CN107739647A - A kind of die quenching protection oil and preparation method thereof - Google Patents
A kind of die quenching protection oil and preparation method thereof Download PDFInfo
- Publication number
- CN107739647A CN107739647A CN201711019645.XA CN201711019645A CN107739647A CN 107739647 A CN107739647 A CN 107739647A CN 201711019645 A CN201711019645 A CN 201711019645A CN 107739647 A CN107739647 A CN 107739647A
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- China
- Prior art keywords
- parts
- protection oil
- quenching protection
- die quenching
- surfactant
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/10—Compounds containing silicon
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/287—Partial esters
- C10M2207/289—Partial esters containing free hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/242—Hot working
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Heat Treatment Of Articles (AREA)
Abstract
The invention discloses a kind of die quenching protection oil, it is prepared by the composition of following mass fractions：0.1 ~ 0.5 part of 100 parts of base oil, 1 ~ 5 part of three nitrogen Zo of benzo, 1 ~ 3 part of sorbitan monooleate, 10 ~ 20 parts of fatty acid monoglyceride, 10 ~ 12 parts of chlorinated paraffin, 0.5 ~ 1 part of sulfoacid calcium, 1 ~ 3 part of rust-inhibiting additive, 1 ~ 5 part of surfactant, 1 ~ 3 part of antioxidant and scale inhibitor.The present invention is directed to the characteristic of mould steel, and quenching protection oil is infiltrated after mould is quenched, can ensure that the mould steel after quenching forms certain hardness, reduce deformation and the cracking rate of mould.
Description
Technical field
The present invention relates to mould preparing technical field, and oil and preparation method thereof is protected more particularly to a kind of die quenching.
Background technology
In order to which the material of mould is improved, it usually needs the mould of metal material is heat-treated, conventional heat
Handling process has the heat treatment methods such as quenching, tempering, annealing, normalizing.Wherein, quenching is to will warm up the bow and arrow of austenitic state
It is quickly cooled to form martensite lamp quenching structure with speed more than critical cooling rate, after Quenching Treatment, work can be improved
The hardness of part.During die steel is quenched, easily cause the internal stress inside steel excessive, so as to cause workpiece
Cracking, therefore, parameter setting of the research high-strength die in quenching process, and the addition of auxiliary material is significant.
The content of the invention
The present invention solves the technical problem of provide a kind of die quenching protection oil and preparation method thereof.
In order to solve the above technical problems, one aspect of the present invention is：
A kind of die quenching protection oil is provided, is prepared by the composition of following mass fractions：100 parts of base oil, benzo
Three 1 ~ 5 part of nitrogen Zo, 1 ~ 3 part of sorbitan monooleate, 10 ~ 20 parts of fatty acid monoglyceride, 10 ~ 12 parts of chlorinated paraffin, sulphur
0.1 ~ 0.5 part of sour 0.5 ~ 1 part of calcium, 1 ~ 3 part of rust-inhibiting additive, 1 ~ 5 part of surfactant, 1 ~ 3 part of antioxidant and scale inhibitor.
In a preferred embodiment of the present invention, the scale inhibitor is organic phosphoric acid.
In a preferred embodiment of the present invention, the surfactant is the mixing of hydrophilic silicon dioxide and glycerine
Thing.
Present invention also offers the preparation method of above-mentioned die quenching protection oil, comprise the steps：By base oil, lose
Water sorbitol monooleate, fatty acid monoglyceride mixing, after be heated to 80 ~ 90 DEG C, stir and be incubated 30min, then cool
To 50 DEG C ~ 55 DEG C, add chlorinated paraffin, sulfoacid calcium, continue to stir, stand add after 30min benzo three nitrogen Zo, antirust addition,
Surfactant, antioxidant and scale inhibitor, stir and obtain finished product quenching protection oil.
The beneficial effects of the invention are as follows：A kind of die quenching protection oil of the present invention, for the characteristic of mould steel, enters in mould
Quenching protection oil is infiltrated after row quenching, can ensure that the mould steel after quenching forms certain hardness, reduce mould
Deformation and cracking rate.
Embodiment
Presently preferred embodiments of the present invention is described in detail below so that advantages and features of the invention can be easier to by
It will be appreciated by those skilled in the art that apparent clearly defined so as to be made to protection scope of the present invention.
Embodiment 1：A kind of die quenching protection oil, is prepared by the composition of following mass fractions：Base oil 100
Part, 2 parts of three nitrogen Zo of benzo, 3 parts of sorbitan monooleate, 15 parts of fatty acid monoglyceride, 10 parts of chlorinated paraffin, sulfoacid calcium
0.2 part of 1 part, 2 parts of rust-inhibiting additive, 3 parts of surfactant, 2 parts of antioxidant and scale inhibitor.
Wherein, the scale inhibitor is organic phosphoric acid, and the surfactant is the mixing of hydrophilic silicon dioxide and glycerine
Thing.
Embodiment 2：A kind of die quenching protection oil, is prepared by the composition of following mass fractions：100 parts of base oil,
5 parts of three nitrogen Zo of benzo, 2 parts of sorbitan monooleate, 12 parts of fatty acid monoglyceride, 12 parts of chlorinated paraffin, sulfoacid calcium 0.8
Part, 2 parts of rust-inhibiting additive, 3 parts of surfactant, 2 parts of antioxidant and 0.5 part of scale inhibitor.
Embodiment 3：A kind of die quenching protection oil, is prepared by the composition of following mass fractions：Base oil 100
Part, 4 parts of three nitrogen Zo of benzo, 1 part of sorbitan monooleate, 20 parts of fatty acid monoglyceride, 12 parts of chlorinated paraffin, sulfoacid calcium
0.2 part of 1 part, 2 parts of rust-inhibiting additive, 5 parts of surfactant, 2 parts of antioxidant and scale inhibitor.
The preparation method of die quenching protection oil in any of the above-described embodiment, comprises the steps：By base oil, dehydration
Sorbitol monooleate, fatty acid monoglyceride mixing, after be heated to 80 ~ 90 DEG C, stir and be incubated 30min, be then cooled to
50 DEG C ~ 55 DEG C, chlorinated paraffin, sulfoacid calcium are added, continues to stir, the nitrogen Zo of benzo three, antirust addition, table are added after standing 30min
Face activating agent, antioxidant and scale inhibitor, stir and obtain finished product quenching protection oil.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
The equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, it is included within the scope of the present invention.
Claims (4)
1. a kind of die quenching protection oil, it is characterised in that be prepared by the composition of following mass fractions：Base oil
100 parts, 1 ~ 5 part of three nitrogen Zo of benzo, 1 ~ 3 part of sorbitan monooleate, 10 ~ 20 parts of fatty acid monoglyceride, chlorinated paraffin
10 ~ 12 parts, 0.5 ~ 1 part of sulfoacid calcium, 1 ~ 3 part of rust-inhibiting additive, 1 ~ 5 part of surfactant, 1 ~ 3 part of antioxidant and scale inhibitor
0.1 ~ 0.5 part.
2. die quenching protection oil according to claim 1, it is characterised in that the scale inhibitor is organic phosphoric acid.
3. die quenching protection oil according to claim 1, it is characterised in that the surfactant is hydrophilic titanium dioxide
The mixture of silicon and glycerine.
4. the preparation method of the die quenching protection oil according to one of claim 1 ~ 3, it is characterised in that including following steps
Suddenly：By base oil, sorbitan monooleate, fatty acid monoglyceride mix, after be heated to 80 ~ 90 DEG C, stir and be incubated
30min, 50 DEG C ~ 55 DEG C are then cooled to, add chlorinated paraffin, sulfoacid calcium, continue to stir, benzo three is added after standing 30min
Nitrogen Zo, antirust addition, surfactant, antioxidant and scale inhibitor, stir and obtain finished product quenching protection oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711019645.XA CN107739647A (en) | 2017-10-26 | 2017-10-26 | A kind of die quenching protection oil and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711019645.XA CN107739647A (en) | 2017-10-26 | 2017-10-26 | A kind of die quenching protection oil and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107739647A true CN107739647A (en) | 2018-02-27 |
Family
ID=61238332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711019645.XA Pending CN107739647A (en) | 2017-10-26 | 2017-10-26 | A kind of die quenching protection oil and preparation method thereof |
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| Country | Link |
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| CN (1) | CN107739647A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111440926A (en) * | 2020-04-28 | 2020-07-24 | 湖南电力耐磨新材料有限公司 | Water-based quenching liquid and preparation method and use method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5376186A (en) * | 1991-10-18 | 1994-12-27 | Idemitsu Kosan Co., Ltd. | Heat treating oil composition |
| CN104451054A (en) * | 2014-12-01 | 2015-03-25 | 昌利锻造有限公司 | Gear quenching oil and preparation method thereof |
| CN104831028A (en) * | 2015-04-10 | 2015-08-12 | 合肥环照高分子材料厂 | Gear quenching oil and preparation method thereof |
| CN104975150A (en) * | 2015-07-20 | 2015-10-14 | 江苏金基特钢有限公司 | Method for preparing alloy steel quenching oil |
| CN107245690A (en) * | 2017-06-23 | 2017-10-13 | 江苏丰东热处理及表面改性工程技术研究有限公司 | A kind of carburizing quenching process |
-
2017
- 2017-10-26 CN CN201711019645.XA patent/CN107739647A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5376186A (en) * | 1991-10-18 | 1994-12-27 | Idemitsu Kosan Co., Ltd. | Heat treating oil composition |
| CN104451054A (en) * | 2014-12-01 | 2015-03-25 | 昌利锻造有限公司 | Gear quenching oil and preparation method thereof |
| CN104831028A (en) * | 2015-04-10 | 2015-08-12 | 合肥环照高分子材料厂 | Gear quenching oil and preparation method thereof |
| CN104975150A (en) * | 2015-07-20 | 2015-10-14 | 江苏金基特钢有限公司 | Method for preparing alloy steel quenching oil |
| CN107245690A (en) * | 2017-06-23 | 2017-10-13 | 江苏丰东热处理及表面改性工程技术研究有限公司 | A kind of carburizing quenching process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111440926A (en) * | 2020-04-28 | 2020-07-24 | 湖南电力耐磨新材料有限公司 | Water-based quenching liquid and preparation method and use method thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180227 |
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