CN107741158A - One kind produces high chlorine titanium sponge feeder - Google Patents
One kind produces high chlorine titanium sponge feeder Download PDFInfo
- Publication number
- CN107741158A CN107741158A CN201710980344.7A CN201710980344A CN107741158A CN 107741158 A CN107741158 A CN 107741158A CN 201710980344 A CN201710980344 A CN 201710980344A CN 107741158 A CN107741158 A CN 107741158A
- Authority
- CN
- China
- Prior art keywords
- head tank
- storage tank
- feeder
- titanium sponge
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D7/00—Forming, maintaining, or circulating atmospheres in heating chambers
- F27D7/02—Supplying steam, vapour, gases, or liquids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
Abstract
The invention discloses one kind to produce high chlorine titanium sponge feeder, including the storage tank and head tank being connected by connecting tube, storage tank is connected with storage tank filling tube, fills chlorine pipe, head tank filling tube, argon-filled tube, reactor charge pipe and discharge nozzle are provided with the outer surface of head tank, discharge nozzle is connected with agitator, and the both ends of agitator are connected with discharge nozzle.The present invention solves processes that device used in high chlorine titanium sponge is not high to utilization rate of raw materials, and the waste to raw material is serious in the prior art, the problem of high processing costs.
Description
Technical field
The present invention relates to a kind of smelting field of nonferrous metal, and in particular to one kind produces high chlorine titanium sponge feeder.
Background technology
In the modern times prepare the technique of titanium sponge, chlorine can improve the intensity of titanium alloy, and reinforcing of the chlorine to titanium alloy
Effect is higher, and the chlorinity of titanium sponge cannot have the function that alloy strengthening less than 0.005%, therefore often be needed in titanium alloy
Chlorine is added to increase intensity, but domestic efficient processing unit (plant) no at present coordinates processing technology to add chlorine into titanium alloy
Element, the processing unit (plant) that industry is relied at this stage is large-scale smelting furnace, and large-scale smelting furnace is not often high to the utilization rate of raw material, makes
Waste of raw materials is serious, high processing costs, therefore the processing unit (plant) for finding another economical and efficient is extremely urgent.
The content of the invention
It is an object of the invention to provide one kind to produce high chlorine titanium sponge feeder, solves present in prior art
It is low to the utilization rate of raw material, it is serious to waste of raw materials, the problem of high processing costs.
The technical solution adopted in the present invention is that one kind produces high chlorine titanium sponge feeder, including passes through connecting tube
Connected storage tank and head tank, storage tank are connected with storage tank filling tube, fill chlorine pipe, and head tank is connected with head tank material feeding
Pipe, argon-filled tube, reactor charge pipe, reactor charge pipe are connected with reactor, and the bottom of head tank and side wall pass through discharge nozzle
Circulation is connected, and agitator is connected with discharge nozzle.
It is of the invention to be further characterized in that,
Storage tank pressure gauge and storage tank liquid level gauge are additionally provided with the outer surface of storage tank.
Head tank hydraulic ga(u)ge and head tank pressure gauge are additionally provided with the outer surface of head tank.
Storage tank filling tube, fill on chlorine pipe, argon-filled tube, head tank filling tube, connecting tube, reactor charge pipe and discharge nozzle
It is provided with check valve.
Argon-filled tube front end is provided with pressure detector.
The beneficial effects of the invention are as follows：One kind of the present invention produces high chlorine titanium sponge and solves prior art with feeder
Present in the large-scale smelting furnace of processing unit (plant) that is relied on of the high chlorine titanium sponge of processing it is often not high to the utilization rate of raw material, make former material
Material waste it is serious, the problem of processing cost so that the utilization rate of raw material greatly improves, and saves cost, more efficient processing
High chlorine titanium sponge.
Brief description of the drawings
Fig. 1 is a kind of structural representation for producing high chlorine titanium sponge feeder of the present invention.
In figure, 1. head tank hydraulic ga(u)ges, 2. argon-filled tubes, 3. fill chlorine pipe, 4. storage tank pressure gauges, 5. storage tank filling tubes,
6. storage tank liquid level gauge, 7. connecting tubes, 8. head tank filling tubes, 9. agitators, 10. head tank pressure gauges, the charging of 11. reactors
Pipe, 12. head tanks, 13. storage tanks, 14. discharge nozzles.
Embodiment
The present invention is described in detail with reference to the accompanying drawings and detailed description.
The present invention is a kind of high chlorine titanium sponge feeder of production, and its structure is as shown in figure 1, including passing through connecting tube 7
Connected storage tank 13 and head tank 12, storage tank 13 are connected with storage tank filling tube 5, fill chlorine pipe 3, and head tank 12 is connected with height
Position groove filling tube 8, argon-filled tube 2, reactor charge pipe 11, reactor charge pipe 11 are connected with reactor, the bottom of head tank 12
Circulated and connected by discharge nozzle 14 with side wall, agitator 9 is connected with discharge nozzle 14.
Storage tank pressure gauge 4 and storage tank liquid level gauge 6 are additionally provided with the outer surface of storage tank 13.
Head tank hydraulic ga(u)ge 1 and head tank pressure gauge 10 are additionally provided with the outer surface of head tank 12.
Storage tank filling tube 5, fill chlorine pipe 3, argon-filled tube 2, head tank filling tube 8, connecting tube 7, the and of reactor charge pipe 11
Check valve is provided with discharge nozzle 14.
The front end of argon-filled tube 2 is provided with pressure detector.
The present invention is a kind of to be produced high chlorine titanium sponge and is with the application method of feeder：
By taking 10 tons of reactor reduction furnaces as an example, 5 tons of titanium tetrachlorides are added into storage tank 13 by storage tank filling tube 5,
The addition of the titanium tetrachloride in storage tank 13 is detected by storage tank liquid level gauge 6, then chlorine is passed through from filling in chlorine pipe 3 so that
Chlorine is completely dissolved in titanium tetrachloride in storage tank 13；The content of chlorine according to needed for titanium sponge, calculate in storage tank 13
The mixed proportion of titanium tetrachloride and the titanium tetrachloride in head tank 12, determines the titanium tetrachloride added needed for head tank 12,
Titanium tetrachloride is added into head tank 12 by head tank filling tube 8, the valve of connecting tube 7 is opened afterwards, into head tank 12
The titanium tetrachloride of chlorine is mixed with injection storage tank 13, it is to be implanted to finish, the valve of connecting tube 7 is shut, now opens argon filling
The valve of pipe 2, argon gas is filled with so that the pressure in head tank 12 is maintained at 0.03MPa, then opens discharge nozzle into head tank 12
14 valve causes the titanium tetrachloride in head tank 12 is entered in agitator 9 to be sufficiently stirred, then is back to head tank 12
In, it is to be mixed to finish, open reactor charge pipe 11 so that titanium tetrachloride is reacted into reactor.Notice that pressure detects
Pressure in device detection head tank 12, argon gas is supplemented if 0.03MPa is less than at any time.
In addition, the pressure in reactor is maintained between 0.02-0.05MPa, melt temperature, which controls, in reactor exists
Between 720-840 degrees Celsius, the pressure of head tank supplements argon gas to maintain head tank pressure when being less than 0.03MPa, final to obtain
The leading indicator of titanium sponge is：N：0.005-0.01%, C：0.01-0.15%, Fe：0.01-0.03%, Cl：0.045—
0.06%, O：0.05-0.06%.
Claims (5)
1. one kind produces high chlorine titanium sponge feeder, it is characterised in that：Including the storage tank being connected by connecting tube (7)
(13) it is connected with storage tank filling tube (5) with head tank (12), the storage tank (13), fills chlorine pipe (3), the head tank (12)
It is connected with head tank filling tube (8), argon-filled tube (2), reactor charge pipe (11), the reactor charge pipe (11) and reactor
It is connected, the bottom of the head tank (12) and side wall are circulated by discharge nozzle (14) and connected, and are connected with the discharge nozzle (14)
Agitator (9).
A kind of 2. high chlorine titanium sponge feeder of production according to claim 1, it is characterised in that：The storage tank
(13) storage tank pressure gauge (4) and storage tank liquid level gauge (6) are additionally provided with outer surface.
3. a kind of according to claim 1 produce high chlorine titanium sponge feeder, it is characterised in that：The head tank (12)
Outer surface on be additionally provided with head tank hydraulic ga(u)ge (1) and head tank pressure gauge (10).
A kind of 4. high chlorine titanium sponge feeder of production according to claim 1, it is characterised in that：The storage tank note
Expects pipe (5), fill chlorine pipe (3), argon-filled tube (2), head tank filling tube (8), connecting tube (7), reactor charge pipe (11) and discharging
Check valve is provided with pipe (14).
A kind of 5. high chlorine titanium sponge feeder of production according to claim 1, it is characterised in that：The argon-filled tube
(2) front end is provided with pressure detector.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710980344.7A CN107741158A (en) | 2017-10-19 | 2017-10-19 | One kind produces high chlorine titanium sponge feeder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710980344.7A CN107741158A (en) | 2017-10-19 | 2017-10-19 | One kind produces high chlorine titanium sponge feeder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107741158A true CN107741158A (en) | 2018-02-27 |
Family
ID=61237844
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710980344.7A Pending CN107741158A (en) | 2017-10-19 | 2017-10-19 | One kind produces high chlorine titanium sponge feeder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107741158A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB686845A (en) * | 1949-02-15 | 1953-02-04 | Titan Gmbh | Improvements in or relating to the manufacture of, and coating by titanium or alloys of titanium |
| CN102816942A (en) * | 2012-09-11 | 2012-12-12 | 朝阳金达钛业有限责任公司 | Process and device for producing high-nitrogen sponge titanium |
| CN103215462A (en) * | 2013-05-22 | 2013-07-24 | 朝阳金达钛业股份有限公司 | Device and process for producing silicon containing titanium sponge |
| CN203474481U (en) * | 2013-08-05 | 2014-03-12 | 河南龙兴钛业有限公司 | Slurry processing device applicable to titanium tetrachloride production process |
| CN104561607A (en) * | 2015-01-13 | 2015-04-29 | 朝阳金达钛业股份有限公司 | Method for producing carbon-containing titanium sponge and device thereof |
-
2017
- 2017-10-19 CN CN201710980344.7A patent/CN107741158A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB686845A (en) * | 1949-02-15 | 1953-02-04 | Titan Gmbh | Improvements in or relating to the manufacture of, and coating by titanium or alloys of titanium |
| CN102816942A (en) * | 2012-09-11 | 2012-12-12 | 朝阳金达钛业有限责任公司 | Process and device for producing high-nitrogen sponge titanium |
| CN103215462A (en) * | 2013-05-22 | 2013-07-24 | 朝阳金达钛业股份有限公司 | Device and process for producing silicon containing titanium sponge |
| CN203474481U (en) * | 2013-08-05 | 2014-03-12 | 河南龙兴钛业有限公司 | Slurry processing device applicable to titanium tetrachloride production process |
| CN104561607A (en) * | 2015-01-13 | 2015-04-29 | 朝阳金达钛业股份有限公司 | Method for producing carbon-containing titanium sponge and device thereof |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180227 |