CN107597082A - A kind of preparation method of Chinese gooseberry beverage adsorbent - Google Patents
A kind of preparation method of Chinese gooseberry beverage adsorbent Download PDFInfo
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- CN107597082A CN107597082A CN201710908723.5A CN201710908723A CN107597082A CN 107597082 A CN107597082 A CN 107597082A CN 201710908723 A CN201710908723 A CN 201710908723A CN 107597082 A CN107597082 A CN 107597082A
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Abstract
The present invention relates to a kind of preparation method of Chinese gooseberry beverage adsorbent.By weight, chitosan colloidal sol, 2 acrylic acrylic acid are added in a kettle; 3,4,6 three oxygen acetyl group D grape thin malt sugars; apple monoacyl tyrosine, carragheen, under the catalysis of chloroplatinic acid; reaction, removes catalyst after terminating, crosslinking agent is added into product; pore-foaming agent, reaction terminate rear dry solidification, remove pore-foaming agent; product is dried through washing, obtains adsorbent product.
Description
Technical field
The present invention relates to a kind of preparation method of adsorbent, especially a kind of preparation method of Chinese gooseberry beverage adsorbent.
Background technology
Kiwi berry contains abundant mineral matter, including abundant calcium, phosphorus, iron, also containing carrotene and multivitamin,
It is important to keeping health to have the function that.
Kiwi berry can be used as a kind of beverage treatment scurvy.The vitamin C that it contains helps to reduce the courage in blood
Sterol levels, play a part of expanding blood vessel and reduce blood pressure.It also strengthens cardiac muscle.Periodically a kiwi fruit powder is drunk to add
Beverage made of upper appropriate warm water, can help to stablize the level of Blood Cholesterol.
Because it contains abundant nutriment, therefore gross protein level can be improved.In postprandial Kiwi berry of having a drink
Beverage made of powder, can solve the problems, such as stomach weakness.Kiwi berry can effectively treat breathing problem, can also improve your regard
Power.It is used in combination with honey can effectively improve eyesight.In addition, it or a kind of powerful antioxidant, can eliminate wrinkle
Line and microgroove.
CN1915113 discloses a kind of fruit juice, slurry is made from the byproduct of whole fruit extraction orange juice, and extract
Generate primary pericarp fruit juice.It is made into rough pericarp fruit juice and micro-filtration prepares and clarifies rough pericarp fruit juice.It is used
Resin removes this composition, to provide a kind of reinforcing pericarp as adsorbent by the way that pericarp fruit juice is combined with polymeric adsorbent
Orange juice, it can be mixed with other fruit juice.
CN101467756 discloses a kind of Chinese gooseberry beverage, and it includes Kiwi berry fruit block, liquid glucose, preservative and water;
Its percentage by weight is:Kiwi berry fruit block 20% to 25%, liquid glucose 15% to 25%, preservative 0.5% to 1%, remaining is water;Through raw material
Processing, stripping and slicing, after softening sterilization of precooking cool down tinning, note juice in tank, the process finished product such as sterilizing, sealing.
Kiwi berry is inevitably mixed into heavy metal element by the process grown in industrialization production of machinery line and soil,
Existing juice beverage production process does not use adsorbent, or has counterweight as adsorbent using resin and activated carbon
The shortcomings that metallic element assimilation effect is not strong, and the smaller logical fluidity in aperture is poor.
The content of the invention
The purpose of the present invention is：There is provided a kind of manufacture method of Chinese gooseberry beverage adsorbent, it is characterised in that following step
Suddenly：
By weight, chitosan colloidal sol, 2- acrylic acrylic acid, 3,4,6- tri--oxy-acetyl-D- are added in a kettle
Grape thin malt sugar, apple monoacyl tyrosine, carragheen, under the catalysis of chloroplatinic acid, 75-85 DEG C is warming up to, reacts 2-4h, is removed
Catalyst, crosslinking agent is added into product, pore-foaming agent, is stirred with 300-500rpm rotating speed, be warming up to 55-65 DEG C, reaction
4-6h, reacting and stop stirring after terminating, be warming up to 85-95 DEG C of dry solidification 2-3h, remove pore-foaming agent, product is dry through washing,
Obtain adsorbent product.
Described 2- acrylic acrylic acid, its quality dosage are the 0.5-1.5% of chitosan in chitosan colloidal sol.
Described 3,4,6- tri--oxy-acetyls-D-Glucose alkene, its quality dosage are chitosan in chitosan colloidal sol
0.1-0.5%。
Described apple monoacyl tyrosine, its quality dosage are the 1-3% of chitosan in chitosan colloidal sol.
Described carragheen, its quality dosage are the 0.1-0.3% of chitosan in chitosan colloidal sol.
Described crosslinking agent is Geniposide, and its quality dosage is the 2-4% of chitosan in chitosan colloidal sol.
Described pore-foaming agent is polyethylene glycol, and its quality dosage is the 15-25% of chitosan in chitosan colloidal sol.
Described chitosan, 2- acrylic acrylic acid, 3,4,6- tri--oxy-acetyls-D-Glucose alkene, apple monoacyl
Tyrosine, carragheen, chloroplatinic acid, crosslinking agent, dispersant, pore-foaming agent are commercially available prod.
The product of the present invention has the advantages that：
The adsorbent product that the present invention is produced, logical fluidity is good, suitable for adsorbing beverage class product, for the heavy metals such as lead member
Element has excellent absorption property, and compression strength is good, and adsorbent product is non-breakable, is easily isolated.
Embodiment
Following instance is only to further illustrate the present invention, is not limitation the scope of protection of the invention.
Embodiment 1
In a kettle, chitosan colloidal sol 1000Kg, the 2- acrylic acrylic acid 1Kg that mass concentration is 10% is added, 3,4,6-
Three-oxy-acetyl-D-Glucose alkene 0.3Kg, apple monoacyl tyrosine 2Kg, carragheen 0.2Kg, in the catalysis of chloroplatinic acid
Under, 80 DEG C are warming up to, reacts 3h, removes catalyst, crosslinking agent 3Kg, pore-foaming agent 20Kg, with 400rpm's are added into product
Rotating speed stirs, and is warming up to 60 DEG C, reacts 5h, and reaction stops stirring after terminating, is warming up to 90 DEG C of dry solidification 2.5h, removes pore
Agent, product are dried through washing, obtain adsorbent product.
Embodiment 2
In a kettle, chitosan colloidal sol 1000Kg, the 2- acrylic acrylic acid 0.5Kg that mass concentration is 10% is added, 3,4,6-
Three-oxy-acetyl-D-Glucose alkene 0.1Kg, apple monoacyl tyrosine 1Kg, carragheen 0.1Kg, in the catalysis of chloroplatinic acid
Under, 75 DEG C are warming up to, reacts 2h, removes catalyst, crosslinking agent 2Kg, pore-foaming agent 15Kg, with 300rpm's are added into product
Rotating speed stirs, and is warming up to 55 DEG C, reacts 4h, and reaction stops stirring after terminating, is warming up to 85 DEG C of dry solidification 2h, removes pore
Agent, product are dried through washing, obtain adsorbent product.
Embodiment 3
In a kettle, chitosan colloidal sol 1000Kg, the 2- acrylic acrylic acid 1.5Kg that mass concentration is 10% is added, 3,4,6-
Three-oxy-acetyl-D-Glucose alkene 0.5Kg, apple monoacyl tyrosine 3Kg, carragheen 0.3Kg, in the catalysis of chloroplatinic acid
Under, 85 DEG C are warming up to, reacts 4h, removes catalyst, crosslinking agent 4Kg, pore-foaming agent 25Kg, with 500rpm's are added into product
Rotating speed stirs, and is warming up to 65 DEG C, reacts 6h, and reaction stops stirring after terminating, is warming up to 95 DEG C of dry 3h, removes pore-foaming agent, production
Thing is dried through washing, obtains adsorbent product.
Comparative example 1
2- acrylic acrylic acid is added without, other conditions are the same as embodiment 1.
Comparative example 2
3,4,6- tri--oxy-acetyls-D-Glucose alkene is added without, other conditions are the same as embodiment 1.
Comparative example 3
Apple monoacyl tyrosine is added without, other conditions are the same as embodiment 1.
Comparative example 4
Adsorbent is used as using activated carbon.
Embodiment 4
The kiwi-fruit juice aqueous solution that concentration is 30% is passed through in the chromatographic column equipped with embodiment 1-3 and comparative example 1-4 respectively and carried out
Absorption, flow velocity 1BV/h, the saturation lead absorption of the lead content in kiwi-fruit juice and adsorbent product is examined to hold after the completion of absorption
Amount.
The saturation lead adsorption capacity of lead content and adsorbent product in the kiwi-fruit juice of table 1.
Claims (7)
1. a kind of preparation method of Chinese gooseberry beverage adsorbent, it is characterised in that comprise the following steps：
By weight, chitosan colloidal sol, 2- acrylic acrylic acid, 3,4,6- tri--oxy-acetyl-D- are added in a kettle
Grape thin malt sugar, apple monoacyl tyrosine, carragheen, under the catalysis of chloroplatinic acid, 75-85 DEG C is warming up to, reacts 2-4h, is removed
Catalyst, crosslinking agent is added into product, pore-foaming agent, is stirred with 300-500rpm rotating speed, be warming up to 55-65 DEG C, reaction
4-6h, reacting and stop stirring after terminating, be warming up to 85-95 DEG C of dry solidification 2-3h, remove pore-foaming agent, product is dry through washing,
Obtain adsorbent product.
A kind of 2. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described 2- third
Alkenyl acrylic acid, its quality dosage are the 0.5-1.5% of chitosan in chitosan colloidal sol.
A kind of 3. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described 3,4,
Tri--oxy-acetyls of 6--D-Glucose alkene, its quality dosage are the 0.1-0.5% of chitosan in chitosan colloidal sol.
A kind of 4. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described apple
Monoacyl tyrosine, its quality dosage are the 1-3% of chitosan in chitosan colloidal sol.
A kind of 5. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described OK a karaoke club
Glue, its quality dosage are the 0.1-0.3% of chitosan in chitosan colloidal sol.
A kind of 6. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described crosslinking
Agent is Geniposide, and its quality dosage is the 2-4% of chitosan in chitosan colloidal sol.
A kind of 7. preparation method of Chinese gooseberry beverage adsorbent according to claim 1, it is characterised in that：Described pore
Agent is polyethylene glycol, and its quality dosage is the 15-25% of chitosan in chitosan colloidal sol.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710908723.5A CN107597082B (en) | 2017-09-29 | 2017-09-29 | Preparation method of kiwi fruit beverage adsorbent |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710908723.5A CN107597082B (en) | 2017-09-29 | 2017-09-29 | Preparation method of kiwi fruit beverage adsorbent |
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| CN107597082A true CN107597082A (en) | 2018-01-19 |
| CN107597082B CN107597082B (en) | 2020-04-24 |
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| CN201710908723.5A Active CN107597082B (en) | 2017-09-29 | 2017-09-29 | Preparation method of kiwi fruit beverage adsorbent |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445453A (en) * | 2014-11-03 | 2015-03-25 | 芜湖市祥荣食品有限公司 | Blue algae treating agent containing alfalfa roots and preparation method thereof |
| US20160175812A1 (en) * | 2014-12-22 | 2016-06-23 | Nishil Mohammed | PRISTINE AND SURFACE FUNCTIONALIZED CELLULOSE NANOCRYSTALS (CNCs) INCORPORATED HYDROGEL BEADS AND USES THEREOF |
| CN106362703A (en) * | 2016-10-12 | 2017-02-01 | 四川大学 | Improved carageenan-chitosan polyelectrolyte microspheres as well as preparation method and application thereof |
-
2017
- 2017-09-29 CN CN201710908723.5A patent/CN107597082B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445453A (en) * | 2014-11-03 | 2015-03-25 | 芜湖市祥荣食品有限公司 | Blue algae treating agent containing alfalfa roots and preparation method thereof |
| US20160175812A1 (en) * | 2014-12-22 | 2016-06-23 | Nishil Mohammed | PRISTINE AND SURFACE FUNCTIONALIZED CELLULOSE NANOCRYSTALS (CNCs) INCORPORATED HYDROGEL BEADS AND USES THEREOF |
| CN106362703A (en) * | 2016-10-12 | 2017-02-01 | 四川大学 | Improved carageenan-chitosan polyelectrolyte microspheres as well as preparation method and application thereof |
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| CN107597082B (en) | 2020-04-24 |
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