CN107619740A - A kind of preparation method of pure fermented honey moderate wine - Google Patents
A kind of preparation method of pure fermented honey moderate wine Download PDFInfo
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- CN107619740A CN107619740A CN201710874604.2A CN201710874604A CN107619740A CN 107619740 A CN107619740 A CN 107619740A CN 201710874604 A CN201710874604 A CN 201710874604A CN 107619740 A CN107619740 A CN 107619740A
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Abstract
The invention provides a kind of preparation method of pure fermented honey moderate wine, using the low pure fermented honey wine of alcoholic strength 8 18% (V/V) as raw material, when improving alcoholic strength, to ensure the color of pure fermented honey wine, it is fragrant, taste and active ingredient, the distillation technique of tradition raising alcoholic strength is substituted with membrane separation technique, high molecular weight protein is removed with 50nm ceramic membrane, the materials such as colloid, play clarification, ceramic membrane dialyzate crosses 20kD rolling ultrafiltration membrane, further material is clarified, remove macromolecular polysaccharide etc., ultrafiltration dialysis liquid enters the rolling anti-seepage membrane that molecular cut off is 100, it is to retain pure fermented honey wine and women-sensual pursuits that concentrate, which is, it is fragrant, the mother liquor of taste and active ingredient, permeate prepares pure fermented honey moderate wine through distilling obtained foreshot with mother liquor allotment.
Description
Technical field
The present invention relates to membrane technology in terms of the Wine that ferments application field, particularly relate to a kind of pure honey
The preparation method of fermentation moderate wine.
Background technology
Brewageing for hydromel is with a long history, and traditional brewing method is used till today, from spontaneous fermentation to adding song to brewage, although
Brewage process is simple, but quality is unstable.Hydromel does not have grape wine to popularize like that all the time, and one of reason is just a lack of conduct
Comprehensive quality of typical alcoholic beverage.
Honey low wine alcoholic strength is usually brewageed by pure fermented honey and formed in 0.5%~18.0% (V/V), the shelf-life
It is relatively short.Honey moderate wine alcoholic strength is in 18.1%~40.0% (V/V).Distilled by pure fermented honey or edible alcohol is matched somebody with somebody
System forms, and flavor is qualitative more difficult.Degerming, turbidity removal can effectively be carried out to fermented honeymead using membrane separation technique, improve wine
Clarity, and the color of wine can be kept, extend the storage life of wine.Moderate of fermenting hydromel can use vacuum distillation
Dealcoholysis, then the method being dehydrated, then add high concentration alcohol in concentrate and be deployed into honey moderate wine, even if being that use is most careful
Vacuum heat-treating method, also easily change the flavor of product, make honey wine taste not just, without the effect of reverse osmosis membrane separation method
Fruit is good.In general, the storage period of wine, is more permanent, and its taste is better, and price is also higher, but can gradually become mixed during storage
It is turbid, or even there is sediment, the quality of wine is have impact on, if hydromel is separated into two parts, wherein 70% is permeate, separately
Outer 30% is concentrate, then the material that precipitation can be produced in concentrate is in hypersaturated state, thus can accelerate to crystallize and separate out and sink
Form sediment, then precipitation is separated by filter and removed, then long-term place will not also separate out muddy thing, can be effectively improved hydromel
Stability.Li Houyu is in a kind of patent of invention " brewing method of the hydromel of healthy ecology " of application in 2016（Shen Qing Publication
Number A of CN 106047563）The high-quality honey of mature native and pure water are used as primary raw material, fermented rear alcoholic strength is 13-15
Degree.A kind of patent of invention " brew method of hydromel " of scientific research office of Anhui Normal University application in 2016（Application publication number CN
106479811 A）.A kind of patent of invention " mango of three mountain branch company of Hao Yikuai Food Co., Ltd of Wuhu City application in 2016
Core enriching yin hydromel and preparation method thereof "（The A of application publication number CN 105820900）Deng.The hydromel that these patents obtain is all
It is low wine.In order to obtain pure fermented honey moderate wine, and retain the color and active ingredient of pure fermented honey wine, improve
The stability of hydromel, extends the storage life of wine, and the low hydromel that this patent is brewageed using pure fermented honey is adopted as raw material
Pure fermented honey moderate wine is prepared with membrane technology and distillating method.
The content of the invention
This patent provides a kind of preparation method of pure fermented honey moderate wine.The 8- brewageed with pure fermented honey
18% (V/V) low hydromel is raw material, and high molecular weight protein, colloidal solids impurity are removed with ceramic membrane, plays preliminary clarification and makees
With ceramic membrane dialyzate crosses rolling ultrafiltration membrane, and further material is cleaned and clarified, ultrafiltration dialysis liquid crosses rolling anti-seepage membrane, dense
Contracting liquid as to retain the mother liquor of pure fermented honey wine color and luster, fragrance and active ingredient, through distilling obtained foreshot lead to by permeate
Cross and pure fermented honey moderate wine is prepared in the allotment of mother liquor.
The technical solution adopted by the present invention：A kind of preparation method of pure fermented honey moderate wine, it is characterised in that by following
Step operation：Using alcoholic strength 8-18% (V/V) pure fermented honey wine as raw material, substitute tradition with membrane separation technique and improve alcohol
The distillation technique of degree, with 50nm ceramic film process, the roll-to-roll ultrafiltration that ceramic membrane dialyzate is 20kD or so with molecular cut off
Film process, ultrafiltration dialysis liquid molecular cut off are 100 rolling reverse osmosis film process, and it is to retain pure fermented honey that concentrate, which is,
The mother liquor of wine color and active ingredient, permeate prepare pure honey through distilling obtained foreshot by the allotment with mother liquor
Ferment moderate wine.
It is described to be comprised the following steps that with 50nm ceramic film process：Using alcohol 8-18% (V/V) pure fermented honey wine as
Raw material, with 50nm ceramic membrane clarifying treatment, for removing thalline, high molecular weight protein, colloidal impurity, ceramic membrane permeate is clear
Clear liquid, it is standby, when permeate reaches cumulative volume 4.5/5（V/V）When stop concentration, ceramic membrane concentrate is mainly impurity.
The roll-to-roll ultrafiltration film process comprises the following steps that：Take it is above-mentioned tentatively clarify standby permeate through ceramic membrane, use
Rolled film processor filtering equipped with molecular cut off 20kD, further cleans to material, Polysaccharide removing, small molecular protein, rises
To clarification again, when permeate reaches cumulative volume 4.5/5（V/V）When stop concentration, rolled film concentrate be impurity, transmission
Liquid is standby.
The rolling reverse osmosis film process comprises the following steps that：Take the above-mentioned transmission standby through the clarification of roll-to-roll ultrafiltration film process
Liquid, filtered with the rolling anti-seepage membrane processor equipped with molecular cut off 100, when permeate reaches cumulative volume 2.5/3（V/V）When stop
Only concentrate, water and alcohol molecule can overcome naturally osmotic to press and pass through reverse osmosis membrane, and color material and nutriment are then
It is retained in concentrate, concentrate is is to retain the mother liquor of pure fermented honey wine color and luster, fragrance and active ingredient, the concentration
Liquid is standby, and permeate is water and alcohol, and permeate is standby.
The permeate is comprised the following steps that through distilling obtained foreshot by the allotment with mother liquor：Above-mentioned counter-infiltration is standby
Permeate, which is put into distillation still, is distilled, and is collected and is distilled out higher concentration alcohol and counter-infiltration standby concentrate early stage
Pure fermented honey moderate wine is prepared in allotment.
The invention has the advantages that：A kind of preparation method of pure fermented honey moderate wine of the present invention is simple to operate, overall process
It is no added, pollution-free, also without the active component destroyed in honey.Honey moderate wine alcoholic strength is in 18.1%~40.0% (V/
V), distilled by pure fermented honey or edible alcohol forms, its color and principle active component are difficult to be fully retained.
Degerming, turbidity removal can effectively be carried out to fermented honeymead using membrane separation technique, improve the clarity of wine, and can be kept
The color and active ingredient of wine.The moderate wine nutritive value exceedes honey in itself, and it, which removes to contain, makes finished product sweet and sour palatability
Outside monose, also containing various organic acids, contain 17 kinds of amino acid.It is grape wine comprising other various amino acid needed by human
As many as 6 times.In addition to the vitamin C in green molasses is remained, fermentation add vitamin B1 and other mineral matters for example potassium, sodium, calcium,
Magnesium, iron, the content of selenium.
In addition, when the material that can produce precipitation in the concentrate of counter-infiltration is in hypersaturated state, can accelerate to crystallize and separate out
Precipitation, then precipitation is separated by filter and removed, long-term place will not also separate out muddy thing, can be effectively improved hydromel
Stability, extend the storage life of wine.Alcoholic strength is in 18.1%~40.0%vol moderate hydromel, the white wine drunk with people's custom
The number of degrees are close, and are more suitable for the alcohol drinking patterns of Chinese.Hydromel has abundant fructose, organic acid, active peptide, enzyme, antibacterial
Plain, a variety of mineral elements needed by human and vitamins and other nutritious components.Pollen extract and free aminoacid content are extremely rich
It is rich.These small molecule nutriments soluble in water, are easily absorbed by the body, can participate in organism metabolism rapidly, timely and effectively
Needed by human body nutrient is supplemented, patient the old and the weak, excessive physical consumption person is regained one's strength quickly.Often drink hydromel to having a sleepless night, easily forgetting,
Lassitude and sexual deterioration etc. are effective in cure, intestines and stomach chronic disease are taken an evident turn for the better, to chronic bronchitis and asthma
Also there is fine effect etc. disease, can particularly make that skin is ruddy, remains youthful forever, and can anti-aging and strengthen immunity.
Brief description of the drawings
Fig. 1 present invention process schematic flow sheets；
Fig. 2 is the moderate hydromel examining report cover page that alcoholic strength prepared by embodiment 1 is 38 degree；
Fig. 3 is examining report content.
Embodiment
With reference to embodiment, the present invention is described in further detail, but it is not limitation of the invention, this
Invention is using alcoholic strength 8-18% (V/V) pure fermented honey wine as raw material, when improving alcoholic strength, is substituted and passed with membrane separation technique
System improves the distillation technique of alcoholic strength, prepares pure fermented honey moderate wine, but the invention is applied to low fermented wine etc. and needed
Retain color and principle active component improves the fermentation Wine of alcoholic strength.
Embodiment 1：
A kind of preparation method of pure fermented honey moderate wine as shown in Figure 1, is specifically operated in the steps below：
1st, alcoholic strength 8-18% (V/V) mL of pure fermented honey wine 12120 is taken, after interior mycetome, alcohol, pure fermented honey
Color and active ingredient and polysaccharide, albumen etc., are filtered with diatomite, and filtrate is standby.
2nd, diatomite filters the standby mL of filtrate 12000, is filtered with 50nm ceramic membrane processor, when permeate reaches
10800 mL stop concentration, and the mL of ceramic membrane concentrate about 1200 is mainly impurity, and permeate is standby.
3rd, ceramic membrane tentatively clarifies the standby mL of permeate 10800, with the rolling film process equipped with molecular cut off 20kD
Machine filters, and stops concentration when permeate is up to 9720 mL, the mL of rolled film concentrate 1080 is impurity, and permeate is standby.
4th, roll-to-roll ultrafiltration film process clarifies the standby mL of permeate 9720, with the rolling reverse osmosis equipped with molecular cut off 100
Film process machine filters, and when permeate stops concentrating up to 8100 mL, the mL of concentrate about 1620 is standby, and permeate is that water and alcohol are standby
With.
, the standby permeate of counter-infiltration be put into distillation still and distilled, collect distill out early stage higher concentration alcohol with
Pure fermented honey 38%vol moderate wine is prepared in the standby concentrate allotment of counter-infiltration.
6th, the mL of the ceramic membrane concentrate about 1200 and mL of rolled film concentrate 1080 merges, and after placing one week, uses diatomite
Filtering, filtrate can use as raw material.
As can be seen that the 38%vol moderate hydromels prepared, mineral matter is such as potassium, sodium, calcium, magnesium, iron, selenium from Fig. 2,3
Content is high, and containing 17 kinds of amino acid, nutritive value is high, and clarity is high, free from admixture, improve guarantee the quality, storage time.
Embodiment 2：
1st, alcoholic strength 8-18% (V/V) mL of pure fermented honey wine 15150 is taken, after interior mycetome, alcohol, pure fermented honey
Color and active ingredient and polysaccharide, albumen, are filtered, filtrate is standby with diatomite.
2nd, diatomite filters the standby mL of filtrate 15000, is filtered with the ceramic membrane processor equipped with 50nm, works as permeate
Stop concentrating up to 13500 mL, the mL of ceramic membrane concentrate about 1500 is mainly impurity, and permeate is standby.
3rd, ceramic membrane tentatively clarifies the standby mL of permeate 13500, with the rolling film process equipped with molecular cut off 20kD
Machine filters, and stops concentration when permeate is up to 12150 mL, the mL of rolled film concentrate 1350 is impurity, and permeate is standby.
4th, roll-to-roll ultrafiltration film process clarifies the standby mL of permeate 12150, anti-with the rolling equipped with molecular cut off 100
The filtering of film process machine is oozed, when permeate stops concentrating up to 10125 mL, the mL of concentrate about 2025 is standby, and permeate is water and wine
Essence is standby.
, the standby permeate of counter-infiltration be put into distillation still and distilled, collect distill out early stage higher concentration alcohol with
Pure fermented honey 40%vol moderate wine is prepared in the standby concentrate allotment of counter-infiltration.
6th, the mL of the ceramic membrane concentrate about 1500 and mL of rolled film concentrate 1350 merges, and after placing one week, uses diatomite
Filtering, filtrate can use as raw material.
Claims (5)
1. a kind of preparation method of pure fermented honey moderate wine, it is characterised in that be prepared according to the following steps：With alcoholic strength 8-18%
(V/V) pure fermented honey wine is raw material, is filtered with diatomite, filtrate is standby；It is saturating with 50nm ceramic film process, ceramic membrane
The roll-to-roll ultrafiltration film process that liquid is 20kD or so with molecular cut off is analysed, ultrafiltration dialysis liquid molecular cut off is 100 rolling
Reverse osmosis film process, concentrate is is the mother liquor for retaining pure fermented honey wine color and luster, fragrance and active ingredient, and permeate is through distillation
Obtained foreshot prepares pure fermented honey moderate wine with mother liquor allotment.
2. the preparation method of a kind of pure fermented honey moderate wine according to claim 1, it is characterised in that described to use 50nm
Ceramic film process comprise the following steps that：Using alcohol 8-18% (V/V) pure fermented honey wine as raw material, with 50nm ceramic membrane
Clarifying treatment, for removing thalline, high molecular weight protein, colloidal impurity, ceramic membrane permeate is clarified solution, standby, works as permeate
Reach cumulative volume 4.5/5（V/V）When stop concentration, ceramic membrane concentrate is mainly impurity.
3. the preparation method of a kind of pure fermented honey moderate wine according to claim 2, it is characterised in that the rolling surpasses
Filter membrane processing comprises the following steps that：Take it is above-mentioned standby permeate is tentatively clarified through ceramic membrane, with equipped with molecular cut off 20kD
Rolled film processor filtering, further to material clean, Polysaccharide removing, small molecular protein, clarification again is played, when saturating
Cross liquid and reach cumulative volume 4.5/5（V/V）When stop concentration, rolled film concentrate is impurity, and permeate is standby.
4. the preparation method of a kind of pure fermented honey moderate wine according to claim 1, it is characterised in that the rolling is anti-
Film process is oozed to comprise the following steps that：The above-mentioned permeate standby through the clarification of roll-to-roll ultrafiltration film process is taken, with equipped with molecular cut off
100 rolling anti-seepage membrane processor filtering, when permeate reaches cumulative volume 2.5/3（V/V）When stop concentration, water and alcohol molecule
Naturally osmotic can be overcome to press and pass through reverse osmosis membrane, and color material and nutriment are then retained in concentrate, it is dense
For contracting liquid to be to retain the mother liquor of pure fermented honey wine color and luster, fragrance and active ingredient, the concentrate is standby, permeate be water and
Alcohol, permeate are standby.
A kind of 5. preparation method of pure fermented honey moderate wine according to claim 1, it is characterised in that the permeate
Comprised the following steps that through distilling obtained foreshot by the allotment with mother liquor：The standby permeate of above-mentioned counter-infiltration is put into distillation
Distilled in kettle, collect to distill out higher concentration alcohol and counter-infiltration standby concentrate allotment early stage and prepare pure honey and send out
Ferment moderate wine.
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| CN201710874604.2A CN107619740A (en) | 2017-09-25 | 2017-09-25 | A kind of preparation method of pure fermented honey moderate wine |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109182005A (en) * | 2018-10-24 | 2019-01-11 | 留坝县佳仕森中药综合开发有限公司 | A kind of production method of American Ginseng fruit wine |
| CN110791405A (en) * | 2019-11-21 | 2020-02-14 | 四川轻化工大学 | Oak barrel white spirit clarification method and clarification device, and oak barrel white spirit production method and production system |
| CN110885730A (en) * | 2019-12-10 | 2020-03-17 | 宁夏红枸杞产业有限公司 | Production method of Chinese wolfberry fruit wine |
| CN116218626A (en) * | 2023-03-09 | 2023-06-06 | 上海信悉智能技术有限公司 | Small-molecular low-deuterium white spirit and preparation process thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109182005A (en) * | 2018-10-24 | 2019-01-11 | 留坝县佳仕森中药综合开发有限公司 | A kind of production method of American Ginseng fruit wine |
| CN110791405A (en) * | 2019-11-21 | 2020-02-14 | 四川轻化工大学 | Oak barrel white spirit clarification method and clarification device, and oak barrel white spirit production method and production system |
| CN110885730A (en) * | 2019-12-10 | 2020-03-17 | 宁夏红枸杞产业有限公司 | Production method of Chinese wolfberry fruit wine |
| CN116218626A (en) * | 2023-03-09 | 2023-06-06 | 上海信悉智能技术有限公司 | Small-molecular low-deuterium white spirit and preparation process thereof |
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Application publication date: 20180123 |