CN107604702A - A kind of One Bath Dyeing Process of acid dyes and blend dye - Google Patents

A kind of One Bath Dyeing Process of acid dyes and blend dye Download PDF

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Publication number
CN107604702A
CN107604702A CN201710850852.3A CN201710850852A CN107604702A CN 107604702 A CN107604702 A CN 107604702A CN 201710850852 A CN201710850852 A CN 201710850852A CN 107604702 A CN107604702 A CN 107604702A
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CN
China
Prior art keywords
dye
dye vat
steps
acid dyes
blend
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Pending
Application number
CN201710850852.3A
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Chinese (zh)
Inventor
濮坚锋
王爱义
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Zhejiang Yue New Printing And Dyeing Co Ltd
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Zhejiang Yue New Printing And Dyeing Co Ltd
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Application filed by Zhejiang Yue New Printing And Dyeing Co Ltd filed Critical Zhejiang Yue New Printing And Dyeing Co Ltd
Priority to CN201710850852.3A priority Critical patent/CN107604702A/en
Publication of CN107604702A publication Critical patent/CN107604702A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of acid dyes and the One Bath Dyeing Process of blend dye, it is characterised in that:Comprise the following steps:At normal temperatures, fabric is imported into dye vat, nylon antitack agent is added in dye vat;Acid dyes is added in dye vat;Blend dye is added in dye vat;Glauber salt is added in dye vat;Dyeing is completed in cooling after the bath temperature of dye vat is completed into heating for the first time from normal temperature and heated up for the second time.The present invention is once cooled by heating up twice, and the technique that traditional handicraft needs the dyeing of two steps to complete disposably is completed in same dye vat, has the characteristics of energy consumption is small, environmentally friendly.

Description

A kind of One Bath Dyeing Process of acid dyes and blend dye
Technical field
The invention belongs to fabric printing field, the one-bath dyeing work of more particularly to a kind of acid dyes and blend dye Skill.
Background technology
Traditional N/R fabrics need to dye twice, the first step dyeing for acid dyes dyeing, will acid dye vat water temperature by Normal temperature rises to 98 DEG C and dyed, time 30min;Second step dyeing is blend dyeing, by blending dye vat water temperature by normal temperature liter Dyed to 95 DEG C, time 20min.Traditional dyeing process needs two dye vats, heats up twice, has what is taken time and effort to lack Fall into.
The content of the invention
The invention provides a kind of acid dyes and the One Bath Dyeing Process of blend dye, one step solves to dye twice Technique, it has the characteristics of energy consumption is small, environmentally friendly.
To reach above-mentioned purpose, concrete scheme of the invention is as follows:
A kind of One Bath Dyeing Process of acid dyes and blend dye, comprises the following steps:
The first step, at normal temperatures, fabric is imported into dye vat, nylon antitack agent is added in dye vat;
Second step, after some time, acid dyes is added in dye vat;
3rd step, after some time, blend dye is added in dye vat;
4th step, after some time, glauber salt is added in dye vat;
5th step, acetic acid is added, and the bath temperature of dye vat is heated up and maintained;
6th step, the bath temperature of dye vat is heated up and maintained again;
7th step, the bath temperature of dye vat is cooled, complete dyeing.
Preferably,
The second step concretely comprises the following steps:After 4-6min, acid dyes is added in dye vat.
3rd step concretely comprises the following steps:After 8-12min, blend dye is added in dye vat.
4th step concretely comprises the following steps:After 4-6min, glauber salt is added in dye vat.
5th step concretely comprises the following steps:The bath temperature by dye vat is warming up to 80 ± 5 DEG C from normal temperature, maintains 8- 12min;The programming rate is 1.2 DEG C/min.
6th step concretely comprises the following steps:The bath temperature of dye vat is warming up to 95 ± 5 DEG C from 80 ± 5 DEG C, maintains 24- 36min;The programming rate is 1.2 DEG C/min.
7th step concretely comprises the following steps:, the bath temperature of dye vat is cooled to 70 ± 5 DEG C from 95 ± 5 DEG C;The heating speed Spend for 2 DEG C/min.
The nylon antitack agent addition is 0.8-1.2g/L.
The addition of the glauber salt is 5-15g/L.
The acetic acid is 100% acetic acid, and the acetic acid addition is 0.2-0.4g/L
The present invention is once cooled by heating up twice, and traditional handicraft is disposably completed in same dye vat needs the dyeing of two steps to complete Technique, have energy consumption it is small, it is environmentally friendly the characteristics of.
The present invention is further elaborated below by way of brief description of the drawings and embodiment.
Brief description of the drawings
Fig. 1 is the step schematic diagram of the embodiment of the present invention 1.
Embodiment
Purchasing of raw materials side:
Nylon antitack agent RF is purchased from Clariant Corporation;
Glauber salt is purchased from An Xin Chemical Co., Ltd.s of Shaoxin City.
Definition:
Acid dyes is the water-soluble dye that acidic-group is carried on a class formation, is dyed in acid medium.Acidity dye Material is most of to contain sulfonate sodium, can be dissolved in water, and lovely luster, chromatogram are complete.It is mainly used in the dye such as wool, silk and polyamide fibre Color, it can also be used to leather, paper, ink etc..To the general non-coloring power of cellulose fibre.
Blend dye is also known as composite dye, is formed by two or more dyestuff blendings of different nature, or can be by one kind simultaneously The dyestuff of upper two kinds of fibers of dye is formed.The co-bathing dyeing of the fiber mixed fabrics different for two or more dyeabilities.Such as use In the polyester cotton blend dye of polyester/cotton blended fabric printing and dyeing.
Embodiment 1
A kind of One Bath Dyeing Process of acid dyes and blend dye, as shown in figure 1, comprising the following steps:
The first step, in normal temperature(25℃)Under, fabric is imported into dye vat, nylon antitack agent RF is added in dye vat;The nylon is prevented Stick RF is 1 g/L(Nylon antitack agent and amount of solution ratio in dye vat);
Second step, after 5min, acid dyes is added in dye vat;
3rd step, after 10min, blend dye is added in dye vat;
4th step, after 5min, glauber salt is added in dye vat;The addition of the glauber salt is 10g/L;
5th step, 100% acetic acid is added, the acetic acid addition is 0.3g/L
80 DEG C are warming up to from normal temperature with 1.2 DEG C/min speed, maintains 10min;
6th step, 90 DEG C are warming up to from 80 DEG C with 1.2 DEG C/min speed, maintains 30min;
7th step, 70 DEG C are cooled to from 90 DEG C with 2 DEG C/min speed, completes dyeing.
Embodiment 2
A kind of One Bath Dyeing Process of acid dyes and blend dye, comprises the following steps:
The first step, in normal temperature(25℃)Under, fabric is imported into dye vat, nylon antitack agent RF is added in dye vat;The nylon is prevented Stick RF is 0.8 g/L(Nylon antitack agent and amount of solution ratio in dye vat);
Second step, after 4min, acid dyes is added in dye vat;
3rd step, after 8min, blend dye is added in dye vat;
4th step, after 4min, glauber salt is added in dye vat;The addition of the glauber salt is 5g/L;
5th step, 100% acetic acid is added, the acetic acid addition is 0.2g/L, and is heated up with 1.2 DEG C/min speed from normal temperature To 75 DEG C, 10min is maintained;
6th step, 90 DEG C are warming up to from 75 DEG C with 1.2 DEG C/min speed, maintains 30min;
7th step, 65 DEG C are cooled to from 90 DEG C with 2 DEG C/min speed, completes dyeing.Embodiment 3
A kind of One Bath Dyeing Process of acid dyes and blend dye, comprises the following steps:
The first step, in normal temperature(25℃)Under, fabric is imported into dye vat, nylon antitack agent RF is added in dye vat;The nylon is prevented Stick RF is 1.2 g/L(Nylon antitack agent and amount of solution ratio in dye vat);
Second step, after 6min, acid dyes is added in dye vat;
3rd step, after 12min, blend dye is added in dye vat;
4th step, after 6min, glauber salt is added in dye vat;The addition of the glauber salt is 15g/L;
5th step, adds 100% acetic acid, and the acetic acid addition is that 0.4g/L is warming up to 1.2 DEG C/min speed from normal temperature 85 DEG C, maintain 10min;
6th step, 100 DEG C are warming up to from 85 DEG C with 1.2 DEG C/min speed, maintains 30min;
7th step, 75 DEG C are cooled to from 100 DEG C with 2 DEG C/min speed, completes dyeing.
Embodiment 4
A kind of One Bath Dyeing Process of acid dyes and blend dye, comprises the following steps:
The first step, in normal temperature(25℃)Under, fabric is imported into dye vat, nylon antitack agent RF is added in dye vat;The nylon is prevented Stick RF is 1.1 g/L(Nylon antitack agent and amount of solution ratio in dye vat);
Second step, after 5min, acid dyes is added in dye vat;
3rd step, after 11min, blend dye is added in dye vat;
4th step, after 5min, glauber salt is added in dye vat;The addition of the glauber salt is 12g/L;
5th step, 100% acetic acid is added, the acetic acid addition is 0.25g/L, is heated up with 1.2 DEG C/min speed from normal temperature To 83 DEG C, 10min is maintained;
6th step, 95 DEG C are warming up to from 83 DEG C with 1.2 DEG C/min speed, maintains 30min;
7th step, 72 DEG C are cooled to from 95 DEG C with 2 DEG C/min speed, completes dyeing.
The above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, those of ordinary skill in the art are to this hair Other modifications or equivalent substitution that bright technical scheme is made, without departing from the spirit and scope of technical solution of the present invention, It all should cover in scope of the presently claimed invention.

Claims (10)

  1. A kind of 1. One Bath Dyeing Process of acid dyes and blend dye, it is characterised in that:Comprise the following steps:
    The first step, fabric is imported into dye vat, nylon antitack agent is added in dye vat;
    Second step, add acid dyes;
    3rd step, add blend dye;
    4th step, add glauber salt;
    5th step, acetic acid is added, and the bath temperature of dye vat is heated up and maintained;
    6th step, the bath temperature of dye vat is heated up and maintained again;
    7th step, the bath temperature of dye vat is cooled.
  2. 2. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Two steps concretely comprise the following steps:After 4-6min, acid dyes is added in dye vat.
  3. 3. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Three steps concretely comprise the following steps:After 8-12min, blend dye is added in dye vat.
  4. 4. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Four steps concretely comprise the following steps:After 4-6min, glauber salt is added in dye vat.
  5. 5. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Five steps concretely comprise the following steps:The bath temperature by dye vat is warming up to 80 ± 5 DEG C from normal temperature, maintains 8-12min;The programming rate For 1.2 DEG C/min.
  6. 6. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Six steps concretely comprise the following steps:The bath temperature of dye vat is warming up to 95 ± 5 DEG C from 80 ± 5 DEG C, maintains 24-36min;The programming rate For 1.2 DEG C/min.
  7. 7. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:Described Seven steps concretely comprise the following steps:, the bath temperature of dye vat is cooled to 70 ± 5 DEG C from 95 ± 5 DEG C;The programming rate is 2 DEG C/min.
  8. 8. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:The Buddhist nun Imperial antitack agent addition is 0.8-1.2g/L.
  9. 9. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:The member The addition of bright powder is 5-15g/L.
  10. 10. the One Bath Dyeing Process of acid dyes according to claim 1 and blend dye, it is characterised in that:It is described Acetic acid is 100% acetic acid, and the acetic acid addition is 0.2-0.4g/L.
CN201710850852.3A 2017-09-20 2017-09-20 A kind of One Bath Dyeing Process of acid dyes and blend dye Pending CN107604702A (en)

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CN201710850852.3A CN107604702A (en) 2017-09-20 2017-09-20 A kind of One Bath Dyeing Process of acid dyes and blend dye

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CN201710850852.3A CN107604702A (en) 2017-09-20 2017-09-20 A kind of One Bath Dyeing Process of acid dyes and blend dye

Publications (1)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103669047A (en) * 2013-11-27 2014-03-26 浙江东方华强纺织印染有限公司 Black-dyeing one bath process for nylon and cotton mixed fabrics
CN104233865A (en) * 2013-06-17 2014-12-24 无锡市东新织造有限公司 Dyeing process for viscose/brocade blended silks by active/acid dye-bath method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104233865A (en) * 2013-06-17 2014-12-24 无锡市东新织造有限公司 Dyeing process for viscose/brocade blended silks by active/acid dye-bath method
CN103669047A (en) * 2013-11-27 2014-03-26 浙江东方华强纺织印染有限公司 Black-dyeing one bath process for nylon and cotton mixed fabrics

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
李美英: "粘锦混纺针织物一浴一步法染色工艺探讨", 《染整技术》 *
王学元 等: "棉锦交织物浸染一浴法生产实践", 《印染》 *
董耀辉: "《筒子(经轴)纱染色生产技术》", 28 February 2007, 中国纺织出版社 *
邹衡: "《纱线筒子染色工程》", 31 August 2004, 中国纺织出版社 *
陈俊 等: "锦/粘织物一浴法染色", 《印染》 *

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Address after: 312000 North eleven Road, Binhai Industrial Area, Keqiao District, Shaoxing, Zhejiang

Applicant after: Zhejiang Yue new printing and dyeing Co., Ltd.

Address before: 312000 Dashan West Village, an Chang town, Keqiao District, Shaoxing, Zhejiang

Applicant before: Zhejiang Yue new printing and dyeing Co., Ltd.

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Application publication date: 20180119

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