CN107777676A - A kind of new logical oxygen device for being used to produce phosphorus trichloride - Google Patents
A kind of new logical oxygen device for being used to produce phosphorus trichloride Download PDFInfo
- Publication number
- CN107777676A CN107777676A CN201711023938.5A CN201711023938A CN107777676A CN 107777676 A CN107777676 A CN 107777676A CN 201711023938 A CN201711023938 A CN 201711023938A CN 107777676 A CN107777676 A CN 107777676A
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- CN
- China
- Prior art keywords
- oxygen
- air blowing
- stills
- phosphorus trichloride
- main
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/10—Halides or oxyhalides of phosphorus
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
Abstract
A kind of new logical oxygen device for being used to produce phosphorus trichloride, including oxygen-supplying tube and main stills for air blowing, oxygen-supplying tube is sequentially connected product feeding mouth and oxygen distributor, oxygen distributor is arranged on the bottom of main stills for air blowing, the inner hub location of the main stills for air blowing is provided with agitating device, the inwall on right side is provided with oxymeter scale, and main stills for air blowing top is provided with discharging opening, and discharging opening is connected by pipeline with secondary stills for air blowing；It is an advantage of the invention that：Working time is short, process stabilization, and reaction is fully complete, securely and reliably, saves the energy, reduces oxygen consumption, reduce environmental pollution, the device corrosion resistance is extremely strong, is advantageous to operating efficiency of keeping the safety in production and improve.
Description
Technical field
The present invention relates to chemical devices technical field, is filled more particularly, to a kind of new logical oxygen for being used to produce phosphorus trichloride
Put.
Background technology
POCl3 is the non-halogen fire-retardant for plastic of production and plasticizer as a kind of important chemical products（Such as tricresyl phosphate
Second fat）, agricultural chemical insecticide（Such as Spanon）, herbicide（Such as Acetochlor, quinoline and spirit）Primary raw material.
The logical oxygen device of production POCl3 at present, oxidation reaction, industry are directly carried out using oxygen is passed through in POCl3
It is inside to lead to oxygen reaction using in oxygen-supplying tube insertion phosphorus trichloride, is that reaction is insufficient, and draw into certain dead angle, largely to be not anti-
The oxygen answered is excessive, influences environment, in addition, can not fully react, there is an outflow of residual volume, the phosphorus trichloride in phosphorus trichloride compared with
Height, influence product purity.
The content of the invention
To overcome above mentioned problem, the present invention adopts the following technical scheme that：
A kind of new logical oxygen device for being used to produce phosphorus trichloride, including oxygen-supplying tube and main stills for air blowing, oxygen-supplying tube are sequentially connected production
Product feeding mouth and oxygen distributor, oxygen distributor are arranged on the bottom of main stills for air blowing, the inside center position of the main stills for air blowing
Agitating device is installed, the inwall on right side is provided with oxymeter scale, and main stills for air blowing top is provided with discharging opening, and discharging opening passes through pipe
Road is connected with secondary stills for air blowing.
The oxygen-supplying tube is provided with venting valve.
Divide hole provided with 400 circles in the oxygen distributor.
The agitating device is stirred using two-piece type.
The main stills for air blowing and secondary stills for air blowing use identical two.
It is an advantage of the invention that：Working time is short, process stabilization, and reaction is fully complete, securely and reliably, saves the energy, drop
Low oxygen consumption, reduces environmental pollution, and the device corrosion resistance is extremely strong, is advantageous to operating efficiency of keeping the safety in production and improve.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
Embodiment
As shown in figure 1, a kind of new logical oxygen device for being used to produce phosphorus trichloride, including oxygen-supplying tube 1 and main stills for air blowing 4,
Oxygen-supplying tube 1 is sequentially connected product feeding mouth 2 and oxygen distributor 3, and oxygen distributor 3 is arranged on the bottom of main stills for air blowing 4, described
The inner hub location of main stills for air blowing 4 is provided with agitating device 5, and the inwall on right side is provided with oxymeter scale 6, on main stills for air blowing 4
Portion is provided with discharging opening 7, and discharging opening 7 is connected by pipeline with secondary stills for air blowing 8.
The oxygen-supplying tube 1 is provided with venting valve 9.
Divide hole provided with 400 circles in the oxygen distributor 3.
The agitating device 5 is stirred using two-piece type.
The main stills for air blowing 4 and secondary stills for air blowing 8 use identical two.
The course of work is as follows：
In specific production process, oxygen enters oxygen distributor 3 by oxygen-supplying tube 1, by 400 circles point of oxygen distributor 3
Hole, which evenly distributes, is fully reacted, and eliminates dead angle；Oxygen is advanced to become owner of stills for air blowing 4, the agitating device 5 in main reaction kettle 4
Stirring reaction, the oxygen content after stirring were shown on oxygen gauge table 6, and the unreacted oxygen in part enters back into secondary stills for air blowing
8 are further continued for reacting.
Claims (5)
1. a kind of new logical oxygen device for being used to produce phosphorus trichloride, including oxygen-supplying tube（1）With main stills for air blowing（4）, oxygen-supplying tube（1）
It is sequentially connected product feeding mouth（2）And oxygen distributor（3）, oxygen distributor（3）Installed in main stills for air blowing（4）Bottom, its
It is characterised by：The main stills for air blowing（4）Inner hub location be provided with agitating device（5）, the inwall on right side is provided with oxymeter
Scale（6）, main stills for air blowing（4）Top is provided with discharging opening（7）, discharging opening（7）Pass through pipeline and secondary stills for air blowing（8）Connection.
A kind of 2. new logical oxygen device for being used to produce phosphorus trichloride according to claim 1, it is characterised in that：It is described logical
Oxygen pipe（1）It is provided with venting valve（9）.
A kind of 3. new logical oxygen device for being used to produce phosphorus trichloride according to claim 1, it is characterised in that：The oxygen
Qi leel orchestration（3）Inside it is provided with 400 circle point holes.
A kind of 4. new logical oxygen device for being used to produce phosphorus trichloride according to claim 1, it is characterised in that：It is described to stir
Mix device（5）Stirred using two-piece type.
A kind of 5. new logical oxygen device for being used to produce phosphorus trichloride according to claim 1, it is characterised in that：The master
Stills for air blowing（4）With secondary stills for air blowing（8）Using identical two.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711023938.5A CN107777676A (en) | 2017-10-27 | 2017-10-27 | A kind of new logical oxygen device for being used to produce phosphorus trichloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711023938.5A CN107777676A (en) | 2017-10-27 | 2017-10-27 | A kind of new logical oxygen device for being used to produce phosphorus trichloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107777676A true CN107777676A (en) | 2018-03-09 |
Family
ID=61431857
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711023938.5A Withdrawn CN107777676A (en) | 2017-10-27 | 2017-10-27 | A kind of new logical oxygen device for being used to produce phosphorus trichloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107777676A (en) |
-
2017
- 2017-10-27 CN CN201711023938.5A patent/CN107777676A/en not_active Withdrawn
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180309 |
|
| WW01 | Invention patent application withdrawn after publication |