CN107619064A - A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit - Google Patents
A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit Download PDFInfo
- Publication number
- CN107619064A CN107619064A CN201710835791.3A CN201710835791A CN107619064A CN 107619064 A CN107619064 A CN 107619064A CN 201710835791 A CN201710835791 A CN 201710835791A CN 107619064 A CN107619064 A CN 107619064A
- Authority
- CN
- China
- Prior art keywords
- zinc sulfate
- experiment frame
- rotating shaft
- metal sheet
- lithium cell
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The present invention relates to a kind of extracting sulfuric acid zinc crystal unit, more particularly to a kind of waste lithium cell zinc metal sheet to prepare zinc sulfate crystal unit.The technical problem to be solved in the present invention is to provide a kind of waste lithium cell zinc metal sheet to prepare zinc sulfate crystal unit.In order to solve the above-mentioned technical problem, the invention provides such a waste lithium cell zinc metal sheet to prepare zinc sulfate crystal unit, includes experiment frame, electronic scale, beaker, alcolhol burner, adsorbent equipment etc.；Experiment frame inner bottom part is provided with electronic scale and adsorbent equipment, and adsorbent equipment is arranged on the right side of electronic scale, and beaker is provided with electronic scale, alcolhol burner is provided with adsorbent equipment.Invention achieves uniform evaporation solution of zinc sulfate, it can speed up the precipitation of zinc sulfate crystal, peculiar smell can be adsorbed, reduce peculiar smell disperse polluted space environment in air, slewing operation is more stablized, zinc sulfate fluid spills in evaporation are prevented, are easy to produce purer zinc sulfate crystal, the high effect of recovery utilization rate.
Description
Technical field
The present invention relates to a kind of extracting sulfuric acid zinc crystal unit, more particularly to a kind of waste lithium cell zinc metal sheet to prepare zinc sulfate
Crystal unit.
Background technology
Lithium battery refers to the battery containing lithium in electrochemical system, including one-shot battery and lithium metal, lithium ion secondary electricity
Pond.Old and useless battery, which recycles, refers to used battery to be reused by recovery, domestic most commonly used industrial battery
For lead accumulator, lead accounts for battery totle drilling cost more than 50%, mainly takes pyrogenic process, hydrometallurgical processes and Solid phase electrolysis reduction
Technology.Shell is plastics, can regenerate, realize non-secondary pollution substantially.
Zinc sulfate is the primary raw material for manufacturing lithopone and zinc salt, it is also possible to makees the guarantor of printing and dyeing mordant, timber and leather
Deposit agent, and the important auxiliary material of production viscose rayon and vinylon fiber.In addition, answered electroplating and also having in electrolytic industry
With, can be also used for manufacture cable.
The use range of lithium battery is wide in daily life, but not strong, people couple are realized in recovery of the people to waste lithium cell
The purposes of the recycling of waste lithium cell is not clear and definite enough, and the common zinc sulfate for preparing all is to use new zinc metal sheet, and cost is higher
And resource needs to be wasted, the shortcomings that being not easy to promote the use of, therefore a kind of environmentally friendly and easy to spread waste and old lithium used of research and development is needed badly
Battery zinc metal sheet prepares zinc sulfate crystal unit.
The content of the invention
（1）Technical problems to be solved
The present invention is not strong in order to overcome recovery consciousness of the people to waste lithium cell, recycling of the people to waste lithium cell
Purposes is not clear and definite enough, and the common zinc sulfate for preparing all is to use new zinc metal sheet, and cost is higher and resource needs to be wasted, and is not easy to promote
The shortcomings that use, the technical problem to be solved in the present invention is to provide a kind of waste lithium cell zinc metal sheet to prepare zinc sulfate crystal unit.
（2）Technical scheme
In order to solve the above-mentioned technical problem, the invention provides such a waste lithium cell zinc metal sheet to prepare zinc sulfate crystal dress
Put, include experiment frame, electronic scale, beaker, alcolhol burner, adsorbent equipment, retainer ring, evaporating dish, glass bar, geometrical clamp, rotation
Equipment, drawstring, rubber guide pin bushing and draw ring, experiment frame inner bottom part are provided with electronic scale and adsorbent equipment, and adsorbent equipment is arranged on electricity
The right side that son claims, beaker being provided with electronic scale, being provided with alcolhol burner in adsorbent equipment, fixation is provided with right side in experiment frame
Ring, evaporating dish is provided with retainer ring, experiment frame inner top is provided with slewing, geometrical clamp is connected with slewing, Gu
Glass bar is accompanied in clamp, glass bar is located at the surface of evaporating dish, and experiment frame left side wall top is embedded with rubber guide pin bushing, and rotation is set
Standby right side is connected with drawstring, and drawstring passes through rubber guide pin bushing, and the end of drawstring is connected with draw ring.
Preferably, adsorbent equipment includes irony casing, chamber door, activated carbon bag, hinge and magnet strip, on the right side of electronic scale
Experiment frame inner bottom part is provided with irony casing, and looping pit is provided with the top of irony casing, is provided with out on the front side wall of irony casing
Mouthful, chamber door is connected with by hinge on the right side wall of opening, activated carbon bag is provided with the inside of chamber door, the right-hand member of chamber door is connected with
Magnet strip.
Preferably, slewing includes rack, first rotating shaft, sliding block, slide rail, gear and first bearing seat, experiment frame
Inner top is provided with slide rail, and sliding block is provided with slide rail, is connected with rack on front side of sliding block, the experiment frame inner top on front side of slide rail
First bearing seat is provided with, first rotating shaft is installed in first bearing seat, gear is provided with first rotating shaft, gear is arranged on tooth
The front side of bar, rack and pinion engagement, geometrical clamp are connected to the lower end of first rotating shaft, and the left end of drawstring is connected to the right side of rack
End.
Preferably, directive wheel, reel, second bearing seat, the second rotating shaft and handle are also included, right side wall in experiment frame
Top is provided with directive wheel, and middle and lower part is embedded with second bearing seat in experiment frame right side wall, and second turn is provided with second bearing seat
Axle, the left end of the second rotating shaft are connected with reel, and the right-hand member of the second rotating shaft is connected with handle, and drawstring is wound on coiling around directive wheel
On wheel.
Preferably, also include stereoplasm tube, air bag, framework, ball and cam, cam is provided with the second rotating shaft, it is convex
Wheel is arranged on the left side of reel, and the distal end of cam is connected with ball, and right side wall bottom is provided with framework, framework in experiment frame
Perforation is provided with the middle part of bottom, air bag is provided with framework, the bottom of air bag is connected with stereoplasm tube, and stereoplasm tube passes through perforation and iron
The right side wall of matter casing is connected.
Preferably, also include ring buckle, semi-circular fixture block and protective cover, ring buckle is connected with first rotating shaft, annular
Button is arranged between geometrical clamp and gear, and symmetrical expression is combined with semi-circular fixture block, the semi-ring of the left and right sides at left and right sides of ring buckle
Symmetrical expression is connected with protective cover on shape fixture block.
Preferably, screen pack, oscillating rod and rubber sleeve are also included, the middle and upper part rotary type connection of right side wall in experiment frame
There is oscillating rod, the right hand external of oscillating rod sets rubber sleeve, and the left end of oscillating rod is connected with screen pack, and screen pack is arranged on steaming
Send out the surface of ware.
Operation principle：When needing to prepare zinc sulfate, people can be by reclaiming the zinc metal sheet in waste lithium cell, by zinc metal sheet
It is placed into beaker, a certain amount of zinc metal sheet is weighed according to electronic scale, people add in right amount according to the quality of zinc metal sheet into beaker
Dilute sulfuric acid, zinc metal sheet stand after being reacted with dilute sulfuric acid, solution of zinc sulfate are transferred in evaporating dish, and people light alcolhol burner, absorption
Device is to peculiar smell adsorption caused by alcolhol burner, while people will grip glass bar by geometrical clamp, and people are pullled by draw ring
Rope, drawstring drive slewing mild action, so as to which slewing drives micro- turn of glass bar, so as in glass bar stirring evaporating dish
Solution of zinc sulfate, be thus easy to uniformly evaporate solution of zinc sulfate, can speed up the precipitation of zinc sulfate crystal, thus reach useless
The recycling in old lithium pond, turns waste into wealth.
Because adsorbent equipment includes irony casing, chamber door, activated carbon bag, hinge and magnet strip, the reality on the right side of electronic scale
Test frame inner bottom part and be provided with irony casing, looping pit is provided with the top of irony casing, opening is provided with the front side wall of irony casing,
Chamber door is connected with by hinge on the right side wall of opening, activated carbon bag is provided with the inside of chamber door, the right-hand member of chamber door is connected with magnetic
Iron bar, so when alcolhol burner is lighted, the burning of alcolhol burner has peculiar smell unavoidably, and the activated carbon being thus equipped with activated carbon bag can
Play a part of adsorbing peculiar smell, reduce peculiar smell disperse polluted space environment in air, while people are easy to open chamber door, just
In the placement and taking-up of alcolhol burner, activated carbon bag is conveniently replaceable.
Because slewing includes rack, first rotating shaft, sliding block, slide rail, gear and first bearing seat, pushed up in experiment frame
Portion is provided with slide rail, and sliding block is provided with slide rail, is connected with rack on front side of sliding block, and the experiment frame inner top on front side of slide rail is set
There is first bearing seat, first rotating shaft is installed in first bearing seat, gear is provided with first rotating shaft, gear is arranged on rack
Front side, rack and pinion engagement, geometrical clamp are connected to the lower end of first rotating shaft, and the left end of drawstring is connected to the right-hand member of rack, institute
To pull draw ring to be moved left and right by drawstring band carry-over bar as people, rack drives gear positive and negative alternate rotates, so as to glass bar
Zinc sulfate in evaporating dish is stirred, so as to make its evaporation efficiency higher.
Because also including directive wheel, reel, second bearing seat, the second rotating shaft and handle, in experiment frame on right side wall
Portion is provided with directive wheel, and middle and lower part is embedded with second bearing seat in experiment frame right side wall, and the second rotating shaft is provided with second bearing seat,
The left end of second rotating shaft is connected with reel, and the right-hand member of the second rotating shaft is connected with handle, and drawstring is wound on reel around directive wheel
On, so when needing to start slewing, the positive and negative shake handle of people drives the second axis of rotation, and the second rotating shaft drives coiling
Take turns positive and negative alternate to rotate, reel folding and unfolding drawstring, drawstring drives slewing operation, thus enables that slewing operation more
Add stabilization, prevent the dynamics of pullling of people to be difficult to control and make slewing operation is unstable to cause glass bar stirring to fly drop
Splash.
Because also including stereoplasm tube, air bag, framework, ball and cam, cam is provided with the second rotating shaft, cam is set
Put and be connected with ball in the left side of reel, the distal end of cam, right side wall bottom is provided with framework, framework bottom in experiment frame
Middle part be provided with perforation, be provided with air bag in framework, the bottom of air bag is connected with stereoplasm tube, and stereoplasm tube is through perforation and irony case
The right side wall of body is connected, so originally air bag is compressed, when people's positive and negative alternate shake handle drives the second axis of rotation,
Second rotating shaft band moving cam positive and negative alternate rotates, and so as to constantly press pressuring gasbag, and then is dredged by stereoplasm tube into irony casing
Blowing air, ensure adsorbent equipment inner air flow, the combustion flame of alcolhol burner is smooth uniformly, thereby speeds up the precipitation of crystal, rubber
Glueballs can preferably protect air bag, extend the service life of air bag.
Because also including ring buckle, semi-circular fixture block and protective cover, ring buckle is connected with first rotating shaft, ring buckle is set
Put between geometrical clamp and gear, symmetrical expression is combined with semi-circular fixture block, the semi-circular card of the left and right sides at left and right sides of ring buckle
Symmetrical expression is connected with protective cover on block, so after zinc sulfate is placed into evaporating dish, people will pass through semi-circular fixture block and ring
Protective cover is fixed on the periphery of evaporating dish by the cooperation of shape button, can so prevent zinc sulfate fluid spills in evaporation, ensure
The safety of experiment.
Because also including screen pack, oscillating rod and rubber sleeve, the middle and upper part rotary type of right side wall is connected with experiment frame
Oscillating rod, the right hand external of oscillating rod set rubber sleeve, and the left end of oscillating rod is connected with screen pack, and screen pack is arranged on evaporation
The surface of ware, so after the zinc metal sheet in waste lithium cell and sulfuric acid solution obtain zinc sulfate after completion of the reaction, people will burn
The zinc sulfate produced in cup is so easy to produce purer zinc sulfate by entering back into evaporating dish after filter screen filtration
Crystal, while thus screen pack can be removed, be easy to following by holding the right side of oscillating rod by oscillating rod swing by people
The progress of experimental procedure.
（3）Beneficial effect
Invention achieves uniform evaporation solution of zinc sulfate, the precipitation of zinc sulfate crystal is can speed up, peculiar smell can be adsorbed, is reduced
Peculiar smell disperse polluted space environment in air, slewing operation are more stablized, and prevent zinc sulfate drop in evaporation
Splash, be easy to produce purer zinc sulfate crystal, the high effect of recovery utilization rate.
Brief description of the drawings
Fig. 1 is the main structure diagram of the present invention.
Fig. 2 is the main structure diagram of adsorbent equipment of the present invention.
Fig. 3 is the main structure diagram of slewing of the present invention.
Fig. 4 is the first part main structure diagram of the present invention.
Fig. 5 is second of part main structure diagram of the present invention.
Fig. 6 is the third part main structure diagram of the present invention.
Fig. 7 is the 4th kind of part main structure diagram of the present invention.
Mark in accompanying drawing for：1- experiment frames, 2- electronic scales, 3- beakers, 4- alcolhol burners, 5- adsorbent equipments, 51- irony casees
Body, 52- openings, 53- looping pits, 54- chamber doors, 55- activated carbon bags, 56- hinges, 57- magnet strips, 6- retainer rings, 7- evaporating dishes,
8- glass bars, 9- geometrical clamps, 10- slewings, 101- racks, 102- first rotating shafts, 103- sliding blocks, 104- slide rails, 105- teeth
Wheel, 106- first bearing seats, 11- drawstrings, 12- rubber guide pin bushings, 13- draw rings, 14- directive wheels, 15- reels, 16- second bearings
Seat, the rotating shafts of 17- second, 18- handles, 19- stereoplasm tubes, 20- perforation, 21- air bags, 22- frameworks, 23- balls, 24- cams,
25- ring buckles, 26- semi-circular fixture blocks, 27- protective covers, 28- screen packs, 29- oscillating rods, 30- rubber sleeves.
Embodiment
The present invention is further illustrated with reference to the accompanying drawings and examples.
Embodiment 1
A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit, as shown in figs. 1-7, includes experiment frame 1, electronic scale 2, burns
Cup 3, alcolhol burner 4, adsorbent equipment 5, retainer ring 6, evaporating dish 7, glass bar 8, geometrical clamp 9, slewing 10, drawstring 11, rubber
Guide pin bushing 12 and draw ring 13, the inner bottom part of experiment frame 1 are provided with electronic scale 2 and adsorbent equipment 5, and adsorbent equipment 5 is arranged on electronic scale 2
Right side, beaker 3 being provided with electronic scale 2, being provided with alcolhol burner 4 in adsorbent equipment 5, fixation is provided with right side in experiment frame 1
Ring 6, evaporating dish 7 is provided with retainer ring 6, the inner top of experiment frame 1 is provided with slewing 10, is connected with slewing 10 solid
Clamp 9, glass bar 8 is accompanied on geometrical clamp 9, glass bar 8 is located at the surface of evaporating dish 7, and the left side wall top of experiment frame 1 is embedded with rubber
Glue guide pin bushing 12, the right side of slewing 10 are connected with drawstring 11, and drawstring 11 passes through rubber guide pin bushing 12, and the end of drawstring 11 is connected with
Draw ring 13.
Embodiment 2
A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit, as shown in figs. 1-7, includes experiment frame 1, electronic scale 2, burns
Cup 3, alcolhol burner 4, adsorbent equipment 5, retainer ring 6, evaporating dish 7, glass bar 8, geometrical clamp 9, slewing 10, drawstring 11, rubber
Guide pin bushing 12 and draw ring 13, the inner bottom part of experiment frame 1 are provided with electronic scale 2 and adsorbent equipment 5, and adsorbent equipment 5 is arranged on electronic scale 2
Right side, beaker 3 being provided with electronic scale 2, being provided with alcolhol burner 4 in adsorbent equipment 5, fixation is provided with right side in experiment frame 1
Ring 6, evaporating dish 7 is provided with retainer ring 6, the inner top of experiment frame 1 is provided with slewing 10, is connected with slewing 10 solid
Clamp 9, glass bar 8 is accompanied on geometrical clamp 9, glass bar 8 is located at the surface of evaporating dish 7, and the left side wall top of experiment frame 1 is embedded with rubber
Glue guide pin bushing 12, the right side of slewing 10 are connected with drawstring 11, and drawstring 11 passes through rubber guide pin bushing 12, and the end of drawstring 11 is connected with
Draw ring 13.
Adsorbent equipment 5 includes irony casing 51, chamber door 54, activated carbon bag 55, hinge 56 and magnet strip 57, electronic scale 2
The inner bottom part of experiment frame 1 on right side is provided with irony casing 51, and the top of irony casing 51 is provided with looping pit 53, irony casing 51
Opening 52 is provided with front side wall, chamber door 54 is connected with by hinge 56 on 52 right side wall that is open, the inner side of chamber door 54 is provided with
Activated carbon bag 55, the right-hand member of chamber door 54 are connected with magnet strip 57.
Embodiment 3
A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit, as shown in figs. 1-7, includes experiment frame 1, electronic scale 2, burns
Cup 3, alcolhol burner 4, adsorbent equipment 5, retainer ring 6, evaporating dish 7, glass bar 8, geometrical clamp 9, slewing 10, drawstring 11, rubber
Guide pin bushing 12 and draw ring 13, the inner bottom part of experiment frame 1 are provided with electronic scale 2 and adsorbent equipment 5, and adsorbent equipment 5 is arranged on electronic scale 2
Right side, beaker 3 being provided with electronic scale 2, being provided with alcolhol burner 4 in adsorbent equipment 5, fixation is provided with right side in experiment frame 1
Ring 6, evaporating dish 7 is provided with retainer ring 6, the inner top of experiment frame 1 is provided with slewing 10, is connected with slewing 10 solid
Clamp 9, glass bar 8 is accompanied on geometrical clamp 9, glass bar 8 is located at the surface of evaporating dish 7, and the left side wall top of experiment frame 1 is embedded with rubber
Glue guide pin bushing 12, the right side of slewing 10 are connected with drawstring 11, and drawstring 11 passes through rubber guide pin bushing 12, and the end of drawstring 11 is connected with
Draw ring 13.
Adsorbent equipment 5 includes irony casing 51, chamber door 54, activated carbon bag 55, hinge 56 and magnet strip 57, electronic scale 2
The inner bottom part of experiment frame 1 on right side is provided with irony casing 51, and the top of irony casing 51 is provided with looping pit 53, irony casing 51
Opening 52 is provided with front side wall, chamber door 54 is connected with by hinge 56 on 52 right side wall that is open, the inner side of chamber door 54 is provided with
Activated carbon bag 55, the right-hand member of chamber door 54 are connected with magnet strip 57.
Slewing 10 includes rack 101, first rotating shaft 102, sliding block 103, slide rail 104, gear 105 and clutch shaft bearing
Seat 106, the inner top of experiment frame 1 is provided with slide rail 104, and sliding block 103 is provided with slide rail 104, and the front side connection of sliding block 103 is with teeth
Bar 101, the inner top of experiment frame 1 of the front side of slide rail 104 are provided with first bearing seat 106, first are provided with first bearing seat 106
Rotating shaft 102, gear 105 is provided with first rotating shaft 102, gear 105 is arranged on the front side of rack 101, rack 101 and gear
105 engagements, geometrical clamp 9 are connected to the lower end of first rotating shaft 102, and the left end of drawstring 11 is connected to the right-hand member of rack 101.
Embodiment 4
A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit, as shown in figs. 1-7, includes experiment frame 1, electronic scale 2, burns
Cup 3, alcolhol burner 4, adsorbent equipment 5, retainer ring 6, evaporating dish 7, glass bar 8, geometrical clamp 9, slewing 10, drawstring 11, rubber
Guide pin bushing 12 and draw ring 13, the inner bottom part of experiment frame 1 are provided with electronic scale 2 and adsorbent equipment 5, and adsorbent equipment 5 is arranged on electronic scale 2
Right side, beaker 3 being provided with electronic scale 2, being provided with alcolhol burner 4 in adsorbent equipment 5, fixation is provided with right side in experiment frame 1
Ring 6, evaporating dish 7 is provided with retainer ring 6, the inner top of experiment frame 1 is provided with slewing 10, is connected with slewing 10 solid
Clamp 9, glass bar 8 is accompanied on geometrical clamp 9, glass bar 8 is located at the surface of evaporating dish 7, and the left side wall top of experiment frame 1 is embedded with rubber
Glue guide pin bushing 12, the right side of slewing 10 are connected with drawstring 11, and drawstring 11 passes through rubber guide pin bushing 12, and the end of drawstring 11 is connected with
Draw ring 13.
Adsorbent equipment 5 includes irony casing 51, chamber door 54, activated carbon bag 55, hinge 56 and magnet strip 57, electronic scale 2
The inner bottom part of experiment frame 1 on right side is provided with irony casing 51, and the top of irony casing 51 is provided with looping pit 53, irony casing 51
Opening 52 is provided with front side wall, chamber door 54 is connected with by hinge 56 on 52 right side wall that is open, the inner side of chamber door 54 is provided with
Activated carbon bag 55, the right-hand member of chamber door 54 are connected with magnet strip 57.
Slewing 10 includes rack 101, first rotating shaft 102, sliding block 103, slide rail 104, gear 105 and clutch shaft bearing
Seat 106, the inner top of experiment frame 1 is provided with slide rail 104, and sliding block 103 is provided with slide rail 104, and the front side connection of sliding block 103 is with teeth
Bar 101, the inner top of experiment frame 1 of the front side of slide rail 104 are provided with first bearing seat 106, first are provided with first bearing seat 106
Rotating shaft 102, gear 105 is provided with first rotating shaft 102, gear 105 is arranged on the front side of rack 101, rack 101 and gear
105 engagements, geometrical clamp 9 are connected to the lower end of first rotating shaft 102, and the left end of drawstring 11 is connected to the right-hand member of rack 101.
Also include directive wheel 14, reel 15, second bearing seat 16, the second rotating shaft 17 and handle 18, it is right in experiment frame 1
Side wall upper part is provided with directive wheel 14, and middle and lower part is embedded with second bearing seat 16 in the right side wall of experiment frame 1, pacifies in second bearing seat 16
Equipped with the second rotating shaft 17, the left end of the second rotating shaft 17 is connected with reel 15, and the right-hand member of the second rotating shaft 17 is connected with handle 18, draws
Rope 11 is wound on reel 15 around directive wheel 14.
Also include stereoplasm tube 19, air bag 21, framework 22, ball 23 and cam 24, be provided with the second rotating shaft 17 convex
Wheel 24, cam 24 are arranged on the left side of reel 15, and the distal end of cam 24 is connected with ball 23, in experiment frame 1 under right side wall
Portion is provided with framework 22, and perforation 20 is provided with the middle part of the bottom of framework 22, and air bag 21 is provided with framework 22, and the bottom of air bag 21 connects
Stereoplasm tube 19 is connected to, stereoplasm tube 19 is connected through perforation 20 with the right side wall of irony casing 51.
Also include ring buckle 25, semi-circular fixture block 26 and protective cover 27, ring buckle 25 be connected with first rotating shaft 102,
Ring buckle 25 is arranged between geometrical clamp 9 and gear 105, and the left and right sides symmetrical expression of ring buckle 25 is combined with semi-circular fixture block 26,
Symmetrical expression is connected with protective cover 27 on the semi-circular fixture block 26 of the left and right sides.
Also include screen pack 28, oscillating rod 29 and rubber sleeve 30, the middle and upper part rotary type connection of right side wall in experiment frame 1
There is oscillating rod 29, the right hand external of oscillating rod 29 sets rubber sleeve 30, and the left end of oscillating rod 29 is connected with screen pack 28, filters
Net 28 is arranged on the surface of evaporating dish 7.
Operation principle：When needing to prepare zinc sulfate, people can be by reclaiming the zinc metal sheet in waste lithium cell, by zinc metal sheet
It is placed into beaker 3, a certain amount of zinc metal sheet is weighed according to electronic scale 2, people add in right amount according to the quality of zinc metal sheet into beaker 3
Dilute sulfuric acid, zinc metal sheet and dilute sulfuric acid stand after reacting, solution of zinc sulfate be transferred in evaporating dish 7, and people light alcolhol burner 4,
Adsorbent equipment 5 is to peculiar smell adsorption caused by alcolhol burner 4, while people will grip glass bar 8 by geometrical clamp 9, and people pass through drawing
Ring 13 pulls drawstring 11, and drawstring 11 drives the mild action of slewing 10, so as to which slewing 10 drives micro- turn of glass bar 8, from
And glass bar 8 stirs the solution of zinc sulfate in evaporating dish 7, thus it is easy to uniformly evaporate solution of zinc sulfate, can speed up sulfuric acid
The precipitation of zinc crystal, thus reach the recycling of waste lithium cell, turn waste into wealth.
Because adsorbent equipment 5 includes irony casing 51, chamber door 54, activated carbon bag 55, hinge 56 and magnet strip 57, electronics
The inner bottom part of experiment frame 1 on 2 right sides is claimed to be provided with irony casing 51, the top of irony casing 51 is provided with looping pit 53, irony casing
Opening 52 is provided with 51 front side wall, chamber door 54 is connected with by hinge 56 on 52 right side wall that is open, the inner side of chamber door 54 is set
Activated carbon bag 55 is equipped with, the right-hand member of chamber door 54 is connected with magnet strip 57, so when alcolhol burner 4 is lighted, the burning of alcolhol burner 4 is difficult
Exempt from have peculiar smell, the activated carbon being thus equipped with activated carbon bag 55 can play a part of adsorbing peculiar smell, reduce peculiar smell disperse in sky
Polluted space environment in gas, while people are easy to open chamber door 54, are easy to the placement and taking-up of alcolhol burner 4, are conveniently replaceable work
Property charcoal bag 55.
Because slewing 10 includes rack 101, first rotating shaft 102, sliding block 103, slide rail 104, gear 105 and first
Bearing block 106, the inner top of experiment frame 1 are provided with slide rail 104, and sliding block 103, the front side connection of sliding block 103 are provided with slide rail 104
There is rack 101, the inner top of experiment frame 1 of the front side of slide rail 104 is provided with first bearing seat 106, is provided with first bearing seat 106
First rotating shaft 102, gear 105 is provided with first rotating shaft 102, gear 105 is arranged on the front side of rack 101, rack 101 and tooth
The engagement of wheel 105, geometrical clamp 9 are connected to the lower end of first rotating shaft 102, and the left end of drawstring 11 is connected to the right-hand member of rack 101, so
When people pull draw ring 13 to be moved left and right by drawstring 11 with carry-over bar 101, rack 101 rotates with the positive and negative alternate of moving gear 105,
So as to which glass bar 8 stirs to the zinc sulfate in evaporating dish 7, so as to make its evaporation efficiency higher.
Because also include directive wheel 14, reel 15, second bearing seat 16, the second rotating shaft 17 and handle 18, experiment frame 1
Interior right side wall top is provided with directive wheel 14, and middle and lower part is embedded with second bearing seat 16, second bearing seat 16 in the right side wall of experiment frame 1
On the second rotating shaft 17 is installed, the left end of the second rotating shaft 17 is connected with reel 15, and the right-hand member of the second rotating shaft 17 is connected with handle
18, drawstring 11 is wound on reel 15 around directive wheel 14, so when needing to start slewing 10, the positive and negative shake handle of people
Hand 18 drives the second rotating shaft 17 to rotate, and the second rotating shaft 17 drives the positive and negative alternate of reel 15 to rotate, the folding and unfolding drawstring 11 of reel 15,
Drawstring 11 drives slewing 10 to run, and thus enables that slewing 10 is run more stable, prevents people's to pull power
Degree is unmanageable and running slewing 10 unstable causes the stirring of glass bar 8 to make fluid spills.
Because also including stereoplasm tube 19, air bag 21, framework 22, ball 23 and cam 24, set in the second rotating shaft 17
There is cam 24, cam 24 is arranged on the left side of reel 15, and the distal end of cam 24 is connected with ball 23, the interior right side of experiment frame 1
Wall bottom is provided with framework 22, and perforation 20 is provided with the middle part of the bottom of framework 22, and air bag 21, the bottom of air bag 21 are provided with framework 22
Portion is connected with stereoplasm tube 19, and stereoplasm tube 19 is connected through perforation 20 with the right side wall of irony casing 51, so originally air bag 21
Compressed, when people's positive and negative alternate shake handle 18 drives the second rotating shaft 17 to rotate, the second rotating shaft 17 is positive and negative with moving cam 24
Alternate rotation, so as to constantly press pressuring gasbag 21, and then air is dredged into irony casing 51 by stereoplasm tube 19, ensure absorption
The inner air flow of device 5, the combustion flame of alcolhol burner 4 is smooth uniformly, thereby speeds up the precipitation of crystal, ball 23 can be more preferable
Protection air bag 21, extend air bag 21 service life.
Because also including ring buckle 25, semi-circular fixture block 26 and protective cover 27, ring buckle is connected with first rotating shaft 102
25, ring buckle 25 is arranged between geometrical clamp 9 and gear 105, and the left and right sides symmetrical expression of ring buckle 25 is combined with semi-circular fixture block
26, symmetrical expression is connected with protective cover 27 on the semi-circular fixture block 26 of the left and right sides, so when zinc sulfate is placed into evaporating dish 7
Afterwards, protective cover 27 will be fixed on the periphery of evaporating dish 7, such energy by people by the cooperation of semi-circular fixture block 26 and ring buckle 25
Zinc sulfate fluid spills in evaporation are enough prevented, ensure the safety of experiment.
Because also including screen pack 28, oscillating rod 29 and rubber sleeve 30, the middle and upper part rotary type of right side wall in experiment frame 1
Oscillating rod 29 is connected with, the right hand external of oscillating rod 29 sets rubber sleeve 30, and the left end of oscillating rod 29 is connected with screen pack 28,
Screen pack 28 is arranged on the surface of evaporating dish 7, so when the zinc metal sheet in waste lithium cell and sulfuric acid solution obtain after completion of the reaction
To after zinc sulfate, people are entered back into evaporating dish 7 after the zinc sulfate produced in beaker 3 is filtered by screen pack 28, so
It is easy to produce purer zinc sulfate crystal, while people will can put by holding the right side of oscillating rod 29 before and after oscillating rod 29
It is dynamic, thus screen pack 28 is removed, is easy to the progress of following experimental procedure.
Embodiment described above only expresses the preferred embodiment of the present invention, and its description is more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, some deformations can also be made, improves and substitutes, these belong to this hair
Bright protection domain.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (7)
1. a kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit, it is characterised in that includes experiment frame（1）, electronic scale
（2）, beaker（3）, alcolhol burner（4）, adsorbent equipment（5）, retainer ring（6）, evaporating dish（7）, glass bar（8）, geometrical clamp（9）, rotation
Turn equipment（10）, drawstring（11）, rubber guide pin bushing（12）And draw ring（13）, experiment frame（1）Inner bottom part is provided with electronic scale（2）And suction
Adsorption device（5）, adsorbent equipment（5）It is arranged on electronic scale（2）Right side, electronic scale（2）On be provided with beaker（3）, adsorbent equipment
（5）Inside it is provided with alcolhol burner（4）, experiment frame（1）Retainer ring is provided with interior right side（6）, retainer ring（6）On be provided with evaporating dish
（7）, experiment frame（1）Inner top is provided with slewing（10）, slewing（10）On be connected with geometrical clamp（9）, geometrical clamp（9）
On accompany glass bar（8）, glass bar（8）Positioned at evaporating dish（7）Surface, experiment frame（1）Led embedded with rubber on left side wall top
Set（12）, slewing（10）Right side be connected with drawstring（11）, drawstring（11）Through rubber guide pin bushing（12）, drawstring（11）End
End is connected with draw ring（13）.
2. a kind of waste lithium cell zinc metal sheet according to claim 1 prepares zinc sulfate crystal unit, it is characterised in that absorption
Device（5）Include irony casing（51）, chamber door（54）, activated carbon bag（55）, hinge（56）And magnet strip（57）, electronic scale
（2）The experiment frame on right side（1）Inner bottom part is provided with irony casing（51）, irony casing（51）Top be provided with looping pit（53）,
Irony casing（51）Front side wall on be provided with opening（52）, opening（52）Right side wall on pass through hinge（56）It is connected with chamber door
（54）, chamber door（54）Inner side be provided with activated carbon bag（55）, chamber door（54）Right-hand member be connected with magnet strip（57）.
3. a kind of waste lithium cell zinc metal sheet according to claim 2 prepares zinc sulfate crystal unit, it is characterised in that rotation
Equipment（10）Include rack（101）, first rotating shaft（102）, sliding block（103）, slide rail（104）, gear（105）And clutch shaft bearing
Seat（106）, experiment frame（1）Inner top is provided with slide rail（104）, slide rail（104）On be provided with sliding block（103）, sliding block（103）'s
Front side is connected with rack（101）, slide rail（104）The experiment frame of front side（1）Inner top is provided with first bearing seat（106）, first
Bearing block（106）On first rotating shaft is installed（102）, first rotating shaft（102）On be provided with gear（105）, gear（105）Set
In rack（101）Front side, rack（101）With gear（105）Engagement, geometrical clamp（9）It is connected to first rotating shaft（102）Under
End, drawstring（11）Left end be connected to rack（101）Right-hand member.
4. a kind of waste lithium cell zinc metal sheet according to claim 3 prepares zinc sulfate crystal unit, it is characterised in that also wraps
Directive wheel is included（14）, reel（15）, second bearing seat（16）, the second rotating shaft（17）And handle（18）, experiment frame（1）The interior right side
Side wall upper part is provided with directive wheel（14）, experiment frame（1）Middle and lower part is embedded with second bearing seat in right side wall（16）, second bearing seat
（16）On the second rotating shaft is installed（17）, the second rotating shaft（17）Left end be connected with reel（15）, the second rotating shaft（17）The right side
End is connected with handle（18）, drawstring（11）Around directive wheel（14）It is wound on reel（15）On.
5. a kind of waste lithium cell zinc metal sheet according to claim 4 prepares zinc sulfate crystal unit, it is characterised in that also wraps
Stereoplasm tube is included（19）, air bag（21）, framework（22）, ball（23）And cam（24）, the second rotating shaft（17）On be provided with it is convex
Wheel（24）, cam（24）It is arranged on reel（15）Left side, cam（24）Distal end be connected with ball（23）, experiment frame
（1）Interior right side wall bottom is provided with framework（22）, framework（22）Perforation is provided with the middle part of bottom（20）, framework（22）Inside it is provided with
Air bag（21）, air bag（21）Bottom be connected with stereoplasm tube（19）, stereoplasm tube（19）Through perforation（20）With irony casing（51）
Right side wall be connected.
6. a kind of waste lithium cell zinc metal sheet according to claim 5 prepares zinc sulfate crystal unit, it is characterised in that also wraps
Ring buckle is included（25）, semi-circular fixture block（26）And protective cover（27）, first rotating shaft（102）On be connected with ring buckle（25）, ring
Shape button（25）It is arranged on geometrical clamp（9）And gear（105）Between, ring buckle（25）Left and right sides symmetrical expression is combined with semi-circular card
Block（26）, the semi-circular fixture block of the left and right sides（26）Upper symmetrical expression is connected with protective cover（27）.
7. a kind of waste lithium cell zinc metal sheet according to claim 6 prepares zinc sulfate crystal unit, it is characterised in that also wraps
Screen pack is included（28）, oscillating rod（29）And rubber sleeve（30）, experiment frame（1）The middle and upper part rotary type of interior right side wall is connected with pendulum
Lever（29）, oscillating rod（29）Right hand external set rubber sleeve（30）, oscillating rod（29）Left end be connected with screen pack
（28）, screen pack（28）It is arranged on evaporating dish（7）Surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710835791.3A CN107619064B (en) | 2017-09-16 | 2017-09-16 | A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710835791.3A CN107619064B (en) | 2017-09-16 | 2017-09-16 | A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107619064A true CN107619064A (en) | 2018-01-23 |
| CN107619064B CN107619064B (en) | 2019-07-12 |
Family
ID=61089783
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710835791.3A Active CN107619064B (en) | 2017-09-16 | 2017-09-16 | A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107619064B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786943A (en) * | 2018-07-27 | 2018-11-13 | 陈志阳 | A kind of chemical experiment evaporating dish with automatic stirring function |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101673829A (en) * | 2009-09-25 | 2010-03-17 | 华南师范大学 | Recovery processing method of waste zinc-manganese battery |
| US20110123419A1 (en) * | 2009-11-20 | 2011-05-26 | Korea Institute Of Geoscience And Mineral | Method for preparing manganese sulfate and zinc sulfate from waste batteries containing manganese and zinc |
| CN102352443A (en) * | 2011-10-31 | 2012-02-15 | 太仓市南仓金属材料有限公司 | Method for producing zinc sulfate heptahydrate, crude tin and crude lead by using tin smelting dust |
| CN202220085U (en) * | 2011-09-16 | 2012-05-16 | 安徽亚兰德新能源材料有限公司 | Preparation device for battery grade high-purity zinc sulfate |
| CN103794833A (en) * | 2014-01-23 | 2014-05-14 | 湖南邦普循环科技有限公司 | Method for recovering valuable metal from waste nickel-zinc battery |
| CN106987714A (en) * | 2017-04-10 | 2017-07-28 | 赣州科源甬致科技有限公司 | One kind extracts the nickel sulfate energy-saving extraction equipment of vibration from old and useless battery |
-
2017
- 2017-09-16 CN CN201710835791.3A patent/CN107619064B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101673829A (en) * | 2009-09-25 | 2010-03-17 | 华南师范大学 | Recovery processing method of waste zinc-manganese battery |
| US20110123419A1 (en) * | 2009-11-20 | 2011-05-26 | Korea Institute Of Geoscience And Mineral | Method for preparing manganese sulfate and zinc sulfate from waste batteries containing manganese and zinc |
| CN202220085U (en) * | 2011-09-16 | 2012-05-16 | 安徽亚兰德新能源材料有限公司 | Preparation device for battery grade high-purity zinc sulfate |
| CN102352443A (en) * | 2011-10-31 | 2012-02-15 | 太仓市南仓金属材料有限公司 | Method for producing zinc sulfate heptahydrate, crude tin and crude lead by using tin smelting dust |
| CN103794833A (en) * | 2014-01-23 | 2014-05-14 | 湖南邦普循环科技有限公司 | Method for recovering valuable metal from waste nickel-zinc battery |
| CN106987714A (en) * | 2017-04-10 | 2017-07-28 | 赣州科源甬致科技有限公司 | One kind extracts the nickel sulfate energy-saving extraction equipment of vibration from old and useless battery |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786943A (en) * | 2018-07-27 | 2018-11-13 | 陈志阳 | A kind of chemical experiment evaporating dish with automatic stirring function |
| CN108786943B (en) * | 2018-07-27 | 2020-11-17 | 维沃泰克仪器(扬州)有限公司 | Evaporating dish for chemistry experiments with automatic stirring function |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107619064B (en) | 2019-07-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Furuhashi et al. | Optimum conditions of pH, temperature and preculture for biosorption of europium by microalgae Acutodesmus acuminatus | |
| CN110316898A (en) | A kind of method of absorbing synergic Magnetizing Separation Technology processing waste water from dyestuff | |
| CN107619064A (en) | A kind of waste lithium cell zinc metal sheet prepares zinc sulfate crystal unit | |
| CN102560114A (en) | Method for bioleaching and extracting valuable metal ions in waste batteries | |
| CN107151665A (en) | The method that immobilization endophyte biological adsorption agent handles lead waste water | |
| CN107067920A (en) | A kind of chemical filtering experiment demonstration equipment | |
| CN109103530A (en) | A kind of method and carbon material preparing Fe2O3 doping carbon material using discarded wadding body | |
| CN109761289B (en) | Gas storage type wet recovery process for lithium cobaltate battery | |
| CN106824090B (en) | Preparation method and application of novel magnetic metal organic framework composite material | |
| CN109894092A (en) | A kind of method of biogas residue base adsorbent and Adsorption heavy metals in industrial wastewater | |
| CN102989413A (en) | Preparation method of modified attapulgite for printing and dyeing waste water decoloration | |
| CN209567370U (en) | A kind of desulfurization temporary storage apparatus | |
| CN106299525A (en) | A kind of method separating and recovering waste lithium iron phosphate battery electrolyte | |
| CN116328467A (en) | Waste gas treatment device with high combustion efficiency for steel mill and treatment method thereof | |
| CN105932350A (en) | Recycling method for waste lead-acid storage battery lead plaster desulphurization byproduct | |
| CN205613165U (en) | Filter collector | |
| CN107931313A (en) | A kind of garbage sorting device | |
| CN107930594A (en) | A kind of modification egg film paper and preparation method and application for lithium battery recycling | |
| CN204310923U (en) | A kind of sludge treatment equipment | |
| CN113394474A (en) | Waste storage battery electrolyte recovery processing method | |
| CN208526330U (en) | Membrane for water treatment element protection liquid displacement apparatus | |
| CN207608531U (en) | Marsh gas purifying equipment | |
| CN111112315A (en) | Metal in soil filters collecting device | |
| CN207286803U (en) | Cylinder is collected by filtration in a kind of precipitated crystal | |
| CN214781198U (en) | Comprehensive sewage purification treatment equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20190419 Address after: 230000 B-1512, west of Ganquan Road, Shushan District, Hefei, Anhui. Applicant after: Anhui Eagle Dragon Industrial Design Co., Ltd. Address before: 330038 Red Valley Road 1568, Red Valley, Nanchang, Jiangxi, China. The Red Valley triumph commercial office complex and commercial six 301-10 room (third floors) Applicant before: Nanchang Yi Hong Technology Co., Ltd. |
|
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20190614 Address after: 225600 Guo Ji industrial concentration area, Gaoyou City, Yangzhou City, Jiangsu Province Applicant after: Yangzhou Hai Dedeng industry Co., Ltd Address before: 230000 B-1512, west of Ganquan Road, Shushan District, Hefei, Anhui. Applicant before: Anhui Eagle Dragon Industrial Design Co., Ltd. |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |