CN107604285B - A kind of beta titanium alloy product forging method - Google Patents

A kind of beta titanium alloy product forging method Download PDF

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CN107604285B
CN107604285B CN201711046465.0A CN201711046465A CN107604285B CN 107604285 B CN107604285 B CN 107604285B CN 201711046465 A CN201711046465 A CN 201711046465A CN 107604285 B CN107604285 B CN 107604285B
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forging
titanium alloy
beta
time
slab
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CN107604285A (en
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杨柳
王莹
林崇智
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Chengdu Advanced Metal Materials Industry Technology Research Institute Co Ltd
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Chengdu Advanced Metal Materials Industry Technology Research Institute Co Ltd
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Abstract

The present invention, which discloses, is related to alloy forging technical field, especially a kind of beta titanium alloy product forging method comprising following steps: a, beta-titanium alloy cylinder base being put into heating furnace and is heated;B, beta-titanium alloy cylinder base after the heating time is up, come out of the stove immediately by beta-titanium alloy cylinder base, and beta-titanium alloy cylinder base is forged, One-time forging slab is obtained;C, One-time forging slab is cooled to room temperature;D, One-time forging slab after cooling is put into heating furnace and carries out reheating;E, One-time forging slab is forged, obtains two fire forging slabs;F, two fire forging slabs are put into heating furnace and are heated three times;G, two fire forging slabs are forged, obtains three fire forging slabs;H, step f, step g are repeated, until obtaining beta titanium alloy product.The beta titanium alloy product forging method that the present invention provides a kind of processes is few, forging is high-efficient.

Description

A kind of beta titanium alloy product forging method
Technical field
The present invention relates to alloy forging technical field, especially a kind of beta titanium alloy product forging method.
Background technique
Beta-titanium alloy, annealing are air-cooled to the titanium alloy that room temperature is almost all β phase, and the major advantage of beta-titanium alloy is that have very well It is cold cream and cold formability energy, cold rolling reduction is up to 90% or more.The sheet metal part of medium complexity can be shaped at room temperature, and Rivet and bolt can be cold worked.By ageing treatment, intensity can be normally reached 1000MPa or more, have excellent weldability Energy and corrosion resistance.
The forging temperature of beta-titanium alloy is usually chosen in above 30-50 DEG C of phase transition temperature, it is therefore an objective to avoid the crystal grain under high temperature Fast growth, crystal grain fast growth seriously affect the intensity and plasticity of beta titanium alloy product.Since beta-titanium alloy intensity is high, in phase transformation Point temperature nearby forged to capacity of equipment require it is relatively high, while in order to avoid cracking, Dan Huoci total deformation is also smaller, To considerably increase forging process, the forging processing efficiency of beta titanium alloy product is reduced.
Summary of the invention
The technical problems to be solved by the invention are to provide the beta titanium alloy product forging side that a kind of process is few, forging is high-efficient Method.
The present invention solves a kind of beta titanium alloy product forging method used by its technical problem, includes the following steps:
A, beta-titanium alloy cylinder base is put into heating furnace and is heated, the heating temperature of heating furnace is than beta-titanium alloy circle The phase point temperature of cylindricality base is 350-400 DEG C high;
B, the beta-titanium alloy cylinder base in step a after the heating time is up, come out of the stove immediately by beta-titanium alloy cylinder base, by β titanium Alloy cylinder base is forged, and One-time forging slab is obtained, and stops phase transformation of the temperature than the beta-titanium alloy cylinder base of forging Point temperature is 100-150 DEG C high, and One-time forging slab is at least compared with beta-titanium alloy cylinder base in the deflection of thickness direction 60%;
C, One-time forging slab is cooled to room temperature;
D, One-time forging slab after cooling is put into heating furnace and carries out reheating, the reheating temperature of heating furnace Phase point temperature than the beta-titanium alloy cylinder base is 100-150 DEG C high;
E, after One-time forging slab heating time arrives in step d, One-time forging slab is come out of the stove immediately, by One-time forging slab It is forged, obtains two fire forging slabs;
F, two fire forging slabs are put into heating furnace and are heated three times, the heating temperature three times of heating furnace is than the β titanium The phase point temperature of alloy cylinder base is 50-100 DEG C high;
G, in step f after the heating time is up, two fire forging slabs are come out of the stove immediately, and two fire forging slabs are forged, are obtained To three fire forging slabs;
H, step f, step g are repeated, until obtaining beta titanium alloy product.
Further, in step a, heating time is 0.4-0.6 times of beta-titanium alloy cylinder base diameter, when heating Between unit be min.
Further, One-time forging slab is passed through cooling by water to room temperature in step c.
Further, heating time is 0.5-0.7 times of One-time forging slab thickness, heating time in step d Unit is min.
Further, heating time is 0.5-0.7 times of two fire forging slab thicknesses, heating time in step f Unit is min.
It is heated the beneficial effects of the present invention are: beta-titanium alloy cylinder base is put into heating furnace first, heating furnace Heating temperature is 350-400 DEG C higher than the phase point temperature of the beta-titanium alloy cylinder base, and beta-titanium alloy cylinder base is come out of the stove immediately, will Beta-titanium alloy cylinder base is forged, and One-time forging slab is obtained, One-time forging slab compared with beta-titanium alloy cylinder base, The deflection of thickness direction is at least 60%, so that isometric group of β containing a kind of largely needle-shaped distortion in One-time forging slab It knits, is obtained in a large amount of practices and practice, the β equiaxed structure of the needle-shaped distortion can absorb a large amount of in high-temperature heating process Energy is just slowly decomposed, and restrained effectively growing up for initial grain size so that One-time forging slab is in hot conditions Under (above 100-300 DEG C of phase point temperature), initial grain size still will not occur sharply to grow up, and forge to ensure that The intensity and plasticity of beta titanium alloy product, enable beta titanium alloy product to be forged at high temperature, significantly improve Dan Huoci's Blank deflection reduces the process of beta titanium alloy product forging, improves the forging efficiency of beta titanium alloy product.
Detailed description of the invention
Fig. 1 is a kind of crystal phase schematic diagram of One-time forging slab;
Specific embodiment
The present invention will be further explained below with reference to the attached drawings.
A kind of beta titanium alloy product forging method of the present invention, includes the following steps:
A, beta-titanium alloy cylinder base is put into heating furnace and is heated, the heating temperature of heating furnace is than beta-titanium alloy circle The phase point temperature of cylindricality base is 350-400 DEG C high, and heating time is 0.4-0.6 times of beta-titanium alloy cylinder base diameter, when heating Between unit be min;
B, the beta-titanium alloy cylinder base in step a after the heating time is up, come out of the stove immediately by beta-titanium alloy cylinder base, by β titanium Alloy cylinder base is forged, and One-time forging slab is obtained, and stops phase transformation of the temperature than the beta-titanium alloy cylinder base of forging Point temperature is 100-150 DEG C high, and One-time forging slab is at least compared with beta-titanium alloy cylinder base in the deflection of thickness direction 60%, it that is to say that, in thickness direction, the size of One-time forging slab is less than the 40% of beta-titanium alloy cylinder base size, by big It is obtained in amount practice and test, for One-time forging slab compared with beta-titanium alloy cylinder base, deflection is bigger, One-time forging slab The quantity of the β equiaxed structure of the needle-shaped distortion contained is more, is more conducive to forge One-time forging slab;
C, cooling efficiency be can be improved by water cooling one by cooling by water to room temperature for the cooling of One-time forging slab, Two can reinforce One-time forging slab;
D, One-time forging slab after cooling is put into heating furnace and carries out reheating, the reheating temperature of heating furnace Phase point temperature than the beta-titanium alloy cylinder base is 100-150 DEG C high, and heating time is the 0.5- of One-time forging slab thickness 0.7 times, the unit of heating time is min;
E, after One-time forging slab heating time arrives in step d, One-time forging slab is come out of the stove immediately, by One-time forging slab It is forged, obtains two fire forging slabs;
F, two fire forging slabs are put into heating furnace and are heated three times, the heating temperature three times of heating furnace is than the β titanium The phase point temperature of alloy cylinder base is 50-100 DEG C high, and heating time is 0.5-0.7 times of two fire forging slab thicknesses, heating The unit of time is min;
G, in step f after the heating time is up, two fire forging slabs are come out of the stove immediately, and two fire forging slabs are forged, are obtained To three fire forging slabs;
H, step f, step g are repeated, until obtaining beta titanium alloy product.
Beta-titanium alloy cylinder base is put into heating furnace first and is heated, the heating temperature of heating furnace is than the beta-titanium alloy The phase point temperature of cylindrical base is 350-400 DEG C high, and beta-titanium alloy cylinder base is come out of the stove immediately, and beta-titanium alloy cylinder base is carried out Forging, obtain One-time forging slab, One-time forging slab compared with beta-titanium alloy cylinder base, thickness direction deflection extremely It is less 60%, as shown in Figure 1, making containing a kind of a large amount of β equiaxed structure of needle-shaped distortion in One-time forging slab, a large amount of It is obtained in practice and practice, the β equiaxed structure of the needle-shaped distortion it is just slow can to absorb big energy in high-temperature heating process It decomposes, restrained effectively growing up for initial grain size so that One-time forging slab is in hot conditions (phase point temperature Above 100-300 DEG C) under, initial grain size still will not occur sharply to grow up, and forge beta titanium alloy product to ensure that Intensity and plasticity, so that beta titanium alloy product is forged at high temperature, significantly improve the blank deflection of Dan Huoci, Reduce the process of beta titanium alloy product forging, the forging of general beta titanium alloy product in 3-4 heating process, compare with For preceding at least 6 times, it is remarkably improved the forging efficiency of beta titanium alloy product.
Embodiment 1
A, a kind of beta-titanium alloy cylinder base (TB5) is put into heating furnace and is heated, the beta-titanium alloy cylinder base Diameter 990mm, phase point temperature are 745 DEG C, and the heating temperature of heating furnace is 1095 DEG C, heating time 396min;
B, the beta-titanium alloy cylinder base in step a after the heating time is up, come out of the stove immediately by beta-titanium alloy cylinder base, by β titanium Alloy cylinder base is forged, and One-time forging slab is obtained, and stops phase transformation of the temperature than the beta-titanium alloy cylinder base of forging Point temperature is 100 DEG C high, and One-time forging slab is 65% in the deflection of thickness direction compared with beta-titanium alloy cylinder base, namely It is One-time forging slab with a thickness of 346mm;
C, by the cooling cooling by water that passes through of One-time forging slab to room temperature;
D, One-time forging slab after cooling is put into heating furnace and carries out reheating, the reheating temperature of heating furnace It is 895 DEG C, heating time 173min;
E, after One-time forging slab heating time arrives in step d, One-time forging slab is come out of the stove immediately, by One-time forging slab Forged, obtain two fire forging slabs, two fire forging slabs with a thickness of 220mm;
F, two fire forging slabs being put into heating furnace and is heated three times, the heating temperature three times of heating furnace is 795 DEG C, Heating time is 78min;
G, in step f after the heating time is up, two fire forging slabs are come out of the stove immediately, and two fire forging slabs are forged, are obtained To beta titanium alloy product, the beta titanium alloy product with a thickness of 140mm.
The beta titanium alloy product with a thickness of 140mm is processed into the beta-titanium alloy cylinder base forging that one diameter is 990mm, It only needs to forge three times, significantly reduces the process of forging, improve forging efficiency.
Embodiment 2
A, a kind of beta-titanium alloy cylinder base (TB22) is put into heating furnace and is heated, the beta-titanium alloy cylinder base Diameter 1000mm, phase point temperature are 758 DEG C, and the heating temperature of heating furnace is 1158 DEG C, heating time 600min;
B, the beta-titanium alloy cylinder base in step a after the heating time is up, come out of the stove immediately by beta-titanium alloy cylinder base, by β titanium Alloy cylinder base is forged, and One-time forging slab is obtained, and stops phase transformation of the temperature than the beta-titanium alloy cylinder base of forging Point temperature is 150 DEG C high, and One-time forging slab is 60% in the deflection of thickness direction compared with beta-titanium alloy cylinder base, namely It is One-time forging slab with a thickness of 400mm
C, by the cooling cooling by water that passes through of One-time forging slab to room temperature;
D, One-time forging slab after cooling is put into heating furnace and carries out reheating, the reheating temperature of heating furnace It is 908 DEG C, heating time 280min;
E, after One-time forging slab heating time arrives in step d, One-time forging slab is come out of the stove immediately, by One-time forging slab Forged, obtain two fire forging slabs, two fire forging slabs with a thickness of 280mm;
F, two fire forging slabs being put into heating furnace and is heated three times, the heating temperature three times of heating furnace is 858 DEG C, Heating time is 168min;
G, in step f after the heating time is up, two fire forging slabs are come out of the stove immediately, and two fire forging slabs are forged, are obtained To three fire forging slabs, three fire forging slabs with a thickness of 200mm;
H, three fire forging slabs being put into heating furnace and carries out four heating, the heating temperature three times of heating furnace is 878 DEG C, Heating time is 120min;
I, in the good h of step after the heating time is up, three fire forging slabs are come out of the stove immediately, and three fire forging slabs are forged, Obtain beta titanium alloy product, the beta titanium alloy product with a thickness of 120mm.
The beta-titanium alloy cylinder base forging that one diameter is 1000mm is processed into the beta-titanium alloy production with a thickness of 120mm Product, it is only necessary to forge four times, significantly reduce the process of forging, improve forging efficiency.

Claims (5)

1. a kind of beta titanium alloy product forging method, characterized by the following steps:
A, beta-titanium alloy cylinder base is put into heating furnace and is heated, the heating temperature of heating furnace is than beta-titanium alloy cylinder The phase point temperature of base is 350-400 DEG C high;
B, the beta-titanium alloy cylinder base in step a after the heating time is up, come out of the stove immediately, by beta-titanium alloy by beta-titanium alloy cylinder base Cylindrical base is forged, and One-time forging slab is obtained, and stops transformation temperature temperature of the temperature than the beta-titanium alloy cylinder base of forging Spend 100-150 DEG C high, One-time forging slab is at least 60% compared with beta-titanium alloy cylinder base, in the deflection of thickness direction;
C, One-time forging slab is cooled to room temperature;
D, One-time forging slab after cooling is put into heating furnace and carries out reheating, the reheating temperature of heating furnace is than being somebody's turn to do The phase point temperature of beta-titanium alloy cylinder base is 100-150 DEG C high;
E, after One-time forging slab heating time arrives in step d, One-time forging slab is come out of the stove immediately, and One-time forging slab is carried out Forging obtains two fire forging slabs;
F, two fire forging slabs are put into heating furnace and are heated three times, the heating temperature three times of heating furnace is than the beta-titanium alloy The phase point temperature of cylindrical base is 50-100 DEG C high;
G, in step f after the heating time is up, two fire forging slabs are come out of the stove immediately, and two fire forging slabs are forged, obtain three Fire forging slab;
H, step f, step g are repeated, until obtaining beta titanium alloy product.
2. a kind of beta titanium alloy product forging method as described in claim 1, it is characterised in that: in step a, heating time It is 0.4-0.6 times of beta-titanium alloy cylinder base diameter, the unit of heating time is min.
3. a kind of beta titanium alloy product forging method as described in claim 1, it is characterised in that: in step c, a fire is forged It makes slab and passes through cooling by water to room temperature.
4. a kind of beta titanium alloy product forging method as described in claim 1, it is characterised in that: in step d, heating time It is 0.5-0.7 times of One-time forging slab thickness, the unit of heating time is min.
5. a kind of beta titanium alloy product forging method as described in Claims 1-4 any one, it is characterised in that: in step f In, heating time is 0.5-0.7 times of two fire forging slab thicknesses, and the unit of heating time is min.
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451490A (en) * 2014-11-19 2015-03-25 中南大学 Method for preparing ultrafine grain titanium alloy by using alpha'' orthorhombic martensite microstructure
CN107217221A (en) * 2017-05-22 2017-09-29 西部超导材料科技股份有限公司 A kind of preparation method of high uniform Ti 15Mo titanium alloy bar stocks

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101603163B (en) * 2009-07-08 2010-10-13 西北工业大学 Control method of local loading and shaping equiaxial alpha content of titanium alloy
CN107552697B (en) * 2017-08-31 2019-05-21 湖南金天钛业科技有限公司 TC4 titanium alloy rod bar forging method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104451490A (en) * 2014-11-19 2015-03-25 中南大学 Method for preparing ultrafine grain titanium alloy by using alpha'' orthorhombic martensite microstructure
CN107217221A (en) * 2017-05-22 2017-09-29 西部超导材料科技股份有限公司 A kind of preparation method of high uniform Ti 15Mo titanium alloy bar stocks

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Address before: 610306 Chengdu City, Chengdu, Sichuan, China (Sichuan) free trade test zone, Chengdu City, Qingbaijiang District, xiangdao Boulevard, Chengxiang Town, No. 1509 (room 13, A District, railway port mansion), room 1319

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