CN107670619A - A kind of new proton-exchange reaction stove and application method - Google Patents
A kind of new proton-exchange reaction stove and application method Download PDFInfo
- Publication number
- CN107670619A CN107670619A CN201711021120.XA CN201711021120A CN107670619A CN 107670619 A CN107670619 A CN 107670619A CN 201711021120 A CN201711021120 A CN 201711021120A CN 107670619 A CN107670619 A CN 107670619A
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- China
- Prior art keywords
- wafer
- proton
- exchange reaction
- glass container
- double wall
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J15/00—Chemical processes in general for reacting gaseous media with non-particulate solids, e.g. sheet material; Apparatus specially adapted therefor
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to a kind of proton exchange field, more particularly to a kind of new proton-exchange reaction stove and application method, glass container including horizontal rotation, wafer jig and wafer, proton-exchange reaction solution is provided with the glass container, the wafer jig is axially movably set in the glass container along the glass container inwall, the wafer is laterally embedded in the wafer jig, and the big face of the wafer contacts with the proton-exchange reaction solution, add automatic uniform speed agitating device, improve reaction uniformity, balance reaction environment, and improve the contact surface of wafer and solution, ensure product consistency, make reaction controllability strong, it is easy to operate.
Description
Technical field
The present invention relates to a kind of proton exchange field, more particularly to a kind of new proton-exchange reaction stove and user
Method.
Background technology
Proton exchange is step essential in many chemical reactions, with the continuous development of technology, to proton exchange
The requirement more and more higher of device, and wafer is placed to be vertical in current proton exchange device, without rotating mechanism, only hand
Dynamic shadoof, meeting is insufficient due to stirring, causes liquid in container temperature difference to be up and down present, after solution is reacting a period of time
It will stop reacting when reaching certain balance, stirring need to be lifted manually and promote reaction, make solution concentration uneven, proton exchange is not
Enough abundant, reaction is uneven, and controllability is not strong.
The content of the invention
For above-mentioned weak point of the prior art, the present invention is intended to provide a kind of new proton-exchange reaction stove and making
With method, laterally set using wafer, motion bar is arranged to lift automatically, and adds the automatic Stirring of rotating mechanism, carries
The uniformity of proton-exchange reaction between high wafer, in piece, prevent from being passivated, reach reaction environment balance, make each several part proton
Exchange reaction is consistent, and ensures the temperature constancy of same depth solution in reaction, makes the switching technology process controllability strong, and
It is simple to operate.
To achieve the above object, technical scheme：A kind of new proton-exchange reaction stove and application method, including
Glass container, wafer jig and the wafer of horizontal rotation, proton-exchange reaction solution is provided with the glass container, it is described
Wafer jig is axially movably set in the glass container along the glass container inwall, and the wafer is laterally embedded at described
In wafer jig, and the big face of the wafer contacts with the proton-exchange reaction solution.
Beneficial effects of the present invention：Compared with prior art, a kind of new proton-exchange reaction stove of the present invention and user
Method, lifted using motion bar automatic uniform speed, the rotation of rotating mechanism automatic uniform speed, wafer is horizontal positioned, makes to touch wafer
Solution concentration it is basically identical, so as to control the time of proton-exchange reaction, wafer is fully carried out proton-exchange reaction, ensure
The uniformity and quality stability of proton exchange.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
1- motion bars in accompanying drawing；2- wafer jigs；3- wafers；4- glass containers；5- rotating mechanisms；6- bodies of heater；201-
Screens groove.
Embodiment
The present invention is further described with reference to specific embodiment.
As illustrated, a kind of new proton-exchange reaction stove of the present invention and application method, including the glass of horizontal rotation hold
Device 4, wafer jig 2 and wafer 3, proton-exchange reaction solution, the edge of wafer jig 2 are provided with the glass container 4
The inwall of glass container 4 is axially movably set in the glass container 4, and the wafer 3 is embedded at the wafer jig 2
It is interior, and the 3 big face of wafer contacts with the proton-exchange reaction solution.
Further, motion bar 1 is provided with the wafer jig 2, the top of motion bar 1 is provided with stretching device, institute
State motion bar 1 to be integrally formed with the wafer jig 2, form forked type structure, the stretching device is set as that automatic uniform speed lifts.
Further, in addition to rotating mechanism 5 and body of heater 6, the glass container 4 are fixedly installed on the rotating mechanism 5
Upper end, the main shaft of rotating mechanism 5 pass through the body of heater 6, and the glass container 4 is arranged in the body of heater 6.
Further, the wafer 3 is horizontally set in the wafer jig 2.The wafer 3 includes at least one
Piece, and gap is provided between adjacent two panels.
Further, the wafer jig 2 includes the first double wall and the second double wall that are oppositely arranged, first double wall and
Second double wall upper end is connected by a connecting plate, and multiple relative screens grooves are provided with the inside of first double wall and the second double wall
201, first double wall and the second double wall cross section can be square or circular arc type, and first double wall, the second double wall and company
Fishplate bar is integrally formed.
A kind of application method of new proton-exchange reaction stove, is comprised the following steps that：
S1：The proton-exchange reaction solution of setting is placed in the glass container 4；
S2：Motion bar 1 drives wafer to be stirred about 3；
S3：Rotating mechanism 5 drives the Stirring proton-exchange reaction solution of glass container 4；
S4：Wafer 3 and the abundant haptoreaction of proton-exchange reaction solution, obtain proton exchange product.
Further, it is simple to operate using this method, the motion of motion bar 1 and the automatic uniform speed of rotating mechanism 5, improve wafer
The uniformity that piece 3 contacts with proton-exchange reaction solution, preventing from being passivated, balance reaction environment, whole controllability of reacting is strong, and
It can guarantee that the uniformity and stability of proton exchange product.
The technical scheme provided above the embodiment of the present invention is described in detail, specific case used herein
The principle and embodiment of the embodiment of the present invention are set forth, the explanation of above example is only applicable to help and understands this
The principle of inventive embodiments；Meanwhile for those of ordinary skill in the art, according to the embodiment of the present invention, in specific embodiment party
There will be changes in formula and application, in summary, this specification content should not be construed as limiting the invention.
Claims (7)
1. a kind of new proton-exchange reaction stove, it is characterised in that glass container (4), wafer jig (2) including horizontal rotation
With wafer (3), proton-exchange reaction solution is provided with the glass container (4), the wafer jig (2) is along the glass
Container (4) inwall is axially movably set in the glass container (4), and the wafer (3) is embedded at the wafer jig (2)
It is interior, and the big face of the wafer (3) contacts with the proton-exchange reaction solution.
A kind of 2. new proton-exchange reaction stove as claimed in claim 1, it is characterised in that：Set on the wafer jig (2)
Motion bar (1) is equipped with, motion bar (1) top is provided with stretching device.
A kind of 3. new proton-exchange reaction stove as claimed in claim 1, it is characterised in that：Also include rotating mechanism (5) and
Body of heater (6), the glass container (4) are fixedly installed on the rotating mechanism (5) upper end, and rotating mechanism (5) main shaft passes through
The body of heater (6), the glass container (4) are arranged in the body of heater (6).
A kind of 4. new proton-exchange reaction stove as claimed in claim 1, it is characterised in that：The wafer (3) laterally sets
It is placed in the wafer jig (2).
A kind of 5. new proton-exchange reaction stove as claimed in claim 1, it is characterised in that：The wafer (3) is included extremely
It is few a piece of, and gap is provided between adjacent two panels.
A kind of 6. new proton-exchange reaction stove as claimed in claim 1, it is characterised in that：The wafer jig (2) includes
The first double wall and the second double wall being oppositely arranged, first double wall and the second double wall upper end are connected by a connecting plate, described
Multiple screens grooves (201) are provided with the inside of first double wall and the second double wall.
A kind of 7. application method of new proton-exchange reaction stove, it is characterised in that
S1：The proton-exchange reaction solution of setting is placed in the glass container (4)；
S2：Motion bar (1) drives wafer (3) to stir up and down；
S3：Rotating mechanism (5) drives glass container (4) Stirring solution；
S4：Wafer (3) and the abundant haptoreaction of solution, obtain proton exchange product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711021120.XA CN107670619A (en) | 2017-10-27 | 2017-10-27 | A kind of new proton-exchange reaction stove and application method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711021120.XA CN107670619A (en) | 2017-10-27 | 2017-10-27 | A kind of new proton-exchange reaction stove and application method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107670619A true CN107670619A (en) | 2018-02-09 |
Family
ID=61142260
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711021120.XA Pending CN107670619A (en) | 2017-10-27 | 2017-10-27 | A kind of new proton-exchange reaction stove and application method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107670619A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06281830A (en) * | 1993-03-25 | 1994-10-07 | Ngk Insulators Ltd | Manufacture of optical waveguide substrate |
| JP2000241646A (en) * | 1999-02-17 | 2000-09-08 | Tokimec Inc | Manufacture of optical waveguide |
| CN205570297U (en) * | 2016-03-17 | 2016-09-14 | 广东裕田霸力科技股份有限公司 | Can regulate and control stirring reation kettle of temperature automatically |
-
2017
- 2017-10-27 CN CN201711021120.XA patent/CN107670619A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06281830A (en) * | 1993-03-25 | 1994-10-07 | Ngk Insulators Ltd | Manufacture of optical waveguide substrate |
| JP2000241646A (en) * | 1999-02-17 | 2000-09-08 | Tokimec Inc | Manufacture of optical waveguide |
| CN205570297U (en) * | 2016-03-17 | 2016-09-14 | 广东裕田霸力科技股份有限公司 | Can regulate and control stirring reation kettle of temperature automatically |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180209 |