CN107631755A - A kind of mass spectrograph humiture, wind speed monitoring system - Google Patents

A kind of mass spectrograph humiture, wind speed monitoring system Download PDF

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Publication number
CN107631755A
CN107631755A CN201710924710.7A CN201710924710A CN107631755A CN 107631755 A CN107631755 A CN 107631755A CN 201710924710 A CN201710924710 A CN 201710924710A CN 107631755 A CN107631755 A CN 107631755A
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CN
China
Prior art keywords
wind speed
temperature
control unit
monitoring system
temperature sensor
Prior art date
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Pending
Application number
CN201710924710.7A
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Chinese (zh)
Inventor
刘召贵
刘建魁
游小燕
张伟
李林
周立
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Jiangsu Skyray Instrument Co Ltd
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Jiangsu Skyray Instrument Co Ltd
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Publication date
Application filed by Jiangsu Skyray Instrument Co Ltd filed Critical Jiangsu Skyray Instrument Co Ltd
Priority to CN201710924710.7A priority Critical patent/CN107631755A/en
Publication of CN107631755A publication Critical patent/CN107631755A/en
Pending legal-status Critical Current

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Abstract

The invention discloses mass spectrograph humiture, wind speed monitoring system, including:Control unit and sensing control unit and power subsystem, the sensing control unit includes multi way temperature sensing control component, humidity sensor control assembly and wind speed sensing control component, described control unit includes host computer, communication unit, micro controller module and ADC modular converters, the sensing control unit gathered data passes to described control unit and carries out feedback control to corresponding component according to preset value, and the power subsystem is connected with the TEMP control unit;Mass spectrograph humiture disclosed by the invention, wind speed monitoring system, by complexity experimental studies have found that, the key element of some specific key elements and ad-hoc location is controlled and can be very good to reach whole detection and control, and under given conditions, losses of ions can be reached to a desired value, so as to greatly improve the resolution ratio of instrument.

Description

A kind of mass spectrograph humiture, wind speed monitoring system
Technical field
The invention belongs to gas chromatograph field, more particularly to a kind of detector of gas chromatograph.
Background technology
Mass spectrograph is mainly made up of sampling system, ion gun, electro-ionic osmosis and ion transmission, mass analyzer, detector. In inductivity coupled plasma mass spectrometry analytical instrument, the species and content of element micro in sample are detected, member Element is changed into after by ion gun in lens combination of the ionic condition into mass spectrometer, filters out optimal ion.Environment In humiture have important influence to the resolution ratio of ion, requirement of the system to air draft is also critically important, in ion source portion The speed of air draft directly affects the deflection of ion, so that causing the ion extraction rate bad, therefore wants the temperature of real-time monitoring system Humidity and wind speed.
Temperature is to play the function of a power-off protection in instrument in the market, can not realize the real-time prison of temperature Control, and the humidity around system is even more not account for, wind speed then can not be adjusted directly, be operated with fixed speed, existing apparatus Adjustability and monitoring property deficiency be difficult to meet that instrument reaches optimal state so that losses of ions is more severe, so as to Influence resolution ratio, it is therefore desirable to find a kind of more preferable control method.
The content of the invention
In view of this, it is necessary to overcome at least one in drawbacks described above of the prior art.The invention provides a germplasm Spectrometer humiture, wind speed monitoring system, including:Control unit and sensing control unit and power subsystem, the sensing control Unit includes multi way temperature sensing control component, humidity sensor control assembly and wind speed sensing control component, described control unit Including host computer, communication unit, micro controller module and ADC modular converters, the sensing control unit gathered data transmission Feedback control, the power subsystem and the TEMP control are carried out to corresponding component to described control unit and according to preset value Unit processed is connected;
The multi way temperature sensing control component includes multi way temperature sensor and temperature sensor module, the temperature sensor The temperature data of collection is passed into the ADC modular converters through the temperature sensing module and passes to the microcontroller mould Block and the host computer;
The humidity sensor control assembly includes humidity sensor and moisture sensor module, and the humidity sensor is by collection Humidity data passes to the ADC modular converters through the humidity sensor module and passes to the micro controller module and described Host computer;
The wind speed sensing control component includes the air velocity transducer and the wind speed sensing module, and the air velocity transducer will The air speed data of collection passes to the ADC modular converters through the wind speed sensing module and passes to the micro controller module And the host computer.
According in this patent background technology to described in prior art, in the market in instrument temperature simply play one it is disconnected The function of electric protection, the real-time monitoring of temperature can not be realized, and the humidity around system is even more not account for, wind speed then can not be straight Regulation is connect, is operated with fixed speed, the adjustability and monitoring property deficiency of existing apparatus are difficult to meet that instrument reaches optimal State so that losses of ions is more severe, so as to influence resolution ratio;And mass spectrograph humiture disclosed by the invention, wind speed are supervised Control system, by complexity experimental studies have found that, the key element of some specific key elements and ad-hoc location is controlled can be very Good reaches whole detection and control, and under given conditions, losses of ions can be reached to a desired value, so as to significantly Improve the resolution ratio of instrument.
In addition, following additional technical feature is also had according to mass spectrograph humiture disclosed by the invention, wind speed monitoring system:
Further, the power subsystem is constant current source module, and the constant current source module is connected with the temperature sensor module.
Using program controlled constant current source, influence of the lead to temperature acquisition can be effectively reduced, constant current source power supply can be in temperature Sensor side obtains linear temperature-voltage value, facilitates the collection and control in real time of temperature.
Further, the multi way temperature sensing control component is four road TEMP control assemblies, four tunnel temperature Sensing control component includes No. four temperature sensors and four tunnel temperature sensor modules, and No. four temperature sensor includes placing Temperature sensor in plasma chamber body, the temperature sensor being placed at ion source interface, it is placed on the temperature of instrument internal Degree sensor and the temperature sensor being placed on outside instrument.
Further, the temperature sensor uses four line platinum resistance thermometer sensor, PT100.
Further, the temperature of the multi way temperature sensor lay down location in the multi way temperature sensing control component is equal Control is less than or equal to 60 degrees Celsius.
Further, the blast velocity control of the air velocity transducer lay down location more than or equal to 5m/s and is being less than or equal to 40m/s.
Further, the system also include signal conditioning circuit, the temperature sensor or the air velocity transducer or The humidity sensor passes to the ADC modular converters again by the signal conditioning circuit.
Further, the system also includes being used for the display for including displays temperature or humidity or wind speed or combinations thereof Device.
Further, the display also includes being used to control the people for including temperature or humidity or wind speed or combinations thereof Machine interaction control section.
The additional aspect of the present invention and advantage will be set forth in part in the description, and will partly become from the following description Obtain substantially, or recognized by the practice of the present invention.
Brief description of the drawings
The above-mentioned and/or additional aspect and advantage of the present invention will become from the following description of the accompanying drawings of embodiments Substantially and it is readily appreciated that, wherein:
Fig. 1 is that icp mses humiture, the principle of wind speed monitoring system are shown according to an embodiment of the invention It is intended to;
Fig. 2 is temperature sensor module theory diagram according to an embodiment of the invention;
Fig. 1 label declarations:1. micro controller module, 2. ADC modular converters, 3. temperature sensor modules, 4. constant current source modules, 5. host computer PC, 6. communication units, 7. moisture sensor modules, 8. air velocity transducer modules
Fig. 2 label declarations:1. micro controller module, 2.ADC modules, 3. temperature sensor modules, 4. constant current source modules, 9. etc. Ion cavity inner temperature sensor, 10. ion source interface temperature sensors, 11. instrument internal temperature sensors, outside 12. instruments Portion's temperature sensor, 13. humidity sensors, 14, air velocity transducer.
Embodiment
Embodiments of the invention are described below in detail, the example of the embodiment is shown in the drawings, wherein from beginning to end Same or similar label represents same or similar element or the element with same or like function.Below with reference to attached The embodiment of figure description is exemplary, is only used for explaining the present invention, and is not construed as limiting the claims.
In the description of the invention, it is to be understood that term " on ", " under ", " bottom ", " top ", "front", "rear", The orientation or position relationship of the instruction such as " interior ", " outer ", " horizontal stroke ", " perpendicular ", " inner side ", " outside " be based on orientation shown in the drawings or Position relationship, it is for only for ease of and describes the present invention and simplify description, rather than indicates or imply that signified device or element must There must be specific orientation, with specific azimuth configuration and operation, therefore be not considered as limiting the invention.
In the description of the invention, it is necessary to which explanation, unless otherwise clearly defined and limited, term " connection ", " connects It is logical ", " connected ", " connection ", " cooperation " should be interpreted broadly, for example, it may be fixedly connected, be integrally connected or It is detachably connected;It can be the connection of two element internals;Can be joined directly together, the indirect phase of intermediary can also be passed through Even;" cooperation " can be the cooperation in face and face or the cooperation in point and face or line and face, and the also cooperation including hole axle is right For one of ordinary skill in the art, the concrete meaning of above-mentioned term in the present invention can be understood with concrete condition.
Below with reference to accompanying drawings come describe the present invention mass spectrograph humiture, wind speed monitoring system, according to the present invention reality Example is applied, as shown in Figure 1, 2, mass spectrograph humiture disclosed by the invention, wind speed monitoring system, including control unit and sensing control Unit and power subsystem, the sensing control unit include multi way temperature sensing control component, humidity sensor control assembly and Wind speed sensing control component, described control unit turn including host computer PC 5, communication unit 6, micro controller module 1 and ADC Block 2 is changed the mold, the sensing control unit gathered data passes to described control unit and corresponding component is carried out according to preset value Feedback control, the power subsystem are connected with the TEMP control unit;
The multi way temperature sensing control component includes multi way temperature sensor and temperature sensor module 3, the TEMP The temperature data of collection is passed to the ADC modular converters 2 through the temperature sensor module 3 and passes to the micro-control by device Device module 1 processed and the host computer PC 5;
The humidity sensor control assembly includes humidity sensor 13 and moisture sensor module 7, and the humidity sensor 13 will The humidity data of collection passes to the ADC modular converters 2 through the moisture sensor module 7 and passes to the microcontroller Module 1 and the host computer PC 5;
The wind speed sensing control component includes the air velocity transducer 14 and the air velocity transducer module 8, and the wind speed passes The air speed data of collection is passed to the ADC modular converters 2 through the air velocity transducer module 8 and passed to described by sensor 14 Micro controller module 1 and the host computer PC 5.
According to described in prior art, temperature simply plays a power-off and protected in instrument in the market in this patent background technology The function of shield, the real-time monitoring of temperature can not be realized, and the humidity around system is even more not account for, wind speed then can not be adjusted directly Section, operated with fixed speed, the adjustability and monitoring property deficiency of existing apparatus are difficult to meet that instrument reaches optimal shape State so that losses of ions is more severe, so as to influence resolution ratio;And mass spectrograph humiture disclosed by the invention, wind speed monitoring system System, by complexity experimental studies have found that, the key element of some specific key elements and ad-hoc location is controlled and can be very good Reach whole detection and control, and under given conditions, losses of ions can be reached to a desired value, so as to greatly improve The resolution ratio of instrument.
In addition, also have the following supplementary technology special according to mass spectrograph humiture disclosed by the invention, wind speed monitoring system Sign:
According to some embodiments of the present invention, the power subsystem is constant current source module 4, the constant current source module 4 and the temperature Degree sensor assembly 3 is connected.
Using program controlled constant current source, influence of the lead to temperature acquisition can be effectively reduced, constant current source power supply can be in temperature Sensor side obtains linear temperature-voltage value, facilitates the collection and control in real time of temperature.
According to one embodiment of present invention, the multi way temperature sensing control component is four road TEMP control groups Part, the four roads TEMP control assembly include No. four temperature sensors and four tunnel temperature sensor modules 3, four tunnel temperature Degree sensor includes the temperature sensor being placed in plasma chamber body, the temperature sensor being placed at ion source interface, puts Put the temperature sensor in instrument internal and the temperature sensor that is placed on outside instrument.
According to one embodiment of present invention, the temperature sensor uses four line platinum resistance thermometer sensor, PT100.
According to some embodiments of the present invention, the multi way temperature sensor in the multi way temperature sensing control component The temperature of lay down location is controlled less than or equal to 60 degrees Celsius.
According to some embodiments of the present invention, the blast velocity control of the air velocity transducer lay down location more than or equal to 5m/s and Less than or equal to 40m/s.
According to some embodiments of the present invention, the system also includes signal conditioning circuit, the temperature sensor or institute State air velocity transducer 14 or the humidity sensor 13 and the ADC modular converters are passed to by the signal conditioning circuit again 2。
According to some embodiments of the present invention, the system also include be used for include displays temperature or humidity or wind speed or State the display of combination.
Further, the display also includes being used to control including the man-machine of temperature or humidity or wind speed or combinations thereof Interactive control section.
It is any to refer to that " one embodiment ", " embodiment ", " illustrative examples " etc. mean to combine embodiment description Specific component, structure or feature are contained at least one embodiment of the present invention.This specification everywhere this is schematic Statement is not necessarily referring to identical embodiment.Specific component, structure or s person's feature are described with reference to any embodiment moreover, working as When, advocated, component, structure or feature with reference to as being realized other embodiments all fall within those skilled in the art Within the scope of.
Although detailed retouch is carried out to the embodiment of the present invention with reference to multiple illustrative examples of the present invention State, it must be understood that those skilled in the art can be designed that various other improvement and embodiment, these improve and implemented Example will fall within spirit and scope.Specifically, in the scope of foregoing disclosure, accompanying drawing and claim Within, rational variations and modifications can be made in terms of the arrangement that parts and/or sub-combination are laid out, without departing from The spirit of the present invention.Except the variations and modifications in terms of parts and/or layout, its scope is by appended claims and its is equal Thing limits.

Claims (9)

1. a kind of mass spectrograph humiture, wind speed monitoring system, it is characterised in that including:Control unit and sensing control unit with And power subsystem, the sensing control unit include multi way temperature sensing control component, humidity sensor control assembly and wind speed and passed Feel control assembly, described control unit includes host computer, communication unit, micro controller module and ADC modular converters, the biography Sense control unit gathered data passes to described control unit and carries out feedback control, the electricity to corresponding component according to preset value Source unit is connected with the TEMP control unit;
The multi way temperature sensing control component includes multi way temperature sensor and temperature sensor module, the temperature sensor The temperature data of collection is passed into the ADC modular converters through the temperature sensing module and passes to the microcontroller mould Block and the host computer;
The humidity sensor control assembly includes humidity sensor and moisture sensor module, and the humidity sensor is by collection Humidity data passes to the ADC modular converters through the humidity sensor module and passes to the micro controller module and described Host computer;
The wind speed sensing control component includes the air velocity transducer and the wind speed sensing module, and the air velocity transducer will The air speed data of collection passes to the ADC modular converters through the wind speed sensing module and passes to the micro controller module And the host computer.
2. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the power subsystem is Constant current source module, the constant current source module are connected with the temperature sensor module.
3. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the multi way temperature passes Sense control assembly is four road TEMP control assemblies, the four roads TEMP control assembly include No. four temperature sensors and Four tunnel temperature sensor modules, No. four temperature sensor include temperature sensor, the placement being placed in plasma chamber body Temperature sensor at ion source interface, is placed on the temperature sensor of instrument internal and the temperature being placed on outside instrument passes Sensor.
4. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the temperature sensor Using four line platinum resistance thermometer sensor, PT100.
5. according to described mass spectrograph humiture, the wind speed monitoring system of any one of claim 1 or 3, it is characterised in that institute The temperature for stating the multi way temperature sensor lay down location in multi way temperature sensing control component is controlled less than or equal to 60 Degree Celsius.
6. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the air velocity transducer The blast velocity control of lay down location more than or equal to 5m/s and is being less than or equal to 40m/s.
7. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the system also includes Signal conditioning circuit, the temperature sensor or the air velocity transducer or the humidity sensor pass through the signal condition Circuit passes to the ADC modular converters again.
8. mass spectrograph humiture according to claim 1, wind speed monitoring system, it is characterised in that the system also includes For including the display of displays temperature or humidity or wind speed or combinations thereof.
9. mass spectrograph humiture according to claim 8, wind speed monitoring system, it is characterised in that the display also wraps Including includes the human-computer interaction control section of temperature or humidity or wind speed or combinations thereof for controlling.
CN201710924710.7A 2017-10-01 2017-10-01 A kind of mass spectrograph humiture, wind speed monitoring system Pending CN107631755A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110646499A (en) * 2019-09-06 2020-01-03 清华大学 Intelligent self-adaptive mass spectrometer based on working condition monitoring
CN111403257A (en) * 2020-02-27 2020-07-10 中国科学院广州地球化学研究所 Ion probe laboratory monitoring system and method
WO2021043179A1 (en) * 2019-09-06 2021-03-11 清华大学 Adaptive correction method and apparatus for mass spectrometer, and intelligent adaptive mass spectrometer

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US20100206065A1 (en) * 2009-02-19 2010-08-19 Delta Electronics, Inc. Wind speed detecting circuit capable of detecting the timing for replacing dust-proof element of electronic device
WO2012093326A1 (en) * 2011-01-07 2012-07-12 Koninklijke Philips Electronics N.V. Incubator assembly and associated control apparatus that controls humidity rate
CN102768262A (en) * 2012-07-17 2012-11-07 沈阳产品质量监督检验院 Combined intelligent detecting system with large-capacity environmental chamber and GC-MS (gas chromatography-mass spectrometer)
CN203965967U (en) * 2014-07-15 2014-11-26 江苏天瑞仪器股份有限公司 Temperature-control circuit
CN204347045U (en) * 2015-01-27 2015-05-20 肖洋 For the Environmental emergency monitoring car of flow detection volatile organic matter
CN105929870A (en) * 2016-07-15 2016-09-07 江苏天瑞仪器股份有限公司 Novel light chamber constant-temperature system

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100206065A1 (en) * 2009-02-19 2010-08-19 Delta Electronics, Inc. Wind speed detecting circuit capable of detecting the timing for replacing dust-proof element of electronic device
WO2012093326A1 (en) * 2011-01-07 2012-07-12 Koninklijke Philips Electronics N.V. Incubator assembly and associated control apparatus that controls humidity rate
CN102768262A (en) * 2012-07-17 2012-11-07 沈阳产品质量监督检验院 Combined intelligent detecting system with large-capacity environmental chamber and GC-MS (gas chromatography-mass spectrometer)
CN203965967U (en) * 2014-07-15 2014-11-26 江苏天瑞仪器股份有限公司 Temperature-control circuit
CN204347045U (en) * 2015-01-27 2015-05-20 肖洋 For the Environmental emergency monitoring car of flow detection volatile organic matter
CN105929870A (en) * 2016-07-15 2016-09-07 江苏天瑞仪器股份有限公司 Novel light chamber constant-temperature system

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110646499A (en) * 2019-09-06 2020-01-03 清华大学 Intelligent self-adaptive mass spectrometer based on working condition monitoring
WO2021043179A1 (en) * 2019-09-06 2021-03-11 清华大学 Adaptive correction method and apparatus for mass spectrometer, and intelligent adaptive mass spectrometer
CN111403257A (en) * 2020-02-27 2020-07-10 中国科学院广州地球化学研究所 Ion probe laboratory monitoring system and method

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