulfate, 10 parts of sodium lignin sulfonate, 10 parts of sodium acid carbonate, polymethyl siloxane 5 Part, 10 parts of ammonium chloride, 5 parts of chitosan, 5 parts of olein, 10 parts of plant powder, 20 parts of ethanol, 5 parts of triethanolamine, go from Sub- 50 parts of water.
- A kind of 7. preparation method of any described soaping agent in 1-6 using the claims, it is characterised in that：Specific steps It is as follows：Step 1, deionized water 30-50 parts, maleic anhydride-polypropylene copolymer 20-30 parts, ammonium persulfate are added in a kettle 5-7 parts, polymethyl siloxane 3-5 parts, rise temperature nitrogen protection, 500-1000 revs/min, stir 20-30 to 50-60 DEG C Minute；Step 2, first by plant powder 5-10 parts, ethanol 10-20 parts, triethanolamine 3-5 parts, with ultrasonic disperse, ultrasonic power is 500-1000W, ultrasonic time are 20-30 minutes；Step 3, the solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 10-20 minutes；Step 4, it is cooled to 30-40 DEG C, adds sodium lignin sulfonate 5-10 parts, olein 3-5 parts, 500-1000 revs/min Clock, stir 20-30 minutes；Step 5, sodium acid carbonate 5-10 parts, ammonium chloride 5-10 parts, chitosan 3-5 parts are added, 500-1000 revs/min, stirs 10- 20 minutes；Step 6, stirring is closed down, the liquid soaping agent prepared；Step 7, stand and be cooled in stirred tank liquid soaping agent temperature and be less than 20 DEG C, blowing encapsulation, finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859016.1A CN107779275A (en) | 2017-09-21 | 2017-09-21 | A kind of soaping agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710859016.1A CN107779275A (en) | 2017-09-21 | 2017-09-21 | A kind of soaping agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107779275A true CN107779275A (en) | 2018-03-09 |
Family
ID=61433514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710859016.1A Pending CN107779275A (en) | 2017-09-21 | 2017-09-21 | A kind of soaping agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107779275A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1198184A (en) * | 1995-08-31 | 1998-11-04 | 科尔加特·帕尔莫利弗公司 | Stable fabric softener compositions |
| CN103571645A (en) * | 2013-11-20 | 2014-02-12 | 上海德桑精细化工有限公司 | Novel cryogenic soaping agent and preparation method thereof |
| CN105524726A (en) * | 2016-01-29 | 2016-04-27 | 常州永宝利染丝有限公司 | Production method of acid soaping agent |
| CN105670833A (en) * | 2016-02-26 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | Non-foaming low-temperature soaping agent for reactive dye and preparation method thereof |
| CN105802753A (en) * | 2016-04-12 | 2016-07-27 | 湖州吉昌丝绸有限公司 | Soaping agent applicable to wool fabric |
| CN106566726A (en) * | 2016-11-14 | 2017-04-19 | 苏州联胜化学有限公司 | Low-temperature reactive dye soaping agent as well as preparation method and application thereof |
-
2017
- 2017-09-21 CN CN201710859016.1A patent/CN107779275A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1198184A (en) * | 1995-08-31 | 1998-11-04 | 科尔加特·帕尔莫利弗公司 | Stable fabric softener compositions |
| CN103571645A (en) * | 2013-11-20 | 2014-02-12 | 上海德桑精细化工有限公司 | Novel cryogenic soaping agent and preparation method thereof |
| CN105524726A (en) * | 2016-01-29 | 2016-04-27 | 常州永宝利染丝有限公司 | Production method of acid soaping agent |
| CN105670833A (en) * | 2016-02-26 | 2016-06-15 | 苏州三和开泰花线织造有限公司 | Non-foaming low-temperature soaping agent for reactive dye and preparation method thereof |
| CN105802753A (en) * | 2016-04-12 | 2016-07-27 | 湖州吉昌丝绸有限公司 | Soaping agent applicable to wool fabric |
| CN106566726A (en) * | 2016-11-14 | 2017-04-19 | 苏州联胜化学有限公司 | Low-temperature reactive dye soaping agent as well as preparation method and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| 姜生: "提高亚麻织物活性染色的皂洗牢度", 《印染》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103409244B (en) | Soaping enzyme, soaping method thereof and application of soaping enzyme in washed and dyed fabric | |
| CN103498348B (en) | A kind of salt-free low alkali colouring method shortening the reactive dyeing time | |
| CN105369584B (en) | A kind of reduction washing process in iron-free finishing process | |
| CN110172843A (en) | A kind of cold-rolling heap staining method of nylon fiber | |
| CN111172791B (en) | Enzyme dyeing one-bath dyeing process for cotton fabric | |
| CN109322178A (en) | It is a kind of to wash the/dyeing and finishing processing method of cellulose fibre intertexture jacquard fabric | |
| CN107059386B (en) | Colored velvet cold pad-batch decoloring method | |
| CN107268300B (en) | A kind of colour bar colouring method of tencel interwoven fabric | |
| CN109629255A (en) | A kind of high color fastness dyeing of terylen cotton knitting fabric | |
| CN107723118A (en) | A kind of acidic reduction cleaner and preparation method thereof | |
| CN107740288A (en) | A kind of wool anhydrous printing ink and preparation method thereof | |
| CN113957731B (en) | Process for improving fastness of soaping solution of cellulose fiber and polyester blended dark fabric | |
| CN101349021B (en) | Reactive dye post treatment accessory ingredient and processing method using the same | |
| CN111321612A (en) | One-bath dyeing process of disperse/neutral dye for polyester/viscose fabric | |
| CN106120387A (en) | A kind of dyeing of the dyeing line of silkworm silk strand reactive dye | |
| CN107779275A (en) | A kind of soaping agent and preparation method thereof | |
| CN105040477A (en) | Reactive dye printing technology of pure cotton cloth | |
| CN104818625A (en) | Pure cotton jersey reactive dye cold pad-batch dyeing method | |
| CN107740294A (en) | A kind of preparation method of dye fixing agent | |
| CN103669045B (en) | The reactive dyeing process of the dark heavy colour of a kind of real silk | |
| CN112301761A (en) | Printing method free of washing or less washing | |
| CN112252060A (en) | Polyester cotton dyeing reduction-free cleaning process | |
| CN110331603A (en) | A kind of acid dyeing and calico-printer's soap detergent composition and preparation method thereof | |
| CN103469638B (en) | A kind of washing methods improving textile color stability | |
| CN113638218B (en) | Short-process high-color-fastness improving method for polyester fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180309 |
|
| RJ01 | Rejection of invention patent application after publication |