CN107651864A - A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film - Google Patents
A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film Download PDFInfo
- Publication number
- CN107651864A CN107651864A CN201711113711.XA CN201711113711A CN107651864A CN 107651864 A CN107651864 A CN 107651864A CN 201711113711 A CN201711113711 A CN 201711113711A CN 107651864 A CN107651864 A CN 107651864A
- Authority
- CN
- China
- Prior art keywords
- glass
- film
- reflection film
- vapour deposition
- physical vapour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
- C03C17/3417—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials all coatings being oxide coatings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/70—Properties of coatings
- C03C2217/73—Anti-reflective coatings with specific characteristics
- C03C2217/734—Anti-reflective coatings with specific characteristics comprising an alternation of high and low refractive indexes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/151—Deposition methods from the vapour phase by vacuum evaporation
Abstract
It is vapor-deposited the invention provides a kind of glass physical and adds the technique of anti-fog performance after anti-reflection film, it causes the easy to make, quick of anti-reflection film, and sets anti-fog layer on the surface of anti-reflection film, it is ensured that the anti-fog performance of glass, and it can be suitably used for industrial production.Transmitance is set more than 90% in the visible region of light glass in advance, anti-reflection film program is designed using film design software, program reduced unit is inputted in the fixed routine file of vacuum coating equipment afterwards, the deposition material required for placement in vacuum coating equipment, glass is put on the machine umbrella leaf of vacuum coating equipment afterwards, start vacuum coating equipment operation physical vapour deposition (PVD) program, glass physical vapour deposition anti-reflection film is obtained on the surface of glass, afterwards antifog medicament is sprayed in the exposed surface of physical vapour deposition (PVD) anti-reflection film, dry afterwards, dichroism and antifog grade are measured according to customer requirement.
Description
Technical field
The present invention relates to the technical field of glass surface treatment, add after specially a kind of glass physical vapour deposition anti-reflection film
The technique of anti-fog performance.
Background technology
When the surface of existing glass needs to set anti-reflection film, it needs the technique by complexity to make to form corresponding increasing
Permeable membrane, and the light transmittance for making the anti-reflection film formed can not ensure, and its surface can not ensure anti-fog performance so that it can not be applicable
In field of industrial production.
The content of the invention
Add the work of anti-fog performance after anti-reflection film in view of the above-mentioned problems, being vapor-deposited the invention provides a kind of glass physical
Skill, it causes the easy to make, quick of anti-reflection film, and sets anti-fog layer on the surface of anti-reflection film, it is ensured that the anti-fog performance of glass,
And it can be suitably used for industrial production.
A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film, it is characterised in that：In advance in light glass
Visible region transmitance is set more than 90%, design anti-reflection film program using film design software, program convert afterwards single
In the fixed routine file of position input vacuum coating equipment, the deposition material required for placement in vacuum coating equipment, afterwards
Glass is put on the machine umbrella leaf of vacuum coating equipment, starts vacuum coating equipment operation physical vapour deposition (PVD) program, in glass
Surface obtains glass physical vapour deposition anti-reflection film, sprays antifog medicine in the exposed surface of physical vapour deposition (PVD) anti-reflection film afterwards
Agent, dry afterwards, dichroism and antifog grade are measured according to customer requirement.
It is further characterized by：
The antifog medicament of spraying is clear anti-fog medicament, after the completion of spraying, is dried for 100 DEG C by vertical type oven；
Plate the TiO that thickness is 15nm respectively successively by vacuum coating equipment2Film, the SiO that thickness is 30nm2Film, thickness are
120nm TiO2Film, the SiO that thickness is 89nm2Film, wherein vacuum are 3.0 × 10-5T, temperature is 50 DEG C；
The thickness is 15nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T；
The thickness is 120nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T；
The transmitance of visible region is more than 90% when measuring optical characteristics；
The 10CM that the anti-fog surface of glass is placed in above the rim of a cup on 50 degrees Celsius of cups when measuring antifog grade highly locates.
After technology using the present invention, anti-reflection film program is designed using film design software, it is afterwards that program reduced unit is defeated
In the fixed routine file for entering vacuum coating equipment, the deposition material required for placement in vacuum coating equipment, pass through afterwards
Vacuum coating equipment obtains physical vapour deposition (PVD) anti-reflection film in glass surface, afterwards in the exposed surface of physical vapour deposition (PVD) anti-reflection film
Antifog medicament is sprayed, is dried afterwards, it causes the easy to make, quick of anti-reflection film, and sets anti-fog layer on the surface of anti-reflection film,
Ensure the anti-fog performance of glass, and it can be suitably used for industrial production.
Embodiment
A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film, it is characterised in that：In advance in light glass
Visible region transmitance is set more than 90%, design anti-reflection film program using film design software, program convert afterwards single
In the fixed routine file of position input vacuum coating equipment, the deposition material required for placement in vacuum coating equipment, afterwards
Glass is put on the machine umbrella leaf of vacuum coating equipment, starts vacuum coating equipment operation physical vapour deposition (PVD) program, in glass
Surface obtains glass physical vapour deposition anti-reflection film, sprays antifog medicine in the exposed surface of physical vapour deposition (PVD) anti-reflection film afterwards
Agent, dry afterwards, dichroism and antifog grade are measured according to customer requirement.
Specific embodiment：Anti-reflection film is plated on light glass, being set by film design software needs to plate four tunics, afterwards by journey
In the fixed routine file of sequence reduced unit input vacuum coating equipment, the evaporation material required for the placement in vacuum coating equipment
Glass, is put on the machine umbrella leaf of vacuum coating equipment by material afterwards, starts vacuum coating equipment operation physical vapour deposition (PVD) program, leads to
Cross vacuum coating equipment and plate the TiO that thickness is 15nm respectively successively2Film, the SiO that thickness is 30nm2Film, thickness are 120nm's
TiO2Film, the SiO that thickness is 89nm2Film, wherein vacuum are 3.0 × 10-5T, temperature is 50 DEG C；Thickness is 15nm TiO2Film
Plating film pressure when carrying out plated film is 1.2 × 10-4T；Thickness is 120nm TiO2Plating film pressure when film carries out plated film is 1.2
×10-4T；Antifog medicament is sprayed in the exposed surface of physical vapour deposition (PVD) anti-reflection film afterwards, is dried afterwards, when measuring optical characteristics
The transmitance of visible region is more than 90%, the anti-fog surface of glass is placed on 50 degrees Celsius of cups when measuring antifog grade cup
10CM above mouthful highly locates.
The specific embodiment of the present invention is described in detail above, but content is only the preferable implementation of the invention
Example, it is impossible to be considered as the practical range for limiting the invention.All impartial changes made according to the invention application range
Change and improvement etc., all should still be belonged within this patent covering scope.
Claims (7)
1. add the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film, it is characterised in that：In advance in light glass
Visible region sets transmitance more than 90%, anti-reflection film program is designed using film design software, afterwards by program reduced unit
Input in the fixed routine file of vacuum coating equipment, the deposition material required for placement in vacuum coating equipment, afterwards will
Glass is put on the machine umbrella leaf of vacuum coating equipment, starts vacuum coating equipment operation physical vapour deposition (PVD) program, in the table of glass
Face obtains glass physical vapour deposition anti-reflection film, sprays antifog medicament in the exposed surface of physical vapour deposition (PVD) anti-reflection film afterwards,
Dry afterwards, dichroism and antifog grade are measured according to customer requirement.
2. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 1, its feature exists
In：The antifog medicament of spraying is clear anti-fog medicament, after the completion of spraying, is dried for 100 DEG C by vertical type oven.
3. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 1, its feature exists
In：Plate the TiO that thickness is 15nm respectively successively by vacuum coating equipment2Film, the SiO that thickness is 30nm2Film, thickness 120nm
TiO2Film, the SiO that thickness is 89nm2Film, wherein vacuum are 3.0 × 10-5T, temperature is 50 DEG C.
4. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 3, its feature exists
In：The thickness is 15nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
5. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 3, its feature exists
In：The thickness is 120nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
6. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 1, its feature exists
In：The transmitance of visible region is more than 90% when measuring optical characteristics.
7. adding the technique of anti-fog performance after a kind of glass physical vapour deposition anti-reflection film as claimed in claim 1, its feature exists
In：The 10CM that the anti-fog surface of glass is placed in above the rim of a cup on 50 degrees Celsius of cups when measuring antifog grade highly locates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711113711.XA CN107651864A (en) | 2017-11-13 | 2017-11-13 | A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711113711.XA CN107651864A (en) | 2017-11-13 | 2017-11-13 | A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107651864A true CN107651864A (en) | 2018-02-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711113711.XA Pending CN107651864A (en) | 2017-11-13 | 2017-11-13 | A kind of technique for adding anti-fog performance after glass physical vapour deposition anti-reflection film |
Country Status (1)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108973373A (en) * | 2018-08-01 | 2018-12-11 | 苏州安洁科技股份有限公司 | Be cracked after plated film membrane stress removal technique on a kind of ink layer |
| WO2022107316A1 (en) * | 2020-11-20 | 2022-05-27 | 昭和電工マテリアルズ株式会社 | Method for evaluating water film and method for evaluating anti-fogging agent |
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| JP2011008076A (en) * | 2009-06-26 | 2011-01-13 | Asahi Glass Co Ltd | Optical element and method for producing the same |
| KR101230973B1 (en) * | 2011-11-22 | 2013-02-07 | 한국에너지기술연구원 | Cis/cigs based-thin film solar cell having back side tco layer and method for manufacturing the same |
| CN102998723A (en) * | 2012-11-29 | 2013-03-27 | 法国圣戈班玻璃公司 | Antireflection optical assembly and manufacturing method thereof |
| CN103018796A (en) * | 2012-10-31 | 2013-04-03 | 南京工业大学 | Double-film PC (Polycarbonate) lens for optical display and preparation method thereof |
| CN204820548U (en) * | 2015-07-17 | 2015-12-02 | 成都锐迅新能源科技有限公司 | Anti -reflection type surface nanometer is two -sided prevents static PU membrane |
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| CN106707543A (en) * | 2015-08-20 | 2017-05-24 | 常磊 | Color-variable and blue light-resistant lens |
| CN107108044A (en) * | 2016-05-27 | 2017-08-29 | 深圳市大疆创新科技有限公司 | Optical shield and the filming apparatus and unmanned plane using the optical shield |
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2017
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| JP2011008076A (en) * | 2009-06-26 | 2011-01-13 | Asahi Glass Co Ltd | Optical element and method for producing the same |
| KR101230973B1 (en) * | 2011-11-22 | 2013-02-07 | 한국에너지기술연구원 | Cis/cigs based-thin film solar cell having back side tco layer and method for manufacturing the same |
| CN103018796A (en) * | 2012-10-31 | 2013-04-03 | 南京工业大学 | Double-film PC (Polycarbonate) lens for optical display and preparation method thereof |
| CN102998723A (en) * | 2012-11-29 | 2013-03-27 | 法国圣戈班玻璃公司 | Antireflection optical assembly and manufacturing method thereof |
| CN106137002A (en) * | 2015-04-20 | 2016-11-23 | 无锡市豪雅微纤织物有限公司 | A kind of antifog towel of superfine fibre and preparation technology thereof |
| CN204820548U (en) * | 2015-07-17 | 2015-12-02 | 成都锐迅新能源科技有限公司 | Anti -reflection type surface nanometer is two -sided prevents static PU membrane |
| CN106707543A (en) * | 2015-08-20 | 2017-05-24 | 常磊 | Color-variable and blue light-resistant lens |
| CN107108044A (en) * | 2016-05-27 | 2017-08-29 | 深圳市大疆创新科技有限公司 | Optical shield and the filming apparatus and unmanned plane using the optical shield |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108973373A (en) * | 2018-08-01 | 2018-12-11 | 苏州安洁科技股份有限公司 | Be cracked after plated film membrane stress removal technique on a kind of ink layer |
| WO2022107316A1 (en) * | 2020-11-20 | 2022-05-27 | 昭和電工マテリアルズ株式会社 | Method for evaluating water film and method for evaluating anti-fogging agent |
| WO2022107823A1 (en) * | 2020-11-20 | 2022-05-27 | 昭和電工マテリアルズ株式会社 | Water film evaluation method, and antifogging agent evaluation method |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20180202 |