CN107605124A - The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor - Google Patents

The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor Download PDF

Info

Publication number
CN107605124A
CN107605124A CN201710836524.8A CN201710836524A CN107605124A CN 107605124 A CN107605124 A CN 107605124A CN 201710836524 A CN201710836524 A CN 201710836524A CN 107605124 A CN107605124 A CN 107605124A
Authority
CN
China
Prior art keywords
wood
wood moulding
carbon element
element crystal
electric heating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710836524.8A
Other languages
Chinese (zh)
Inventor
刘明利
李春风
刘彦龙
刘春龙
于双
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beihua University
Original Assignee
Beihua University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beihua University filed Critical Beihua University
Priority to CN201710836524.8A priority Critical patent/CN107605124A/en
Publication of CN107605124A publication Critical patent/CN107605124A/en
Pending legal-status Critical Current

Links

Landscapes

  • Resistance Heating (AREA)
  • Central Heating Systems (AREA)
  • Floor Finish (AREA)

Abstract

The present invention is a kind of preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor, is characterized in:Including:The steps such as the making of preparation, the making of heating layer, the making of carbon element crystal Electric radiant Heating Film, the preparation of wood moulding powder, the making of wood moulding upper insulation plate, the making of wood moulding lower insulation plate, anoxic high-temperature process toothed oak outer surface of wood plate and carbon element crystal electric heating wood moulding core plate solid wooden compound floor that carbon is starched.Electric heating floor prepared by the method improves the water resistance and insulating properties of electric heating floor, and can solve long-term electric heating low-temperature radiant heat transfer as dash board using anoxic high-temperature process toothed oak outer surface of wood plate and the problems such as cracking defect easily occur, plate face is 5min the time required to being raised to 25 DEG C, meets national house and town and country construction portion issue JGJ142-2012《Radiant heating cooling technical regulation》Professional standard, the average floor surface temperature of the frequent stacking area of personnel is set as to 25 ~ 27 DEG C of regulation.

Description

The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor
Technical field
The present invention relates to electric heating floor technical field, and in particular to a kind of carbon element crystal electric heating wood moulding core plate solid wood is compoundly The preparation method of plate.
Background technology
Conventional electric heating product has Electric radiant Heating Film, heating cable, boilers heated electrically and carbon-crystal electric hot plate etc. both at home and abroad.In recent years Occurs a kind of new indoor heating mode --- electric heating floor again.It has programming rate is fast, comfortableness is good, mat formation flexibly, The advantages that saving space;Compared with traditional heating system, flooring radiation heating has uniform indoor temperature, feel temperature height, heat Comfortableness is good, is easy to Region control, saves floor space, safeguards the advantages that easy to use, achievable household metering, is that one kind subtracts Few building energy consumption, the preferable heating system for improving thermal comfort;So as to improve former electric heating floor have the thermal efficiency it is low, peace Dress maintenance is inconvenient, easily comes unglued, the defects of dash board easily ftractures, service life is short.Herein for all excessively orthogonal examination of these problems Proved recipe method, study Electric radiant Heating Film is disposable compound with solid wooden floor board progress.So as to improve the performance of electric heating floor.
Carbon element crystal heating plate has uniformity, insulating properties, the ageing resistance of product and wear-resisting during heating Energy aspect is all better than the carbon heating product effect of same type.The appearance of carbon crystal plate is the great tribute to plane exothermic material field Offer.It is ultra-thin, durable, the thermal efficiency is high, heating is rapid, self limiting temperature function and flexible power, temperature control technology make carbon crystal plate Once emerging, that is, the concern of underground heat industry is obtained.
China's building thermal performance design is divided into five areas, i.e. severe cold area, cold district, hot-summer and cold-winter area, summer by weather The hot winter warms up regional, gentle area.Wherein, severe cold area and cold district winter are needed to configure heating facility by regulation;The energy disappears Consume huge, environmental pollution is serious;Hot-summer and cold-winter area needs heating.But compared with severe cold area and cold district, these are non- The architectural feature of heating districts, climatic characteristic, heating feature are all different from northern area, and their Heating Season is short, Building Heat is born Lotus is smaller, the fluctuation of morning and evening indoor/outdoor temperature-difference is larger etc..These features cause electric heating floor to be developed rapidly.
The present invention carries out self-control exothermic material, and the progress innovated using far-infrared electric ink, chemical fiber non-woven fabric It is compound with wood plastic composite progress, greatly improve the water resistance and insulating properties of electric heating floor.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of scientific and reasonable, strong applicability, and effect is good, it is possible to increase electricity The water resistance and insulating properties of heating floor, and can solve long-term electric heating low-temperature radiant heat transfer easily occur being cracked defect etc. and ask The preparation method of the carbon element crystal electric heating wood moulding core plate solid wooden compound floor of topic.
Its technical problem is solved the technical scheme adopted is that a kind of carbon element crystal electric heating wood moulding core plate solid wooden compound floor Preparation method, it is characterized in that:It comprises the following steps:
1)The preparation of carbon slurry:In parts by mass, by 20 ~ 100 parts of carbon element crystal conductive carbon powder and 40 ~ 200 parts of melamine Resin mixes, and stir obtained carbon slurry;
2)The making of heating layer:By step 1)Uniformly coated on flexible chemical fiber non-woven fabric, it is applied obtained carbon slurry It is 60 ~ 150 DEG C to measure as 80 ~ 250g/ ㎡, drying, drying temperature, and after drying time is 5 ~ 30min, heating layer is made;
3)The making of carbon element crystal Electric radiant Heating Film:By step 2)Obtained heating layer carries out normal temperature densification;Finger gauge control product is thick Degree, pressure is 0.3 ~ 0.5MPa, and carbon element crystal Electric radiant Heating Film is made;
4)The preparation of wood moulding powder:By 250 ~ 380 μm of wood powders and particle diameter 450-830um linear low density polyethylene (LLDPE) powders according to matter Amount is than being 3:2 preparations obtain wood moulding powder;
5)The making of wood moulding upper insulation plate:The wood moulding powder for measuring product materials half quality is laid on mould, it is necessary to Ensure uniformly and tile;
6)The making of wood moulding lower insulation plate:With step 5), it is placed in carbon element crystal Electric radiant Heating Film;
7)Anoxic high-temperature process toothed oak outer surface of wood plate:Using anoxic high-temperature process kiln, treatment temperature is 160 ~ 200 DEG C, and the time is that 2-4 is small When, humidity 100%;
8)The making of carbon element crystal electric heating wood moulding core plate solid wooden compound floor:By step 3)Obtained carbon element crystal Electric radiant Heating Film and wood Modeling upper insulation plate, wood moulding lower insulation plate, anoxic high-temperature process toothed oak outer surface of wood plate are disposably compounded to form carbon element crystal electric heating wood moulding core Plate solid wooden compound floor.Finally, carbon crystal heating layer and wood plastic composite are subjected to disposable assembly hot pressing of mating formation, wherein, heat Pressure mode is suppressed for hot press, and temperature is 160 ~ 180 DEG C;Time is 20-40 minutes, and pressure is 2.5 ~ 3.0MPa, hot-forming Afterwards, it is 2.5 ~ 3.1MPa with cold press, pressure, suppresses at room temperature, water channel cooling and shaping to 50 DEG C of depannings, obtains carbon element crystal electricity Hot wood moulding core plate solid wooden compound floor element plate, then cover with paint, lacquer, colour wash, etc. to obtain finished product through conventional sanding excessively, sanction lock tenon, UV.
The preparation method of a kind of carbon element crystal electric heating wood moulding core plate solid wooden compound floor of the present invention, by carbon element crystal electric heating Ink is well mixed with melmac, and on the surface of flexible chemical fiber non-woven fabric, coating contains cellulose crystal electric heating oil Black far infrared coating, carbon crystalline substance is finally disposably compounded to form with lower insulation plate, anoxic high-temperature process toothed oak outer surface of wood plate etc. in wood moulding Body electric heating wood moulding core plate solid wooden compound floor.Its advantage is:Can effectively raise electric heating floor water resistance and Insulating properties;Solve long-term electric heating low-temperature radiant heat transfer the problems such as cracking defect easily occur and realize first during floor heating Aldehyde discharges problem.
Brief description of the drawings
Fig. 1 is carbon element crystal electric heating wood moulding core plate solid wooden compound floor illustraton of model of the embodiment of the present invention;
Fig. 2 show the carbon element crystal electric heating wood moulding core plate solid wooden compound floor of different carbon dust coated weights obtained by the embodiment of the present invention Heating curve figure.
Embodiment
Invention is further illustrated with reference to embodiment.
Embodiment 1:A kind of preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor of embodiment 1, including The step of have:
1)The preparation of carbon slurry:The carbon element crystal conductive carbon powder for weighing 30g mixes with 100g melmac, and uses electric mixing The machine of mixing stirs obtained carbon slurry;
2)The making of heating layer:By step 1)Obtained carbon slurry is uniformly coated in 800x120mm flexibility chemical fiber non-woven fabrics On, its coating amount is 180g/ ㎡, is dried with electric heating constant-temperature blowing drying box, and drying temperature is 100 DEG C, drying time After 10min, heating layer is made;
3)The making of carbon element crystal Electric radiant Heating Film:By step 2)Obtained heating layer carries out normal temperature densification;Finger gauge control product is thick Degree, pressure is 0.3 ~ 0.5MPa, and carbon element crystal Electric radiant Heating Film is made;
4)The preparation of wood moulding powder:By 250 ~ 380 μm of wood powders and particle diameter 450-830um linear low density polyethylene (LLDPE) powders according to matter Amount is than being 3:2 preparations obtain wood moulding powder;
5)The making of wood moulding upper insulation plate:The wood moulding powder for measuring product materials half quality is laid on mould, it is necessary to Ensure uniformly and tile;
6)The making of wood moulding lower insulation plate:With step 5), it is placed in carbon element crystal Electric radiant Heating Film;
7)Anoxic high-temperature process toothed oak outer surface of wood plate:Using anoxic high-temperature process kiln, treatment temperature is 160 ~ 200 DEG C, and the time is that 2-4 is small When, humidity 100%;
8)The making of carbon element crystal electric heating wood moulding core plate solid wooden compound floor:By step 3)Obtained carbon element crystal Electric radiant Heating Film and wood Modeling upper insulation plate, wood moulding lower insulation plate, anoxic high-temperature process toothed oak outer surface of wood plate are disposably compounded to form carbon element crystal electric heating wood moulding core Plate solid wooden compound floor.Finally, carbon crystal heating layer and wood plastic composite are subjected to disposable assembly hot pressing of mating formation, wherein, heat Pressure mode is suppressed for hot press, and temperature is 160 ~ 180 DEG C;Time is 20-40 minutes, and pressure is 2.5 ~ 3.0MPa, hot-forming Afterwards, it is 2.5 ~ 3.1MPa with cold press, pressure, suppresses at room temperature, water channel cooling and shaping to 50 DEG C of depannings, obtains carbon element crystal electricity Hot wood moulding core plate solid wooden compound floor element plate, then cover with paint, lacquer, colour wash, etc. to obtain finished product through conventional sanding excessively, sanction lock tenon, UV.
4 pieces of electric heating floor test specimens series connection obtained by embodiment 1 and transformer, universal meter, temperature control equipment, temperature Monitoring device is attached, and the probe of temperature sensor then is bonded in into test specimen surface with heat-conducting glue, to measure When obtain accurate data, finally the test specimen of connection is put into ready incubator, after switching on power, used on demand Transformer carries out pressure regulation and carries out heating test, records Temperature numerical at regular intervals, draws the relation of time and plate face temperature Figure, it be 17min that temperature as shown in Figure 2, which is raised to the time required to 25 DEG C, meet national house and town and country construction portion issue JGJ142- 2012《Radiant heating cooling technical regulation》Professional standard, the average floor surface temperature of the frequent stacking area of personnel is set as 25 ~ 27 DEG C of regulation.
Embodiment 2, a kind of preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor of embodiment 2, including The step of it is same as Example 1, except that
1)The preparation of carbon slurry:The carbon element crystal conductive carbon powder for weighing 60g mixes with 150g melmac, and uses electric mixing The machine of mixing stirs obtained carbon slurry;
2)The making of heating layer:By step 1)Obtained carbon slurry is uniformly coated in 800x120mm flexibility chemical fiber non-woven fabrics On, its coating amount is 200g/ ㎡, is dried with electric heating constant-temperature blowing drying box, and drying temperature is 125 DEG C, drying time After 20min, heating layer is made.
Plate face temperature is 5min the time required to being raised to 25 DEG C, meets house and town and country construction portion issue JGJ142-2012 《Radiant heating cooling technical regulation》Professional standard, the average floor surface temperature of the frequent stacking area of personnel is set as 25 ~ 27 DEG C regulation.It about shortens 2/3rds the time required to reaching target temperature compared with Example 1, it is contemplated that human body sensory Comfortableness, it is slightly short the time required to reaching target temperature, so embodiment 1 is more suitable for floor heating.
Embodiment 3, a kind of preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor of embodiment 3, including The step of it is same as Example 1, except that
1)The preparation of carbon slurry:The carbon element crystal conductive carbon powder for weighing 100g mixes with 200g melmac, and with electronic Mixer stirs obtained carbon slurry;
2)The making of heating layer:By step 1)Obtained carbon slurry is uniformly coated in 800x120mm flexibility chemical fiber non-woven fabrics On, its coating amount is 250g/ ㎡, is dried with electric heating constant-temperature blowing drying box, and drying temperature is 150 DEG C, drying time After 30min, heating layer is made.
It is 3min that test specimen 3, which is raised to the time used in 25 DEG C of target temperature, and it reaches target temperature and taken compared with Example 1 Between about shorten 5/6ths, it is contemplated that the comfortableness of human body sensory, it reaches shorter the time required to target temperature, so implementing Example 1 is more suitable for floor heating.

Claims (1)

1. a kind of preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor, it is characterized in that:It comprises the following steps:
1)The preparation of carbon slurry:In parts by mass, by 20 ~ 100 parts of carbon element crystal conductive carbon powder and 40 ~ 200 parts of melamine Resin mixes, and stir obtained carbon slurry;
2)The making of heating layer:By step 1)Uniformly coated on flexible chemical fiber non-woven fabric, it is applied obtained carbon slurry It is 60 ~ 150 DEG C to measure as 80 ~ 250g/ ㎡, drying, drying temperature, and after drying time is 5 ~ 30min, heating layer is made;
3)The making of carbon element crystal Electric radiant Heating Film:By step 2)Obtained heating layer carries out normal temperature densification;Finger gauge control product is thick Degree, pressure is 0.3 ~ 0.5MPa, and carbon element crystal Electric radiant Heating Film is made;
4)The preparation of wood moulding powder:By 250 ~ 380 μm of wood powders and particle diameter 450-830um linear low density polyethylene (LLDPE) powders according to matter Amount is than being 3:2 preparations obtain wood moulding powder;
5)The making of wood moulding upper insulation plate:The wood moulding powder for measuring product materials half quality is laid on mould, it is necessary to Ensure uniformly and tile;
6)The making of wood moulding lower insulation plate:With step 5), it is placed in carbon element crystal Electric radiant Heating Film;
7)Anoxic high-temperature process toothed oak outer surface of wood plate:Using anoxic high-temperature process kiln, treatment temperature is 160 ~ 200 DEG C, and the time is that 2-4 is small When, humidity 100%;
8)The making of carbon element crystal electric heating wood moulding core plate solid wooden compound floor:By step 3)Obtained carbon element crystal Electric radiant Heating Film and wood Modeling upper insulation plate, wood moulding lower insulation plate, anoxic high-temperature process toothed oak outer surface of wood plate are disposably compounded to form carbon element crystal electric heating wood moulding core Plate solid wooden compound floor;
Finally, carbon crystal heating layer and wood plastic composite are subjected to disposable assembly hot pressing of mating formation, wherein, hot pressing mode is hot pressing Machine is suppressed, and temperature is 160 ~ 180 DEG C;Time is 20-40 minutes, and pressure is 2.5 ~ 3.0MPa, after hot-forming, with cold press, Pressure is 2.5 ~ 3.1MPa, is suppressed at room temperature, water channel cooling and shaping to 50 DEG C of depannings, obtains carbon element crystal electric heating wood moulding core plate reality Wood composite floor element plate, then cover with paint, lacquer, colour wash, etc. to obtain finished product through conventional sanding excessively, sanction lock tenon, UV.
CN201710836524.8A 2017-09-16 2017-09-16 The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor Pending CN107605124A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710836524.8A CN107605124A (en) 2017-09-16 2017-09-16 The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710836524.8A CN107605124A (en) 2017-09-16 2017-09-16 The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor

Publications (1)

Publication Number Publication Date
CN107605124A true CN107605124A (en) 2018-01-19

Family

ID=61060465

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710836524.8A Pending CN107605124A (en) 2017-09-16 2017-09-16 The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor

Country Status (1)

Country Link
CN (1) CN107605124A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108930387A (en) * 2018-08-09 2018-12-04 杭州凡顿新材料科技有限公司 Intelligent heating integrated floor

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07150741A (en) * 1993-12-01 1995-06-13 Misawa Homes Co Ltd Floor structure
CN101600270A (en) * 2009-07-14 2009-12-09 王柏泉 Conductive exothermal material and comprise the floor and the manufacture method of this conductive exothermal material
CN201751485U (en) * 2010-03-26 2011-02-23 戴阿建 Electric heating strengthen floor
CN102644960A (en) * 2012-04-24 2012-08-22 武汉拜尔木业有限公司 Wooden floor supporting direct electric heating and manufacturing and laying methods thereof
CN204609108U (en) * 2015-05-04 2015-09-02 海宁欧派工贸有限公司 A kind of wallboard
CN205955103U (en) * 2016-06-20 2017-02-15 乐山吉象地板制品有限公司 Spontaneous heating floor

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07150741A (en) * 1993-12-01 1995-06-13 Misawa Homes Co Ltd Floor structure
CN101600270A (en) * 2009-07-14 2009-12-09 王柏泉 Conductive exothermal material and comprise the floor and the manufacture method of this conductive exothermal material
CN201751485U (en) * 2010-03-26 2011-02-23 戴阿建 Electric heating strengthen floor
CN102644960A (en) * 2012-04-24 2012-08-22 武汉拜尔木业有限公司 Wooden floor supporting direct electric heating and manufacturing and laying methods thereof
CN204609108U (en) * 2015-05-04 2015-09-02 海宁欧派工贸有限公司 A kind of wallboard
CN205955103U (en) * 2016-06-20 2017-02-15 乐山吉象地板制品有限公司 Spontaneous heating floor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108930387A (en) * 2018-08-09 2018-12-04 杭州凡顿新材料科技有限公司 Intelligent heating integrated floor

Similar Documents

Publication Publication Date Title
CN108192467A (en) A kind of phase-change thermal storage coating and preparation method and application
CN100522880C (en) Method for preparing heat insulation composite material by microwave
CN103644595B (en) Heat consolidated floor
CN110006946A (en) The indoor simulation test macro and method of a kind of bituminous pavement temperature field
CN102587516A (en) Vacuum insulation plate for wall of building and preparation method of vacuum insulation plate
CN105385180A (en) Heat-conducting wood composite material and preparation method thereof
CN105801070A (en) Ochre carbon fiber coating plate
CN107605124A (en) The preparation method of carbon element crystal electric heating wood moulding core plate solid wooden compound floor
CN106278129B (en) A kind of fast vigour wet stock of 3D printing magnesium phosphate cement and preparation method thereof
He et al. Modeling and simulation of heat-mass transfer and its application in wood thermal modification
CN101864053A (en) Modified phenolic resin for bamboo structure material and preparation method thereof
CN106365566A (en) Aerogel composite sandstone plate and preparation method thereof
CN101400192B (en) Moisture proof and warming electric heating board and preparation thereof
CN207794520U (en) A kind of aluminum wood ground heating system
Kirilovs et al. Low density hemp shive particleboards for latent thermal energy storage performance
CN105263199A (en) Flexible carbon crystal electric warming materials and manufacturing method thereof
CN207132412U (en) A kind of floor heating
CN207162710U (en) A kind of New Electrothermal Film floor heating
CN107011752A (en) It is a kind of for waterproof heat-insulating coating of external wall and preparation method thereof
CN110879110A (en) Indoor simulation method for temperature field and cooling durability of thermochromic asphalt pavement
CN105367104B (en) The preparation method of electric heating floor
CN103342931B (en) Wood-based plate edge sealing back cover high reactivity water-based powder is starched
CN201123136Y (en) Combined far-infrared heating plate
CN106082809B (en) Heat-reflecting insulating coating and preparation method thereof
CN110076858A (en) Wooden floor based on carbon paper as heating layer and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180119