CN107597051A - Reaction device for industrially preparing functionalized graphene - Google Patents

Reaction device for industrially preparing functionalized graphene Download PDF

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Publication number
CN107597051A
CN107597051A CN201711049850.0A CN201711049850A CN107597051A CN 107597051 A CN107597051 A CN 107597051A CN 201711049850 A CN201711049850 A CN 201711049850A CN 107597051 A CN107597051 A CN 107597051A
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CN
China
Prior art keywords
shell
gear
angular wheel
tank body
pipe
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Pending
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CN201711049850.0A
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Chinese (zh)
Inventor
石世光
何怀文
宋喜佳
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University of Electronic Science and Technology of China Zhongshan Institute
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University of Electronic Science and Technology of China Zhongshan Institute
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Application filed by University of Electronic Science and Technology of China Zhongshan Institute filed Critical University of Electronic Science and Technology of China Zhongshan Institute
Priority to CN201711049850.0A priority Critical patent/CN107597051A/en
Publication of CN107597051A publication Critical patent/CN107597051A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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Abstract

The invention provides a reaction device for industrially preparing functionalized graphene, which comprises a servo motor, a shell, a screw rod, a feeding pipe, a quick joint, a rotating shaft, a first conical gear, a second conical gear, a double-spiral-belt-type stirring rod, a spiral heat-conducting pipe and a transverse pipeline, wherein the feeding pipe is arranged at the lower end of the quick joint, the feeding pipe is arranged at the upper end of the shell, the screw rod is arranged at the right end of the servo motor, the design realizes the simultaneous addition of a plurality of raw materials and also carries out primary stirring, the outer end of the transverse pipeline is provided with the spiral heat-conducting pipe, the double-spiral-belt-type stirring rod is arranged in the transverse pipeline, the second conical gear is arranged at the left end of the double-spiral-belt-type stirring rod, the first conical gear is arranged at the left end of, the production efficiency is improved, the energy consumption is reduced, and the reliability is high.

Description

A kind of reaction unit of preparation of industrialization functionalization graphene
Technical field
The present invention is a kind of reaction unit of preparation of industrialization functionalization graphene, belongs to graphene production field.
Background technology
Graphene is that the two dimension for the only one layer atomic thickness for being stripped out from graphite material, being made up of carbon atom is brilliant Body.Graphene is both most thin material, and most tough material, 200 times more taller than best steel of fracture strength.Simultaneously It has good elasticity again, and stretch range can reach the 20% of own dimensions.Graphene most potential application at present is to turn into silicon Substitute, manufacture ultra micro transistor npn npn, for produce future supercomputer.Substitute silicon, computer disposal with graphene The speed of service of device will be fast hundreds times.In addition, graphene is almost fully transparent, 2.3% light is only absorbed.On the other hand, It is very fine and close, even minimum gas atom can not also penetrate.These features cause it to be highly suitable as transparent electron The raw material of product.
The reaction unit of existing graphene, it is necessary to add different material, but only has one in production on reaction unit Or two charging apertures, so different material needs being added slowly successively, production efficiency is poor, the reaction dress of existing graphene The puddler put is identical with the radius of reaction unit, and after being stirred work for a long time, puddler is easily broken off, and uses the longevity Small while independent mixing plant is ordered, its stirring efficiency is low, and the reaction unit of existing graphene is in discharging process, because of product The middle substantial amounts of heat energy of mixing, usually can carry out cooling processing to product, can waste substantial amounts of heat energy, increase the consumption of the energy.
The content of the invention
In view of the deficienciess of the prior art, it is an object of the present invention to provide a kind of the anti-of preparation of industrialization functionalization graphene Device is answered, to solve the problems mentioned in the above background technology, the present invention is easy to use, improves production efficiency, reduces the energy and disappears Consumption, reliability are high.
To achieve these goals, the present invention is to realize by the following technical solutions:A kind of preparation of industrialization function The reaction unit of graphite alkene, including feeding mechanism, rabbling mechanism and discharge mechanism, the feeding mechanism right-hand member are provided with stirring Mechanism, the rabbling mechanism right-hand member are provided with discharge mechanism, and the feeding mechanism includes servomotor, shell, screw rod, charging Pipe and snap joint, the snap joint lower end are provided with feed pipe, and the feed pipe is arranged on shell upper end, and the shell is left End is provided with servomotor, and the servomotor right-hand member is provided with screw rod, and the screw rod is installed inside the housing, the spiral Bar is connected through shell with servomotor, and the snap joint is connected by feed pipe with shell, the rabbling mechanism bag Tank body, asessory shaft, main shaft, equipment gear, travelling gear and stepper motor are included, the tank body upper end is provided with stepper motor, institute State stepper motor lower end and be provided with main shaft, the main shaft side is provided with asessory shaft, and the asessory shaft is provided with equipment gear, described Equipment gear the inner is provided with travelling gear, and the travelling gear is arranged on main shaft, and the tank interior is provided with asessory shaft, master Axle, equipment gear and travelling gear, the travelling gear carry out gear with equipment gear and engaged, and the tank body left end is provided with outer Shell, the discharge mechanism include connecting pipe, rotary shaft, vertical duct, angular wheel one, angular wheel two, double helix belt Puddler, spiral heat conducting pipe and horizontal pipeline, the connecting pipe lower end are provided with vertical duct, the vertical duct right-hand member Horizontal pipeline is installed, the horizontal pipeline outer end is provided with spiral heat conducting pipe, double helix is provided with inside the horizontal pipeline Ribbon blender bar, the double helix ribbon blender bar left end are provided with angular wheel two, and the left end of angular wheel two is provided with cone Shape gear one, the upper end of angular wheel one are provided with rotary shaft, and the rotary shaft, angular wheel one and angular wheel two are pacified Inside vertical duct, the connecting pipe is arranged on tank body right-hand member.
Further, the shell lower end is provided with bracing piece, and bracing piece is fixed on tank body left end, and the shell is by adding Strong bar is connected with tank body.
Further, the feed pipe and snap joint are equipped with least two, and at least two feed pipes are equidistant Installed in shell upper end, switch valve and flowmeter are installed on the feed pipe.
Further, the tank body lower end is provided with equipment all-in-one, and equipment all-in-one includes ultrasonic device and condensation Equipment etc..
Further, the asessory shaft and equipment gear are equipped with two, and the equipment gear is symmetrically mounted on transmission Gear left and right ends, at least two paddles are mounted on the asessory shaft and main shaft.
Further, valve is installed on the connecting pipe, at least two flabellums, institute are uniformly provided with the rotary shaft State angular wheel one to engage with the progress gear of angular wheel two, the horizontal pipeline right-hand member is provided with low temperature water bath, double spiral shells Rotation ribbon blender bar is connected by bearing with vertical duct, and the rotary shaft is connected with vertical duct by bearing.
Beneficial effects of the present invention:A kind of reaction unit of preparation of industrialization functionalization graphene, the present invention pass through addition Fast Installation different material delivery pipe is easy in servomotor, shell, screw rod, feed pipe and snap joint, the design, can be real Existing plurality of raw materials is added simultaneously, improves production efficiency, while is also stirred for the first time, increases mixing efficiency, and then improve product Quality, solve the reaction unit of existing graphene in production, it is necessary to add different material, but there was only one on reaction unit Or two charging apertures, so different material needs being added slowly successively, the problems such as production efficiency difference.
Because of addition asessory shaft, main shaft, equipment gear, travelling gear and stepper motor, the design can make asessory shaft and Main shaft is rotated against, and then realizes two-way stirring, improves stirring efficiency, while also increases paddle intensity, and improving it makes With the life-span, the puddler solved on the reaction unit of existing graphene is identical with the radius of reaction unit, is stirred for a long time After mixing work, puddler is easily broken off, and service life is small, while independent mixing plant, the problems such as its stirring efficiency is low.
Because of addition rotary shaft, vertical duct, angular wheel one, angular wheel two, double helix ribbon blender bar, spirally lead Heat pipe and horizontal pipeline, the design can realize stirring work using the flowing of liquid, increase distributing for heat, improve heat energy Organic efficiency, energy resource consumption is reduced, reduce production cost, solve the reaction unit of existing graphene in discharging process, because of production Substantial amounts of heat energy is mixed in product, can usually cooling processing be carried out to product, substantial amounts of heat energy can be wasted, increase the consumption etc. of the energy Problem.
Because adding bracing piece, the design can improve the stability of shell, and because of addition switch valve and flowmeter, the design is just It is controlled and observes in the dispensing to raw material, because adding paddle, agitating function is realized in the design, because adding low temperature water-bath Case, the design, which is realized, carries out cooling processing to product, and the present invention is easy to use, improves production efficiency, reduces energy resource consumption, reliably Property it is high.
Brief description of the drawings
The detailed description made by reading with reference to the following drawings to non-limiting example, further feature of the invention, Objects and advantages will become more apparent upon:
Fig. 1 is a kind of structural representation of the reaction unit of preparation of industrialization functionalization graphene of the present invention;
Fig. 2 is the schematic diagram of feeding mechanism in a kind of reaction unit of preparation of industrialization functionalization graphene of the present invention;
Fig. 3 is the schematic diagram of rabbling mechanism in a kind of reaction unit of preparation of industrialization functionalization graphene of the present invention;
Fig. 4 is the schematic diagram of discharge mechanism in a kind of reaction unit of preparation of industrialization functionalization graphene of the present invention;
In figure:1- feeding mechanisms, 2- rabbling mechanisms, 3- discharge mechanisms, 4- servomotors, 5- shells, 6- screw rods, 7- chargings Pipe, 8- snap joints, 9- tank bodies, 10- asessory shafts, 11- main shafts, 12- equipment gears, 13- travelling gears, 14- stepper motors, 15- connecting pipes, 16- rotary shafts, 17- vertical ducts, 18- angular wheels one, 19- angular wheels two, 20- double helix belts are stirred Mix the spiral heat conducting pipe of bar, 21-, 22- horizontal pipelines.
Embodiment
To be easy to understand the technical means, the inventive features, the objects and the advantages of the present invention, with reference to Embodiment, the present invention is expanded on further.
Fig. 1-Fig. 4 is referred to, the present invention provides a kind of technical scheme:A kind of reaction of preparation of industrialization functionalization graphene Device, including feeding mechanism 1, rabbling mechanism 2 and discharge mechanism 3, the right-hand member of feeding mechanism 1 are provided with rabbling mechanism 2, rabbling mechanism 2 right-hand members are provided with discharge mechanism 3.
Feeding mechanism 1 includes servomotor 4, shell 5, screw rod 6, feed pipe 7 and snap joint 8, under snap joint 8 End is provided with feed pipe 7, and feed pipe 7 is arranged on the upper end of shell 5, and the left end of shell 5 is provided with servomotor 4, and the right-hand member of servomotor 4 is set There is screw rod 6, screw rod 6 is arranged on inside shell 5, and screw rod 6 is connected through shell 5 with servomotor 4, snap joint 8 It is connected by feed pipe 7 with shell 5, the design is realized plurality of raw materials while added.
Rabbling mechanism 2 includes tank body 9, asessory shaft 10, main shaft 11, equipment gear 12, travelling gear 13 and stepper motor 14, the upper end of tank body 9 is provided with stepper motor 14, and the lower end of stepper motor 14 is provided with main shaft 11, and the side of main shaft 11 is provided with asessory shaft 10, Asessory shaft 10 is provided with equipment gear 12, and the inner of equipment gear 12 is provided with travelling gear 13, and travelling gear 13 is arranged on main shaft On 11, the inside of tank body 9 is provided with asessory shaft 10, main shaft 11, equipment gear 12 and travelling gear 13, travelling gear 13 and assist tooth Wheel 12 carries out gear engagement, and the left end of tank body 9 is provided with shell 5, and the design can be rotated against asessory shaft 10 and main shaft 11.
Discharge mechanism 3 includes connecting pipe 15, rotary shaft 16, vertical duct 17, angular wheel 1, angular wheel two 19th, double helix ribbon blender bar 20, spiral heat conducting pipe 21 and horizontal pipeline 22, the lower end of connecting pipe 15 are provided with vertical duct 17, the right-hand member of vertical duct 17 is provided with horizontal pipeline 22, and the outer end of horizontal pipeline 22 is provided with spiral heat conducting pipe 21, horizontal pipeline 22 Inside is provided with double helix ribbon blender bar 20, and the left end of double helix ribbon blender bar 20 is provided with angular wheel 2 19, angular wheel 2 19 left ends are provided with angular wheel 1, and the upper end of angular wheel 1 is provided with rotary shaft 16, rotary shaft 16, angular wheel 1 And angular wheel 2 19 is installed in inside vertical duct 17, connecting pipe 15 is arranged on the right-hand member of tank body 9, and the design is available Stirring work is realized in the flowing of liquid.
The lower end of shell 5 is provided with bracing piece, and bracing piece is fixed on the left end of tank body 9, and shell 5 passes through bracing piece and the phase of tank body 9 Connection, feed pipe 7 and snap joint 8 are equipped with least two, and at least two feed pipes 7 are equidistantly mounted on the upper end of shell 5, enter Switch valve and flowmeter are installed, the lower end of tank body 9 is provided with equipment all-in-one, and equipment all-in-one includes ultrasound in expects pipe 7 Device and condensing plant etc., asessory shaft 10 and equipment gear 12 are equipped with two, and equipment gear 12 is symmetrically mounted on driving cog 13 left and right ends are taken turns, at least two paddles are mounted on asessory shaft 10 and main shaft 11, valve is installed on connecting pipe 15 , at least two flabellums are uniformly provided with rotary shaft 16, angular wheel 1 carries out gear with angular wheel 2 19 and engaged, laterally The right-hand member of pipeline 22 is provided with low temperature water bath, and double helix ribbon blender bar 20 is connected by bearing with vertical duct 17, rotary shaft 16 are connected with vertical duct 17 by bearing.
Embodiment:In progress in use, staff first is checked the present invention, check for scarce Fall into, can not just carry out using if there is defect, now need to notify maintenance personal to be repaired, if there is no asking It can be carried out using if topic, before use, delivery pipe and different feeds of the staff using snap joint 8 different material Pipe 7 is attached, and then staff opens the upper switch valve of feed pipe 7, makes different material by feed pipe 7 while enters shell In 5, while staff starts servomotor 4, and the work of servomotor 4 drives screw rod 6 to rotate, and the rotation of screw rod 6 can be right Plurality of raw materials is stirred for the first time, plurality of raw materials can also be transported inside tank body 9, Fast Installation different material is easy in the design Delivery pipe, plurality of raw materials can be achieved and add simultaneously, improve production efficiency, while also stirred for the first time, increase mixing efficiency, enter And improve product quality.
After raw material enters tank body 9, staff starts stepper motor 14, and the work of stepper motor 14 drives main shaft 11 to revolve Turn, the rotating band nutating gear 13 of main shaft 11 rotates, and is engaged because travelling gear 13 carries out gear with equipment gear 12, so transmission The rotating band dynamic auxiliary gear 12 of gear 13 rotates, and the rotating band dynamic auxiliary axle 10 of equipment gear 12 rotates, and realizes main shaft 11 and auxiliary Axle 10 carries out relative motion, and then realizes stirring work, and the design can be rotated against asessory shaft 10 and main shaft 11, enter And two-way stirring is realized, stirring efficiency is improved, while also increase paddle intensity, improve its service life.
When needing discharge, staff opens valve, the product in tank body 9 is entered vertical duct by connecting pipe 15 In road 17, then product moves down in vertical duct 17 under self gravitation effect, and product, which moves down, can drive flabellum Rotate, flabellum, which rotates, drives rotary shaft 16 to rotate, and the rotational band of rotary shaft 16 is moved angular wheel 1 and rotated, because of angular wheel 1 Gear is carried out with angular wheel 2 19 to engage, so the rotational band of angular wheel 1 is moved angular wheel 2 19 and rotated, angular wheel 2 19 rotations drive double helix ribbon blender bar 20 to rotate, and the rotation of double helix ribbon blender bar 20 is realized to be stirred to product, Accelerate heat energy in product to distribute, the heat energy distributed can carry out heat exchange processing, Jin Ershi with the medium in spiral heat conducting pipe 21 Stirring work now can be realized using the current of liquid to the recovery of heat energy, the design, increase distributing for heat, heat energy is improved and return Produce effects rate, reduce energy resource consumption, reduce production cost.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above, for this area skill For art personnel, it is clear that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing substantially from the present invention spirit or In the case of essential characteristic, the present invention can be realized in other specific forms.Which point therefore, no matter from the point of view of, all should incite somebody to action Embodiment regards exemplary as, and be it is nonrestrictive, the scope of the present invention by appended claims rather than on state Bright restriction, it is intended that all changes fallen in the implication and scope of the equivalency of claim are included in the present invention It is interior.Any reference in claim should not be considered as to the involved claim of limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims (6)

1. a kind of reaction unit of preparation of industrialization functionalization graphene, including feeding mechanism(1), rabbling mechanism(2)And row Expect mechanism(3), it is characterised in that:The feeding mechanism(1)Right-hand member is provided with rabbling mechanism(2), the rabbling mechanism(2)Right-hand member is pacified Equipped with discharge mechanism(3);
The feeding mechanism(1)Including servomotor(4), shell(5), screw rod(6), feed pipe(7)And snap joint (8), the snap joint(8)Lower end is provided with feed pipe(7), the feed pipe(7)Installed in shell(5)Upper end, the shell (5)Left end is provided with servomotor(4), the servomotor(4)Right-hand member is provided with screw rod(6), the screw rod(6)It is arranged on Shell(5)Inside, the screw rod(6)Through shell(5)With servomotor(4)It is connected, the snap joint(8)By entering Expects pipe(7)With shell(5)It is connected;
The rabbling mechanism(2)Including tank body(9), asessory shaft(10), main shaft(11), equipment gear(12), travelling gear(13) And stepper motor(14), the tank body(9)Upper end is provided with stepper motor(14), the stepper motor(14)Lower end is provided with main shaft (11), the main shaft(11)Side is provided with asessory shaft(10), the asessory shaft(10)It is provided with equipment gear(12), it is described auxiliary Help gear(12)The inner is provided with travelling gear(13), the travelling gear(13)It is arranged on main shaft(11)On, the tank body(9) Inside is provided with asessory shaft(10), main shaft(11), equipment gear(12)And travelling gear(13), the travelling gear(13)With it is auxiliary Help gear(12)Carry out gear engagement, the tank body(9)Left end is provided with shell(5);
The discharge mechanism(3)Including connecting pipe(15), rotary shaft(16), vertical duct(17), angular wheel one(18), cone Shape gear two(19), double helix ribbon blender bar(20), spiral heat conducting pipe(21)And horizontal pipeline(22), the connecting tube Road(15)Lower end is provided with vertical duct(17), the vertical duct(17)Right-hand member is provided with horizontal pipeline(22), the transverse pipe Road(22)Outer end is provided with spiral heat conducting pipe(21), the horizontal pipeline(22)Inside is provided with double helix ribbon blender bar (20), the double helix ribbon blender bar(20)Left end is provided with angular wheel two(19), the angular wheel two(19)Left end is pacified Equipped with angular wheel one(18), the angular wheel one(18)Upper end is provided with rotary shaft(16), the rotary shaft(16), conical tooth Wheel one(18)And angular wheel two(19)It is installed in vertical duct(17)Inside, the connecting pipe(15)It is arranged on tank body (9)Right-hand member.
A kind of 2. reaction unit of preparation of industrialization functionalization graphene according to claim 1, it is characterised in that:It is described Shell(5)Lower end is provided with bracing piece, and bracing piece is fixed on tank body(9)Left end, the shell(5)Pass through bracing piece and tank body (9)It is connected.
A kind of 3. reaction unit of preparation of industrialization functionalization graphene according to claim 1, it is characterised in that:It is described Feed pipe(7)And snap joint(8)At least two are equipped with, at least two feed pipes(7)It is equidistantly mounted on shell(5) Upper end, the feed pipe(7)On switch valve and flowmeter are installed.
A kind of 4. reaction unit of preparation of industrialization functionalization graphene according to claim 1, it is characterised in that:It is described Tank body(9)Lower end is provided with equipment all-in-one, and equipment all-in-one includes ultrasonic device and condensing plant etc..
A kind of 5. reaction unit of preparation of industrialization functionalization graphene according to claim 1, it is characterised in that:It is described Asessory shaft(10)And equipment gear(12)Two are equipped with, the equipment gear(12)It is symmetrically mounted on travelling gear(13)It is left Right both ends, the asessory shaft(10)And main shaft(11)On be mounted at least two paddles.
A kind of 6. reaction unit of preparation of industrialization functionalization graphene according to claim 1, it is characterised in that:It is described Connecting pipe(15)On valve, the rotary shaft are installed(16)On be uniformly provided with least two flabellums, the angular wheel one (18)With angular wheel two(19)Carry out gear engagement, the horizontal pipeline(22)Right-hand member is provided with low temperature water bath, double spiral shells Revolve ribbon blender bar(20)Pass through bearing and vertical duct(17)It is connected, the rotary shaft(16)With vertical duct(17)Pass through Bearing is connected.
CN201711049850.0A 2017-10-31 2017-10-31 Reaction device for industrially preparing functionalized graphene Pending CN107597051A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108636565A (en) * 2018-07-23 2018-10-12 扬州市政兴树脂有限公司 A kind of screw resin feeding agitating device
CN108927090A (en) * 2018-05-25 2018-12-04 湖北省联投生物科技股份有限公司 A kind of amino acid extraction neutralization device
CN112643919A (en) * 2019-10-12 2021-04-13 西安新三力汽车零部件有限公司 Dispersion devices of graphene in unsaturated polyester resin

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CN206295861U (en) * 2016-12-26 2017-07-04 重庆市永川区新泰防水材料有限公司 A kind of water-repellent paint agitator tank
CN107008199A (en) * 2017-04-17 2017-08-04 上海电信工程有限公司 A kind of Additive Production raw material evenly mixing device
CN207430290U (en) * 2017-10-31 2018-06-01 电子科技大学中山学院 Reaction device for industrially preparing functionalized graphene

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Publication number Priority date Publication date Assignee Title
EP2078897A2 (en) * 2008-01-10 2009-07-15 KWB - Kraft und Wärme aus Biomasse Gesellschaft m.b.H. Discharge system
CN204380550U (en) * 2014-12-11 2015-06-10 龙鳞丰 A kind of Horizontal type mixer mixed
CN205066486U (en) * 2015-10-21 2016-03-02 上饶市广丰区方正非矿开发有限公司 Heat recovery who uses in black talc production utilizes system
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CN106362622A (en) * 2016-12-01 2017-02-01 苏州金泉新材料股份有限公司 Color paste stirring device
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Publication number Priority date Publication date Assignee Title
CN108927090A (en) * 2018-05-25 2018-12-04 湖北省联投生物科技股份有限公司 A kind of amino acid extraction neutralization device
CN108636565A (en) * 2018-07-23 2018-10-12 扬州市政兴树脂有限公司 A kind of screw resin feeding agitating device
CN112643919A (en) * 2019-10-12 2021-04-13 西安新三力汽车零部件有限公司 Dispersion devices of graphene in unsaturated polyester resin

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