CN107722869A - A kind of paper lantern is modified glutinous rice glue with high bond strength - Google Patents
A kind of paper lantern is modified glutinous rice glue with high bond strength Download PDFInfo
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- CN107722869A CN107722869A CN201710879996.1A CN201710879996A CN107722869A CN 107722869 A CN107722869 A CN 107722869A CN 201710879996 A CN201710879996 A CN 201710879996A CN 107722869 A CN107722869 A CN 107722869A
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- glutinous rice
- rice flour
- modified
- soybean oil
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Glutinous rice glue is modified with high bond strength the invention discloses a kind of paper lantern, its raw material includes by weight：40 60 parts of cornstarch, epoxidized soybean oil is modified 15 25 parts of glutinous rice flour, carboxymethyl modified 25 35 parts of glutinous rice flour, 15 35 parts of acetate starch, 13 parts of crosslinking agent, 12 parts of polyglycerolpolyrici.oleate, 12 parts of D mannitols, 12 parts of malic acid, 13 parts of stabilizer, 12 parts of preservative, 12 parts of thickener, 150 250 parts of water.Paper lantern proposed by the present invention is modified glutinous rice glue with high bond strength, and not only adhesion strength is high, and stability is good, and can effectively avoid the condensation under hot environment in the overflow and cooling procedure of moisture, at the same can effective delaying aging, improve the good appearance degree of paper lantern.
Description
Technical field
The present invention relates to paper lantern technical field, more particularly to a kind of paper lantern to be modified glutinous rice glue with high bond strength.
Background technology
Lantern is a kind of caged light fixture.It is a kind of very ancient folk custom artifacts.The lantern of China is referred to as lamp again
Coloured silk, originating from Western Han Dynastry's period before more than 1800 years, before and after the annual Lantern Festival in the lunar calendar first month of the lunar year 15, people hang up symbol reunion
The red lantern of meaning, to build a kind of celebrating atmosphere, later lantern is just into the celebrating symbol of Chinese.By successive dynasties lantern
The succession and development of artist, forms colourful kind and superb technological level.
Paper lantern is more with the skeleton processed such as the thin thin bamboo strip or iron wire at present, coordinates glue adhesion papery outer container, internal combustion lamps and candles or use
Bulb, for illuminating, decorating or enjoy, with internal combustion lamps and candles with or bulb long-time generate heat, this to using glue bonding it is strong
Degree and thermal stability requirement are high.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of paper lantern high bond strength and is modified glutinous rice
Glue, not only adhesion strength is high, and stability is good, and can effectively avoid cold in the overflow and cooling procedure of moisture under hot environment
It is solidifying, at the same can effective delaying aging, improve the good appearance degree of paper lantern.
A kind of paper lantern proposed by the present invention is modified glutinous rice glue with high bond strength, and its raw material includes by weight：Corn
Starch 40-60 parts, epoxidized soybean oil are modified glutinous rice flour 15-25 parts, carboxymethyl modified glutinous rice flour 25-35 parts, acetate starch 15-
35 parts, crosslinking agent 1-3 parts, polyglycerolpolyrici.oleate 1-2 parts, D-mannital 1-2 parts, malic acid 1-2 parts, stabilizer 1-3
Part, preservative 1-2 parts, thickener 1-2 parts, water 150-250 parts.
Preferably, epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：Glutinous rice flour, water are well mixed, added
Sodium chloride is well mixed, and regulation system pH value is 7.5-8.5, stirring, adds epoxidized soybean oil, PPG, silane coupled
Agent mixes, and under nitrogen protection, temperature reaction, then temperature reaction obtain epoxidized soybean oil and be modified glutinous rice flour.
Preferably, epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：Glutinous rice flour, water are well mixed, added
Sodium chloride is well mixed, and is 7.5-8.5 with sodium hydroxide regulation system pH value, stirs 2-8min, adds epoxidized soybean oil, polyethers
Polyalcohol, silane coupler mixing, under nitrogen protection, 120-135 DEG C of reaction 40-60min is warming up to, then be warming up to 175-185
DEG C reaction 5-15min, obtain epoxidized soybean oil be modified glutinous rice flour.
Preferably, epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：By weight by 22-30 parts glutinous rice flour,
60-100 part water is well mixed, and is added 1-2 part sodium chloride and is well mixed, is 7.5-8.5 with sodium hydroxide regulation system pH value, stirs
2-8min is mixed, adds 4-15 parts epoxidized soybean oil, 1-2 parts PPG, the mixing of 0.5-1.2 parts silane coupler, nitrogen is protected
Under shield, 120-135 DEG C of reaction 40-60min is warming up to, then is warming up to 175-185 DEG C of reaction 5-15min, obtains epoxidized soybean oil
Modified glutinous rice flour.
Preferably, crosslinking agent is potassium metapbosphate.
Preferably, stabilizer is glycerin monostearate, bi-tristearin, acetylation monostearate fat acid glycerol
At least one of ester, the sweet fat of laurate monostearate, disodium ethylene diamine tetraacetate, tetrasodium ethylenediamine tetraacetate.
The present invention is free of organic solvent, does not detect formaldehyde, safety and environmental protection, nontoxic, have no irritating odor.The ring of the present invention
In the soybean oil modified glutinous rice flour of oxygen, glutinous rice flour is handled under the cooperation of tween through sodium chloride, and toughness increases, not easy to break, uses hydrogen
Compound with epoxidized soybean oil after sodium oxide molybdena activation, under the catalysis of silane coupler, reacted using PPG, form network
Shape macromolecular, not only viscosity increase, and with carboxymethyl modified glutinous rice flour, the good dispersion of acetate starch, match somebody with somebody by improvement
Side, promote the stability of the present invention good, and viscosity adds polyglycerolpolyrici.oleate, D- sweet dews also superior to like product
Sugar alcohol acts on, and can effectively avoid the condensation under hot environment in the overflow and cooling procedure of moisture, and can effective delaying aging, protect
The sense organ color and luster of the present invention is protected, improves the good appearance degree of paper lantern.
Peel strength and viscosity test are carried out using paper lantern made from glutinous rice glue of the present invention, peel strength is in 18mN/mm
More than, viscosity has the characteristics of bonding force is strong in more than 128000cps, is incubated 5h at 70 DEG C in addition, remain to keep 50% it is viscous
Knotting strength.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of paper lantern is modified glutinous rice glue with high bond strength, and its raw material includes by weight：40 parts of cornstarch, epoxy
Soybean oil modified 25 parts of glutinous rice flour, carboxymethyl modified 25 parts of glutinous rice flour, 35 parts of acetate starch, 1 part of crosslinking agent, polyglycereol castor-oil plant
2 parts of carboxylic ester, 1 part of D-mannital, 2 parts of malic acid, 1 part of stabilizer, 2 parts of preservative, 1 part of thickener, 250 parts of water.
Embodiment 2
A kind of paper lantern is modified glutinous rice glue with high bond strength, and its raw material includes by weight：60 parts of cornstarch, epoxy
Soybean oil modified 15 parts of glutinous rice flour, carboxymethyl modified 35 parts of glutinous rice flour, 15 parts of acetate starch, 3 parts of potassium metapbosphate, polyglycereol
1 part of ricinoleate, 2 parts of D-mannital, 1 part of malic acid, 3 parts of glycerin monostearate, 1 part of preservative, 2 parts of thickener,
150 parts of water.
Epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：Glutinous rice flour, water are well mixed, sodium chloride is added and mixes
Close uniformly, regulation system pH value is 7.5-8.5, stirring, adds epoxidized soybean oil, PPG, silane coupler mixing, nitrogen
Under gas shielded, temperature reaction, then temperature reaction obtain epoxidized soybean oil and are modified glutinous rice flour.
Embodiment 3
A kind of paper lantern is modified glutinous rice glue with high bond strength, and its raw material includes by weight：45 parts of cornstarch, epoxy
Soybean oil modified 22 parts of glutinous rice flour, carboxymethyl modified 28 parts of glutinous rice flour, 30 parts of acetate starch, 1.5 parts of potassium metapbosphate, gather sweet
Oily 1.8 parts of ricinoleate, 1.2 parts of D-mannital, 1.7 parts of malic acid, 0.6 part of bi-tristearin, ethylenediamine tetrem
0.6 part of acid disodium, 1.8 parts of preservative, 1.2 parts of thickener, 220 parts of water.
Epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：Glutinous rice flour, water are well mixed, sodium chloride is added and mixes
Close uniformly, be 7.5-8.5 with sodium hydroxide regulation system pH value, stir 5min, add epoxidized soybean oil, PPG, silicon
Alkane coupling agent mixes, and under nitrogen protection, is warming up to 128 DEG C of reaction 50min, then is warming up to 180 DEG C of reaction 10min, obtains epoxy
Soybean oil modified glutinous rice flour.
Embodiment 4
A kind of paper lantern is modified glutinous rice glue with high bond strength, and its raw material includes by weight：55 parts of cornstarch, epoxy
Soybean oil modified 18 parts of glutinous rice flour, carboxymethyl modified 32 parts of glutinous rice flour, 20 parts of acetate starch, 2.5 parts of potassium metapbosphate, gather sweet
Oily 1.2 parts of ricinoleate, 1.8 parts of D-mannital, 1.3 parts of malic acid, acetylation monostearate fatty glyceride 0.6
Part, 0.6 part of the sweet fat of laurate monostearate, 0.6 part of tetrasodium ethylenediamine tetraacetate, 1.4 parts of preservative, 1.6 parts of thickener, water
180 parts.
Epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：22 parts of glutinous rice flours, 100 parts of water are mixed by weight
Uniformly, add 1 part of sodium chloride to be well mixed, be 7.5-8.5 with sodium hydroxide regulation system pH value, stir 8min, add 4 parts of rings
Oxygen soybean oil, 2 parts of PPGs, 0.5 part of silane coupler mixing, under nitrogen protection, 135 DEG C of reaction 40min are warming up to, then
185 DEG C of reaction 5min are warming up to, epoxidized soybean oil is obtained and is modified glutinous rice flour.
Embodiment 5
A kind of paper lantern is modified glutinous rice glue with high bond strength, and its raw material includes by weight：50 parts of cornstarch, epoxy
Soybean oil modified 20 parts of glutinous rice flour, carboxymethyl modified 30 parts of glutinous rice flour, 25 parts of acetate starch, 2 parts of potassium metapbosphate, polyglycereol
1.5 parts of ricinoleate, 1.5 parts of D-mannital, 1.5 parts of malic acid, 1.5 parts of stabilizer, 1.6 parts of preservative, thickener 1.4
Part, 200 parts of water.
Epoxidized soybean oil is modified glutinous rice flour and prepared using following technique：30 parts of glutinous rice flours, 60 parts of water are mixed by weight
Uniformly, 2 parts of sodium chloride are added to be well mixed, is 7.5-8.5 with sodium hydroxide regulation system pH value, stir 2min, add 15 parts
Epoxidized soybean oil, 1 part of PPG, 1.2 parts of silane coupler mixing, under nitrogen protection, 120 DEG C of reaction 60min are warming up to,
175 DEG C of reaction 15min are warming up to again, are obtained epoxidized soybean oil and are modified glutinous rice flour.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (6)
1. a kind of paper lantern is modified glutinous rice glue with high bond strength, it is characterised in that its raw material includes by weight：Cornstarch
40-60 parts, epoxidized soybean oil are modified glutinous rice flour 15-25 parts, carboxymethyl modified glutinous rice flour 25-35 parts, acetate starch 15-35
Part, crosslinking agent 1-3 parts, polyglycerolpolyrici.oleate 1-2 parts, D-mannital 1-2 parts, malic acid 1-2 parts, stabilizer 1-3 parts,
Preservative 1-2 parts, thickener 1-2 parts, water 150-250 parts.
2. paper lantern is modified glutinous rice glue with high bond strength according to claim 1, it is characterised in that epoxidized soybean oil is modified
Glutinous rice flour is prepared using following technique：Glutinous rice flour, water are well mixed, sodium chloride is added and is well mixed, regulation system pH value is
7.5-8.5, stirring, epoxidized soybean oil, PPG, silane coupler mixing are added, under nitrogen protection, temperature reaction, then
Temperature reaction obtains epoxidized soybean oil and is modified glutinous rice flour.
3. paper lantern according to claim 1 or claim 2 is modified glutinous rice glue with high bond strength, it is characterised in that epoxidized soybean oil
Modified glutinous rice flour is prepared using following technique：Glutinous rice flour, water are well mixed, sodium chloride is added and is well mixed, use sodium hydroxide
Regulation system pH value is 7.5-8.5, stirs 2-8min, adds epoxidized soybean oil, PPG, silane coupler mixing, nitrogen
Under gas shielded, 120-135 DEG C of reaction 40-60min is warming up to, then is warming up to 175-185 DEG C of reaction 5-15min, it is big to obtain epoxy
Soya-bean oil is modified glutinous rice flour.
4. stating paper lantern high bond strength according to any one of claim 1-3 is modified glutinous rice glue, it is characterised in that epoxy soybean
The modified glutinous rice flour of oil is prepared using following technique：22-30 parts glutinous rice flour, 60-100 part water are well mixed by weight, added
1-2 part sodium chloride is well mixed, and is 7.5-8.5 with sodium hydroxide regulation system pH value, stirs 2-8min, adds 4-15 part epoxies
Soybean oil, 1-2 parts PPG, the mixing of 0.5-1.2 parts silane coupler, under nitrogen protection, are warming up to 120-135 DEG C of reaction
40-60min, then 175-185 DEG C of reaction 5-15min is warming up to, obtain epoxidized soybean oil and be modified glutinous rice flour.
5. stating paper lantern high bond strength according to any one of claim 1-4 is modified glutinous rice glue, it is characterised in that crosslinking agent is
Potassium metapbosphate.
6. stating paper lantern high bond strength according to any one of claim 1-5 is modified glutinous rice glue, it is characterised in that stabilizer is
Glycerin monostearate, bi-tristearin, acetylation monostearate fatty glyceride, the sweet fat of laurate monostearate,
At least one of disodium ethylene diamine tetraacetate, tetrasodium ethylenediamine tetraacetate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710879996.1A CN107722869A (en) | 2017-09-26 | 2017-09-26 | A kind of paper lantern is modified glutinous rice glue with high bond strength |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710879996.1A CN107722869A (en) | 2017-09-26 | 2017-09-26 | A kind of paper lantern is modified glutinous rice glue with high bond strength |
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| CN107722869A true CN107722869A (en) | 2018-02-23 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115011308A (en) * | 2022-07-20 | 2022-09-06 | 杭州志和新材料有限公司 | Composite adhesive capable of being simultaneously used for cold adhesive wall cloth and hot adhesive wall cloth and preparation thereof |
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|---|---|---|---|---|
| CN104263275A (en) * | 2014-09-10 | 2015-01-07 | 上海金大塑胶有限公司 | Environment-friendly self-adhesive label material |
| CN106381089A (en) * | 2016-08-31 | 2017-02-08 | 桐乡嘉力丰实业股份有限公司 | Edible environmentally-friendly glutinous rice glue composition used for pasting wallpapers, and production method thereof |
| CN106554732A (en) * | 2015-09-29 | 2017-04-05 | 什邡市美的家木业有限责任公司 | A kind of preparation method of adhesion agent for artificial board |
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2017
- 2017-09-26 CN CN201710879996.1A patent/CN107722869A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104263275A (en) * | 2014-09-10 | 2015-01-07 | 上海金大塑胶有限公司 | Environment-friendly self-adhesive label material |
| CN106554732A (en) * | 2015-09-29 | 2017-04-05 | 什邡市美的家木业有限责任公司 | A kind of preparation method of adhesion agent for artificial board |
| CN106381089A (en) * | 2016-08-31 | 2017-02-08 | 桐乡嘉力丰实业股份有限公司 | Edible environmentally-friendly glutinous rice glue composition used for pasting wallpapers, and production method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115011308A (en) * | 2022-07-20 | 2022-09-06 | 杭州志和新材料有限公司 | Composite adhesive capable of being simultaneously used for cold adhesive wall cloth and hot adhesive wall cloth and preparation thereof |
| CN115011308B (en) * | 2022-07-20 | 2023-06-16 | 杭州志和新材料有限公司 | Composite adhesive capable of being used for cold adhesive wall cloth and hot adhesive wall cloth simultaneously and preparation method thereof |
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