CN107619108A - Anaerobic grain sludge cultural method and culture apparatus - Google Patents

Anaerobic grain sludge cultural method and culture apparatus Download PDF

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Publication number
CN107619108A
CN107619108A CN201710857206.XA CN201710857206A CN107619108A CN 107619108 A CN107619108 A CN 107619108A CN 201710857206 A CN201710857206 A CN 201710857206A CN 107619108 A CN107619108 A CN 107619108A
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China
Prior art keywords
sludge
anaerobic grain
culture apparatus
grain sludge
anaerobic
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Pending
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CN201710857206.XA
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Chinese (zh)
Inventor
吴鹏
印雯
陈亚
沈耀良
徐乐中
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Suzhou University of Science and Technology
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Suzhou University of Science and Technology
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Priority to CN201710857206.XA priority Critical patent/CN107619108A/en
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Abstract

The present invention relates to field of Environment Protection, more particularly to a kind of anaerobic grain sludge cultural method and culture apparatus.Anaerobic grain sludge culture apparatus, including body, it is arranged on intrinsic multiple artificial sludge's beds, chemicals dosing plant for from the day addition nutrient solution to the body, for keeping the thermostat of constant temperature and the control device being arranged on body in the body, blast pipe and mud discharging mouth are additionally provided with the body.The present invention can improve the culture stability of anaerobic grain sludge using culture apparatus, while also have the advantages that cultivation cycle is short, and culture efficiency is high.

Description

Anaerobic grain sludge cultural method and culture apparatus
Technical field
The present invention relates to field of Environment Protection, more particularly to a kind of anaerobic grain sludge cultural method and culture apparatus.
Background technology
Anaerobic Biotechnology is widely used in food, chemical industry at present, and wherein Anaerobic Microbiological Treatment Technology is that have The best-of-breed technology of machine pollution control, it is especially more obvious to the treatment effect of high concentrated organic wastewater.Waste water fermentation handles skill Granule sludge activity has considerable influence to processing waste water effect in art, while granule sludge is evolving, granule sludge quantity It is on the increase, particle diameter constantly increases and tends to be uniform.It is influenced by factors in the culture excessively of anaerobic grain sludge at present, Often result in that the granule sludge performance to be formed is unstable, and impact resistance is poor, it is bad to adapt to external environment changing capability, cultivates simultaneously Complete anaerobic grain sludge and also need to secondary domestication, substantially increase time cost and production cost.
The content of the invention
In view of the foregoing, the present invention be in order to solve the deficiencies in the prior art and provide one kind can improve anaerobic grain dirt The culture stability of mud, cultivation cycle is short, the anaerobic grain sludge cultural method and culture apparatus of culture efficiency height etc..
To reach above-mentioned purpose, the technical solution adopted for the present invention to solve the technical problems is:
A kind of anaerobic grain sludge cultural method, it comprises the following steps:
A. floc sludge is filled in culture apparatus, nutrient solution is added in anaerobic grain sludge culture apparatus, it is described Nutrient solution includes organic wastewater and microelement substance;
B. the initial COD concentration of organic wastewater is 3000-5000mg/L, by the organic waste in anaerobic grain sludge culture apparatus Water pH value is controlled between 6.5-7.5, and temperature control is at 25-45 DEG C, the body of floc sludge and anaerobic grain sludge culture apparatus Product is than being 1:16-1:25;
C. anaerobic grain sludge culture apparatus sample tap COD value is determined, when COD clearances reach 80%-90%, from detesting Oxygen granule sludge culture apparatus bottom intakes, and impacts sludge in anaerobic grain sludge culture apparatus, makes sludge dirty in anaerobic grain Contact and assemble thereon with sludge bed in mud culture apparatus;
D. such as occurs sludge bulking suspension during the course of the reaction, suspended sludge discharge will be expanded by opening the first valve;When detesting Oxygen granularity accounts for the 70%-80% of sludge sum in 2-7mm sludge, the second valve on mud discharging mouth is opened, by dirt Mud particle is discharged.
Preferably, between 35-45 DEG C, pH value controls in 6.8-7.2 temperature control in the reaction whole process.
Preferably, the initial COD concentration of organic wastewater in the nutrient solution is 3000mg/L, C:N:P=210:5.5:1 Ratio matched, micro urmaterie includes iron, nickel and manganese.
Preferably, the step b is before start first by the constant temperature of the heated at constant temperature of anaerobic grain sludge culture apparatus Device is heated to 25-45 DEG C.
Preferably, granule sludge stage of ripeness hydraulic detention time is 7 hours in the step c.
Preferably, the volume ratio of the floc sludge and anaerobic grain sludge culture apparatus is 1:19.
The anaerobic grain sludge culture apparatus of the present invention, including body, are arranged on intrinsic multiple artificial sludges Bed, for the chemicals dosing plant of the day addition nutrient solution into the body, for keeping the thermostat of constant temperature in the body And the control device on body is arranged on, it is additionally provided with blast pipe and mud discharging mouth on the body.
Preferably, the control device is electrically connected with being arranged on intrinsic detector, and the detector includes PH Detector, temperature detector, level switch and potential value detector.
Preferably, the chemicals dosing plant includes dosing tank, liquid level gauge is provided with the dosing tank, for detecting liquid Liquid level.
Preferably, artificial sludge's bed includes the first fixed mount, the second fixed mount and support tube, and described first Fixed mount and the second fixed mount are fixedly connected with body, and the support tube is arranged between the first fixed mount and the second fixed mount, The support tube is provided with equally distributed carbon fibre tow.
It can be seen from the above technical scheme that the culture that the present invention can improve anaerobic grain sludge using culture apparatus is steady It is qualitative, while also there is the advantages that cultivation cycle is short, and culture efficiency is high;It may be such that the particle to be formed is dirty by artificial sludge's bed Mud stable performance, granule sludge impact resistance is good, and adaptation external environment changing capability is strong, and granularity is big, mud bed The coefficient of expansion is high;Simultaneously anaerobic grain sludge transformation after can come into operation immediately, reduce secondary domestication time and into This, realizes the automated production of anaerobic grain sludge culture.
Brief description of the drawings
Fig. 1 is a kind of anaerobic grain sludge culture apparatus structural representation of the present invention.
Description of reference numerals:1- bodies, 2- dosing tanks, 3- water inlets, 4- measuring pumps, 5- blast pipes, 6- control devices, 7- Sludge import, the fixed mounts of 8- first, the valves of 9- first, 10- support tubes, 11- carbon fibre tows, 12- thermostats, 13- second Fixed mount, 14- mud discharging mouths.
Embodiment
With reference to specific embodiment, present disclosure is described in further detail:
Refering to Fig. 1, anaerobic grain sludge culture apparatus of the invention, including body 1, it is arranged on more in the body 1 Individual artificial Sludge Bed layer, the more preferably described body 1 of the present invention is interior to be provided with 1,2 artificial Sludge Bed layers, for described The chemicals dosing plant of day addition nutrient solution in body 1, for keeping the thermostat 12 of constant temperature in the body 1 and being arranged on body Control device 6 on 1, is additionally provided with sludge import 7, blast pipe 5 and mud discharging mouth 14 on the body 1, on the mud discharging mouth 14 Provided with the second valve, the pipeline between the chemicals dosing plant and body 1 is provided with measuring pump 4, the measuring pump 4 and chemicals dosing plant Between pipeline be provided with the 3rd valve, described body side surface is provided with the first valve 9.
The control device 6 and the detector that is arranged in body 1 are electrically connected with, the detector include PH detector, Temperature detector, level switch and potential value detector.
The chemicals dosing plant includes dosing tank 2 and water inlet 3, and the dosing tank 2 is provided with liquid level gauge, for detecting liquid Liquid level, the dosing tank 2 is built with the nutritious liquid configured.
Artificial sludge's bed includes the first fixed mount 8, the second fixed mount 13 and support tube 10, and described first fixes The fixed mount 13 of frame 8 and second is fixedly connected with body 1, and the support tube 10 is arranged on the first fixed mount 8 and the second fixed mount 13 Between, the support tube 10 is provided with equally distributed carbon fibre tow 11.
Embodiment 1
Shown in Fig. 1, a kind of anaerobic grain sludge cultural method, it comprises the following steps:
A. floc sludge is filled in culture apparatus, nutrient solution is added in anaerobic grain sludge culture apparatus, it is described Nutrient solution includes organic wastewater and microelement substance;
B. the initial COD concentration of organic wastewater is 3000mg/L, by the organic wastewater PH in anaerobic grain sludge culture apparatus Value control is between 7, and for temperature control at 32 DEG C, the volume ratio of floc sludge and anaerobic grain sludge culture apparatus is 1:21;
C. anaerobic grain sludge culture apparatus sample tap COD value is determined, when COD clearances reach 82%, from anaerobism The bottom of device water inlet of grain culturing sludge, impacts sludge in anaerobic grain sludge culture apparatus, sludge is trained in anaerobic grain sludge Support and contact and assemble thereon with sludge bed in device;
D. such as occurs sludge bulking suspension during the course of the reaction, opening the first valve 9 will expansion suspended sludge discharge;When detesting Oxygen granularity accounts for the 75% of sludge sum in 2-7mm sludge, the second valve on mud discharging mouth 14 is opened, by sludge Grain discharge.
Between 32 DEG C, pH value controls 7 temperature control in the reaction whole process.
The initial COD concentration of organic wastewater in the nutrient solution is 3000mg/L, C:N:P=210:5.5:1 ratio is entered Row proportioning, micro urmaterie include iron, nickel and manganese.
The step b before start first heats the thermostat 12 of the heated at constant temperature of anaerobic grain sludge culture apparatus To 32 DEG C.
Granule sludge stage of ripeness hydraulic detention time is 7 hours in the step c.
Embodiment 2
Shown in Fig. 1, a kind of anaerobic grain sludge cultural method, it comprises the following steps:
A. floc sludge is filled in culture apparatus, nutrient solution is added in anaerobic grain sludge culture apparatus, it is described Nutrient solution includes organic wastewater and microelement substance;
B. the initial COD concentration of organic wastewater is 3500mg/L, by the organic wastewater pH in anaerobic grain sludge culture apparatus Value control is between 7.1, and for temperature control at 35 DEG C, the volume ratio of floc sludge and anaerobic grain sludge culture apparatus is 1:19;
C. anaerobic grain sludge culture apparatus sample tap COD value is determined, when COD clearances reach 87%, from anaerobism The bottom of device water inlet of grain culturing sludge, impacts sludge in anaerobic grain sludge culture apparatus, sludge is trained in anaerobic grain sludge Support and contact and assemble thereon with sludge bed in device;
D. such as occurs sludge bulking suspension during the course of the reaction, opening the first valve 9 will expansion suspended sludge discharge;When detesting Oxygen granularity accounts for the 74% of sludge sum in 2-7mm sludge, the second valve on mud discharging mouth 14 is opened, by sludge Grain discharge.
Between 35 DEG C, pH value controls 7.1 temperature control in the reaction whole process.
The initial COD concentration of organic wastewater in the nutrient solution is 3500mg/L, C:N:P=210:5.5:1 ratio is entered Row proportioning, micro urmaterie include iron, nickel and manganese.
The step b before start first heats the thermostat 12 of the heated at constant temperature of anaerobic grain sludge culture apparatus To 35 DEG C.
Granule sludge stage of ripeness hydraulic detention time is 7 hours in the step c.
Embodiment 3
Shown in Fig. 1, a kind of anaerobic grain sludge cultural method, it comprises the following steps:
A. floc sludge is filled in culture apparatus, nutrient solution is added in anaerobic grain sludge culture apparatus, it is described Nutrient solution includes organic wastewater and microelement substance;
B. the initial COD concentration of organic wastewater is 3800mg/L, by the organic wastewater PH in anaerobic grain sludge culture apparatus Value control is between 6.9, and for temperature control at 38 DEG C, the volume ratio of floc sludge and anaerobic grain sludge culture apparatus is 1:20;
C. anaerobic grain sludge culture apparatus sample tap COD value is determined, when COD clearances reach 86%, from anaerobism The bottom of device water inlet of grain culturing sludge, impacts sludge in anaerobic grain sludge culture apparatus, sludge is trained in anaerobic grain sludge Support and contact and assemble thereon with sludge bed in device;
D. such as occurs sludge bulking suspension during the course of the reaction, opening the first valve 9 will expansion suspended sludge discharge;When detesting Oxygen granularity accounts for the 76% of sludge sum in 2-7mm sludge, the second valve on mud discharging mouth 14 is opened, by sludge Grain discharge.
Between 38 DEG C, pH value controls 6.9 temperature control in the reaction whole process.
The initial COD concentration of organic wastewater in the nutrient solution is 3800mg/L, C:N:P=210:5.5:1 ratio is entered Row proportioning, micro urmaterie include iron, nickel and manganese.
The step b before start first heats the thermostat 12 of the heated at constant temperature of anaerobic grain sludge culture apparatus To 38 DEG C.
Granule sludge stage of ripeness hydraulic detention time is 7 hours in the step c.
Above-described embodiment only technical concept to illustrate the invention and, feature, its object is to allow be familiar with technique Personage can understand present disclosure and be carried out, and it is not intended to limit the scope of the present invention, all according to this hair The equivalent change or modification that bright Spirit Essence is made, it should all cover within the scope of the present invention.

Claims (10)

1. a kind of anaerobic grain sludge cultural method, it is characterised in that it comprises the following steps:
A. floc sludge is filled in culture apparatus, nutrient solution, the nutrition is added in anaerobic grain sludge culture apparatus Liquid includes organic wastewater and microelement substance;
B. the initial COD concentration of organic wastewater is 3000-5000mg/L, by the organic wastewater pH in anaerobic grain sludge culture apparatus Value control is between 6.5-7.5, and temperature control is at 25-45 DEG C, the volume ratio of floc sludge and anaerobic grain sludge culture apparatus For 1:16-1:25;
C. anaerobic grain sludge culture apparatus sample tap COD value is determined, when COD clearances reach 80%-90%, from anaerobism The bottom of device water inlet of grain culturing sludge, impacts sludge in anaerobic grain sludge culture apparatus, sludge is trained in anaerobic grain sludge Support and contact and assemble thereon with sludge bed in device;
D. such as occurs sludge bulking suspension during the course of the reaction, suspended sludge discharge will be expanded by opening the first valve;When anaerobism Grain sludge particle diameter accounts for the 70%-80% of sludge sum in 2-7mm sludge, the second valve on mud discharging mouth is opened, by sludge Grain discharge.
2. anaerobic grain sludge cultural method according to claim 1, it is characterised in that the reaction whole process medium temperature Between 35-45 DEG C, pH value is controlled in 6.8-7.2 for degree control.
3. anaerobic grain sludge cultural method according to claim 1, it is characterised in that the organic waste in the nutrient solution The initial COD concentration of water is 3000mg/L, C:N:P=210:5.5:1 ratio is matched, micro urmaterie include iron, nickel and Manganese.
4. anaerobic grain sludge cultural method according to claim 1, it is characterised in that the step b is first before start The thermostat of the heated at constant temperature of anaerobic grain sludge culture apparatus is first heated to 25-45 DEG C.
5. anaerobic grain sludge cultural method according to claim 1, it is characterised in that granule sludge in the step c Stage of ripeness hydraulic detention time is 7 hours.
6. anaerobic grain sludge cultural method according to claim 1, it is characterised in that the floc sludge and anaerobism The volume ratio of grain culturing sludge device is 1:19.
7. a kind of anaerobic grain sludge culture apparatus, it is characterised in that including body, be arranged on described intrinsic multiple artificial Sludge bed, for the chemicals dosing plant of the day addition nutrient solution into the body, for keeping the constant temperature of constant temperature in the body Device and the control device being arranged on body, blast pipe and mud discharging mouth are additionally provided with the body.
8. anaerobic grain sludge culture apparatus according to claim 7, it is characterised in that the control device is with being arranged on Intrinsic detector is electrically connected with, and the detector includes PH detector, temperature detector, level switch and potential value inspection Survey device.
9. anaerobic grain sludge culture apparatus according to claim 7, it is characterised in that the chemicals dosing plant includes dosing Case, liquid level gauge is provided with the dosing tank, for detecting the liquid level of liquid.
10. anaerobic grain sludge culture apparatus according to claim 7, it is characterised in that artificial sludge's bed bag The first fixed mount, the second fixed mount and support tube are included, first fixed mount and the second fixed mount are fixedly connected with body, institute State support tube to be arranged between the first fixed mount and the second fixed mount, the support tube is provided with equally distributed carbon fiber wire Beam.
CN201710857206.XA 2017-09-20 2017-09-20 Anaerobic grain sludge cultural method and culture apparatus Pending CN107619108A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110550737A (en) * 2019-08-21 2019-12-10 万创青绿(北京)环境科技有限公司 Granular sludge preparation method and reactor

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101767873A (en) * 2010-01-14 2010-07-07 四川大学 Method for quickly culturing anaerobic hydrogen-producing granular sludge
CN103043792A (en) * 2013-01-19 2013-04-17 东北电力大学 Method and device for cultivating anaerobic granular sludge
CN106396096A (en) * 2016-11-04 2017-02-15 苏州依斯倍环保装备科技有限公司 Method and device for culturing anaerobic granular sludge

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101767873A (en) * 2010-01-14 2010-07-07 四川大学 Method for quickly culturing anaerobic hydrogen-producing granular sludge
CN103043792A (en) * 2013-01-19 2013-04-17 东北电力大学 Method and device for cultivating anaerobic granular sludge
CN106396096A (en) * 2016-11-04 2017-02-15 苏州依斯倍环保装备科技有限公司 Method and device for culturing anaerobic granular sludge

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110550737A (en) * 2019-08-21 2019-12-10 万创青绿(北京)环境科技有限公司 Granular sludge preparation method and reactor
CN110550737B (en) * 2019-08-21 2022-04-29 万创青绿(北京)环境科技有限公司 Granular sludge preparation method and reactor

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