CN107668719A - A kind of preparation method of celestial grass concentrate - Google Patents
A kind of preparation method of celestial grass concentrate Download PDFInfo
- Publication number
- CN107668719A CN107668719A CN201711191367.6A CN201711191367A CN107668719A CN 107668719 A CN107668719 A CN 107668719A CN 201711191367 A CN201711191367 A CN 201711191367A CN 107668719 A CN107668719 A CN 107668719A
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- celestial grass
- concentrate
- preparation
- small molecule
- flavor substance
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- 244000025254 Cannabis sativa Species 0.000 title claims abstract description 92
- 239000012141 concentrate Substances 0.000 title claims abstract description 79
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000012528 membrane Substances 0.000 claims abstract description 50
- 239000000796 flavoring agent Substances 0.000 claims abstract description 47
- 235000019634 flavors Nutrition 0.000 claims abstract description 47
- 239000000126 substance Substances 0.000 claims abstract description 45
- 150000003384 small molecules Chemical class 0.000 claims abstract description 36
- 239000000919 ceramic Substances 0.000 claims abstract description 24
- 238000001223 reverse osmosis Methods 0.000 claims abstract description 18
- 239000000341 volatile oil Substances 0.000 claims abstract description 8
- 238000001802 infusion Methods 0.000 claims description 32
- 239000007788 liquid Substances 0.000 claims description 28
- 239000000463 material Substances 0.000 claims description 28
- 239000003292 glue Substances 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
- 238000001914 filtration Methods 0.000 claims description 15
- 230000001954 sterilising effect Effects 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 12
- 238000004659 sterilization and disinfection Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 238000012859 sterile filling Methods 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 6
- 238000011084 recovery Methods 0.000 claims description 6
- 230000000149 penetrating effect Effects 0.000 claims description 5
- 244000307697 Agrimonia eupatoria Species 0.000 abstract description 5
- 235000000125 common agrimony Nutrition 0.000 abstract description 5
- 150000004676 glycans Polymers 0.000 abstract description 5
- 229920001282 polysaccharide Polymers 0.000 abstract description 5
- 239000005017 polysaccharide Substances 0.000 abstract description 5
- 150000004804 polysaccharides Polymers 0.000 abstract description 5
- 125000003118 aryl group Chemical group 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 3
- 238000000926 separation method Methods 0.000 description 4
- 238000000108 ultra-filtration Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 102000011759 adducin Human genes 0.000 description 1
- 108010076723 adducin Proteins 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229910052809 inorganic oxide Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Botany (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation method of celestial grass concentrate, celestial grass aromatic substance is collected using essential oil retracting device first, hairgvein agrimony poly saccharide gum is intercepted with ceramic membrane and concentrated again, then concentrate the small molecule flavor substance of permeation ceramic membrane with reverse osmosis membrane and concentrated, finally celestial grass aromatic substance, ceramic membrane concentrate and reverse osmosis membrane concentrate are mixed, natural flavour mountaineous celestial grass concentrate is made.The present invention can farthest collect and retain the natural flavour mountaineous of celestial grass, so as to ensure that not only concentration is higher than market like product to the celestial grass concentrate of preparation, and with completely unique celestial grass fragrance matter, and extend the service life of membrane component.
Description
Technical field
The present invention relates to biological technical field, and in particular to a kind of preparation method of celestial grass concentrate.
Background technology
Existing celestial grass concentrate on the market, all it is that will directly be concentrated extract solution after celestial grass progress infusion, it is a kind of
Mode is to use vacuum-concentrcted, and its shortcoming is the evaporation with moisture, and the aromatic substance of celestial grass is all lost in.Now on the market
Generally directly concentrated using reverse osmosis membrane concentration, its advantage is can to retain aromatic substance, but because is burnt among celestial grass concentrate
Containing substantial amounts of natural plant gum, this sticky celestial grass glue is very easy to block the hole of membrane component, thus in concentration process with
The increase of concentration carrys out huge pressure to film strips, because the material of reverse osmosis membrane is all organic fiber film, proof pressure is limited, mistake
The concentration of degree can cause the damage of membrane component.So the existing celestial grass glue concentrate made on the market using film concentration technique, its is dense
Degree is no more than 6 ° of B é.In addition, sticky celestial grass glue, which blocks membrane component, causes not easy cleaning, the residual of larger molecular organics matter is easy
Breed bacteria, have a strong impact on the life-span of membrane component.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of preparation method of celestial grass concentrate, uses
Celestial grass concentrate concentration prepared by this method is higher, and can extend the service life of membrane component.
To achieve the above object, the present invention uses following technical scheme:
A kind of preparation method of celestial grass concentrate, comprises the following steps:
1) infusion and recovery volatile materials
Celestial grass is put into counterflow extraction apparatus, by material-water ratio 1:15-20 adds 95-98 DEG C of water, and celestial grass infusion 1.5-2 is small
When, while open the collection infusion of essential oil retracting device and cross volatile materials caused by Cheng Qian 25-30min, the volatility of collection
Material is about 1 with the celestial grass proportion of input:1;
Adverse current extraction process, for celestial grass from advancing toward next device orientation at dog-house, the volatile materials of collection is from celestial grass
Dog-house is put into play for celestial grass fragrance from volatile materials caused by this stage at dog-house 2-3 rice, the stage to celestial grass
The most dense stage;
2)Filtering
After infusion terminates, feed liquid is cooled down and centrifuges, filter;
3)Ceramic membrane concentrates
Feed liquid after filtering uses aperture to be concentrated for 180-200nm ceramic membrane, it will divide greatly under conditions of high flow capacity high pressure
Sub- celestial grass glue(Molecular weight about 5-20 ten thousand)Separated with small molecule flavor substance, and it is dense that macromolecular celestial grass glue is concentrated to give into celestial grass glue
Contracting liquid;
4)Reverse osmosis membrane concentrates
The small molecule flavor substance that will transmit through ceramic membrane is concentrated using reverse osmosis membrane, by small point under conditions of high flow capacity high pressure
Sub- flavor substance and water are separated, and small molecule flavor substance is concentrated to give into small molecule flavor substance concentrate;
5)Mixing filling
By step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule
Flavor substance concentrate mixes, and obtains celestial grass concentrate, then carries out high-temperature instantaneous sterilization, sterile filling.
The step 1), material-water ratio 1:15.
The step 1), infusion process keeps water to be in slight boiling condition toward spraying into steam in counterflow extraction apparatus.
The step 2)Concrete operations be:Steam off, open heat exchanger and feed liquid is cooled down, control drop temperature
Below 45 DEG C, feed liquid is centrifuged using disk centrifugal separator, is then filtered.
The step 2), the feed liquid turbidity control after filtering is in below 30NTU.
The step 3), the concentration for the celestial grass glue concentrate being concentrated to give is 10-15 ° of B é.
The step 4), the concentration for the small molecule flavor substance concentrate being concentrated to give is 10-15 ° of B é.
The step 5), be mixed to get the concentration of celestial grass concentrate is 13-14 ° of B é.
The step 5), sterilization temperature is 134-140 DEG C, and sterilizing time is the 4-6 seconds.
The present invention uses above technical scheme, on the characteristic for being fully understood by celestial grass natural plant gum and the basis of molecular structure
On, first using essential oil retracting device, its volatile materials is collected during the extraction of celestial grass infusion, then by extract solution
Filtering, is divided the celestial grass flavor substance of the hairgvein agrimony poly saccharide gum in extract solution and other small molecules using ultrafiltration ceramic membrane element
From, while hairgvein agrimony poly saccharide gum is concentrated, because using ultrafiltration ceramic membrane, its material is to use inorganic oxide zirconium, tool
There are antipollution, high mechanical strength, heatproof, the advantages of high pressure resistant, permeability is good, regenerability is good, hairgvein agrimony poly saccharide gum concentration can be dense
10-15 ° of B é is reduced to, then again by the dialyzate of ultrafiltration(That is celestial grass flavor substance)Concentrated with reverse osmosis membrane, because the material
Hairgvein agrimony poly saccharide gum has not been contained in liquid, it is inviscid, it is not easily blocked, is not easy to pollute membrane component, can improve membrane component uses the longevity
Life, therefore the burden of reverse osmosis membrane concentration can be substantially reduced, celestial grass dialyzate can be concentrated into the case of same operation pressure
10-15 ° of B é, volatile materials, celestial grass glue concentrate and small molecule flavor substance concentrate then in conjunction with collection, mixing system
Into with natural flavour mountaineous celestial grass concentrate.
Farthest collected in whole process procedure of the invention and retain the natural flavour mountaineous of celestial grass, plus advanced high temperature
Wink sterilization technology and sterile filling, so as to ensure that not only concentration is higher than the similar production in market for celestial grass concentrate prepared by the inventive method
Product, and with completely unique celestial grass fragrance matter, there is peerless flavor advantage.
Embodiment
A kind of preparation method of celestial grass concentrate, comprises the following steps:
1) infusion and recovery volatile materials
Celestial grass is put into counterflow extraction apparatus, by material-water ratio 1:15-20 adds 95-98 DEG C of water, and celestial grass infusion 1.5-2 is small
When, infusion process keeps water to be in slight boiling condition toward penetrating steam in counterflow extraction apparatus, while opens essential oil retracting device receipts
Volatile materials caused by Cheng Qian 25-30min is crossed in collection infusion, and the volatile materials of collection is about 1 with the celestial grass proportion of input:
2;
2)Filtering
After infusion terminates, steam off, open heat exchanger and feed liquid is cooled down, control drop temperature is below 45 DEG C, feed liquid
Centrifuged using disk centrifugal separator, then filtered, feed liquid turbidity is controlled in below 30NTU.
3)Ceramic membrane concentrates
Feed liquid after filtering uses aperture to be concentrated for 180-200nm ceramic membrane, it will divide greatly under conditions of high flow capacity high pressure
Sub- celestial grass glue and small molecule flavor substance separation, and macromolecular celestial grass glue is concentrated to give celestial grass glue of the concentration for 10-15 ° of B é
Concentrate;
4)Reverse osmosis membrane concentrates
The small molecule flavor substance that will transmit through ceramic membrane is concentrated using reverse osmosis membrane, by small point under conditions of high flow capacity high pressure
Sub- flavor substance and water are separated, and small molecule flavor substance is concentrated to give into small molecule flavor of the concentration for 10-15 ° of B é
Material concentrate;
5)Mixing filling
By step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule
Flavor substance concentrate mixes, and obtains celestial grass concentrate(Concentration is 13-14 ° of B é), then carry out high-temperature instantaneous sterilization(Temperature
134-140 DEG C, the sterilizing time 4-6 seconds), sterile filling.
Embodiment 1
A kind of preparation method of celestial grass concentrate, comprises the following steps:
1) infusion and recovery volatile materials
Celestial grass is put into counterflow extraction apparatus, by material-water ratio 1:15 add 95 DEG C of water, by celestial grass infusion 1.5 hours, infusion
Process keeps water to be in slight boiling condition toward penetrating steam in counterflow extraction apparatus, while opens essential oil retracting device and collect infusion
Volatile materials caused by Cheng Qian 25min;
2)Filtering
After infusion terminates, steam off, open heat exchanger and feed liquid is cooled down, control drop temperature is below 45 DEG C, feed liquid
Centrifuged using disk centrifugal separator, then filtered, feed liquid turbidity is controlled in below 30NTU.
3)Ceramic membrane concentrates
Feed liquid after filtering uses aperture to be concentrated for 180nm ceramic membrane, it is under conditions of high flow capacity high pressure that macromolecular is celestial
Herb rubber and the separation of small molecule flavor substance, and macromolecular celestial grass glue is concentrated to give celestial grass glue concentrate of the concentration for 10 ° of B é;
4)Reverse osmosis membrane concentrates
The small molecule flavor substance that will transmit through ceramic membrane is concentrated using reverse osmosis membrane, by small point under conditions of high flow capacity high pressure
Sub- flavor substance and water are separated, and small molecule flavor substance is concentrated to give into small molecule flavor substance of the concentration for 10 ° of B é
Concentrate;
5)Mixing filling
By step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule
Flavor substance concentrate mixes, and obtains celestial grass concentrate, then carries out high-temperature instantaneous sterilization(134 DEG C of temperature, sterilizing time 6
Second), sterile filling.
Embodiment 2
A kind of preparation method of celestial grass concentrate, comprises the following steps:
1) infusion and recovery volatile materials
Celestial grass is put into counterflow extraction apparatus, by material-water ratio 1:20 add 98 DEG C of water, by celestial grass infusion 2 hours, infusion
Journey keeps water to be in slight boiling condition toward penetrating steam in counterflow extraction apparatus, while opens essential oil retracting device and collect infusion process
Volatile materials caused by preceding 30min;
2)Filtering
After infusion terminates, steam off, open heat exchanger and feed liquid is cooled down, control drop temperature is below 45 DEG C, feed liquid
Centrifuged using disk centrifugal separator, then filtered, feed liquid turbidity is controlled in 30 below NTU.
3)Ceramic membrane concentrates
Feed liquid after filtering uses aperture to be concentrated for 200nm ceramic membrane, it is under conditions of high flow capacity high pressure that macromolecular is celestial
Herb rubber and the separation of small molecule flavor substance, and macromolecular celestial grass glue is concentrated to give celestial grass glue concentrate of the concentration for 15 ° of B é;
4)Reverse osmosis membrane concentrates
The small molecule flavor substance that will transmit through ceramic membrane is concentrated using reverse osmosis membrane, by small point under conditions of high flow capacity high pressure
Sub- flavor substance and water are separated, and small molecule flavor substance is concentrated to give into small molecule flavor substance of the concentration for 15 ° of B é
Concentrate;
5)Mixing filling
By step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule
Flavor substance concentrate mixes, and obtains celestial grass concentrate, then carries out high-temperature instantaneous sterilization(140 DEG C of temperature, sterilizing time 4
Second), sterile filling.
Embodiment 3
A kind of preparation method of celestial grass concentrate, comprises the following steps:
1) infusion and recovery volatile materials
Celestial grass is put into counterflow extraction apparatus, by material-water ratio 1:18 add 96 DEG C of water, by celestial grass infusion 1.8 hours, infusion
Process keeps water to be in slight boiling condition toward penetrating steam in counterflow extraction apparatus, while opens essential oil retracting device and collect infusion
Volatile materials caused by Cheng Qian 30min;
2)Filtering
After infusion terminates, steam off, open heat exchanger and feed liquid is cooled down, control drop temperature is below 45 DEG C, feed liquid
Centrifuged using disk centrifugal separator, then filtered, feed liquid turbidity is controlled in 30 below NTU.
3)Ceramic membrane concentrates
Feed liquid after filtering uses aperture to be concentrated for 200nm ceramic membrane, it is under conditions of high flow capacity high pressure that macromolecular is celestial
Herb rubber and the separation of small molecule flavor substance, and macromolecular celestial grass glue is concentrated to give celestial grass glue concentrate of the concentration for 13 ° of B é;
4)Reverse osmosis membrane concentrates
The small molecule flavor substance that will transmit through ceramic membrane is concentrated using reverse osmosis membrane, by small point under conditions of high flow capacity high pressure
Sub- flavor substance and water are separated, and small molecule flavor substance is concentrated to give into small molecule flavor substance of the concentration for 13 ° of B é
Concentrate;
5)Mixing filling
By step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule
Flavor substance concentrate mixes, and obtains celestial grass concentrate, then carries out high-temperature instantaneous sterilization(138 DEG C of temperature, sterilizing time 5
Second), sterile filling.
The foregoing is only presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification, it should all belong to the covering scope of the present invention.
Claims (9)
- A kind of 1. preparation method of celestial grass concentrate, it is characterised in that:It comprises the following steps:1) infusion and recovery volatile materialsCelestial grass is put into counterflow extraction apparatus, by material-water ratio 1:15-20 adds 95-98 DEG C of water, and celestial grass infusion 1.5-2 is small When, while open the collection infusion of essential oil retracting device and cross volatile materials caused by Cheng Qian 25-30min;2)FilteringAfter infusion terminates, feed liquid is cooled down and centrifuges, filter;3)Ceramic membrane concentratesFeed liquid after filtering uses aperture to be concentrated for 180-200nm ceramic membrane, obtains by the macromolecular celestial grass of ceramic membrane interception The small molecule flavor substance of glue and permeation ceramic membrane, and macromolecular celestial grass glue is concentrated to give celestial grass glue concentrate,4)Reverse osmosis membrane concentratesAbove-mentioned small molecule flavor substance is concentrated using reverse osmosis membrane, small molecule flavor substance and water are separated, and will be small Molecule flavor substance is concentrated to give small molecule flavor substance concentrate;5)Mixing fillingBy step 1)Obtained volatile materials, step 3)The collection celestial grass glue concentrate and step 4 obtained)Obtained small molecule Flavor substance concentrate mixes, and obtains celestial grass concentrate, then carries out high-temperature instantaneous sterilization, sterile filling.
- A kind of 2. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 1), expect water Than for 1:15.
- A kind of 3. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 1), infusion Process keeps water to be in slight boiling condition toward penetrating steam in counterflow extraction apparatus.
- A kind of 4. preparation method of celestial grass concentrate according to claim 3, it is characterised in that:The step 2)It is specific Operate and be:Steam off, open heat exchanger and feed liquid is cooled down, for control drop temperature below 45 DEG C, feed liquid uses dish-style Centrifuge is centrifuged, and is then filtered.
- A kind of 5. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 2), filtering Feed liquid turbidity afterwards is controlled in below 30NTU.
- A kind of 6. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 3), concentration The concentration of obtained celestial grass glue concentrate is 10-15 ° of B é.
- A kind of 7. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 4), concentration The concentration of obtained small molecule flavor substance concentrate is 10-15 ° of B é.
- A kind of 8. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 5), mixing Obtain the concentration of celestial grass concentrate is 13-14 ° of B é.
- A kind of 9. preparation method of celestial grass concentrate according to claim 1, it is characterised in that:The step 5), sterilization Temperature is 134-140 DEG C, and sterilizing time is the 4-6 seconds.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108477615A (en) * | 2018-04-16 | 2018-09-04 | 福建省力菲克生物技术有限公司 | A kind of celestial grass composite powder and preparation method thereof |
CN110521894A (en) * | 2019-08-16 | 2019-12-03 | 湖南艾达伦科技有限公司 | A kind of sweet Momordica grosvenori Flavor decoloration inspissated juice and preparation method thereof |
CN113877241A (en) * | 2021-11-25 | 2022-01-04 | 凭祥生和堂健康食品有限公司 | Preparation method of Mesona chinensis Benth concentrated solution |
CN115005354A (en) * | 2022-06-25 | 2022-09-06 | 可菲生物科技有限公司 | Preparation method of compound herbaceous plant reaction flavor substance |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108477615A (en) * | 2018-04-16 | 2018-09-04 | 福建省力菲克生物技术有限公司 | A kind of celestial grass composite powder and preparation method thereof |
CN110521894A (en) * | 2019-08-16 | 2019-12-03 | 湖南艾达伦科技有限公司 | A kind of sweet Momordica grosvenori Flavor decoloration inspissated juice and preparation method thereof |
CN113877241A (en) * | 2021-11-25 | 2022-01-04 | 凭祥生和堂健康食品有限公司 | Preparation method of Mesona chinensis Benth concentrated solution |
CN115005354A (en) * | 2022-06-25 | 2022-09-06 | 可菲生物科技有限公司 | Preparation method of compound herbaceous plant reaction flavor substance |
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