CN107722724A - A kind of water-based heat sublimation ink and preparation method thereof - Google Patents
A kind of water-based heat sublimation ink and preparation method thereof Download PDFInfo
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- CN107722724A CN107722724A CN201711178786.6A CN201711178786A CN107722724A CN 107722724 A CN107722724 A CN 107722724A CN 201711178786 A CN201711178786 A CN 201711178786A CN 107722724 A CN107722724 A CN 107722724A
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- dispersant
- water
- heat sublimation
- based heat
- dispersion liquid
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/328—Inkjet printing inks characterised by colouring agents characterised by dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/003—Transfer printing
- D06P5/004—Transfer printing using subliming dyes
- D06P5/006—Transfer printing using subliming dyes using specified dyes
Abstract
The invention discloses a kind of water-based heat sublimation ink and preparation method thereof, it is made up of following components in percentage by weight：Disperse dyes dispersion liquid (18 50%), the second dispersant (0.5 5%), the second NMF (20 30%), surfactant (0.5 2%), the second bactericide (0.05 0.2%) and deionized water (25 45%).When making, the second NMF, the second bactericide, surfactant and deionized water are mixed evenly under normal temperature, obtain mixed liquor；Dye dispersion liquid is added into above-mentioned mixed liquor, stirring at low speed 0.5 2 hours under 100 400rpm rotating speed, obtains ink semi-finished product；The physical and chemical parameter for the ink semi-finished product that sampling and testing obtains, its color is adjusted to meeting acceptance criteria.The water-based heat sublimation ink of the present invention has concentration height, and splendid color effect is exported under conditions of few ink ejection amount, and rate of drying is fast, disclosure satisfy that the long-term needs continuously printed.
Description
Technical field
The present invention relates to digital ink-jet printed field, specifically discloses a kind of water-based heat sublimation ink and preparation method thereof.
Background technology
Digital ink-jet printed technology can be satisfied with consumption with its small lot, short processes flow and the characteristics of quickly deliver
The clothes digit printing field of personalized, diversified, the fast fashion of person.Ink-jet printing ink is the key in inkjet technology.
The water-based sublimable ink of digit printing, with its low smell, low volatility, thus has environment-friendly feature, is disappeared by numerous
The person of expense favors.
Polyester fiber is that one of most important textile fabric kind, disperse dyes can be by sublimating into polyester fibre in the world
Tie up intermolecular and make fabric coloring, do not influence the feel of fabric.Status of the disperse dyes in polyester textile is ink-jet printed simultaneously
Very prominent, preparing the water-base ink using disperse dyes as major colorants has important actual application value.Disperse dyes
Water is insoluble or slightly soluble in, therefore surface modification is carried out to disperse dyes by using dispersant, disperse dyes are uniform
It is scattered in WATER AS FLOW MEDIUM, and the performance of keeping humidity of ink is improved by adding appropriate water-miscible organic solvent.To surface-active
The screening of agent is then particularly significant, and suitable surfactant, which may be such that ink while have, adapts to shower nozzle and ultra-thin heat-transferring printing paper.
Heat sublimation ink (also known as thermal transfer ink) is exactly low energy, and the disperse dyes easily to distil are fabricated to digital printing
Ink, it is printed upon on transfer paper, can be within the most short time by the porcelain, metal, change of image making to fineness by heating
In the materials such as fine cloth, being especially suitable for the market of individualized development needs and environmentally friendly requirement.
Thermal transfer ink can be described as heat sublimation ink again, and for heating rotary bat printing product, heat sublimation ink is bright in colour,
It is light clear to be printed upon pattern on paper, after heat transfer machine heating transfer, image clearly, color rendition degree is high, and China's mesh
The producer of previous existence heat production transfer ink has focused largely on Shelter in South China Cities at present, but domestic thermal transfer ink color and luster is shallower, for low
The heat-transferring printing paper of grammes per square metre, it is low the color rate of transform occur, is printed upon on heat-transferring printing paper and easily occurs wrinkling and scratching printhead, causes
Core part (the high loss of printhead).
The content of the invention
The present invention reaches the concentration for improving ink, makes it in few ink ejection amount by preparing a kind of water-based heat sublimation ink
Under conditions of export splendid color effect, while meet the long-term needs continuously printed.
Aqueous dispersion dye paste is ground to nanoscale by advanced high-power nano-milled equipment by the present invention, and
Dispersion is stable；By adjusting physical and chemical parameter, and collocation of colour, it is set to be applied to the digit printing of different type printhead
Machine, have excellent output fluency and shower nozzle performance of keeping humidity, applicability wide.
The technical scheme is that：
A kind of water-based heat sublimation ink, is made up of following components in percentage by weight：
One kind as above technical scheme is improved, and the disperse dyes dispersion liquid is by following components in percentage by weight system
Into：
One kind as above technical scheme is improved, and second dispersant is high polymer dispersion, is propylene
Modified polyether class dispersant, polyacrylate dispersant, the macromolecule containing amino of acids dispersant, the affinity groups containing pigment
Block polymer type dispersant, the high-molecular block copolymer type dispersant of the affinity groups containing pigment, acetylenic diols dispersant with
And any one in surfactant-based dispersant or its any a variety of combination.
One kind as above technical scheme is improved, and second NMF is glycerine, ethylene glycol, ethanol, diethyl two
It is any in alcohol, n-butanol, BDO, diethylene glycol ether, triglyme, butyl carbitol and 1,3-PD
A kind of or its any a variety of combination.
One kind as above technical scheme is improved, and the surfactant is anionic surface surfactant and non-
The combination of any one or two kinds in ionic surfactant.
One kind as above technical scheme is improved, and second bactericide is that BIT class is killed
Microbial inoculum.
One kind as above technical scheme is improved, and the first dispersant in the water-based heat sublimation ink component is high score
The compound of sub- polymer dispersant and small molecule type dispersant, wherein high molecular polymer type dispersant are acrylic compounds point
Powder, modified polyether class dispersant, polyacrylate dispersant, the polymer blocks containing amino of the affinity groups containing pigment gather
High-molecular block copolymer type dispersant, acetylenic diols dispersant and the surface of compound type dispersant, the affinity groups containing pigment
Any one in activating agent class dispersant or its any a variety of combination, small molecule type dispersant are naphthalene sulfonic formaldehyde condensation
Any one in thing, Lignin Dispersants and acetylenic diols dispersant or its any a variety of combination.
As above technical scheme one kind improve, first NMF be ethylene glycol, 1,2-PD, glycerine,
Polyethylene glycol 200, polyethylene glycol 400, Macrogol 600, BDO, 1,2- pentanediols, diethylene glycol and two contractings three
Any one in ethylene glycol or its any a variety of combination, first bactericide is BIT class
Bactericide.
The invention also provides for preparing above-mentioned disperse dyes dispersion liquid method, comprise the following steps：
Step 1：First dispersant, the first NMF, the first bactericide and deionized water are mixed under normal temperature
It is even, obtain mixed liquor；
Step 2：Disperse dyes are added in the mixed liquor obtained into step 1 to grind with grinding zirconium pearl progress high speed shear
Mill, obtain shearing dispersion liquid；
Step 3：The shearing dispersion liquid obtained into step 2 carries out circular grinding with abrasive media, obtains disperse dyes
Dispersion liquid.
The invention also provides the method for preparing above-mentioned water-based heat sublimation ink, comprise the following steps：
Step 1：Second NMF, the second bactericide, surfactant and deionized water are mixed under normal temperature
It is even, obtain mixed liquor；
Step 2：Dye dispersion liquid is added in the mixed liquor obtained into step 1, it is low under 100-400rpm rotating speed
Speed stirring 0.5-2 hours, obtain ink semi-finished product；
Step 3：The physical and chemical parameter of the ink semi-finished product obtained in sampling and testing step 2, adjust its color and test to meeting
Receipts standard.
The present invention is applied in digital decorating machine upper nozzle type based on market, develops two major class high concentration heat sublimation inks：
(1) based on Epson DX5, DX7,5113, TX600, XP800, TFP printhead, Panasonic (Panasonic) printhead
High concentration heat sublimation ink；
(2) it is based on the high concentration heat sublimation of the technical grade printhead such as FujiFilm StarFire 1024, Ricoh GEN5
Ink.
The key technical indexes is as follows：
(1) particle diameter：
(2) physical and chemical parameter：
Suitable for the sublimable ink of Epson Panasonic printheads
Suitable for FujiFilm StarFire 1024, the sublimable ink of the technical grade printhead such as Ricoh GEN5
Compared with prior art, what the present invention obtained has the beneficial effect that：
The water-based heat sublimation ink of the present invention, there is concentration height, the ink dye concentration 1-1.5 used on open market
Times, splendid color effect can be exported under conditions of few ink ejection amount, while meet the long-term needs continuously printed.This project
Heat sublimation ink can be suitably used for ultra-thin heat-transferring printing paper (grammes per square metre ＜ 40g/ ㎡), reach traditional thermal transfer printing paper cost.This item
Mesh heat sublimation ink ink ejection amount is few, and rate of drying is fast, avoids the contamination of collection after stamp graphic printing, while improves the table of ink
Face tension force, prevent that ink is dry in shower nozzle and blocks shower nozzle, it is defeated that the printing of Single pass high-speed digital printings machine can be fully achieved
Go out and holistic cost is suitable with traditional thermal transfer printing cost.
Embodiment
The specific embodiment of the present invention is described in detail below.
Embodiment 1：
Disperse dyes dispersion liquid is made up of following components in percentage by weight：
30% disperse dyes；
20% the first dispersant (acrylic dispersants, modified polyether class dispersant, the polypropylene of the affinity groups containing pigment
Esters of gallic acid dispersant, naphthalene sulfonic formaldehyde condensation compound, Lignin Dispersants and acetylenic diols dispersant, mass ratio 1:1:1:
1:1:1)；
20% the first NMFs (ethylene glycol, 1,2- propane diols, glycerine, polyethylene glycol 200, polyethylene glycol 400 and poly-
Ethylene glycol 600, mass ratio 1:1:1:1:1:1)；
0.2% the first bactericide (BIT series bactericidal agent)；
29.8% deionized water.
Wherein disperse dyes can need to select according to the color of reality, including yellow cultivars are C.I. disperse yellows 34,50,
54,56,60,64,114；Red cultivar is C.I. disperse reds 5,60,75,121,146,179,189,202；Blue kind is
C.I. disperse blue 3,43,54,56,60,83,96,165,295,359,360；Black varieties are C.I. disperse blues 72, disperse blue
359, disperse blue 360, disperse brown 1, disperse brown BR, disperse brown 27, disperse brown BF, disperse red 60, disperse yellow 54, in it is a variety of mixed
Close dyestuff.
First dispersant, the first NMF, the first bactericide and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；The progress high speed shear grinding of zirconium pearl is ground after disperse dyes are added into above-mentioned mixed liquor, obtains shearing dispersion liquid；Again
Abrasive media is added into the shearing dispersion liquid of acquisition and carries out circular grinding, obtains disperse dyes dispersion liquid.
Embodiment 2：
Disperse dyes dispersion liquid is made up of following components in percentage by weight：
20% disperse dyes；
25% the first dispersant (modified polyether class dispersant, polyacrylate dispersant, the wood of the affinity groups containing pigment
Quality dispersant and acetylenic diols dispersant, mass ratio 1:1:2:1)；
(Macrogol 600, BDO, 1,2- pentanediols and diethylene glycol, mass ratio are 25% the first NMFs
1:1:2:2)；
0.5% the first bactericide (BIT series bactericidal agent)；
29.5% deionized water.
Wherein disperse dyes can need to select according to the color of reality, including yellow cultivars are C.I. disperse yellows 34,50,
54,56,60,64,114；Red cultivar is C.I. disperse reds 5,60,75,121,146,179,189,202；Blue kind is
C.I. disperse blue 3,43,54,56,60,83,96,165,295,359,360；Black varieties are C.I. disperse blues 72, disperse blue
359, disperse blue 360, disperse brown 1, disperse brown BR, disperse brown 27, disperse brown BF, disperse red 60, disperse yellow 54, in it is a variety of mixed
Close dyestuff.
First dispersant, the first NMF, the first bactericide and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；The progress high speed shear grinding of zirconium pearl is ground after disperse dyes are added into above-mentioned mixed liquor, obtains shearing dispersion liquid；Again
Abrasive media is added into the shearing dispersion liquid of acquisition and carries out circular grinding, obtains disperse dyes dispersion liquid.
Embodiment 3：
Disperse dyes dispersion liquid is made up of following components in percentage by weight：
16% disperse dyes；
23% the first dispersants (disperse by the high-molecular block copolymer type dispersant of the affinity groups containing pigment, acetylenic diols
Agent, surfactant-based dispersant and naphthalene sulfonic formaldehyde condensation compound, mass ratio 1:1:2:3)；
24% the first NMF (diethylene glycol and triethylene-glycol, mass ratioes 1:1)；
0.3% the first bactericide (BIT series bactericidal agent)；
36.7% deionized water.
Wherein disperse dyes can need to select according to the color of reality, including yellow cultivars are C.I. disperse yellows 34,50,
54,56,60,64,114；Red cultivar is C.I. disperse reds 5,60,75,121,146,179,189,202；Blue kind is
C.I. disperse blue 3,43,54,56,60,83,96,165,295,359,360；Black varieties are C.I. disperse blues 72, disperse blue
359, disperse blue 360, disperse brown 1, disperse brown BR, disperse brown 27, disperse brown BF, disperse red 60, disperse yellow 54, in it is a variety of mixed
Close dyestuff.
First dispersant, the first NMF, the first bactericide and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；The progress high speed shear grinding of zirconium pearl is ground after disperse dyes are added into above-mentioned mixed liquor, obtains shearing dispersion liquid；Again
Abrasive media is added into the shearing dispersion liquid of acquisition and carries out circular grinding, obtains disperse dyes dispersion liquid.
Embodiment 4
Water-based heat sublimation ink is made up of following components in percentage by weight：
50% disperse dyes dispersion liquid；
1% the second dispersant (acrylic dispersants, modified polyether class dispersant, the polypropylene of the affinity groups containing pigment
The polymer blocks copolymerization of esters of gallic acid dispersant, the polymer blocks polymer dispersant containing amino, the affinity groups containing pigment
Thing type dispersant and surfactant-based dispersant, mass ratio 1:1:1:1:1:1)；
22% the second NMF (glycerine, ethylene glycol, ethanol, diethylene glycol and n-butanol, mass ratioes 1:1:1:1:
1)；
1.9% surfactant (anionic surface surfactant and nonionic surface active agent, mass ratio 1:
1)；
0.1% the second bactericide (BIT series bactericidal agent)；
25% deionized water.
Second NMF, the second bactericide, surfactant and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；Dye dispersion liquid is added into above-mentioned mixed liquor, the stirring at low speed 0.5-2 hours under 100-400rpm rotating speed,
Obtain ink semi-finished product；The physical and chemical parameter for the ink semi-finished product that sampling and testing obtains, its color is adjusted to meeting acceptance criteria.
Embodiment 5
Water-based heat sublimation ink is made up of following components in percentage by weight：
30% disperse dyes dispersion liquid；
4% the second dispersant (acrylic dispersants, the modified polyether class dispersants and poly- third of the affinity groups containing pigment
Olefin(e) acid esters dispersant, mass ratio 1:2:1)；
28% the second NMF (BDO, diethylene glycol ether, triglyme, butyl carbitol and 1,3-
Propane diols, mass ratio 1:1:2:2:1)；
1.8% surfactant (anionic surface surfactant and nonionic surface active agent, mass ratio 2:
1)；
0.2% the second bactericide (BIT series bactericidal agent)；
36% deionized water.
Second NMF, the second bactericide, surfactant and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；Dye dispersion liquid is added into above-mentioned mixed liquor, the stirring at low speed 0.5-2 hours under 100-400rpm rotating speed,
Obtain ink semi-finished product；The physical and chemical parameter for the ink semi-finished product that sampling and testing obtains, its color is adjusted to meeting acceptance criteria.
Embodiment 6
Water-based heat sublimation ink is made up of following components in percentage by weight：
20% disperse dyes dispersion liquid；
4% the second dispersant (the polymer blocks polymer dispersant containing amino, the macromolecules of the affinity groups containing pigment
Block copolymer type dispersant, acetylenic diols dispersant and surfactant-based dispersant, mass ratio 1:1:1:3)；
30% the second NMF (ethanol, diethylene glycol and n-butanol, mass ratioes 1:1:3)；
1.8% surfactant (anionic surface surfactant)；
0.2% the second bactericide (BIT series bactericidal agent)；
44% deionized water.
Second NMF, the second bactericide, surfactant and deionized water are mixed evenly under normal temperature, obtained
Mixed liquor；Dye dispersion liquid is added into above-mentioned mixed liquor, the stirring at low speed 0.5-2 hours under 100-400rpm rotating speed,
Obtain ink semi-finished product；The physical and chemical parameter for the ink semi-finished product that sampling and testing obtains, its color is adjusted to meeting acceptance criteria.
By the disperse dyes dispersion liquid obtained in above-described embodiment, and with its as it is above-mentioned apply component ratio in example made from water
Property heat sublimation ink have that concentration is high, and splendid color effect is exported under conditions of few ink ejection amount, rate of drying is fast, energy
It is enough to meet the long-term needs continuously printed.
The above embodiment of the present invention is only intended to clearly illustrate example of the present invention, and is not to the present invention
Embodiment restriction, for those of ordinary skill in the field, can also make on the basis of the above description
Other various forms of changes or variation, can not be exhaustive to all embodiments here, every skill for belonging to the present invention
The obvious changes or variations that art scheme is extended out still in protection scope of the present invention within.
Claims (10)
- A kind of 1. water-based heat sublimation ink, it is characterised in that：It is made up of following components in percentage by weight：
- 2. water-based heat sublimation ink according to claim 1, it is characterised in that：The disperse dyes dispersion liquid is by following heavy The component of amount percentage is made：
- 3. water-based heat sublimation ink according to claim 1, it is characterised in that：Second dispersant is high molecular polymerization Thing dispersant, disperse for acrylic dispersants, modified polyether class dispersant, the polyacrylate of the affinity groups containing pigment Agent, the polymer blocks polymer dispersant containing amino, the affinity groups containing pigment high-molecular block copolymer type dispersant, Any one in acetylenic diols dispersant and surfactant-based dispersant or its any a variety of combination.
- 4. water-based heat sublimation ink according to claim 1, it is characterised in that：Second NMF is glycerine, second Glycol, ethanol, diethylene glycol, n-butanol, BDO, diethylene glycol ether, triglyme, butyl carbitol and 1, Any one in ammediol or its any a variety of combination.
- 5. water-based heat sublimation ink according to claim 1, it is characterised in that：The surfactant is anionic surface The combination of any one or two kinds in surfactant and nonionic surface active agent.
- 6. water-based heat sublimation ink according to claim 1, it is characterised in that：Second bactericide is 1,2- benzisoxas Thiazoline -3- ketone bactericide.
- 7. water-based heat sublimation ink according to claim 2, it is characterised in that：First dispersant is high molecular polymerization The compound of thing type dispersant and small molecule type dispersant, wherein high molecular polymer type dispersant be acrylic dispersants, Modified polyether class dispersant, polyacrylate dispersant, the polymer blocks polymer containing amino of the affinity groups containing pigment High-molecular block copolymer type dispersant, acetylenic diols dispersant and the surface-active of type dispersant, the affinity groups containing pigment Any a variety of combination of any one or its in agent class dispersant, small molecule type dispersant be naphthalene sulfonic formaldehyde condensation compound, Any one in Lignin Dispersants and acetylenic diols dispersant or its any a variety of combination.
- 8. water-based heat sublimation ink according to claim 2, it is characterised in that：First NMF be ethylene glycol, 1, 2- propane diols, glycerine, polyethylene glycol 200, polyethylene glycol 400, Macrogol 600, BDO, 1,2- pentanediols, two Any one in ethylene glycol and triethylene-glycol or its any a variety of combination, first bactericide is 1,2- benzos Isothiazoline -3- ketone bactericide.
- A kind of 9. method of the disperse dyes dispersion liquid prepared described in claim 2, it is characterised in that：Methods described includes following Step：Step 1：First dispersant, the first NMF, the first bactericide and deionized water are mixed evenly under normal temperature, Obtain mixed liquor；Step 2：Disperse dyes are added in the mixed liquor obtained into step 1 with carrying out high speed shear grinding after grinding zirconium pearl, Obtain shearing dispersion liquid；Step 3：Abrasive media is added in the shearing dispersion liquid obtained into step 2 and carries out circular grinding, obtains disperse dyes Dispersion liquid.
- A kind of 10. method for preparing the water-based heat sublimation ink described in claim 1, it is characterised in that：Methods described include with Lower step：Step 1：Second NMF, the second bactericide, surfactant and deionized water are mixed evenly under normal temperature, Obtain mixed liquor；Step 2：Dye dispersion liquid is added in the mixed liquor obtained into step 1, low speed stirs under 100-400rpm rotating speed Mix 0.5-2 hours, obtain ink semi-finished product；Step 3：The physical and chemical parameter of the ink semi-finished product obtained in sampling and testing step 2, adjust its color and marked to examination is met It is accurate.
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Address after: 529400 1st floor, building 3, Shalan Xianke Industrial Park, dahuazhen, Enping City, Jiangmen City, Guangdong Province Applicant after: Guangdong Hongcai New Material Co.,Ltd. Address before: 529467 Shalan Xianke Industrial Park, dahuazhen, Enping, Jiangmen City, Guangdong Province Applicant before: ENPING HONGCAI DIGITAL TECHNOLOGY Co.,Ltd. |
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Application publication date: 20180223 |