CN107630274A - A kind of production technology of the black sewing thread of high intensity - Google Patents

A kind of production technology of the black sewing thread of high intensity Download PDF

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Publication number
CN107630274A
CN107630274A CN201710876796.0A CN201710876796A CN107630274A CN 107630274 A CN107630274 A CN 107630274A CN 201710876796 A CN201710876796 A CN 201710876796A CN 107630274 A CN107630274 A CN 107630274A
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China
Prior art keywords
sewing thread
black
fiber solution
high intensity
kettle
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CN201710876796.0A
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Chinese (zh)
Inventor
陈建忠
马强
刘明义
闻继善
庄洋
张文强
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CHUZHOU ANXING ENVIRONMENTAL PROTECTION COLOR-FIBER Co Ltd
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CHUZHOU ANXING ENVIRONMENTAL PROTECTION COLOR-FIBER Co Ltd
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Priority to CN201710876796.0A priority Critical patent/CN107630274A/en
Publication of CN107630274A publication Critical patent/CN107630274A/en
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Abstract

The invention discloses a kind of production technology of the black sewing thread of high intensity, comprise the following steps:S1, using terephthalic acid (TPA) and ethylene glycol as Material synthesis polyester fiber, add colouring agent and silicone oil, produce coloring polyester fiber solution;S2, by polyamide and epoxy resin is dry, section, heating are melted, add melt index conditioning agent, chlorinated paraffin, ultra-violet absorber, colouring agent and silicone oil, it is well mixed to produce auxiliary fiber solution;S3, by coloring polyester fiber solution and the blend spinning of auxiliary fiber solution, solidification, vacuum cooled, produce composite fibre;S4, by composite fibre dewing and hair shredding, cotton carding, drafting, the immersion of enhancing liquid, rove, drawing-off, spun yarn, double twisting, produce the black sewing thread of high intensity.Production technology proposed by the present invention, simple to operate, production cost is low, production process is pollution-free, the black sewing thread color fastness and tensile strength of preparation are high, and resistance to elevated temperatures is excellent, is not easy to knot, service life length.

Description

A kind of production technology of the black sewing thread of high intensity
Technical field
The present invention relates to sewing thread production technical field, more particularly to a kind of production technology of the black sewing thread of high intensity.
Background technology
Sewing thread is to be knitted the line needed for clothes product, and sewing thread can be divided into natural fiber sewing thread, synthesis by raw material Fiber sewing thread and mixing sewing thread three major types.Natural fiber sewing thread is the sewing thread prepared using natural fiber as raw material, its Water suction, air permeable effect are good, the abundance of raw material, but sewing thread made of natural fiber easily deforms in use, The trend and tensile strength of sewing thread are influenceed, and the raw material that natural fiber uses extracts, increase spinning cumbersome with processing procedure The difficulty of technique;The tensile strength of synthetic fibers sewing thread is significantly stronger than natural fiber, and in the production process of sewing thread It is simple to operate also more traditional natural fiber sewing thread, but the resistance to elevated temperatures of existing synthetic fibers sewing thread is poor, temperature More than 250 DEG C sewing threads easily break, and difficulty is brought to production;Mixing sewing thread solves lacking for synthetic line non-refractory Point, but need to carry out the concerned process steps of cored in production process, it is necessary to increase special equipment, increase production cost, and increase Sewing thread production difficulty, extend the sewing thread production cycle.And the dark sewing thread produced at present, especially black are sewed The fast colours degree of line is poor, fades in use more serious.Based on this, the present invention proposes a kind of black sewing thread of high intensity Production technology.
The content of the invention
The invention aims to solve shortcoming present in prior art, and the black sewing thread of a kind of high intensity proposed Production technology.
A kind of production technology of the black sewing thread of high intensity, comprises the following steps:
S1, coloring polyester fiber solution preparation:Using antimony acetate as catalyst, passed through using terephthalic acid (TPA) and ethylene glycol as raw material The five direct synthetic polyester fibers of kettle working system, then colouring agent and silicone oil are added into polyester fiber, heating fusing, and mix equal It is even, coloring polyester fiber solution is produced, it is standby;
S2, auxiliary fiber solution preparation:Polyamide and epoxy resin are respectively placed in dryer and dry water removal, then is turned Move in slicer and cut into slices, be subsequently placed in melting machine and heat fusing, then keeping temperature adds melt index conditioning agent, chlorination stone Wax, ultra-violet absorber, colouring agent and silicone oil, it is well mixed to produce auxiliary fiber solution, it is standby;
S3, composite fibre preparation:The S1 coloring polyester fiber solution prepared and S2 the auxiliary fiber solution prepared are placed in mixed In the different barrels for closing spinning-drawing machine, and it is 2~4 according to coloring polyester fiber solution and auxiliary fiber solution:1~3 ratio is entered Row blend spinning, then cured, vacuum cooled, produce composite fibre;
It is prepared by S4, finished product:Composite fibre prepared by S3 steps is subjected to dewing and hair shredding, cotton carding and mixing in doubling step produce again Condensating fiber ripe bar, then fiber ripe bar is immersed in into 30~60min in enhancing liquid, then takes out, drains, then through rove, drawing-off, thin Yarn and double twisting process, produce the black sewing thread of high intensity.
Preferably, polyamide in the auxiliary fiber solution, epoxy resin, melt index conditioning agent, chlorinated paraffin, The mass ratio of ultra-violet absorber, colouring agent and silicone oil is 60~86:20~43:0.5~1.5:1~3:0.05~0.15:1~ 3:12~18.
Preferably, the enhancing liquid is with 1%~3% molybdenum disulfide, 2%~6% nano silicon, 10%~16% liquid Body paraffin, the mineral oil of surplus mix.
Preferably, five kettle is one kettle of esterification, is esterified two kettles, the kettle of polycondensation one, the kettle of polycondensation two and the kettle of polycondensation three, esterification one Kettle, two kettles of esterification, the kettle of polycondensation one, the kettle of polycondensation two and the kettle of polycondensation three are sequentially connected.
Preferably, the colouring agent is high-carbon black pigment.
Preferably, the addition of colouring agent is the 1%~3% of polyester fiber quality in the coloring polyester fiber solution, institute The addition for stating silicone oil in coloring polyester fiber solution is the 3%~6% of polyester fiber quality.
Preferably, the density of the black sewing thread of the production is 1.13~1.53dtex, and length is 35~41mm.
Production technology proposed by the present invention, it is simple to operate, production cost is low, production process is pollution-free, the black sewing of production Line mass is stable, and colouring agent is mixed into the initial fiber solution of black sewing thread by the way of original liquid coloring, to improve coloring The color firmness of agent, and silicone oil is added to improve dispersed homogeneous degree of the colouring agent in fiber solution, and also fiber is with polyester Fiber and the auxiliary fiber of special preparation are combined, and improve fiber overall tensile strength and resistance to elevated temperatures, make system Standby black sewing thread can add ultra-violet absorber with resistance to more than 300 DEG C of high temperature in the auxiliary fiber of special preparation, to improve The anti-uv-ray of black sewing thread, influence of the ultraviolet to black sewing thread color and luster is reduced, and then extend black sewing thread and use the longevity Life;Blend spinning is carried out again using separately preparing fiber solution in production, can improve spinning efficiency, and it is compound after spinning Fibre property uniformity, stability is good, is selected when composite fibre post-processes with molybdenum disulfide, nano silicon, liquid The enhancing liquid of paraffin and mineral oil composition carries out performance enhancement, can significantly improve the fast colours degree and tension of black sewing thread Intensity is stretched, and the knotting frequency of black sewing thread can be reduced, improves the service life of black sewing thread.
Embodiment
The present invention is made with reference to specific embodiment further to explain.
Embodiment one
A kind of production technology of the black sewing thread of high intensity proposed by the present invention, comprises the following steps:
S1, coloring polyester fiber solution preparation:Using antimony acetate as catalyst, passed through using terephthalic acid (TPA) and ethylene glycol as raw material The five direct synthetic polyester fibers of kettle working system, then add into polyester fiber the high-carbon black pigment and polyester of polyester fiber quality 2% The silicone oil of fiber quality 5%, heating fusing, and be well mixed, coloring polyester fiber solution is produced, it is standby;
S2, auxiliary fiber solution preparation:Polyamide and epoxy resin are respectively placed in dryer and dry water removal, then is turned Move in slicer and cut into slices, be subsequently placed in melting machine and heat fusing, then keeping temperature adds melt index conditioning agent, chlorination stone Wax, ultra-violet absorber, high-carbon black pigment and silicone oil, it is well mixed to produce auxiliary fiber solution, it is standby;
S3, composite fibre preparation:The S1 coloring polyester fiber solution prepared and S2 the auxiliary fiber solution prepared are placed in mixed In the different barrels for closing spinning-drawing machine, and it is 3 according to coloring polyester fiber solution and auxiliary fiber solution:2 ratio is mixed Spinning, then cured, vacuum cooled, produce composite fibre;
It is prepared by S4, finished product:Composite fibre prepared by S3 steps is subjected to dewing and hair shredding, cotton carding and mixing in doubling step produce again Condensating fiber ripe bar, then by fiber ripe bar be immersed in enhancing liquid in 40min, then take out, drain, then through rove, drawing-off, spun yarn and Double twisting process, produce the black sewing thread of high intensity.
In the present invention, polyamide, epoxy resin, melt index conditioning agent, chlorination stone in the auxiliary fiber solution Wax, ultra-violet absorber, the mass ratio of colouring agent and silicone oil are 72:20~43:1:2:0.1:2:15;The enhancing liquid is with 2% Molybdenum disulfide, 4% nano silicon, 13% atoleine, the mineral oil of surplus mix.
Embodiment two
A kind of production technology of the black sewing thread of high intensity proposed by the present invention, comprises the following steps:
S1, coloring polyester fiber solution preparation:Using antimony acetate as catalyst, passed through using terephthalic acid (TPA) and ethylene glycol as raw material The five direct synthetic polyester fibers of kettle working system, then add into polyester fiber the high-carbon black pigment and polyester of polyester fiber quality 3% The silicone oil of fiber quality 4%, heating fusing, and be well mixed, coloring polyester fiber solution is produced, it is standby;
S2, auxiliary fiber solution preparation:Polyamide and epoxy resin are respectively placed in dryer and dry water removal, then is turned Move in slicer and cut into slices, be subsequently placed in melting machine and heat fusing, then keeping temperature adds melt index conditioning agent, chlorination stone Wax, ultra-violet absorber, high-carbon black pigment and silicone oil, it is well mixed to produce auxiliary fiber solution, it is standby;
S3, composite fibre preparation:The S1 coloring polyester fiber solution prepared and S2 the auxiliary fiber solution prepared are placed in mixed In the different barrels for closing spinning-drawing machine, and it is 4 according to coloring polyester fiber solution and auxiliary fiber solution:3 ratio is mixed Spinning, then cured, vacuum cooled, produce composite fibre;
It is prepared by S4, finished product:Composite fibre prepared by S3 steps is subjected to dewing and hair shredding, cotton carding and mixing in doubling step produce again Condensating fiber ripe bar, then by fiber ripe bar be immersed in enhancing liquid in 60min, then take out, drain, then through rove, drawing-off, spun yarn and Double twisting process, produce the black sewing thread of high intensity.
In the present invention, polyamide, epoxy resin, melt index conditioning agent, chlorination stone in the auxiliary fiber solution Wax, ultra-violet absorber, the mass ratio of colouring agent and silicone oil are 66:29:1.5:2:0.15:1:14;The enhancing liquid is with 1% Molybdenum disulfide, 6% nano silicon, 10% atoleine, the mineral oil of surplus mix.
Embodiment three
A kind of production technology of the black sewing thread of high intensity proposed by the present invention, comprises the following steps:
S1, coloring polyester fiber solution preparation:Using antimony acetate as catalyst, passed through using terephthalic acid (TPA) and ethylene glycol as raw material The five direct synthetic polyester fibers of kettle working system, then add into polyester fiber the high-carbon black pigment and polyester of polyester fiber quality 1% The silicone oil of fiber quality 6%, heating fusing, and be well mixed, coloring polyester fiber solution is produced, it is standby;
S2, auxiliary fiber solution preparation:Polyamide and epoxy resin are respectively placed in dryer and dry water removal, then is turned Move in slicer and cut into slices, be subsequently placed in melting machine and heat fusing, then keeping temperature adds melt index conditioning agent, chlorination stone Wax, ultra-violet absorber, high-carbon black pigment and silicone oil, it is well mixed to produce auxiliary fiber solution, it is standby;
S3, composite fibre preparation:The S1 coloring polyester fiber solution prepared and S2 the auxiliary fiber solution prepared are placed in mixed In the different barrels for closing spinning-drawing machine, and it is 2 according to coloring polyester fiber solution and auxiliary fiber solution:3 ratio is mixed Spinning, then cured, vacuum cooled, produce composite fibre;
It is prepared by S4, finished product:Composite fibre prepared by S3 steps is subjected to dewing and hair shredding, cotton carding and mixing in doubling step produce again Condensating fiber ripe bar, then by fiber ripe bar be immersed in enhancing liquid in 50min, then take out, drain, then through rove, drawing-off, spun yarn and Double twisting process, produce the black sewing thread of high intensity.
In the present invention, polyamide, epoxy resin, melt index conditioning agent, chlorination stone in the auxiliary fiber solution Wax, ultra-violet absorber, the mass ratio of colouring agent and silicone oil are 60:20:1:2:0.05:2:12;The enhancing liquid is with the two of 2% Molybdenum sulfide, 4% nano silicon, 14% atoleine, the mineral oil of surplus mix.
The performance of the black sewing thread produced to the production technology of embodiment one~tri- detects, and testing result is as follows:
Embodiment One Two Three
Fracture strength cN/dtex 7.2 6.9 7.1
300 DEG C of lasting 60min State is unchanged State is unchanged State is unchanged
Wash firmness 5 grades 5 grades 5 grades
Wet friction firmness 5 grades 5 grades 5 grades
Exposure to Sunlight firmness 7 grades 7 grades 7 grades
Chlorine floats firmness 4 grades 4 grades 4 grades
Test result indicates that the fast colours degree of black sewing thread can reach 4 grades caused by the production technology of embodiment one~tri- More than and, fracture strength can reach more than 6.5cN/dtex, continue 60min under the conditions of 300 DEG C, the state of black sewing thread is not Change, and black sewing thread similar nature caused by the production technology of embodiment one~tri-, show:Black sewing thread proposed by the present invention Stable processing technique, the fast colours degree of the black sewing thread of production is good, fracture strength is high, resistance to elevated temperatures is excellent.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (7)

1. a kind of production technology of the black sewing thread of high intensity, it is characterised in that comprise the following steps:
S1, coloring polyester fiber solution preparation:Using antimony acetate as catalyst, passed through using terephthalic acid (TPA) and ethylene glycol as raw material The five direct synthetic polyester fibers of kettle working system, then colouring agent and silicone oil are added into polyester fiber, heating fusing, and mix equal It is even, coloring polyester fiber solution is produced, it is standby;
S2, auxiliary fiber solution preparation:Polyamide and epoxy resin are respectively placed in dryer and dry water removal, then is turned Move in slicer and cut into slices, be subsequently placed in melting machine and heat fusing, then keeping temperature adds melt index conditioning agent, chlorination stone Wax, ultra-violet absorber, colouring agent and silicone oil, it is well mixed to produce auxiliary fiber solution, it is standby;
S3, composite fibre preparation:The S1 coloring polyester fiber solution prepared and S2 the auxiliary fiber solution prepared are placed in mixed In the different barrels for closing spinning-drawing machine, and it is 2~4 according to coloring polyester fiber solution and auxiliary fiber solution:1~3 ratio is entered Row blend spinning, then cured, vacuum cooled, produce composite fibre;
It is prepared by S4, finished product:Composite fibre prepared by S3 steps is subjected to dewing and hair shredding, cotton carding and mixing in doubling step produce again Condensating fiber ripe bar, then fiber ripe bar is immersed in into 30~60min in enhancing liquid, then takes out, drains, then through rove, drawing-off, thin Yarn and double twisting process, produce the black sewing thread of high intensity.
A kind of 2. production technology of the black sewing thread of high intensity according to claim 1, it is characterised in that the auxiliary fiber Polyamide in solution, epoxy resin, melt index conditioning agent, chlorinated paraffin, ultra-violet absorber, colouring agent and silicone oil Mass ratio is 60~86:20~43:0.5~1.5:1~3:0.05~0.15:1~3:12~18.
A kind of 3. production technology of the black sewing thread of high intensity according to claim 1, it is characterised in that it is described enhancing liquid with 1%~3% molybdenum disulfide, 2%~6% nano silicon, 10%~16% atoleine, the mineral oil of surplus Mix.
4. the production technology of the black sewing thread of a kind of high intensity according to claim 1, it is characterised in that five kettle is ester Change a kettle, two kettles of esterification, the kettle of polycondensation one, the kettle of polycondensation two and the kettle of polycondensation three, one kettle of esterification, two kettles of esterification, the kettle of polycondensation one, polycondensation two Kettle and the kettle of polycondensation three are sequentially connected.
5. the production technology of the black sewing thread of a kind of high intensity according to claim 1, it is characterised in that the colouring agent is High-carbon black pigment.
A kind of 6. production technology of the black sewing thread of high intensity according to claim 1, it is characterised in that the pigmented polyester The addition of colouring agent is the 1%~3% of polyester fiber quality in fiber solution, silicone oil in the coloring polyester fiber solution Addition is the 3%~6% of polyester fiber quality.
A kind of 7. production technology of the black sewing thread of high intensity according to claim 1, it is characterised in that the production it is black The density of sewing thread is 1.13~1.53dtex, and length is 35~41mm.
CN201710876796.0A 2017-09-25 2017-09-25 A kind of production technology of the black sewing thread of high intensity Pending CN107630274A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108842251A (en) * 2018-08-03 2018-11-20 江苏中祥线带有限公司 A kind of preparation method of anti-electrostatic polyester sewing thread
CN111607840A (en) * 2020-07-09 2020-09-01 福州运泉织带有限公司 High-strength fiber for anti-cutting woven tape and preparation method thereof
CN111719198A (en) * 2019-03-21 2020-09-29 上海菲佐环保科技有限公司 Preparation method of p84 fiber and pps fiber composite fiber
CN113913986A (en) * 2021-11-04 2022-01-11 际华三五零九纺织有限公司 Polyester yarn and production method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108842251A (en) * 2018-08-03 2018-11-20 江苏中祥线带有限公司 A kind of preparation method of anti-electrostatic polyester sewing thread
CN111719198A (en) * 2019-03-21 2020-09-29 上海菲佐环保科技有限公司 Preparation method of p84 fiber and pps fiber composite fiber
CN111607840A (en) * 2020-07-09 2020-09-01 福州运泉织带有限公司 High-strength fiber for anti-cutting woven tape and preparation method thereof
CN113913986A (en) * 2021-11-04 2022-01-11 际华三五零九纺织有限公司 Polyester yarn and production method thereof

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