CN107620074A - Heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof - Google Patents
Heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof Download PDFInfo
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- CN107620074A CN107620074A CN201610547056.8A CN201610547056A CN107620074A CN 107620074 A CN107620074 A CN 107620074A CN 201610547056 A CN201610547056 A CN 201610547056A CN 107620074 A CN107620074 A CN 107620074A
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- heavy oil
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- 239000000295 fuel oil Substances 0.000 title claims abstract description 40
- 239000012459 cleaning agent Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000000203 mixture Substances 0.000 title claims abstract description 14
- 239000000463 material Substances 0.000 title claims abstract description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 84
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 28
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 28
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 28
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims abstract description 28
- 235000019795 sodium metasilicate Nutrition 0.000 claims abstract description 28
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 28
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 28
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims abstract description 15
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims abstract description 15
- 239000010665 pine oil Substances 0.000 claims description 26
- 238000003756 stirring Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 4
- 229940043237 diethanolamine Drugs 0.000 abstract 2
- 239000011297 pine tar Substances 0.000 abstract 2
- 229940068124 pine tar Drugs 0.000 abstract 2
- 239000003921 oil Substances 0.000 description 13
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
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- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof, wherein, the composition includes water, citric acid, sodium metasilicate, diethanol amine, pine tar, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate；Wherein, relative to the water of 1000 parts by weight, the content of the citric acid is 50 200 parts by weight, the content of the sodium metasilicate is 10 80 parts by weight, the content of the diethanol amine is 10 50 parts by weight, the content of the pine tar is 10 30 parts by weight, and the content of the disodium ethylene diamine tetraacetate is 50 100 parts by weight, and the content of the tetrasodium pyrophosphate is 10 80 parts by weight.By above-mentioned design, heavy oil dirt can effectively be removed by realizing, and greatly improve the effect of cleaning efficiency.
Description
Technical Field
The invention relates to the field of production and preparation of cleaning agents, in particular to a heavy oil cleaning agent material composition, a heavy oil cleaning agent and a preparation method thereof.
Background
In industrial production, a lot of industrial oil such as lubricating oil and the like cannot be used, the used industrial oil is easy to cause the oil stain on the surface of equipment to be overweight, particularly, thick oil stain is accumulated on the surface of the equipment along with the prolonging of the service life, and operators cannot clean the equipment every day due to the problems of production efficiency and the like, so that the accumulated oil stain is difficult to clean, and each cleaning is very troublesome.
Therefore, the invention provides a heavy oil cleaning agent material composition which can effectively remove heavy oil stains and greatly improve the cleaning efficiency, a heavy oil cleaning agent and a preparation method thereof, and aims to solve the problems in urgent need.
Disclosure of Invention
Aiming at the prior art, the invention aims to overcome the problems that industrial oil used in the prior art is very easy to cause overweight oil stains on the surface of equipment, particularly thick oil stains are accumulated on the surface of the equipment along with the prolonging of the service time, and operators are not easy to clean every day due to the problems of production efficiency and the like, so that the accumulated oil stains are difficult to clean, and the cleaning is very troublesome every time, thereby providing a heavy oil cleaner material composition, a heavy oil cleaner and a preparation method thereof, which can effectively remove the heavy oil stains and greatly improve the cleaning efficiency.
In order to achieve the above object, the present invention provides a heavy oil detergent material composition, wherein the composition comprises water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylenediaminetetraacetate, and tetrasodium pyrophosphate; wherein,
the content of the citric acid is 50-200 parts by weight, the content of the sodium metasilicate is 10-80 parts by weight, the content of the diethanolamine is 10-50 parts by weight, the content of the pine oil is 10-30 parts by weight, the content of the disodium edetate is 50-100 parts by weight, and the content of the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
The invention also provides a preparation method of the heavy oil cleaning agent, wherein the preparation method comprises the following steps: mixing water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate to prepare a heavy oil cleaning agent; wherein,
the citric acid is 50-200 parts by weight, the sodium metasilicate is 10-80 parts by weight, the diethanolamine is 10-50 parts by weight, the pine oil is 10-30 parts by weight, the disodium edetate is 50-100 parts by weight, and the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
The invention also provides a heavy oil cleaning agent prepared by the preparation method.
According to the technical scheme, the heavy oil cleaning agent is prepared by mixing water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate according to a certain proportion, so that the heavy oil cleaning agent prepared by mixing the materials can effectively clean heavy oil, and the problem of difficulty in cleaning due to over-thick accumulated oil stains is greatly solved.
Additional features and advantages of the invention will be set forth in the detailed description which follows.
Detailed Description
The following describes in detail specific embodiments of the present invention. It should be understood that the detailed description and specific examples, while indicating the present invention, are given by way of illustration and explanation only, not limitation.
The invention provides a heavy oil cleaning agent material composition, wherein the composition comprises water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate; wherein,
the content of the citric acid is 50-200 parts by weight, the content of the sodium metasilicate is 10-80 parts by weight, the content of the diethanolamine is 10-50 parts by weight, the content of the pine oil is 10-30 parts by weight, the content of the disodium edetate is 50-100 parts by weight, and the content of the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
According to the design, the heavy oil cleaning agent is prepared by mixing water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate according to a certain proportion, so that the heavy oil cleaning agent prepared by mixing the materials can effectively clean heavy oil, and the problem that the cleaning is difficult due to over-thick oil stain accumulation is greatly avoided.
In a preferred embodiment of the present invention, in order to improve the cleaning effect of the produced heavy oil cleaning agent, the citric acid is 80 to 150 parts by weight, the sodium metasilicate is 30 to 60 parts by weight, the diethanolamine is 20 to 40 parts by weight, the pine oil is 15 to 25 parts by weight, the disodium ethylenediaminetetraacetate is 70 to 90 parts by weight, and the tetrasodium pyrophosphate is 40 to 60 parts by weight, based on 1000 parts by weight of the water.
The invention also provides a preparation method of the heavy oil cleaning agent, wherein the preparation method comprises the following steps: mixing water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate to prepare a heavy oil cleaning agent; wherein,
the citric acid is 50-200 parts by weight, the sodium metasilicate is 10-80 parts by weight, the diethanolamine is 10-50 parts by weight, the pine oil is 10-30 parts by weight, the disodium edetate is 50-100 parts by weight, and the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
Likewise, in a preferred embodiment of the present invention, the citric acid is used in an amount of 80 to 150 parts by weight, the sodium metasilicate is used in an amount of 30 to 60 parts by weight, the diethanolamine is used in an amount of 20 to 40 parts by weight, the pine oil is used in an amount of 15 to 25 parts by weight, the disodium edetate is used in an amount of 70 to 90 parts by weight, and the tetrasodium pyrophosphate is used in an amount of 40 to 60 parts by weight, relative to 1000 parts by weight of the water.
The mixing process may be conducted under mixing conditions conventionally employed in the art, although in a more preferred embodiment of the present invention, the temperature of the mixing process is 40-60 deg.C in order to further enhance the mixing effect and thus greatly enhance the cleaning effect of the heavy oil cleaning agent.
The mixing process may be carried out in a manner conventional in the art, for example, in a preferred embodiment, the mixing process may be stirred mixing at a stirring rate of 200-400 r/min.
The invention also provides a heavy oil cleaning agent prepared by the preparation method.
The present invention will be described in detail below by way of examples. In the following examples, the citric acid, the sodium metasilicate, the diethanolamine, the pine oil, the disodium ethylenediaminetetraacetate, and the tetrasodium pyrophosphate are conventional commercial products.
Example 1
1000g of water, 80g of citric acid, 30g of sodium metasilicate, 20g of diethanolamine, 15g of pine oil, 70g of disodium ethylenediamine tetraacetic acid and 40g of tetrasodium pyrophosphate are stirred and mixed at the temperature of 40 ℃ at the stirring speed of 200r/min to prepare the heavy oil cleaning agent A1.
Example 2
1000g of water, 150g of citric acid, 60g of sodium metasilicate, 40g of diethanolamine, 25g of pine oil, 90g of disodium ethylenediamine tetraacetic acid and 60g of tetrasodium pyrophosphate are stirred and mixed at the temperature of 60 ℃ at the stirring speed of 400r/min to prepare the heavy oil cleaning agent A2.
Example 3
1000g of water, 120g of citric acid, 50g of sodium metasilicate, 30g of diethanolamine, 20g of pine oil, 80g of disodium ethylenediamine tetraacetic acid and 50g of tetrasodium pyrophosphate are stirred and mixed at the temperature of 50 ℃ at the stirring speed of 300r/min to prepare the heavy oil cleaning agent A3.
Example 4
The heavy oil cleaning agent A4 was prepared according to the preparation method of example 1, except that 50g of citric acid, 10g of sodium metasilicate, 10g of diethanolamine, 10g of pine oil, 50g of disodium edetate and 10g of tetrasodium pyrophosphate were used.
Example 5
The heavy oil cleaning agent A5 was prepared according to the preparation method of example 2, except that the citric acid was used in an amount of 200g, the sodium metasilicate was used in an amount of 80g, the diethanolamine was used in an amount of 50g, the pine oil was used in an amount of 30g, the disodium ethylenediaminetetraacetate was used in an amount of 100g, and the tetrasodium pyrophosphate was used in an amount of 80 g.
Comparative example 1
The preparation was carried out according to the preparation method of example 3 except that the amount of citric acid was 20g, the amount of sodium metasilicate was 5g, the amount of diethanolamine was 5g, the amount of pine oil was 5g, the amount of disodium edetate was 20g, and the amount of tetrasodium pyrophosphate was 5g, to obtain cleaning agent D1.
Comparative example 2
The preparation was carried out according to the preparation method of example 3, except that the amount of citric acid was 300g, the amount of sodium metasilicate was 100g, the amount of diethanolamine was 80g, the amount of pine oil was 50g, the amount of disodium edetate was 120g, and the amount of tetrasodium pyrophosphate was 100g, to obtain cleaning agent D2.
Test example
After the metal sheet with the surface deposited with the greasy dirt is placed in the prepared A1-A5, D1 and D2 to be soaked for 10min, the metal sheet is washed clean by water, and the greasy dirt condition of the metal surface is detected, and the obtained results are shown in Table 1.
TABLE 1
| Numbering | Surface oil stain |
| A1 | Without greasy dirt |
| A2 | Without greasy dirt |
| A3 | Without greasy dirt |
| A4 | No obvious greasy dirt |
| A5 | No obvious greasy dirt |
| D1 | Oil stain deposition is severe |
| D2 | Apparent greasy dirt |
The preferred embodiments of the present invention have been described in detail, however, the present invention is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present invention within the technical idea of the present invention, and these simple modifications are within the protective scope of the present invention.
It should be noted that the various technical features described in the above embodiments can be combined in any suitable manner without contradiction, and the invention is not described in any way for the possible combinations in order to avoid unnecessary repetition.
In addition, any combination of the various embodiments of the present invention is also possible, and the same should be considered as the disclosure of the present invention as long as it does not depart from the spirit of the present invention.
Claims (7)
1. A heavy oil cleaning agent material composition, characterized in that the composition comprises water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylenediaminetetraacetate and tetrasodium pyrophosphate; wherein,
the content of the citric acid is 50-200 parts by weight, the content of the sodium metasilicate is 10-80 parts by weight, the content of the diethanolamine is 10-50 parts by weight, the content of the pine oil is 10-30 parts by weight, the content of the disodium edetate is 50-100 parts by weight, and the content of the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
2. The composition as claimed in claim 1, wherein the citric acid is contained in an amount of 80-150 parts by weight, the sodium metasilicate is contained in an amount of 30-60 parts by weight, the diethanolamine is contained in an amount of 20-40 parts by weight, the pine oil is contained in an amount of 15-25 parts by weight, the disodium ethylenediaminetetraacetate is contained in an amount of 70-90 parts by weight, and the tetrasodium pyrophosphate is contained in an amount of 40-60 parts by weight, with respect to 1000 parts by weight of the water.
3. The preparation method of the heavy oil cleaning agent is characterized by comprising the following steps: mixing water, citric acid, sodium metasilicate, diethanolamine, pine oil, disodium ethylene diamine tetraacetate and tetrasodium pyrophosphate to prepare a heavy oil cleaning agent; wherein,
the citric acid is 50-200 parts by weight, the sodium metasilicate is 10-80 parts by weight, the diethanolamine is 10-50 parts by weight, the pine oil is 10-30 parts by weight, the disodium edetate is 50-100 parts by weight, and the tetrasodium pyrophosphate is 10-80 parts by weight, relative to 1000 parts by weight of the water.
4. The preparation method of claim 3, wherein the citric acid is used in an amount of 80 to 150 parts by weight, the sodium metasilicate is used in an amount of 30 to 60 parts by weight, the diethanolamine is used in an amount of 20 to 40 parts by weight, the pine oil is used in an amount of 15 to 25 parts by weight, the disodium ethylenediaminetetraacetate is used in an amount of 70 to 90 parts by weight, and the tetrasodium pyrophosphate is used in an amount of 40 to 60 parts by weight, relative to 1000 parts by weight of the water.
5. The production method according to claim 3 or 4, wherein the temperature during the mixing is 40 to 60 ℃.
6. The preparation method according to claim 3 or 4, wherein the mixing process is stirring mixing, and the stirring speed is 200-400 r/min.
7. A heavy oil cleaning agent prepared by the preparation method according to any one of claims 3 to 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610547056.8A CN107620074A (en) | 2016-07-13 | 2016-07-13 | Heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610547056.8A CN107620074A (en) | 2016-07-13 | 2016-07-13 | Heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof |
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| CN107620074A true CN107620074A (en) | 2018-01-23 |
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| CN201610547056.8A Pending CN107620074A (en) | 2016-07-13 | 2016-07-13 | Heavy oil cleaning agent material compositions and heavy oil cleaning agent and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108929793A (en) * | 2018-05-25 | 2018-12-04 | 湖北三环化学新材料股份有限公司 | A kind of aqua type heavy oil cleaning agent |
| CN112522038A (en) * | 2020-12-17 | 2021-03-19 | 厦门美林克达科技有限公司 | Oil stain cleaning agent |
-
2016
- 2016-07-13 CN CN201610547056.8A patent/CN107620074A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108929793A (en) * | 2018-05-25 | 2018-12-04 | 湖北三环化学新材料股份有限公司 | A kind of aqua type heavy oil cleaning agent |
| CN112522038A (en) * | 2020-12-17 | 2021-03-19 | 厦门美林克达科技有限公司 | Oil stain cleaning agent |
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Application publication date: 20180123 |
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