CN107663001A - A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent - Google Patents
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent Download PDFInfo
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- CN107663001A CN107663001A CN201710866223.XA CN201710866223A CN107663001A CN 107663001 A CN107663001 A CN 107663001A CN 201710866223 A CN201710866223 A CN 201710866223A CN 107663001 A CN107663001 A CN 107663001A
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- trichloroethanes
- sewage sludge
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/004—Sludge detoxification
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/36—Organic compounds containing halogen
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
- C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
- C02F2103/365—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds from petrochemical industry (e.g. refineries)
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fire-Extinguishing Compositions (AREA)
- Treatment Of Sludge (AREA)
Abstract
The invention discloses a kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：8 15 parts of acrylamide, 48 parts of bodied ferric sulfate, 38 parts of flavonoids, 38 parts of butyric acid potassium, 25 parts of sodium metaaluminate, 5 10 parts of hydroxylamine hydrochloride, 14 parts of tartaric acid, 28 parts of yellow cinnamon leaf, 28 parts of corncob, 49 parts of blue-green algae, 36 parts of activated carbon, 25 parts of magnesium phosphate, 13 parts of enoxolone, 13 parts of alkyl-glucoside, 13 parts of enuatrol, 0.1 1 parts of ethylparaben.The trichloroethanes Contaminated Sewage Sludge inorganic agent of the present invention has the advantages of processing method is simple, treatment effeciency is high, and with strong points, trichloroethanes fixed rate is more than 96.2%；Preparation technology is simple, and equipment requirement is low, beneficial to industrialized production and marketing.
Description
Technical field
The present invention relates to a kind of sludge treating agent, specifically a kind of trichloroethanes Contaminated Sewage Sludge efficient process agent.
Background technology
With China's rapid development of economy, automobile quantity steeply rises, and gas station and buried tank are in each geaster sieve
Scattered all over like men on a chessboard and quantity is growing day by day.But because design management is not good at, for these oil storage tanks when embedded, majority does not take into full account tank body
Intensity and corresponding leakage barrier measure, once a leak occurs, will cause seriously to pollute to Soil Surrounding, underground water.Especially with
The aging of Oil Tank Body, this problem will be protruded more.Therefore, pollution of the industry such as oil and chemical industry to soil, especially
It is that wherein substantial amounts of volatile organic matter (Volatile Organic Compounds, VOCs) is polluted to caused by soil,
China increasingly attracts people's attention.
Volatile organic matter in soil has it to be different from the dirt of other pollutants as a kind of special soil pollutant
Characteristic is contaminated, and because of its complicated component and harmfulness, is listed in environment the murder by poisoning contact scar that potentially danger is big, answers priority acccess control
Thing.Therefore, external many developed countries have expressly provided, to that must be carried out appropriate place by volatile organic matter contaminated soil
Put, to ensure the safety of biology and its environment.Although China not yet puts into effect corresponding standard to VOCs-contaminated Soils
It is controlled with regulation, but has caused portion of government in domestic a small number of flourishing cities such as Shanghai, the harm problem of volatile organic matter
The great attention of door, how rationally and effectively to dispose VOCs-contaminated Soils turns into the technical barrier for being badly in need of solving.
Trichloroethanes is as a kind of volatile organism, the raw material as vinylidene chloride, the intermediate of resin, agriculturally
Fumigant, insecticide, grease, wax, rubber, the solvent of acetate fiber, dyestuff, the extractant etc. of spices, high dose has anesthesia
Effect, can cause death when serious；Therefore the improvement and reparation to trichloroethanes Contaminated Sewage Sludge, is very urgent task.It is existing
Some sludge treating agents do not have specific aim, and treatment effect is poor；Meanwhile preparation process is cumbersome, equipment requirement is high, is unfavorable for work
Industry metaplasia is produced and marketing.Therefore, the present invention provides a kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, and provides the trichlorine
The preparation method of ethane Contaminated Sewage Sludge efficient process agent.
The content of the invention
It is an object of the invention to provide a kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, to solve above-mentioned background technology
The problem of middle proposition.
To achieve the above object, the present invention provides following technical scheme：
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：Acrylamide 8-15 parts,
Bodied ferric sulfate 4-8 parts, flavonoids 3-8 parts, butyric acid potassium 3-8 parts, sodium metaaluminate 2-5 parts, hydroxylamine hydrochloride 5-10 parts, winestone
Sour 1-4 parts, yellow cinnamon leaf 2-8 parts, corncob 2-8 parts, blue-green algae 4-9 parts, activated carbon 3-6 parts, magnesium phosphate 2-5 parts, enoxolone 1-3
Part, alkyl-glucoside 1-3 parts, enuatrol 1-3 parts, ethylparaben 0.1-1 parts.
As the further scheme of the present invention：Include the raw material of following parts by weight：10 parts of acrylamide, bodied ferric sulfate
7 parts, 5 parts of flavonoids, 5 parts of butyric acid potassium, 4 parts of sodium metaaluminate, 6 parts of hydroxylamine hydrochloride, 2 parts of tartaric acid, 5 parts of yellow cinnamon leaf, corn
5 parts of core, 6 parts of blue-green algae, 4 parts of activated carbon, 3 parts of magnesium phosphate, 2 parts of enoxolone, 2 parts of alkyl-glucoside, 2 parts of enuatrol, Ni Bo
Golden 0.5 part of ethyl ester.
As the further scheme of the present invention：The flavonoids uses Quercetin, cyanidenon, catechin and OPC
In one or more.
A kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent, preparation process are：
(1) by acrylamide, bodied ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid
Mixing, by mixer mixing 25-40min, obtains mixture A；
(2) magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, passes through mixer mixing 10-
20min, obtain mixture B；
(3) yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, sieve 50-100 mesh,
Then mix and produce mixed-powder, mixed-powder is placed at 5-15 DEG C and stored, it is standby；
(4) mixed-powder obtained by upper step is mixed with mixture A, mixture B, is sealed at 5-10 DEG C and be stirred 25-
40min, 10-20min is then shaken using microwave, got product.
As the further scheme of the present invention：Step (1) is by acrylamide, bodied ferric sulfate, flavonoids, indolebutyric acid
Potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid mixing, by mixer mixing 30min, obtain mixture A.
As the further scheme of the present invention：Step (2) is by magnesium phosphate, enoxolone, ethylparaben and alkyl grape
Glucosides mixes, and by mixer mixing 14min, obtains mixture B.
As the further scheme of the present invention：Step (3) mixes yellow cinnamon leaf, activated carbon, corncob and blue-green algae, passes through respectively
Cross and dry, after grinding, sieve 60 mesh, then mixes and produces mixed-powder, mixed-powder is placed at 8 DEG C and stored, standby.
As the further scheme of the present invention：Step (4) mixes mixed-powder obtained by upper step with mixture A, mixture B
Close, sealed at 6 DEG C and be stirred 32min, 12min is then shaken using microwave, got product.
As the further scheme of the present invention：The power of step (4) the sonic oscillation processing is 1000-2000W.
Compared with prior art, the beneficial effects of the invention are as follows：
The trichloroethanes Contaminated Sewage Sludge inorganic agent of the present invention is a kind of having for the serious Contaminated Sewage Sludge soil of trichloroethanes
The processing soil treatment agent of effect, it has significant treatment effect, and trichloroethanes fixed rate is more than 96.2%；Processing method is simple, place
Efficiency high is managed, the present invention can make to be reached GB15618-2008 marks by the physical and chemical index of the serious Contaminated Sewage Sludge soil of trichloroethanes
It is accurate；Preparation technology of the present invention is simple, and equipment requirement is low, beneficial to industrialized production and marketing.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Embodiment 1
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：8 parts of acrylamide, gather
Close 4 parts of ferric sulfate, 3 parts of flavonoids, 3 parts of butyric acid potassium, 2 parts of sodium metaaluminate, 5 parts of hydroxylamine hydrochloride, 1 part of tartaric acid, yellow cinnamon leaf 2
Part, 2 parts of corncob, 4 parts of blue-green algae, 3 parts of activated carbon, 2 parts of magnesium phosphate, 1 part of enoxolone, 1 part of alkyl-glucoside, enuatrol 1
Part, 0.1 part of ethylparaben.The flavonoids uses Quercetin.
A kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent, preparation process are：(1) by acrylamide, poly-
Ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid mixing are closed, by mixer mixing 25min,
Obtain mixture A；(2) magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, mixed by mixer
10min, obtain mixture B；(3) yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, mistake
50 mesh are sieved, then mixes and produces mixed-powder, mixed-powder is placed at 5 DEG C and stored, it is standby；(4) by mixed powder obtained by upper step
End mixes with mixture A, mixture B, and sealing at 5 DEG C is stirred 25min, then shakes 10min using microwave, produces into
Product；The power of sonic oscillation processing is 1000W.
Embodiment 2
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：15 parts of acrylamide, gather
Close 8 parts of ferric sulfate, 8 parts of flavonoids, 8 parts of butyric acid potassium, 5 parts of sodium metaaluminate, 10 parts of hydroxylamine hydrochloride, 4 parts of tartaric acid, yellow cinnamon leaf
8 parts, 8 parts of corncob, 9 parts of blue-green algae, 6 parts of activated carbon, 5 parts of magnesium phosphate, 3 parts of enoxolone, 3 parts of alkyl-glucoside, enuatrol 3
Part, 1 part of ethylparaben.The flavonoids is using Quercetin, cyanidenon.
A kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent, preparation process are：(1) by acrylamide, poly-
Ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid mixing are closed, by mixer mixing 40min,
Obtain mixture A；(2) magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, mixed by mixer
20min, obtain mixture B；(3) yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, mistake
100 mesh are sieved, then mixes and produces mixed-powder, mixed-powder is placed at 15 DEG C and stored, it is standby；(4) will be mixed obtained by upper step
Powder mixes with mixture A, mixture B, is sealed at 10 DEG C and is stirred 40min, then shakes 20min using microwave, i.e.,
Obtain finished product；The power of sonic oscillation processing is 2000W.
Embodiment 3
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：10 parts of acrylamide, gather
Close 7 parts of ferric sulfate, 5 parts of flavonoids, 5 parts of butyric acid potassium, 4 parts of sodium metaaluminate, 6 parts of hydroxylamine hydrochloride, 2 parts of tartaric acid, yellow cinnamon leaf 5
Part, 5 parts of corncob, 6 parts of blue-green algae, 4 parts of activated carbon, 3 parts of magnesium phosphate, 2 parts of enoxolone, 2 parts of alkyl-glucoside, enuatrol 2
Part, 0.5 part of ethylparaben.The flavonoids is using Quercetin, cyanidenon, catechin.
A kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent, preparation process are：(1) by acrylamide, poly-
Ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid mixing are closed, by mixer mixing 30min,
Obtain mixture A.(2) magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, mixed by mixer
14min, obtain mixture B.(3) yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, mistake
60 mesh are sieved, then mixes and produces mixed-powder, mixed-powder is placed at 8 DEG C and stored, it is standby.(4) by mixed powder obtained by upper step
End mixes with mixture A, mixture B, is sealed at 6 DEG C and is stirred 32min, then shaken 12min using microwave, produce into
Product.The power of sonic oscillation processing is 1200W.
Embodiment 4
A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, include the raw material of following parts by weight：9 parts of acrylamide, gather
Close 7 parts of ferric sulfate, 4.5 parts of flavonoids, 7 parts of butyric acid potassium, 3.5 parts of sodium metaaluminate, 8.5 parts of hydroxylamine hydrochloride, tartaric acid 1.5
Part, 7.5 parts of yellow cinnamon leaf, 2.8 parts of corncob, 4.9 parts of blue-green algae, 3.5 parts of activated carbon, 2.5 parts of magnesium phosphate, 2.5 parts of enoxolone, alkane
1.8 parts of base glucoside, 2.5 parts of enuatrol, 0.2 part of ethylparaben.The flavonoids is using Quercetin, cyanidenon, youngster
Theine and OPC.
A kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent, preparation process are：(1) by acrylamide, poly-
Ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid mixing are closed, by mixer mixing 28min,
Obtain mixture A；(2) magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, mixed by mixer
18min, obtain mixture B；(3) yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, mistake
90 mesh are sieved, then mixes and produces mixed-powder, mixed-powder is placed at 11 DEG C and stored, it is standby；(4) by mixed powder obtained by upper step
End mixes with mixture A, mixture B, is sealed at 8 DEG C and is stirred 36min, then shaken 11min using microwave, produce into
Product；The power of sonic oscillation processing is 1500W.
Experimental example
Excavated using excavator to polluting soil to be repaired, above-described embodiment 1-4 inorganic agent is added in dirt
After the surface of the soil of dye applies the inorganic agent of 2cm thickness, by soil thick polluted soil top layer 20cm and the processing of application
Agent is well mixed by way of turning over, and after 7 days, carries out sampling monitoring, test result see the table below.
Table sampling monitoring result
As can be seen here, the trichloroethanes Contaminated Sewage Sludge inorganic agent that prepared by the present invention is that one kind seriously pollutes for trichloroethanes
The effective processing soil treatment agent of sludge soil, it has significant treatment effect, and trichloroethanes fixed rate is more than 96.2%；Processing
Method is simple, and treatment effeciency is high, and the present invention can reach the physical and chemical index by the serious Contaminated Sewage Sludge soil of trichloroethanes
GB15618-2008 standards；Preparation technology of the present invention is simple, and equipment requirement is low, beneficial to industrialized production and marketing.
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, can also be on the premise of this patent objective not be departed from one skilled in the relevant art's possessed knowledge
Make a variety of changes.
Claims (9)
1. a kind of trichloroethanes Contaminated Sewage Sludge efficient process agent, it is characterised in that include the raw material of following parts by weight：Acryloyl
Amine 8-15 parts, bodied ferric sulfate 4-8 parts, flavonoids 3-8 parts, butyric acid potassium 3-8 parts, sodium metaaluminate 2-5 parts, hydroxylamine hydrochloride 5-
10 parts, it is tartaric acid 1-4 parts, yellow cinnamon leaf 2-8 parts, corncob 2-8 parts, blue-green algae 4-9 parts, activated carbon 3-6 parts, magnesium phosphate 2-5 parts, sweet
Careless hypo acid 1-3 parts, alkyl-glucoside 1-3 parts, enuatrol 1-3 parts, ethylparaben 0.1-1 parts.
2. trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 1, it is characterised in that including following parts by weight
Several raw materials：10 parts of acrylamide, 7 parts of bodied ferric sulfate, 5 parts of flavonoids, 5 parts of butyric acid potassium, 4 parts of sodium metaaluminate, hydrochloric acid
6 parts of azanol, 2 parts of tartaric acid, 5 parts of yellow cinnamon leaf, 5 parts of corncob, 6 parts of blue-green algae, 4 parts of activated carbon, 3 parts of magnesium phosphate, enoxolone 2
Part, 2 parts of alkyl-glucoside, 2 parts of enuatrol, 0.5 part of ethylparaben.
3. trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 1, it is characterised in that the flavonoids uses
One or more in Quercetin, cyanidenon, catechin and OPC.
4. a kind of preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent as described in claim 1-3 is any, its feature
It is, preparation process is：
（1）Acrylamide, bodied ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid are mixed,
By mixer mixing 25-40min, mixture A is obtained；
（2）Magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, by mixer mixing 10-20min,
Obtain mixture B；
（3）Yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, sieve 50-100 mesh, then
Mix and produce mixed-powder, mixed-powder is placed at 5-15 DEG C and stored, it is standby；
（4）Mixed-powder obtained by upper step is mixed with mixture A, mixture B, is sealed at 5-10 DEG C and is stirred 25-
40min, 10-20min is then shaken using microwave, got product.
5. the preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 4, it is characterised in that step
（1）Acrylamide, bodied ferric sulfate, flavonoids, butyric acid potassium, sodium metaaluminate, hydroxylamine hydrochloride and tartaric acid are mixed, passed through
Mixer mixing 30min, obtains mixture A.
6. the preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 4, it is characterised in that step
（2）Magnesium phosphate, enoxolone, ethylparaben and alkyl-glucoside are mixed, by mixer mixing 14min, mixed
Compound B.
7. the preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 4, it is characterised in that step
（3）Yellow cinnamon leaf, activated carbon, corncob and blue-green algae are mixed, respectively after drying, grinding, sieve 60 mesh, then mixes and produces
Mixed-powder, mixed-powder is placed at 8 DEG C and stored, it is standby.
8. the preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 4, it is characterised in that step
（4）Mixed-powder obtained by upper step is mixed with mixture A, mixture B, is sealed at 6 DEG C and is stirred 32min, then used
Microwave shakes 12min, gets product.
9. the preparation method of trichloroethanes Contaminated Sewage Sludge efficient process agent according to claim 4, it is characterised in that described
Step（4）The power of sonic oscillation processing is 1000-2000W.
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| CN201710866223.XA CN107663001A (en) | 2017-09-22 | 2017-09-22 | A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent |
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| CN201710866223.XA CN107663001A (en) | 2017-09-22 | 2017-09-22 | A kind of trichloroethanes Contaminated Sewage Sludge efficient process agent |
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| CN108373250A (en) * | 2018-04-02 | 2018-08-07 | 陈钦先 | A kind of river pollution mud administers material and its preparation method and application |
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| CN104307019A (en) * | 2014-10-30 | 2015-01-28 | 上海今拓环保设备工程有限公司 | Plant extract deodorizer for removing harmful gases |
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| CN108358412A (en) * | 2018-04-02 | 2018-08-03 | 陈鹏 | A kind of paper mill sludge treatment agent and its preparation method and application |
| CN108373250A (en) * | 2018-04-02 | 2018-08-07 | 陈钦先 | A kind of river pollution mud administers material and its preparation method and application |
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Application publication date: 20180206 |