CN107643240A - A kind of A types rendrock permeability test method - Google Patents

A kind of A types rendrock permeability test method Download PDF

Info

Publication number
CN107643240A
CN107643240A CN201611077491.5A CN201611077491A CN107643240A CN 107643240 A CN107643240 A CN 107643240A CN 201611077491 A CN201611077491 A CN 201611077491A CN 107643240 A CN107643240 A CN 107643240A
Authority
CN
China
Prior art keywords
rendrock
types
piston
briquetting
cylinder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201611077491.5A
Other languages
Chinese (zh)
Other versions
CN107643240B (en
Inventor
王亚琴
张金梅
张玉霞
张会光
王康
吴保意
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
State Administration Of Quality And Technical Supervision's Register Of Chemicals Center
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
Original Assignee
State Administration Of Quality And Technical Supervision's Register Of Chemicals Center
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by State Administration Of Quality And Technical Supervision's Register Of Chemicals Center, China Petroleum and Chemical Corp, Sinopec Qingdao Safety Engineering Institute filed Critical State Administration Of Quality And Technical Supervision's Register Of Chemicals Center
Priority to CN201611077491.5A priority Critical patent/CN107643240B/en
Publication of CN107643240A publication Critical patent/CN107643240A/en
Application granted granted Critical
Publication of CN107643240B publication Critical patent/CN107643240B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

The invention discloses a kind of A types rendrock permeability test method, its A type rendrocks infiltration experiment device used includes test chamber, the piston that can be inserted into the test chamber and matches somebody with somebody the briquetting for merging pressure needed for A type rendrocks when providing experiment with the piston.This method comprises the following steps:A. by A types rendrock with being put into cylinder after high-quality gauze wrapped;B. piston is put into cylinder, briquetting is placed on piston, A types rendrock is recorded in all oilholes set on cylinder lateral wall by certain pressure and is occurred the time required during oil droplet sign first;C. result evaluation:If oozing out the time in liquid is more than setting time value, then it is assumed that A type rendrocks are safe, and liquid oozes out the time and is less than or equal to setting time value, then it is assumed that A type rendrocks are unsafe;Wherein, the environment temperature for carrying out above-mentioned A types rendrock permeability test method is 15~25 DEG C.The inventive method can be very good to carry out risk assessment to A types rendrock.

Description

A kind of A types rendrock permeability test method
Technical field
The present invention relates to a kind of A types rendrock permeability test method.
Background technology
A type rendrocks are the materials containing liquid organic nitrate, such as nitroglycerine or nitroglycerine and one kind or one The mixture of kind above composition, such as digest cellulose, ammonium nitrate or other inorganic nitrates, aromatic nitro derivative or flammable Material.When A types rendrock contains the liquid nitrate esters higher than 40%, not only to pass through《Suggestion on Dangerous Goods Transport Book-experiment and manual of standards》In the experiment enumerated, should also meet the requirement of permeability test, just be considered safe, can carry out Road transport.But the country there is no A type rendrock permeability test methods at present, danger can not be carried out to this kind of explosive and commented Estimate.
The content of the invention
It is an object of the invention to propose a kind of A types rendrock permeability test method, whether to assess A types rendrock Safety.
To achieve these goals, the present invention adopts the following technical scheme that:
A kind of A types rendrock permeability test method, the A type rendrock infiltration experiment devices that methods described uses include Test chamber, can be inserted into the test chamber piston and with the piston with merges offer experiment when A types rendrock institute Need the briquetting of pressure;The test chamber includes container base and cylinder, wherein, the sealed bottom of cylinder is arranged on container base On, the open top of cylinder;It is sequentially provided with some groups of oilholes from bottom to top in the side wall of cylinder, and between two adjacent groups oilhole Gauge is from equal;Oilhole quantity in every group of oilhole is multiple, and is evenly arranged in the one of cylinder lateral wall with multiple oilholes of group On individual circumferencial direction;The shapes and sizes of piston are adapted with the cylinder, and piston has pointed top;The briquetting is in inversion Cup-shaped, the inverted draw cut being engaged with pointed top is offered on briquetting bottom wall;Several oilholes are offered in briquetting side wall Peep hole;Methods described comprises the following steps:
A. by A types rendrock with being put into cylinder after high-quality gauze wrapped;
B. piston is put into cylinder, briquetting is placed on piston, A types rendrock is recorded in cylinder by certain pressure Occurs the time required during oil droplet sign first in all oilholes set on body sidewall;
C. result evaluation:If oozing out the time in liquid is more than setting time value, then it is assumed that A type rendrocks are safety , liquid oozes out the time and is less than or equal to setting time value, then it is assumed that A type rendrocks are unsafe;
Wherein, the environment temperature for carrying out above-mentioned A types rendrock permeability test method is 15~25 DEG C.
Preferably, the test chamber, piston and briquetting are made of bronze material;The internal diameter of cylinder is 15.7mm, external diameter 20mm, depth 40mm;Oilhole has four groups, and the oilhole quantity in every group of oilhole is five, each oilhole A diameter of 0.5mm;The spacing distance of two adjacent groups oilhole is 5mm, and the one group of oilhole of position most on the lower and appearance in four groups of oilholes The distance of device susceptor surface is 5mm;A diameter of 15.6mm of piston columnar part below pointed top;Piston and briquetting Weight sum be 2220g;The length of the A types rendrock is 30mm, a diameter of 15mm, weight 5-8g;
The pressure that A types rendrock is subject in stepb is 120kPa;Setting time is 5 minutes in step c.
Preferably, the thickness of the container base is 15mm.
Preferably, the length of the piston is 52mm, wherein, the pointed long 4mm in top, the work below the pointed top The long 48mm of stick harness body portion.
Preferably, the internal diameter of the briquetting is 100mm, and the external diameter of briquetting is 106mm, and the length of briquetting is 88mm.
Preferably, the quantity of the oilhole peep hole is four, and the width of each oilhole peep hole is 46mm, is highly 56mm。
The invention has the advantages that:
The infiltration experiment device that the inventive method uses includes test chamber, piston and briquetting, wherein, test chamber bag Cylinder and container base are included, the present invention is rationally designed to the structure of cylinder, piston and briquetting.At the trial, first The A type rendrocks of certain length are put into cylinder, then piston is also placed in cylinder, briquetting is placed on piston, is led to Cross briquetting and piston gives A type rendrocks certain pressure, it is required when occurring oil droplet sign first by recording on cylinder Time judges whether rendrock is safe.The present invention can be very good to carry out risk assessment to A types rendrock.
Brief description of the drawings
Fig. 1 is the structural representation of test chamber in the embodiment of the present invention;
Fig. 2 is the structural representation of piston in the embodiment of the present invention;
Fig. 3 is the structural representation of briquetting in the embodiment of the present invention;
Fig. 4 is the cooperation schematic diagram of test chamber, piston and briquetting when carrying out permeability test in the embodiment of the present invention;
Wherein, 1- test chambers, 2- pistons, 3-A type rendrocks, 4- briquettings, 5- container bases, 6- cylinders, 7- are pointed Top, 8- inverted draw cuts, 9- oilholes, 10- oilhole peep holes, 11- piston columnar parts.
Embodiment
Below in conjunction with the accompanying drawings and embodiment is described in further detail to the present invention:
With reference to shown in Fig. 1 to Fig. 3, a kind of A types rendrock infiltration experiment device, including test chamber 1, pluggable experiment The piston 2 of container 1 and the briquetting 4 for matching somebody with somebody pressure needed for A types rendrock 3 when offer experiment is provided with piston 2.
Wherein, test chamber 1 includes container base 5 and cylinder 6, and the sealed bottom of cylinder 6 is arranged on container base 5, The open top of cylinder 6.
It is sequentially provided with some groups of oilholes from bottom to top in the side wall of cylinder 6, and the spacing distance of two adjacent groups oilhole is equal. The quantity of oilhole 9 in every group of oilhole is multiple, and a circumferencial direction of cylinder lateral wall is evenly arranged in the multiple oilholes organized On.
The shapes and sizes of piston 2 are adapted with cylinder 6, to ensure that piston 2 is inserted into cylinder 6.Piston 2 has Pointed top 7, the pointed top 7 are used to support briquetting 4.
Briquetting 4 is in inverted cup-shaped, and the inverted draw cut 8 being engaged with pointed top 7 is offered on the bottom wall of briquetting 4, and briquetting 4 is put Put on the piston 2;Several oilhole peep holes 10 are offered in the side wall of briquetting 4.
The present invention can carry out the experiment of A type rendrocks risk assessment using test chamber 1, piston 2 and briquetting 4.
It shown below is a preferred embodiment and illustrate the present invention:
Test chamber 1, piston 2 and briquetting 4 are made of bronze material.For test chamber 1, piston 2 and The size and weight of briquetting 4 have carried out following design respectively:
The internal diameter d1 of cylinder 6 is 15.7mm, outer diameter D 1 is 20mm, depth h1 is 40mm.
The thickness L1 of container base 5 is 15mm.
Oilhole has four groups, and the quantity of oilhole 9 in every group of oilhole is five.
The diameter D3 of each oilhole 9 is 0.5mm.The spacing distance L2 of two adjacent groups oilhole is 5mm, and four groups of oilhole middle positions It is also 5mm to put one group of oilhole most on the lower and the distance L3 on the surface of container base 5.
The length L4 of piston 2 is 52mm, wherein, the 7 long 4mm of pointed top of piston, the work below the pointed top 11 long 48mm of stick harness body portion, the diameter D4 of piston columnar part 11 is 15.6mm.
Because the diameter of piston columnar part 11 is less than the internal diameter of cylinder 6, it is ensured that in piston insertion cylinder 6.
The internal diameter d2 of briquetting 4 is 100mm, and the outer diameter D 2 of briquetting 4 is 106mm, and the length L5 of briquetting 4 is 88mm;Piston 2 with The weight sum of briquetting 4 is 2220g.
The quantity of oilhole peep hole 10 can be four, and the width of each oilhole peep hole is 46mm, is highly 56mm, oil The bottom edge distance of the lower edge of hole peep hole to briquetting is 8mm;The bottom wall thickness 14mm of briquetting 4.
By above-mentioned oilhole peep hole 10 it is observed that all oilholes 9.Certainly it can also be designed as needed His quantity, accordingly, the size of oilhole peep hole 10 changes.
In addition, the length of A type rendrocks is 30mm, a diameter of 15mm, weight 5-8g.When piston 2 and briquetting 4 are placed When on to A type rendrocks, 120kPa pressure can be provided for the A type rendrocks.
A types rendrock permeability test method is in the embodiment of the present invention:
1. by A types rendrock with being put into cylinder 6 after high-quality gauze wrapped;
2. piston 2 is put into cylinder 6, briquetting 4, which is put, on the piston 2, makes pressure of the A types rendrock by 120kPa, note There is the time required during oil droplet (nitroglycerine) sign first in all oilholes 9 set in the side wall of cylinder 6 in record;
3. result evaluation:If oozing out the time in liquid is more than 5 minutes (i.e. setting time value), then it is assumed that A type explosions are fried Medicine is safe, and liquid oozed out the time less than or equal to 5 minutes, then it is assumed that A type rendrocks are unsafe
Wherein, the environment temperature for carrying out above-mentioned A types rendrock permeability test method is 15~25 DEG C.
It is, of course, also possible to the setting time value oozed out according to the size reasonable of above-mentioned pressure values adjustment liquid.Such as work as pressure When intensity values improve, the setting time value that liquid oozes out accordingly shortens, and concrete numerical value corresponding relation can be obtained by testing.
Certainly, described above is only presently preferred embodiments of the present invention, and the present invention is not limited to enumerate above-described embodiment, should When explanation, any those skilled in the art are all equivalent substitutes for being made, bright under the teaching of this specification Aobvious variant, all falls within the essential scope of this specification, ought to be protected by the present invention.

Claims (6)

  1. A kind of 1. A types rendrock permeability test method, it is characterised in that the A types rendrock infiltration examination that methods described uses Experiment device includes test chamber, the piston that can be inserted into the test chamber and with the piston with A types when merging offer experiment The briquetting of pressure needed for rendrock;The test chamber includes container base and cylinder, wherein, the sealed bottom of cylinder is set On container base, the open top of cylinder;It is sequentially provided with some groups of oilholes, and adjacent two from bottom to top in the side wall of cylinder The spacing distance of group oilhole is equal;Oilhole quantity in every group of oilhole is multiple, and is evenly arranged in cylinder with multiple oilholes of group On one circumferencial direction of body sidewall;The shapes and sizes of piston are adapted with the cylinder, and piston has pointed top;It is described Briquetting is in inverted cup-shaped, and the inverted draw cut being engaged with pointed top is offered on briquetting bottom wall;Offered in briquetting side wall Several oilhole peep holes;Methods described comprises the following steps:
    A. by A types rendrock with being put into cylinder after high-quality gauze wrapped;
    B. piston is put into cylinder, briquetting is placed on piston, A types rendrock is recorded in cylinder side by certain pressure Occurs the time required during oil droplet sign first in all oilholes set on wall;
    C. result evaluation:If oozing out the time in liquid is more than setting time value, then it is assumed that A type rendrocks are safe, liquid Body oozes out the time and is less than or equal to setting time value, then it is assumed that A type rendrocks are unsafe;
    Wherein, the environment temperature for carrying out above-mentioned A types rendrock permeability test method is 15~25 DEG C.
  2. A kind of 2. A types rendrock permeability test method according to claim 1, it is characterised in that the test chamber, Piston and briquetting are made of bronze material;The internal diameter of the cylinder is 15.7mm, external diameter 20mm, depth are 40mm;The oilhole has four groups, and the oilhole quantity in every group of oilhole is five, a diameter of 0.5mm of each oilhole;Two adjacent groups The spacing distance of oilhole is 5mm, and position one group of oilhole most on the lower and the distance on container base surface are in four groups of oilholes 5mm;A diameter of 15.6mm of piston columnar part below pointed top;The weight sum of piston and briquetting is 2220g; The length of the A types rendrock is 30mm, a diameter of 15mm, weight 5-8g;
    The pressure that A types rendrock is subject in stepb is 120kPa;Setting time is 5 minutes in step c.
  3. A kind of 3. A types rendrock permeability test method according to claim 2, it is characterised in that the container base Thickness be 15mm.
  4. A kind of 4. A types rendrock permeability test method according to claim 2, it is characterised in that wherein, the piston Length be 52mm, wherein, the pointed long 4mm in top, the long 48mm of piston columnar part below the pointed top.
  5. A kind of 5. A types rendrock permeability test method according to claim 2, it is characterised in that the briquetting it is interior Footpath is 100mm, and the external diameter of briquetting is 106mm, and the length of briquetting is 88mm.
  6. A kind of 6. A types rendrock permeability test method according to claim 2, it is characterised in that the oilhole observation The quantity in hole is four, and the width of each oilhole peep hole is 46mm, is highly 56mm.
CN201611077491.5A 2016-11-30 2016-11-30 A kind of A type rendrock permeability test method Active CN107643240B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611077491.5A CN107643240B (en) 2016-11-30 2016-11-30 A kind of A type rendrock permeability test method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611077491.5A CN107643240B (en) 2016-11-30 2016-11-30 A kind of A type rendrock permeability test method

Publications (2)

Publication Number Publication Date
CN107643240A true CN107643240A (en) 2018-01-30
CN107643240B CN107643240B (en) 2019-09-03

Family

ID=61110116

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611077491.5A Active CN107643240B (en) 2016-11-30 2016-11-30 A kind of A type rendrock permeability test method

Country Status (1)

Country Link
CN (1) CN107643240B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112595656A (en) * 2020-12-09 2021-04-02 中国兵器工业第五九研究所 Testing device and evaluation method for adaptability of explosive device long-storage environment for bomb

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201016907Y (en) * 2007-03-19 2008-02-06 岳辉 Compression type meat water content detecting instrument
CN104406968A (en) * 2014-11-25 2015-03-11 山西北方兴安化学工业有限公司 Chemical stability detection method for nitroglycerin-containing product
CN204359655U (en) * 2014-11-05 2015-05-27 山东科技大学 A kind of gas hydrate porosity and osmotic coefficient investigating device
CN105572013A (en) * 2015-12-24 2016-05-11 太原理工大学 Apparatus and method for testing permeability of porous material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201016907Y (en) * 2007-03-19 2008-02-06 岳辉 Compression type meat water content detecting instrument
CN204359655U (en) * 2014-11-05 2015-05-27 山东科技大学 A kind of gas hydrate porosity and osmotic coefficient investigating device
CN104406968A (en) * 2014-11-25 2015-03-11 山西北方兴安化学工业有限公司 Chemical stability detection method for nitroglycerin-containing product
CN105572013A (en) * 2015-12-24 2016-05-11 太原理工大学 Apparatus and method for testing permeability of porous material

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
孙光: "《反爆炸学》", 29 February 2012, 群众出版社 *
孟祥尧 等: "爆炸物中炸药成分渗出机理", 《鱼雷技术》 *
由中明: "《火药管理》", 30 June 1973, 燃料化学工业出版社 *
胡双启 等: "《火炸药安全技术》", 28 February 2014, 北京理工大学出版 *
谈行华 等: "国外起爆药柱概况", 《爆破器材》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112595656A (en) * 2020-12-09 2021-04-02 中国兵器工业第五九研究所 Testing device and evaluation method for adaptability of explosive device long-storage environment for bomb
CN112595656B (en) * 2020-12-09 2022-05-27 中国兵器工业第五九研究所 Testing device and evaluation method for adaptability of explosive device long-storage environment for bomb

Also Published As

Publication number Publication date
CN107643240B (en) 2019-09-03

Similar Documents

Publication Publication Date Title
Soret et al. Petrological evidence for stepwise accretion of metamorphic soles during subduction infancy (Semail ophiolite, Oman and UAE)
DE102013111600B4 (en) Support structure for holding containers for substances for medical, pharmaceutical or cosmetic applications, as well as transport and packaging containers with the same
WO2008067274A3 (en) System and method for packaging of mass-fabricated custom items
DE102012103899B4 (en) Method and device for treating containers for storing substances for medical or pharmaceutical applications
ATE468076T1 (en) METHOD AND MACHINE FOR HANDLING TOXIC SUBSTANCES
WO2008027994A3 (en) Funnel
CN107643240A (en) A kind of A types rendrock permeability test method
CN107702601A (en) Gel state solid-liquid high-energy fuel bodies of charges dilatancy characterizing method
NO20053708L (en) Safety Containers for Biologically Active Compounds and Methods for Preparing This Container
NZ730132A (en) Multi-well sample testing apparatus and methods of sample testing using the same
EP2929313B1 (en) Apparatus and method for determining the average layer thickness and the permeation rate of a packaging material
ATE380152T1 (en) SYSTEM FOR HOLDING AND DISPENSING A PRODUCT IN WHICH GAS IS DISSOLVED
CN107643241A (en) A kind of A types rendrock infiltration experiment device
MX2015005807A (en) Method and apparatus for adding buffers and other substances to medical cartridges.
AT522704B1 (en) packaging for pharmaceutical products
MX2009008572A (en) Stable pharmaceutical drug aerosols.
WO2019142220A4 (en) Preservation method of a wine and cap for implementing the method
CN109668933A (en) Chemicals antiknock system safety testing device and method
DE3843920A1 (en) TEST CONTAINER FOR GAS MEASURING AND DETECTING DEVICES
CA2828066A1 (en) Test specimen with impact detection means
WO2008083685A3 (en) Device for deep-freezing portions of organic material
Atmani et al. Diffusion of heptane in polyethylene vinyl acetate: Modelisation and experimentation
CN205484230U (en) Store device of autoinjection bottle
DE102012110973A1 (en) Annular holding element for holding e.g. vial for substances for cosmetic, medical or pharmaceutical applications, has container arranged on holding structure through aperture, such that element rests in sections on edge of aperture
US20230039282A1 (en) Sealable devices to cause deposition of vapors into samples

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant