CN206082401U - Graphite alkene thick liquids integration disperse system - Google Patents
Graphite alkene thick liquids integration disperse system Download PDFInfo
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- CN206082401U CN206082401U CN201621015159.1U CN201621015159U CN206082401U CN 206082401 U CN206082401 U CN 206082401U CN 201621015159 U CN201621015159 U CN 201621015159U CN 206082401 U CN206082401 U CN 206082401U
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- pipeline
- temperature adjustment
- pipe
- integration
- ultrasonic wave
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Abstract
The utility model discloses a graphite alkene thick liquids integration disperse system. Including ball mill, first transfer cauldron, sand mill, second transfer cauldron and ultrasonic dispersion device, the discharge gate of ball mill is through first pipe connection the feed inlet of first transfer cauldron, the discharge gate of first transfer cauldron passes through the second pipe connection the feed inlet of sand mill, the discharge gate of sand mill pass through the third pipeline with the feed inlet of second transfer cauldron is connected, the discharge gate of second transfer cauldron passes through fourth pipe connection ultrasonic dispersion device, all be equipped with the diaphragm pump in first pipeline, second pipeline and the fourth pipeline. The utility model provides a graphite alkene thick liquids integration disperse system solves the problem that the current high solid content graphite alkene thick liquids of high viscosity dispersion is with high costs, thick liquids are inhomogeneous, dispersion efficiency is not high.
Description
Technical field
The utility model is related to chemical field, more particularly to a kind of Graphene slurry integration decentralized system.
Background technology
Graphene（Graphene）Be it is a kind of by carbon atom with sp2 hydridization Gui Dao Group into hexangle type in honeycomb lattice plane
Film, only a Ge carbon atom thickness bis- Victoria materials.It is but also most hard nano material that Graphene is currently world most thin,
It is almost fully transparent, only absorb 2.3% light；Heat conduction system Number Gao Da 5300W/m, higher than CNT and diamond, under normal temperature its
Electron mobility is more than 15000cm2/Vs and higher than CNT or silicon crystal, and resistivity only about 10-8 Ω/m, than copper or
Silver is lower, and the material grapheme material for being world resistivity minimum is a kind of two-dimensional material, its excellent physics and architectural characteristic
It is made in electronics, sensing and photoelectric device etc. is multi-field shows outstanding application potential.Existing grapheme material is adopted mostly
Prepared with oxidation-reduction method.The advantages of oxidation-reduction method prepares grapheme material and has simple to operate, product machinability is good,
But the stability of product is poor.
Existing graphene dispersion equipment generally comprises following two：
（1）Ultrasonic wave dispersing apparatus：Laboratory scale, low-viscosity media dispersed graphite alkene are especially suitable for, for middle and high viscous
Can be restricted during degree medium.
（2）Grinding distribution equipment：It is adapted to dispersed graphite alkene on a large scale, middle viscous media dispersed graphite alkene.
Therefore, the dispersing apparatus that neither one is adapted to high viscosity high solids content Graphene slurry are up to the present gone back.
Application number 201320763674.8 discloses a kind of duplex dosing mixing plant of multi-layer graphene slurry, described many
The duplex dosing mixing plant of layer graphene slurry is exclusively used in dosing, agitation grinding slurry etc., and it mainly includes：Duplex is stirred
Bucket, disturbing flow device, agitating device, delivery pump, conveyance conduit, support and control system etc..The equipment is unsuitable for high viscosity Gao Gu
Content Graphene slurry.
Application number 201520858922.6 discloses a kind of agitating device of industrial Graphene slurry, and annular reaction kettle sets
Double-deck loop configuration is set to, annular incubation cavity is provided with the inner barn wall of internal layer annular reaction kettle, the surrounding of annular reaction kettle sets
Charging aperture is put, temperature sensor and several is arranged at intervals with charging aperture " W " shape structure blanking chamber, " W " shape structure blanking bottom of chamber
Two of portion converge lower end of duct and are provided with ring rotation disk, and spirality paddle, ring are provided with the inwall of ring rotation disk
Shape rotating disk lower end connects the feed opening of cone structure, and the lateral wall of ring rotation disk is provided with driven gear, driven gear and
Driving gear connects, and driving gear takes full advantage of the space of reactor by motor control.But, the device is viscous for high
The degree dispersion effect of Graphene or undesirable.
Utility model content
For above-mentioned technical problem, the utility model proposes a kind of Graphene slurry integration decentralized system, solves existing
High viscosity high solids content Graphene slurry dispersion high cost, slurry are uneven, solid content is low, the not high problem of dispersion efficiency.
In order to realize above-mentioned technical purpose, the concrete technical scheme that the utility model is adopted is as follows：
A kind of Graphene slurry integration decentralized system, including ball mill, the first transfer kettle, sand mill, the second transfer kettle
And ultrasonic wave distributing device, the discharging opening of the ball mill connects the charging aperture of the first transfer kettle by the first pipeline,
The discharging opening of the first transfer kettle connects the charging aperture of the sand mill by second pipe, and the discharging opening of the sand mill leads to
Cross the 3rd pipeline to be connected with the charging aperture of the second transfer kettle, the discharging opening of the second transfer kettle is connected by the 4th pipeline
Ultrasonic wave distributing device, in first pipeline, second pipe and the 4th pipeline membrane pump is equipped with；The ultrasonic wave distributing
Put including：Ultrasonic generating mechanism, dispersing chamber and rabbling mechanism；The ultrasonic wave vibration plate of the ultrasonic generating mechanism and the dispersing chamber
Outer surface contact；The dispersing chamber includes shell and interior room, the interior room is formed with dispersion chamber, and the rabbling mechanism is stirred
Mix bar to extend in the dispersion chamber；Also include the first temperature sensor, control module and temperature adjustment pipe；First TEMP
Device is arranged in the dispersion chamber；The temperature adjustment pipe is arranged at interior room periphery, temperature adjustment pipe be provided with temperature adjustment water inlet tube mouth and
Temperature adjustment pipe delivery port, the temperature adjustment water inlet tube mouth passes sequentially through pipeline, water pump, storage tank and is connected with water tap, running water
Tap is provided with the first magnetic valve, and second temperature sensor, heater are provided with storage tank, sets on the temperature adjustment pipe delivery port
There is the second magnetic valve；The membrane pump.Ultrasonic generating mechanism, the stirring motor of rabbling mechanism, water pump, the first temperature sensor,
Second temperature sensor, the first magnetic valve, the second magnetic valve and heater are connected with control module control, and described first
Pipeline, second pipe, the 3rd pipeline and the 4th pipeline are anticorrosion pipeline, comprising pipeline body, anti-corrosion layer；The pipe
Road is originally provided with vivo fluid passage；The inwall of the fluid passage equably arranges fluted；The anti-corrosion layer is arranged on
The inwall of fluid passage, and insert in groove.
The groove is linearly arranged.
The groove is arranged in the shape of a spiral.
Bottom of the opening portion of the groove less than groove.
The anti-corrosion layer is made up of fluoroplastics.
It is formed between the shell and the interior room and accommodates the areas of dielectric for conducting liquid medium for ultrasonic wave.
The beneficial effects of the utility model are：
Have the effect that compared with prior art：First, this method carried out using ball milling method it is pre-dispersed, can be by graphite
Alkene powder is uniform with solvent, dispersant, then slurry is further disperseed by way of sand milling, finally using ultrasonic wavelength-division
Dissipate, the whole dispersion process of the utility model device realizes full automation using control module control, can efficiently, stably
Dispersion obtains Graphene.
Pipeline in the utility model adopts anticorrosion pipeline；On the inwall of the fluid passage in pipeline body equably
Arrange fluted；The anti-corrosion layer is arranged on the inwall of fluid passage, and inserts in groove, so that anti-corrosion layer is more steady
Gu, difficult for drop-off, especially the groove is arranged in shape of threads, because groove is not parallel with the center line of fluid passage, is used
When, anti-corrosion layer is difficult entirety and integrally comes off with the flow direction of fluid；Further, bottom of the opening portion of the groove less than groove
Portion, can prevent radial direction of the anti-corrosion layer along fluid passage from coming off；The utility model simple structure, anti-corrosion layer is difficult for drop-off.
Description of the drawings
Fig. 1 is a kind of Graphene slurry integration decentralized system structural representation of the utility model；
Wherein, 1. ball mill；2. the first transfer kettle；3. sand mill；4. the second transfer kettle；5. ultrasonic wave distributing device；
51. ultrasonic wave vibration plates；5231. import；5232. outlet；52. dispersing chambers；521. shell；522. areas of dielectric；523. interior room；
524. heat-insulation layer；53. rabbling mechanisms；54. temperature sensors；55. feed pipes；56. temperature adjustment pipes；561. temperature adjustment water inlet tube mouths；
562. temperature adjustment pipe delivery ports；57. telescoping mechanisms；6. membrane pump；
Fig. 2 is the structural representation of anticorrosion pipeline；
Wherein, 701. pipeline body；702. fluid passage；703. groove；704. anti-corrosion layer.
Specific embodiment
Embodiment of the present utility model is elaborated below in conjunction with the accompanying drawings, the present embodiment is with the utility model technical side
Premised on case, detailed embodiment and specific operating process are given, but protection domain of the present utility model is not limited to down
The embodiment stated.
Embodiment one
Fig. 1 is referred to, Fig. 1 is a kind of structural representation of Graphene slurry integration decentralized system of the present utility model.
As shown in figure 1, a kind of Graphene slurry integration decentralized system, including ball mill, the first transfer kettle, sand mill,
Second transfer kettle and ultrasonic wave distributing device, the discharging opening of the ball mill connects the first transfer kettle by the first pipeline
Charging aperture, the discharging opening of the first transfer kettle connects the charging aperture of the sand mill, the sand mill by second pipe
Discharging opening be connected with the charging aperture of the second transfer kettle by the 3rd pipeline, the discharging opening of the second transfer kettle is by the
The ultrasonic wave distributing device of four pipelines connection, in first pipeline, second pipe and the 4th pipeline membrane pump is equipped with；It is described super
Sound wave dispersal device includes：Ultrasonic generating mechanism, dispersing chamber and rabbling mechanism；The ultrasonic wave vibration plate of the ultrasonic generating mechanism with
The outer surface of the dispersing chamber contacts；The dispersing chamber includes shell and interior room, and the interior room is formed with dispersion chamber, described to stir
The puddler for mixing mechanism is extended in the dispersion chamber；Also include the first temperature sensor, control module and temperature adjustment pipe；Described
One temperature sensor is arranged in the dispersion chamber；The temperature adjustment pipe is arranged at the interior room periphery, and temperature adjustment pipe is provided with temperature adjustment
Water inlet tube mouth and temperature adjustment pipe delivery port, the temperature adjustment water inlet tube mouth passes sequentially through pipeline, water pump, storage tank with water tap phase
Even, water tap is provided with the first magnetic valve, second temperature sensor, heater, the temperature adjustment pipe is provided with storage tank
Delivery port is provided with the second magnetic valve；The membrane pump.It is ultrasonic generating mechanism, the stirring motor of rabbling mechanism, water pump, first warm
Degree sensor, second temperature sensor, the first magnetic valve, the second magnetic valve and heater connect with control module control
Connect, first pipeline, second pipe, the 3rd pipeline and the 4th pipeline are anticorrosion pipeline, comprising pipeline body, corrosion resistant
Erosion layer；Fluid passage is provided with the pipeline body；The inwall of the fluid passage equably arranges fluted；The corrosion resistant
Erosion layer is arranged on the inwall of fluid passage, and inserts in groove.
Used as the further improvement of technical solutions of the utility model, the groove is linearly arranged.
Used as the further improvement of technical solutions of the utility model, the groove is arranged in the shape of a spiral.
Used as the further improvement of technical solutions of the utility model, the opening portion of the groove is less than the bottom of groove.
Used as the further improvement of technical solutions of the utility model, the anti-corrosion layer is made up of fluoroplastics.
As the further improvement of technical solutions of the utility model, receiving is formed between the shell and the interior room and is used
The areas of dielectric of liquid medium is conducted in ultrasonic wave.
The use process of above-mentioned process units is as follows：
The top of ball mill 1 is provided with dog-house, and by dog-house solvent and dispersant are first put into, and first ball milling disperses dispersion liquid, then
Graphene powder is put into by dog-house, ball milling dispersion a period of time, mixture is well mixed；Will by membrane pump 6 on ball mill 1
Material is evacuated in the first transfer kettle 2, and material in first transfer kettle 2 is evacuated in sand mill 3 by membrane pump 6 on sand mill 3 carried out
Sand milling, the material after sand milling is beaten into the second transfer kettle 4, and period controls the rotating speed of sand mill 3 and material flow (pump speed)
To control jitter time, membrane pump 6 is equipped with by the second transfer kettle 3 after the completion of dispersion material is evacuated to into ultrasonic wave distributing device 5
In further disperseed, the ultrasonic wave distributing device 5 includes：Ultrasonic generating mechanism, dispersing chamber 52 and rabbling mechanism；It is described
The ultrasonic wave vibration plate 51 of ultrasonic generating mechanism contacts with the outer surface of the dispersing chamber 52；The dispersing chamber 52 include shell and
Interior room, the interior room is formed with dispersion chamber, and the puddler of the rabbling mechanism is extended in the dispersion chamber；Also include that first is warm
Degree sensor, control module and temperature adjustment pipe 56；First temperature sensor is arranged in the dispersion chamber, for disperseing chamber
The temperature of interior stirring material carries out real-time detection；The temperature adjustment pipe is arranged at the interior room periphery, and temperature adjustment pipe is provided with temperature adjustment pipe
Water inlet 561 and temperature adjustment pipe delivery port 562, the temperature adjustment water inlet tube mouth 561 passes sequentially through pipeline and storage tank 57 and running water
Tap is connected, and water tap is provided with the first magnetic valve, storage tank 57 and is provided with second temperature sensor and heater, institute
State temperature adjustment pipe delivery port 562 and be provided with the second magnetic valve；The first temperature threshold and second are previously provided with the control module
Temperature threshold, the dispersion chamber temperature that first temperature sensor is transmitted is compared with the first temperature threshold, if dispersion chamber temperature
More than the first temperature threshold, then start and water pump, make the cold water in storage tank enter temperature adjustment pipe, to the cooling of dispersion chamber, work as dispersion
When chamber temperature is less than the first temperature threshold, water storage cavity inner heating device is opened, heater is by water temp. heating in storage tank to the
When two temperature thresholds are interval, control module control heater stop heating, and while the second magnetic valve of unlatching and water pump, one side
Cold water in temperature adjustment pipe is released by the second magnetic valve, while increasing identical with second temperature threshold value into temperature adjustment pipe by water pump
The water of water temperature, so that dispersion chamber remains at certain temperature range, dispersion effect is more preferable；In order that material in dispersion chamber
Preferably dispersion and thermally equivalent effect are further obtained, also including telescoping mechanism, the telescoping mechanism is rotated under state
Rabbling mechanism dispersion chamber in upper and lower reciprocating motion, the telescoping mechanism include be connected to motor top expansion link and
The power set on expansion link top are connected to, the power set are connected with control module control.
Claims (6)
1. a kind of Graphene slurry integration decentralized system, is characterized in that：Including ball mill, the first transfer kettle, sand mill, second
Transfer kettle and ultrasonic wave distributing device, the discharging opening of the ball mill connects entering for the first transfer kettle by the first pipeline
Material mouth, the discharging opening of the first transfer kettle connects the charging aperture of the sand mill by second pipe, and the sand mill goes out
Material mouth is connected by the 3rd pipeline with the charging aperture of the second transfer kettle, and the discharging opening of the second transfer kettle is by the 4th pipe
The ultrasonic wave distributing device of road connection, in first pipeline, second pipe and the 4th pipeline membrane pump is equipped with；The ultrasonic wave
Dispersal device includes：Ultrasonic generating mechanism, dispersing chamber and rabbling mechanism；The ultrasonic wave vibration plate of the ultrasonic generating mechanism with it is described
The outer surface of dispersing chamber contacts；The dispersing chamber includes shell and interior room, and the interior room is formed with dispersion chamber, the mixer
The puddler of structure is extended in the dispersion chamber；Also include the first temperature sensor, control module and temperature adjustment pipe；Described first is warm
Degree sensor is arranged in the dispersion chamber；The temperature adjustment pipe is arranged at the interior room periphery, and temperature adjustment pipe is provided with temperature adjustment pipe and enters
The mouth of a river and temperature adjustment pipe delivery port, the temperature adjustment water inlet tube mouth passes sequentially through pipeline, water pump, storage tank and is connected with water tap,
Water tap is provided with the first magnetic valve, and second temperature sensor, heater, the temperature adjustment pipe water outlet are provided with storage tank
Mouth is provided with the second magnetic valve；The membrane pump, ultrasonic generating mechanism, the stirring motor of rabbling mechanism, water pump, the first temperature are passed
Sensor, second temperature sensor, the first magnetic valve, the second magnetic valve and heater are connected with control module control, institute
State the first pipeline, second pipe, the 3rd pipeline and the 4th pipeline and be anticorrosion pipeline, comprising pipeline body, anti-corrosion layer；
Fluid passage is provided with the pipeline body；The inwall of the fluid passage equably arranges fluted；The anti-corrosion layer
The inwall of fluid passage is arranged on, and is inserted in groove.
2. Graphene slurry integration decentralized system according to claim 1, is characterized in that：The groove linearly sets
Put.
3. Graphene slurry integration decentralized system according to claim 1, is characterized in that：The groove sets in the shape of a spiral
Put.
4. Graphene slurry integration decentralized system according to claim 1, is characterized in that：The opening portion of the groove is little
In the bottom of groove.
5. Graphene slurry integration decentralized system according to claim 1, is characterized in that：The anti-corrosion layer is moulded by fluorine
Material is made.
6. Graphene slurry integration decentralized system according to claim 1, is characterized in that：The shell and the interior room
Between be formed with accommodate for ultrasonic wave conduct liquid medium areas of dielectric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621015159.1U CN206082401U (en) | 2016-08-31 | 2016-08-31 | Graphite alkene thick liquids integration disperse system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621015159.1U CN206082401U (en) | 2016-08-31 | 2016-08-31 | Graphite alkene thick liquids integration disperse system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206082401U true CN206082401U (en) | 2017-04-12 |
Family
ID=58477867
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621015159.1U Expired - Fee Related CN206082401U (en) | 2016-08-31 | 2016-08-31 | Graphite alkene thick liquids integration disperse system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206082401U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021102825A1 (en) * | 2019-11-28 | 2021-06-03 | 谢建光 | Graphene dispersion device |
-
2016
- 2016-08-31 CN CN201621015159.1U patent/CN206082401U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021102825A1 (en) * | 2019-11-28 | 2021-06-03 | 谢建光 | Graphene dispersion device |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170412 Termination date: 20180831 |
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| CF01 | Termination of patent right due to non-payment of annual fee |