CN107774218A - A kind of multifunctional reaction still - Google Patents

A kind of multifunctional reaction still Download PDF

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Publication number
CN107774218A
CN107774218A CN201711106142.6A CN201711106142A CN107774218A CN 107774218 A CN107774218 A CN 107774218A CN 201711106142 A CN201711106142 A CN 201711106142A CN 107774218 A CN107774218 A CN 107774218A
Authority
CN
China
Prior art keywords
kettle
hole
screen pipe
sealing plate
discharging opening
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201711106142.6A
Other languages
Chinese (zh)
Inventor
李华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Kede Chemical Co Ltd
Original Assignee
Tianjin Kede Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin Kede Chemical Co Ltd filed Critical Tianjin Kede Chemical Co Ltd
Priority to CN201711106142.6A priority Critical patent/CN107774218A/en
Publication of CN107774218A publication Critical patent/CN107774218A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/24Particle separators, e.g. dust precipitators, using rigid hollow filter bodies
    • B01D46/2403Particle separators, e.g. dust precipitators, using rigid hollow filter bodies characterised by the physical shape or structure of the filtering element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0073Sealings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/005Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest

Abstract

The invention provides a kind of multifunctional reaction still, including kettle, kettle cover, charge door, discharging opening, motor, agitating shaft, paddle, the kettle is provided with sealing plate with kettle cover junction below the kettle cover, screen pipe is provided with above the sealing plate, the screen pipe is connected with the discharging opening, first through hole is provided with the sealing plate center, the agitating shaft is through the first through hole and extends to the autoclave body bottom, the second through hole is provided with the side of the sealing plate, the screen pipe connects through second through hole and with the kettle.The present invention is provided with filter before the discharging opening of reactor, solves the problems, such as the blocking of reactor drain pipe, Material Cost is saved, unnecessary waste will not be caused, reduce the man power and material of dredging reactor drain pipe simultaneously, also reduce destruction of the gambling plug thing to reactor valve and pipeline, cost is cheap, structurally simple, economical high efficiency.

Description

A kind of multifunctional reaction still
Technical field
The present invention relates to technical field of chemical, more particularly, to a kind of multifunctional reaction still.
Background technology
Sulfonating reaction is carried out in sulfonating reaction kettle, and sulfonation process has waste gas discharge, and waste gas is together with product steam After condensation discharge, product purity substantially reduces, it is also necessary to filter operation is carried out in filter, more procedures hold with regard to product Secondary pollution is easily caused, influences final products purity and quality;Secondly because always contain certain impurity in waste gas, therefore During waste gas condensation is discharged, impurity can be bonded in the pipeline of discharge, and in the course of time, pipeline can be blocked, and influenceed normal Use and operating efficiency.
The content of the invention
In order to solve the above technical problems, the technical solution adopted by the present invention is:A kind of multifunctional reaction still, including kettle, Kettle cover, charge door, discharging opening, motor, agitating shaft, paddle, the charge door are located at kettle side upper end, the discharging Mouthful at the top of the kettle cover, the kettle and kettle cover junction are provided with sealing plate below the kettle cover, on the sealing plate Side is provided with screen pipe, and the screen pipe is connected with the discharging opening, and first through hole, the stirring are provided with the sealing plate center Axle is through the first through hole and extends to the autoclave body bottom, and the second through hole, the mistake are provided with the side of the sealing plate Chimney filter connects through second through hole and with the kettle.
Further, the curved coil-shape of the screen pipe, multiple segment filters layer is provided with the screen pipe.
Further, bearing is provided between the first through hole and the agitating shaft.
Further, sealing-plug is provided between second through hole and the screen pipe.
Further, fairlead is provided with the top of the kettle, the fairlead connects with the kettle, draws described Outlet pipe is provided with pressure gauge.
Further, one end sealing of the fairlead away from the kettle.
The present invention has the advantage that is with beneficial effect:The present invention before the discharging opening of reactor due to being provided with filtering dress Put, it is outer and finally drop to and continues to react in kettle that the macromolecular raw material not reacted completely is trapped in screen pipe, waste gas or other are small Molecular impurity can be intercepted in hollow tube-shape filter, and the reacted gaseous product obtained completely is in reactor Through hole in empty tube shape filter is evaporated to discharging opening, and the filter of reactor solves asking for reactor drain pipe blocking Topic, has saved Material Cost, will not cause unnecessary waste, while reduces the manpower and thing of dredging reactor drain pipe Power, also reduces the destruction to reactor valve and pipeline, and cost is cheap, structurally simple, economical high efficiency.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
Wherein:1st, kettle 2, kettle cover 3, sealing plate 4, motor 5, agitating shaft 6, charge door 7, discharging opening 8, filtering Pipe 9, first through hole 10, the second through hole 11, bearing 12, sealing-plug 13, fairlead 14, pressure gauge
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.
As shown in figure 1, the invention provides a kind of multifunctional reaction still, including kettle 1, kettle cover 2, charge door 6, discharging opening 5th, motor 4, agitating shaft 5, paddle, the charge door 6 are located at the side upper end of kettle 1, and the discharging opening 5 is located at the kettle The top of lid 2, the kettle 1 is provided with sealing plate 3 with the junction of kettle cover 2 below the kettle cover 2, and the top of sealing plate 3 is provided with Screen pipe 8, the screen pipe 8 are connected with the discharging opening 5, and the curved type coil-shape of screen pipe 8 is set, and increases gas Distance of passing through in screen pipe 8, ensure filter effect, multiple segment filters layer is provided with the screen pipe 8, the filter layer is used In small molecule waste gas or other impurities.
First through hole 10 is provided with the center of sealing plate 3, the agitating shaft 5 is through the first through hole 10 and extends to The bottom of kettle 1, the second through hole 11 is provided with the side of the sealing plate 3, and the screen pipe 8 passes through second through hole 11 And connected with the kettle 1.Further, bearing 11 is provided between the first through hole 10 and the agitating shaft 5, to reduce length Abrasion under time rotation to sealing plate 3 and agitating shaft 5.Further, set between second through hole 11 and the screen pipe 8 There is sealing-plug 12, avoid steam from being scurried out at second through hole 11 to filtering tube outer surface and pollute.
Further, fairlead 13 being provided with the top of the kettle 1, the fairlead 13 connects with the kettle 1, The fairlead 13 is provided with pressure gauge 14.Steam pressure can be detected immediately, avoid steam pressure excessive to screen pipe 8 mouthfuls make Into destruction.One end sealing of the fairlead 13 away from the kettle 1, avoids steam from being contacted with external environment and causes vapor (steam) temperature Decline, pressure reduces, and build-up of pressure test result is relatively low, causes potential safety hazard.
One embodiment of the present of invention is described in detail above, but the content is only the preferable implementation of the present invention Example, it is impossible to be considered as the practical range for limiting the present invention.All equivalent changes made according to the present patent application scope and improvement Deng, all should still belong to the present invention patent covering scope within.

Claims (6)

1. a kind of multifunctional reaction still, including kettle (1), kettle cover (2), charge door (6), discharging opening (7), motor (4), agitating shaft (5), paddle, the charge door (6) are located at the kettle (1) side upper end, and the discharging opening (7) is located at the kettle cover (2) Top, it is characterised in that:The kettle (1) is provided with sealing plate (3) with kettle cover (2) junction below the kettle cover (2), described Screen pipe (8) is provided with above sealing plate (3), the screen pipe (8) is connected with the discharging opening (7), in the sealing plate (3) The heart is provided with first through hole (9), and the agitating shaft (5) is through the first through hole (9) and extends to the kettle (1) bottom, The side of the sealing plate (3) is provided with the second through hole (10), the screen pipe (8) through second through hole (10) and with it is described Kettle (1) connects.
2. the reactor of tool filtering function according to claim 1, it is characterised in that:The curved disk of the screen pipe (8) Around shape, multiple segment filters layer is provided with the screen pipe (8).
3. multifunctional reaction still according to claim 1, it is characterised in that:The first through hole (9) and the agitating shaft (5) bearing (11) is provided between.
4. multifunctional reaction still according to claim 1, it is characterised in that:Second through hole (10) and the screen pipe (8) sealing-plug (12) is provided between.
5. multifunctional reaction still according to claim 1, it is characterised in that:It is provided with and draws in the top of the kettle (1) Manage (13), the fairlead (13) is connected with the kettle (1), and pressure gauge (14) is provided with the fairlead (13).
6. multifunctional reaction still according to claim 5, it is characterised in that:The fairlead (13) is away from the kettle (1) one end sealing.
CN201711106142.6A 2017-11-10 2017-11-10 A kind of multifunctional reaction still Withdrawn CN107774218A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711106142.6A CN107774218A (en) 2017-11-10 2017-11-10 A kind of multifunctional reaction still

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711106142.6A CN107774218A (en) 2017-11-10 2017-11-10 A kind of multifunctional reaction still

Publications (1)

Publication Number Publication Date
CN107774218A true CN107774218A (en) 2018-03-09

Family

ID=61433260

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711106142.6A Withdrawn CN107774218A (en) 2017-11-10 2017-11-10 A kind of multifunctional reaction still

Country Status (1)

Country Link
CN (1) CN107774218A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110051560A (en) * 2019-04-10 2019-07-26 绍兴美琪医疗科技有限公司 A kind of sterile facial mask production technology
CN112354510A (en) * 2020-11-16 2021-02-12 徐超 Multi-stage tubular reactor with vertical spacing sections

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110051560A (en) * 2019-04-10 2019-07-26 绍兴美琪医疗科技有限公司 A kind of sterile facial mask production technology
CN110051560B (en) * 2019-04-10 2022-04-05 绍兴美琪医疗科技有限公司 Aseptic mask production process
CN112354510A (en) * 2020-11-16 2021-02-12 徐超 Multi-stage tubular reactor with vertical spacing sections

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WW01 Invention patent application withdrawn after publication
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Application publication date: 20180309