CN107596319A - Massage herbal medicine ball and preparation method thereof - Google Patents
Massage herbal medicine ball and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of massage herbal medicine ball and preparation method thereof, the massage includes ball handle portion and ball body part with herbal medicine ball, ball body is formed by herbal medicine by gauze wrapped, the useful load of herbal medicine is 50 200g/ herbal medicine balls, and the herbal medicine includes lemon grass extract, purple ginger, orange peel, salt, Radix Curcumae extract, tamarind, turmeric, trifoliate jewelvine extract, buchanan cryptolepis root extract, galangal rhizome extract, Ginger P.E, camphor, thorn stamen grass extract.Herbal medicine ball is used in massage of the present invention, and by fumigation, the position of myalgia and swelling directly on skin is massaged, blood flow can be strengthened, alleviate myalgia, reduce swelling and muscle cramp, there is anti-inflammatory, hemostasis, analgesia, beauty, health care, the effect of calming the nerves.
Description
Technical field
The present invention relates to herbal medicine technical field, and in particular to one kind massage herbal medicine ball and preparation method thereof.
Background technology
Early in ancient Chinese, medicinal herbs bag is just entered cloth bag by people, is sewn into medicinal herbs bag, for mosquito expelling, smokes clothes, this
Not only have no side effect but also very environmentally friendly.
The patent of invention of Application No. 201510040752.5 discloses a kind of medium-height grass pack, by the original of following weight proportion
Material is made：Sword bean 700-1200 parts, chestnut 1000-1300 parts, black soya bean 600-800 parts, rhizoma zingiberis 800-1200 parts, moxa 500-900
Part, lycopodium calvatum 700-1000 parts, teasel root 400-800 parts, rhizoma homalonemae 600-900 parts, salt 1000-1200 parts, bark of eucommia 600-900
Part, root of Chinese clematis 800-1200 parts and dragon's blood 600-1000 parts.Chinese medicine preparation of the present invention by it is a variety of have nourishing, pain of alleviation,
Wind-expelling pain-stopping, promoting blood circulation and removing blood stasis, the medicinal material combination that strengthens muscles and bones and other effects, play the synergy of each raw material, medium-height grass pack are made,
Using warming and activating meridian as principle, closed for the void six of human body three, venting QI-blood, correction sun, normal circulation of qi and blood can be so made one, to neck lumbar vertebrae disease
Disease, sciatica, scapulohumeral periarthritis, old stomach cold, kidney deficiency waist is wet, palace cold dysmenorrhoea, the symptom such as mammary gland disease lobular hyperplasia, can see in time
Effect.
Herbal medicine ball includes plurality of herbal elite, after reeky herbal medicine ball and skin contact, rapidly opens pore, grass
The elite of medicine directly penetrates into cortex and muscle and muscle connective tissue of releiving, reaches and exclude vivotoxin, alleviate muscle therewith
Bone, make general joint more it is movable freely, and mitigate muscle pain and improve blood circulation, strengthen autoimmunity ability the effect of.
It is to excessive fatigue, muscle and joint pain, skin sensitivity, nervous disorder, pressure is overweight, headache is murky, endocrinopathy, stomach
Gastral cavity inflatable, intestines, which buy constipation, insomnia, poor sleep and asthma etc., the effect of highly significant, especially have to postpartum women wind-dispelling,
The effect dried and invigorated blood circulation.
The content of the invention
The present invention seeks to what is be achieved through the following technical solutions：
One of technical problems to be solved by the invention are to provide a kind of massage herbal medicine ball.
The invention discloses a kind of massage herbal medicine ball, including ball handle portion and ball body part, ball body part be play by
The effect to rub with health care, ball handle portion are hand-held for the convenience of the users；Ball handle portion and ball body part can use physics side
Formula, such as paste, bundle, rivet mode connects.
Ball body is formed by herbal medicine by gauze wrapped, and the useful load of herbal medicine is 50-200g/ herbal medicine ball, and the herbal medicine includes
Lemon grass extract, purple ginger, orange peel, salt, Radix Curcumae extract, tamarind, turmeric, trifoliate jewelvine extract, buchanan cryptolepis root extraction
Thing, galangal rhizome extract, Ginger P.E, camphor, thorn stamen grass extract.
Specifically, the herbal medicine forms according to the following ratio：Lemon grass extract 20-30wt%, purple ginger 30-40wt%,
Orange peel 10-15wt%, salt 3-7wt%, Radix Curcumae extract 2-5wt%, tamarind 2-5wt%, turmeric 2-5wt%, trifoliate jewelvine
Extract 1-2wt%, buchanan cryptolepis root extract 1-2wt%, galangal rhizome extract 1-2wt%, Ginger P.E 1-2wt%, camphor
0.5-1.5wt%, thorn stamen grass extract 0.5-1.5wt%.
The preparation process of the galangal rhizome extract is：Galangal extract part is crushed, 40-60 mesh sieves is crossed, obtains powder
End；By powder and extraction solvent with solid-to-liquid ratio 1：(10-15) (g/mL) is well mixed, and 1.5-5 hours are extracted in 90-100 DEG C,
Obtain extract solution；Extract solution is concentrated into 3-4 hours under conditions of 50-60 DEG C, vacuum 0.06-0.07MPa, concentrated
Liquid；Water and petroleum ether, extraction are added into concentrate, concentrate is 1 with the volume ratio of water and petroleum ether：(0.5-0.8)：(1-
2) petroleum ether phase, is collected；Petroleum ether is mutually dried into 5-10 hours under conditions of 50-60 DEG C, vacuum 0.06-0.07MPa, obtained
To galangal rhizome extract.Wherein, the extraction with solvent can be water, volume fraction be 80-95% ethanol waters, methanol,
One kind in ethyl acetate, ether.
The galangal extract part is the one or more in rhizome, flower, fruit, ground cauline leaf.
In the prior art during galangal rhizome extract is prepared, generally ground leaves and stemses point are removed, only with root
Stem is as extract part.But in fact, the ground leaves and stemses of galangal point contain Galangin, Galangin -3- methyl ethers, Himalayan pine
Element, dihydro galangal alcohol and Kaempferol isoreactivity material, these active materials have the function of reducing anti-oxidant reduction blood glucose.
Inventor passes through exploration discovery, and when preparing galangal rhizome extract, galangal rhizome part and the distribution conjunction of ground leaves and stemses are made
With being extracted, obtained galangal rhizome extract effect is more excellent.
In some technical schemes of the present invention, the ball body gauze is commercially available natural cotton gauze.
In some technical schemes of the present invention, the ball body is with the gauze that gauze is that area load has compound particle.
Described compound particle is essential oil/polymer composite particle, SiO2Or modified SiO2In/essential oil/polymer composite particle
One kind or composition.
It is with the concrete operations of load compound particle on gauze in ball body：Compound particle and polyethylene glycol are added to compound
In the deionized water that 20 times of particle weight, wherein polyethylene glycol weight is 5 times of compound particle, is stirred with 400 revs/min of rotating speed
Mix 30 minutes, obtain dressing liquid；Gauze is boiled 2 hours in 100 DEG C of water, dried 7 hours in 80 DEG C, the yarn after being dried
Cloth；Gauze after drying is immersed in dressing liquid, the solid-to-liquid ratio of gauze and dressing liquid is 1：80 (g/mL), pass through roller printing
Two pressurization rod extruding wet gauzes of machine, the gauze after being arranged；By the gauze after arrangement in 50 DEG C, vacuum 0.07MPa
Under conditions of dry 6 hours, obtain load compound particle gauze.
The preparation process of the essential oil/polymer composite particle is：Essential oil and monomer are well mixed, essential oil and monomer
Mass ratio is (0.04-0.07)：1, monomer is methyl methacrylate and n-butyl acrylate using mol ratio as 1：(1.5-2) is mixed
The mixture formed is closed, 8-15 minutes are stirred with 800-1000 revs/min of rotating speed；Then add hexadecane and initiator
AIBN, hexadecane are the 2.5-5% of monomer mass, and AIBN is the 1.5-4% of monomer mass, is mixed to get oil phase；By allyl oxygen
Base nonyl phenol ether ammonium sulfate salt is dissolved into deionized water, obtains aqueous phase；Under 300-500 revs/min of mixing speed, by oil
It is added in aqueous phase, the solid-to-liquid ratio of monomer and deionized water is (5-8)：10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate
Salt is the 20-30% of monomer mass；Then 10-20 minutes are stirred with 7000-8000 revs/min of rotating speed, obtains emulsion；By breast
After liquid is ultrasonically treated 10-15 minutes using ultrasonic cell disruptor under conditions of ultrasonic power 300-400W, in 70-75 DEG C
React 120-160 minutes；After the completion of reaction, reaction solution is cooled to 20-30 DEG C, centrifuged with 7000-9000 revs/min of rotating speed
20-30 minutes, supernatant is abandoned, collect bottom precipitation；By bottom precipitation in 50-60 DEG C, vacuum 0.06-0.08MPa condition
Lower dry 10-15 hours, obtain essential oil/polymer composite particle.
The SiO2Or modified SiO2The preparation process of/essential oil/polymer composite particle is：By SiO2Or modified SiO2, essence
Oil and monomer are well mixed, SiO2Or modified SiO2, essential oil and monomer mass ratio be (0.012-0.018)：(0.04-0.07)：
1, monomer is methyl methacrylate and n-butyl acrylate using mol ratio as 1：The mixture that (1.5-2) is mixed, with
800-1000 revs/min of rotating speed stirring 8-15 minutes；It is monomer mass then to add hexadecane and initiator A IBN, hexadecane
2.5-5%, AIBN be monomer mass 1.5-4%, be mixed to get oil phase；Allyloxy nonyl phenol ether ammonium sulfate salt is dissolved
Into deionized water, aqueous phase is obtained；Under 300-500 revs/min of mixing speed, oil phase is added in aqueous phase, monomer with
The solid-to-liquid ratio of deionized water is (5-8)：10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate salt are the 20-30% of monomer mass；
Then 10-20 minutes are stirred with 7000-8000 revs/min of rotating speed, obtains emulsion；Emulsion is used into ultrasonic cell disruptor
After being ultrasonically treated 10-15 minutes under conditions of ultrasonic power 300-400W, 120-160 minutes are reacted in 70-75 DEG C；React
Cheng Hou, reaction solution is cooled to 20-30 DEG C, 20-30 minutes are centrifuged with 7000-9000 revs/min of rotating speed, abandon supernatant, are received
Collect bottom precipitation；Bottom precipitation is dried into 10-15 hours under conditions of 50-60 DEG C, vacuum 0.06-0.08MPa, obtained
SiO2Or modified SiO2/ essential oil/polymer composite particle.
The modified SiO2Preparation process be：By SiO2With absolute ethyl alcohol with solid-to-liquid ratio 1：(3-5) (g/mL) is mixed, and is added
Enter deionized water, the volume ratio of absolute ethyl alcohol and deionized water is (10-12)：1, it is well mixed, obtains mixed liquor；Using quality
Fraction is that 20-25% ammoniacal liquor adjusts the pH to 9.0 of mixed liquor, and it is even that silane is added under 200-300 revs/min of stirring action
Join agent KH-570, SiO2Mass ratio with KH-570 is (6-7)：1, react 12-24 hours in 23-25 DEG C；By reaction solution with
4000-5000 revs/min of rotating speed centrifugation 15-20 minutes, collect bottom precipitation；Bottom precipitation is washed with deionized, bottom
It is 1 that portion, which is precipitated with the solid-to-liquid ratio of deionized water,：(300-400) (g/mL), in 50-55 DEG C, vacuum 0.07-0.08MPa bar
8-10 hours are dried under part, obtain being modified SiO2。
During compound particle is prepared, the essential oil is litsea cubeba oil, one kind in rhizome of chuanxiong essential oil or composition.
Preferably, the essential oil is the mixture of litsea cubeba oil and rhizome of chuanxiong essential oil, the wherein quality of litsea cubeba oil and rhizome of chuanxiong essential oil
Than for (3-4)：1.
The preparation of compound particle uses miniemulsion method in the present invention, and obtained compound particle particle is very tiny, reaches and receives
Meter level, therefore do not interfere with the comfort of gauze.And the form for the compound particle emulsion particle being prepared, it is easier to firmly inhale
Gauze surface is attached to, stability is also preferable.
The two of the technical problems to be solved by the invention are to provide a kind of preparation method of massage herbal medicine ball, including following
Step：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40-60 mesh sieves；
S2 batch mixings：Herbal raw material is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 3-5 under conditions of microwave power 200-240KW, microwave frequency 915-2450MHz
Minute；
S4 is filled：By the compound gauze wrapped after sterilizing, ball body is formed, is then attached with ball handle.
Massage of the present invention is with the application method of herbal medicine ball：By massage herbal medicine ball steamed, then take out, every
Clothing to be pressed on human body.Concrete operations are：
S1 takes out herbal medicine ball, immersion 5-15 minutes in water is put it into, to soak herbal medicine ball；
Herbal medicine ball is put into steamer by S2, steams 5-10 minutes, and the effect of making herbal medicine evaporates completely, while avoids herbal medicine
Effect is damaged；
S2 takes out the massage ball of heating, shank position of holding the puck, in ball body outer wrapping towel, with ball body it is not only light across clothing but also
Put ache position or each acupuncture point back and forth soon；
S3 is removed towel, body part massaged using herbal medicine ball, directly when careless ball ball temperature is down to 40-50 DEG C
20-25 DEG C is cooled to herbal medicine ball；
Herbal medicine ball packaging bags or preservative film parcel of the S4 by cooling, it is standby to be placed in 0-2 DEG C of preservation.
When herbal medicine useful load is 100-200g/ herbal medicine balls, the herbal medicine ball can be used for shoulder neck, the back of the body that massage is ached for a long time
Portion；When herbal medicine useful load is 50-100g/ herbal medicine balls, the herbal medicine ball can be used for massaging face and belly.
Herbal medicine ball is used in massage of the present invention, and by fumigation, the position of myalgia and swelling directly on skin is entered
Row massage, can strengthen blood flow, alleviate myalgia, reduce swelling and muscle cramp, have anti-inflammatory, hemostasis, analgesia, U.S.
Appearance, health care, the effect of calming the nerves.
Embodiment
Each raw material and introduction of apparatus in embodiment：
Lemon grass (Cymbopogon citratus), English name lemongress, also referred to as lemon grass, it is tropical rosha, originates in Asia, prints
There is this medicinal herbs plant the torrid areas such as degree, Sri Lanka, Indonesia, Africa.Leaf has dense lemon, grey cone
Flower, whole plant gives out refreshing fragrance.Lemon grass extract is purchased from Xi'an Si Nuote biologies Co., Ltd.10g
Lemon grass (Cymbopogon citratus) obtains 1g lemon grass extracts with water extraction.
Purple ginger, Classification system：Zingiberpurpureum Rosc., it is Zingiber (Zingiberaceae) zingiber
(Zingiber) plant, the Dai nationality's name are mended tired.Purple ginger is the Dai nationality's tradition common medicine, has long medication history in the Dai nationality, includes
In pattra leaves scripture, it is used as medicine with rhizome, bitter, pungent, cold in nature, bury tower.Returns spleen, stomach, the heart, lung channel, there is stomach invigorating, help digestion, send out
Table, cold dispelling, preventing or arresting vomiting, promoting the circulation of qi, broken stasis of blood and other effects.Rhizome fresh goods mashes external application, controls redness and swelling of joints heat pain.Given birth to purchased from Yunnan dragon and phoenix paddy
Thing pharmaceutcal corporation, Ltd.
Orange peel, purchased from Long Xiang lemons Specialty Co-operative Organization of Anyue County.
Salt, purchased from Qinghai Lan Hu Chemical Co., Ltd.s.
Root tuber of aromatic turmeric, it is zingiberaceous plant RADIX CURCUMAE Curcuma rcenyujinY, H.Chenet C.Ling, turmeric Curcuma
LongaL., Guangxi zedoary Curcumakwangsiensis S.G.Lee et C.F.Liang or zedoary Curcumapha
Eocaulis Val. dried root.Excavated after winter cauline leaf is withered, remove silt and radicula, steamed or boil to the saturating heart, dry.
Purchased from Xichou County Xiang Guang medicinal materials Co., Ltd.
Tamarind, Classification system：Tamarindus indica, also known as tamarind, tamarind.Return stomach, the heart channel of Hang-Shaoyin.According to《Book on Chinese herbal medicine
Detailed outline》Record, tamarind have quench the thirst disappear heat, help digestion, the function such as nourish the liver to improve visual acuity.Be usually used in treat heatstroke, indigestion, dyspepsia,
Stomachache, chronic gastritis, constipation, hypertension and iron-deficient heart disease.Promote the production of body fluid to quench thirst, disappear pyrolysis heat, refrigerant tasty and refreshing, enjoy endless aftertastes.
Purchased from southern Yao Ying Li tinkling of pieces of jade commerce and trade Co., Ltd.
Turmeric, Classification system:Curcuma longa L., also known as yellow ginger.For zingiberaceous plant turmeric Curcuma longa
L. dry rhizome.Winter cauline leaf is excavated when withered, is cleaned, and is boiled or is steamed to the saturating heart, shines.Turmeric energy promoting the circulation of qi broken stasis of blood, it is inducing meastruation to relieve menalgia.
Cure mainly chest and abdomen swelling and pain, shoulder arm numbness pain, it is pained unbearably, postpartum blood pain, sore tinea is initial, irregular menstruation, amenorrhoea, traumatic injury.It is purchased from
Bozhou City Xin Yuan Chinese medicines Science and Technology Ltd..
Trifoliate jewelvine, Classification system：DerristrifoliataLour..For pulse family China tree Calamus plant trifoliate jewelvine
DerristrifoliataLour..It is used as medicine with complete stool and root-like stock.Trifoliate jewelvine extract is purchased from Xi'an wheatgrass Chemical Co., Ltd..
10g trifoliate jewelvines obtain 1g trifoliate jewelvine extracts with water extraction.
Buchanan cryptolepis root, Classification system：Cryptolepis buchananii Roem.et Schult..It is the white leaf rattan of alias, white
Horse connects saddle.Enter the heart, kidney two warp.Promoting blood circulation, subside a swelling, analgesia.Control bruise wound, fracture, Low Back Pain stomachache, oedema.Buchanan cryptolepis root extract is purchased
From Nanjing Dao Sifu bio tech ltd.10g buchanan cryptolepis roots obtain 1g buchanan cryptolepis root extracts with water extraction.
Galangal, Classification system：RhizomaAlpiniae Galangae.Warm stomach, cold dispelling, promoting qi circulation and relieving pain.Acrid flavour；Property
Temperature.Abundant original herbal trading section is praised purchased from Yulin City Yuzhou District.
Ginger, Classification system：Zingiber officinale Roscoe, it is Zingiber herbaceos perennial ginger
The new fresh quench stem of (Zingiber officinale Roscoe).Ginger P.E is purchased from the limited public affairs of standing grain biotechnology of Lanzhou hundred
Department.10g gingers obtain 1g Ginger P.Es with water extraction.
Camphor, Classification system：Cinnamomumcamphora(L.)PreslLauruscamphoraL..For canella
The branch of camphor tree, dry, leaf and root, through crystalline particulate made from refinement.Purchased from Kai Di daily use chemicals Products Co., Ltd of Zhongshan city.
Pierce stamen grass, Classification system：Pogostemon glaber.Purchased from Hui nationality's Chinese Medicinal Materials Markets.Pierce stamen grass extract
Purchased from Shaanxi Sen Fu natural products Co., Ltd.10g pierces stamen grass and obtains 1g thorn stamen grass extracts with water extraction.
SiO2, purchased from Xin Chuan mining industry Co., Ltd of Guangdong Nanhai, particle diameter is 800-8000 mesh.
Litsea cubeba oil, purchased from perfumery oil Co., Ltd of Ji'an City Asus.
Methyl methacrylate, No. CAS：80-62-6, purchased from Mei Lan industry (Shanghai) Co., Ltd..
N-butyl acrylate, No. CAS：141-32-2, purchased from Nanjing Kang Manlin chemical industry Industrial Co., Ltd..
Hexadecane, No. CAS：15716-08-2, purchased from Guangzhou Wei Bai Chemical Co., Ltd.s.
Initiator A IBN, i.e. azodiisobutyronitrile, No. CAS：78-67-1, researched and developed purchased from Jiangsu Ai Kang biological medicines limited
Company.
Allyloxy nonyl phenol ether ammonium sulfate salt (allyloxy NPE sulfate), i.e. DNS-86, purchase
From Guangzhou double bond trade Co., Ltd.
Ultrasonic cell disruptor, purchased from Hangzhou David's Science ＆ Teaching Instrument Co., Ltd, model JY98-IIIN.
Silane coupling reagent KH-570, purchased from Nanjing Chuan Shi auxiliary chemicals Co., Ltd.
Rhizome of chuanxiong essential oil, purchased from Guangzhou Xuan Yi essence and flavoring agents Co., Ltd.
Cotton gauze, it is purchased from the fragrant gauze Manufacturing Co., Ltd of Baoding bridge one, yarn count 40*40, density 110*94, breadth
156cm, grammes per square metre 120g/m2, plain weave.
Embodiment 1
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal rhizome is crushed, 40 mesh sieves is crossed, obtains powder；By powder
The ethanol water that last and volume fraction is 90% is with solid-to-liquid ratio 1：10 (g/mL) are well mixed, extract 3 hours, obtain in 95 DEG C
Extract solution；Extract solution is concentrated 4 hours under conditions of 60 DEG C, vacuum 0.07MPa, obtains concentrate；Add into concentrate
Enter water and petroleum ether, extract, concentrate is 1 with the volume ratio of water and petroleum ether：0.5：1, collect petroleum ether phase；By petroleum ether phase
Dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa, obtain galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
Embodiment 2
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal ground cauline leaf is crushed, 40 mesh sieves is crossed, obtains powder；
By ethanol water that powder and volume fraction are 90% with solid-to-liquid ratio 1：10 (g/mL) are well mixed, extracted 3 hours in 95 DEG C,
Obtain extract solution；Extract solution is concentrated 4 hours under conditions of 60 DEG C, vacuum 0.07MPa, obtains concentrate；To concentrate
Middle addition water and petroleum ether, extraction, concentrate are 1 with the volume ratio of water and petroleum ether：0.5：1, collect petroleum ether phase；By oil
Ether is mutually dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa, obtains galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
Embodiment 3
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal rhizome and ground cauline leaf are crushed, rhizome and the aerial stem of plant
The mass ratio of leaf is 2：1,40 mesh sieves are crossed, obtain powder；By ethanol water that powder and volume fraction are 90% with solid-to-liquid ratio
1：10 (g/mL) are well mixed, are extracted 3 hours in 95 DEG C, obtain extract solution；By extract solution in 60 DEG C, vacuum 0.07MPa
Under the conditions of concentrate 4 hours, obtain concentrate；Add water and petroleum ether into concentrate, extraction, concentrate and water and petroleum ether
Volume ratio is 1：0.5：1, collect petroleum ether phase；Petroleum ether is mutually dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa,
Obtain galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
Embodiment 4
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal rhizome and ground cauline leaf are crushed, rhizome and the aerial stem of plant
The mass ratio of leaf is 2：1,40 mesh sieves are crossed, obtain powder；By ethanol water that powder and volume fraction are 90% with solid-to-liquid ratio
1：10 (g/mL) are well mixed, are extracted 3 hours in 95 DEG C, obtain extract solution；By extract solution in 60 DEG C, vacuum 0.07MPa
Under the conditions of concentrate 4 hours, obtain concentrate；Add water and petroleum ether into concentrate, extraction, concentrate and water and petroleum ether
Volume ratio is 1：0.5：1, collect petroleum ether phase；Petroleum ether is mutually dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa,
Obtain galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
The cotton gauze is the cotton gauze that area load has litsea cubeba oil/polymer composite particle, wherein the mountain is grey
The preparation process of sub- essential oil/polymer composite particle is：Litsea cubeba oil and monomer are well mixed, litsea cubeba oil, monomer
Mass ratio be 0.06：1, monomer is methyl methacrylate and n-butyl acrylate using mol ratio as 1：2 mix it is mixed
Compound, stirred 12 minutes with 800 revs/min of rotating speed；It is monomer mass then to add hexadecane and initiator A IBN, hexadecane
3%, AIBN be monomer mass 2%, be mixed to get oil phase；Allyloxy nonyl phenol ether ammonium sulfate salt is dissolved into deionization
In water, aqueous phase is obtained；Under 400 revs/min of mixing speed, oil phase is added in aqueous phase, monomer and deionized water are consolidated
Liquor ratio is 7：10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate salt are the 20% of monomer mass；Then with 7000 revs/min
Rotating speed stirs 15 minutes, obtains emulsion；Emulsion is used into ultrasonic cell disruptor ultrasound under conditions of ultrasonic power 300W
After processing 15 minutes, reacted 120 minutes in 70 DEG C；After the completion of reaction, reaction solution is cooled to 25 DEG C, with 7000 revs/min
Rotating speed centrifuges 25 minutes, abandons supernatant, collects bottom precipitation；By emulsion using ultrasonic cell disruptor in ultrasonic power 300W
Under conditions of be ultrasonically treated 15 minutes after, in 70 DEG C react 120 minutes；After the completion of reaction, reaction solution is cooled to 25 DEG C, with
7000 revs/min of rotating speed centrifuges 25 minutes, abandons supernatant, collects bottom precipitation；By bottom precipitation in 55 DEG C, vacuum
Dried 12 hours under conditions of 0.06MPa, obtain litsea cubeba oil/polymer composite particle.
It is with the concrete operations of load litsea cubeba oil/polymer composite particle on gauze in ball body：By litsea cubeba oil/
Polymer composite particle and polyethylene glycol are added in the deionized water of 20 times of compound particle weight, and wherein polyethylene glycol weight is
5 times of compound particle, stirred 30 minutes with 400 revs/min of rotating speed, obtain dressing liquid；It is small that gauze in 100 DEG C of water is boiled 2
When, dried 7 hours in 80 DEG C, the gauze after being dried；Gauze after drying is immersed in dressing liquid, gauze and dressing liquid
Solid-to-liquid ratio be 1：80 (g/mL), wet gauze, the gauze after being arranged are extruded by two pressurization rods of roller printing machine；Will
Gauze after arrangement is dried 6 hours under conditions of 50 DEG C, vacuum 0.07MPa, and it is multiple to obtain load litsea cubeba oil/polymer
Close the gauze of particle.
Embodiment 5
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal rhizome and ground cauline leaf are crushed, rhizome and the aerial stem of plant
The mass ratio of leaf is 2：1,40 mesh sieves are crossed, obtain powder；By ethanol water that powder and volume fraction are 90% with solid-to-liquid ratio
1：10 (g/mL) are well mixed, are extracted 3 hours in 95 DEG C, obtain extract solution；By extract solution in 60 DEG C, vacuum 0.07MPa
Under the conditions of concentrate 4 hours, obtain concentrate；Add water and petroleum ether into concentrate, extraction, concentrate and water and petroleum ether
Volume ratio is 1：0.5：1, collect petroleum ether phase；Petroleum ether is mutually dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa,
Obtain galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
The cotton gauze is that area load has SiO2The cotton gauze of/litsea cubeba oil/polymer composite particle, wherein described
SiO2The preparation process of/litsea cubeba oil/polymer composite particle is：By SiO2, litsea cubeba oil and monomer be well mixed,
SiO2, litsea cubeba oil and monomer mass ratio be 0.015：0.06：1, monomer is methyl methacrylate and the positive fourth of acrylic acid
Ester is using mol ratio as 1：2 mixtures mixed, stirred 12 minutes with 800 revs/min of rotating speed；Then add hexadecane and
Initiator A IBN, hexadecane are that 3%, AIBN of monomer mass is the 2% of monomer mass, are mixed to get oil phase；By allyloxy
Nonyl phenol ether ammonium sulfate salt is dissolved into deionized water, obtains aqueous phase；Under 400 revs/min of mixing speed, oil phase is added
Into aqueous phase, the solid-to-liquid ratio of monomer and deionized water is 7：10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate salt are monomer matter
The 20% of amount；Then stirred 15 minutes with 7000 revs/min of rotating speed, obtain emulsion；Emulsion is crushed using supersonic cell
After machine is ultrasonically treated 15 minutes under conditions of ultrasonic power 300W, reacted 120 minutes in 70 DEG C；After the completion of reaction, it will react
Liquid is cooled to 25 DEG C, is centrifuged 25 minutes with 7000 revs/min of rotating speed, abandons supernatant, collects bottom precipitation；By bottom precipitation in
55 DEG C, dry 12 hours under conditions of vacuum 0.06MPa, obtain SiO2/ litsea cubeba oil/polymer composite particle.
In ball body with loading SiO on gauze2The concrete operations of/litsea cubeba oil/polymer composite particle are：By SiO2/ mountain
Grey sub- essential oil/polymer composite particle and polyethylene glycol are added in the deionized water of 20 times of compound particle weight, wherein poly- second
Glycol weight is 5 times of compound particle, is stirred 30 minutes with 400 revs/min of rotating speed, obtains dressing liquid；By gauze in 100 DEG C
Boil 2 hours, dried 7 hours in 80 DEG C, the gauze after being dried in water；Gauze after drying is immersed in dressing liquid, yarn
The solid-to-liquid ratio of cloth and dressing liquid is 1：80 (g/mL), wet gauze is extruded by two pressurization rods of roller printing machine, is arranged
Gauze afterwards；Gauze after arrangement is dried 6 hours under conditions of 50 DEG C, vacuum 0.07MPa, obtains loading SiO2/ mountain
The gauze of grey sub- essential oil/polymer composite particle.
Embodiment 6
Herbal medicine ball, including ball handle portion and ball body part are used in massage, and ball body is formed by herbal medicine by cotton gauze parcel, herbal medicine
Useful load is 100g/ herbal medicine ball.
Formula：Lemon grass extract 30wt%, purple ginger 30wt%, orange peel 13wt%, salt 5wt%, root tuber of aromatic turmeric extraction
Thing 4wt%, tamarind 4wt%, turmeric 4wt%, trifoliate jewelvine extract 2wt%, buchanan cryptolepis root extract 2wt%, galangal rhizome extract
2wt%, Ginger P.E 2wt%, camphor 1wt%, thorn stamen grass extract 1wt%.
The preparation process of the galangal rhizome extract is：Galangal rhizome and ground cauline leaf are crushed, rhizome and the aerial stem of plant
The mass ratio of leaf is 2：1,40 mesh sieves are crossed, obtain powder；By ethanol water that powder and volume fraction are 90% with solid-to-liquid ratio
1：10 (g/mL) are well mixed, are extracted 3 hours in 95 DEG C, obtain extract solution；By extract solution in 60 DEG C, vacuum 0.07MPa
Under the conditions of concentrate 4 hours, obtain concentrate；Add water and petroleum ether into concentrate, extraction, concentrate and water and petroleum ether
Volume ratio is 1：0.5：1, collect petroleum ether phase；Petroleum ether is mutually dried 8 hours under conditions of 55 DEG C, vacuum 0.06MPa,
Obtain galangal rhizome extract.
The preparation of massage herbal medicine ball：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 5 minutes under conditions of microwave power 240KW, microwave frequency 2450MHz；
S4 is filled：Compound after sterilizing is wrapped up with cotton gauze, ball body is formed, is then connected with ball handle, described in formation
Herbal medicine ball is used in massage.
The cotton gauze is that area load has modified SiO2The cotton gauze of/litsea cubeba oil/polymer composite particle, wherein
The modified SiO2The preparation process of/litsea cubeba oil/polymer composite particle is：Will modified SiO2, litsea cubeba oil and monomer
It is well mixed, modified SiO2, litsea cubeba oil and monomer mass ratio be 0.015：0.06：1, monomer is methyl methacrylate
With n-butyl acrylate using mol ratio as 1：2 mixtures mixed, stirred 12 minutes with 800 revs/min of rotating speed；Then
It is that 3%, AIBN of monomer mass is the 2% of monomer mass to add hexadecane and initiator A IBN, hexadecane, is mixed to get oil
Phase；Allyloxy nonyl phenol ether ammonium sulfate salt is dissolved into deionized water, the solid-to-liquid ratio of monomer and deionized water is 7：10(g/
ML), aqueous phase is obtained；Under 400 revs/min of mixing speed, oil phase is added in aqueous phase, allyloxy nonyl phenolic ether sulfuric acid
Ammonium salt is the 20% of monomer mass；Then stirred 15 minutes with 7000 revs/min of rotating speed, obtain emulsion；By emulsion using super
After sound wave cell disruptor is ultrasonically treated 15 minutes under conditions of ultrasonic power 300W, reacted 120 minutes in 70 DEG C；React
Cheng Hou, reaction solution is cooled to 25 DEG C, centrifuged 25 minutes with 7000 revs/min of rotating speed, abandon supernatant, collect bottom precipitation；
Bottom precipitation is dried 12 hours under conditions of 55 DEG C, vacuum 0.06MPa, obtains being modified SiO2/ litsea cubeba oil/polymerization
Thing compound particle.
The modified SiO2Preparation process be：By SiO2With absolute ethyl alcohol with solid-to-liquid ratio 1：4 (g/mL) are mixed, and addition is gone
The volume ratio of ionized water, absolute ethyl alcohol and deionized water is 10：1, it is well mixed, obtains mixed liquor；Use mass fraction for
The pH to 9.0 of 20wt% ammoniacal liquor regulation mixed liquor, Silane coupling reagent KH-570 is added under 300 revs/min of stirring action,
SiO2Mass ratio with KH-570 is 7：1, reacted 18 hours in 25 DEG C；Reaction solution is centrifuged 20 with 4000 revs/min of rotating speed
Minute, collect bottom precipitation；Bottom precipitation is washed with deionized, the solid-to-liquid ratio of bottom precipitation and deionized water is 1：300
(g/mL), dried 8 hours under conditions of 55 DEG C, vacuum 0.07MPa, obtain being modified SiO2。
The loaded modified SiO on ball body gauze2The concrete operations of/litsea cubeba oil/polymer composite particle are：It will change
Property SiO2/ litsea cubeba oil/polymer composite particle and polyethylene glycol are added in the deionized water of 20 times of compound particle weight,
Wherein polyethylene glycol weight is 5 times of compound particle, is stirred 30 minutes with 400 revs/min of rotating speed, obtains dressing liquid；By yarn
It is distributed in 100 DEG C of water and boils 2 hours, is dried 7 hours in 80 DEG C, the gauze after being dried；Gauze after drying is immersed in whole
Manage in liquid, the solid-to-liquid ratio of gauze and dressing liquid is 1：80 (g/mL), wet gauze is extruded by two pressurization rods of roller printing machine,
Gauze after being arranged；Gauze after arrangement is dried 6 hours under conditions of 50 DEG C, vacuum 0.07MPa, loaded
Modified SiO2The gauze of/litsea cubeba oil/polymer composite particle.
Embodiment 7
It is substantially the same manner as Example 6, differ only in：Litsea cubeba oil is replaced with into rhizome of chuanxiong essential oil.
Embodiment 8
It is substantially the same manner as Example 6, differ only in：Litsea cubeba oil is replaced with into the mixed of rhizome of chuanxiong essential oil and rhizome of chuanxiong essential oil
Compound, the wherein mass ratio of litsea cubeba oil and rhizome of chuanxiong essential oil are 3:1.
Test case 1
Test sample：Men and women half and half, is randomly divided into 8 groups, every group 50.The occupation of experimenter is evenly distributed in civil servant enterprise
Career management personnel, specialty and culture and education scientific and technical personnel, service sales personnel, worker, retired personnel, other.
8 groups of experimenters respectively using the present invention herbal medicine ball massaged, massage one month, 2 times a week, carry out blood pressure and
The test of heart rate.Measuring instrument (is purchased from Suzhou Ming Zhao numeral science and technology Co., Ltd, model using Omron intelligent electronic blood pressure meter
For HEM-6021).During measurement, sphygmomanometer is uniformly worn on left finesse, and sphygmomanometer staggers with left hand pubis, develops simultaneously to heart and puts down
During row amount, subjects all keep sight look straight ahead, it is impossible to observed reading of bowing.
Specific test result is shown in Table 1.
Table 1：Blood pressure and heart rate test result table
As it can be seen from table 1 after the massage of herbal medicine ball, the drop in blood pressure of experimenter, the rhythm of the heart becomes gentle, illustrates this hair
The bright massage herbal medicine ball has the function that positive for regulation blood pressure, fatigue-relieving.
Test case 2
Pittsburgh Sleep Quality Index questionnaire (Pittsburgh Sleep Quality Index, PSQI) is for sleep
The investigation of obstacle.State can be widely applied to personality manifest anxiety scale (State-TraitAnxiety Inventory, STAI)
The anxiety for evaluating internal medicine, surgery, psychosomatic disease and spirit also can be used to the relevant anxiety problem of the various specific crowds of examination,
And the therapeutive effect of evaluation.Wherein, STAI marks examination papers including SAI and TAI.
8 groups of experimenters are massaged using the herbal medicine ball of the present invention respectively, are massaged one month, 2 times a week, fill in questionnaires tune
Table look-up.
Specific evaluating result is shown in Table 2.
Table 2：Evaluating result table
| PSQI | SAI | TAI | |
| Embodiment 1 | 6.85 | 56.17 | 55.29 |
| Embodiment 2 | 7.23 | 57.42 | 56.38 |
| Embodiment 3 | 6.57 | 55.38 | 54.71 |
| Embodiment 4 | 6.09 | 51.25 | 51.44 |
| Embodiment 5 | 5.14 | 47.19 | 48.52 |
| Embodiment 6 | 4.82 | 42.58 | 42.07 |
| Embodiment 7 | 4.16 | 41.71 | 41.65 |
| Embodiment 8 | 3.35 | 38.04 | 39.82 |
From table 2 it can be seen that using massage of the present invention with after herbal medicine ball, experimenter is easier to enter relaxation state,
This explanation massage serves good control action with herbal medicine ball to the overall mood of experimenter, for psychological adjustment and changes
It is kind to serve Expected Results.
With reference to Tables 1 and 2 as can be seen that galangal rhizome extract uses rhizome extract in embodiment 1；It is high in embodiment 2
Rhizoma Alpiniae Officinarum extract uses ground stem-leaf extract, ground leaves and stemses point containing Galangin, Galangin -3- methyl ethers, pinocembrin,
Dihydro galangal alcohol and Kaempferol isoreactivity material, these active materials have the function of reducing anti-oxidant reduction blood glucose；Implement
In example 3 when preparing galangal rhizome extract, use is closed into galangal rhizome part and the distribution of ground leaves and stemses and extracted, is obtained
Galangal rhizome extract effect it is more excellent.Inventor both may be used in practice it is found that load essential oil on the gauze of herbal medicine ball ball body
, again can be with repellent worm ant to improve the therapeutic effect of herbal medicine ball.But essential oil is typically easy to volatilize, to air, temperature and photosensitive
Sense, it is easy to vapor away quickly.Embodiment 4 loads litsea cubeba oil/polymer composite particle, resin film on ball body gauze
Essential oil is coated, the rate of volatilization of essential oil can be suppressed, the volatile problem for solving essential oil.Embodiment 5 uses SiO2/
Litsea cubeba oil/polymer composite particle is loaded to ball body with gauze, is as a result found, the health care of embodiment 5 is calmed the nerves effect
Better than embodiment 4, the embedded SiO of this explanation2The evaporation rate of essential oil can be reduced., will for embodiment 6 is compared to embodiment 5
SiO2It is replaced with modified SiO2, modified silica has hydrophobicity, has stronger affinity with essential oil, be easy to adsorb
Essential oil, further improve the effect of calming the nerves of herbal medicine ball.
Preferred embodiment of the invention described in detail above.It should be appreciated that one of ordinary skill in the art without
Creative work can is needed to make many modifications and variations according to the design of the present invention.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical scheme, all should be in the protection domain being defined in the patent claims.
Claims (10)
1. herbal medicine ball is used in one kind massage, it is characterised in that including ball handle portion and ball body part, ball body is by herbal medicine by gauze wrapped
Form, the useful load of herbal medicine is 50-200g/ herbal medicine ball, and the herbal medicine includes lemon grass extract, purple ginger, orange peel, food
Salt, Radix Curcumae extract, tamarind, turmeric, trifoliate jewelvine extract, buchanan cryptolepis root extract, galangal rhizome extract, Ginger P.E, camphor tree
Brain, thorn stamen grass extract.
2. herbal medicine ball is used in massage as claimed in claim 1, it is characterised in that the herbal medicine forms according to the following ratio：Lemon grass (Cymbopogon citratus)
Extract 20-30wt%, purple ginger 30-40wt%, orange peel 10-15wt%, salt 3-7wt%, Radix Curcumae extract 2-
5wt%, tamarind 2-5wt%, turmeric 2-5wt%, trifoliate jewelvine extract 1-2wt%, buchanan cryptolepis root extract 1-2wt%, galangal
Extract 1-2wt%, Ginger P.E 1-2wt%, camphor 0.5-1.5wt%, thorn stamen grass extract 0.5-1.5wt%.
3. herbal medicine ball is used in massage as claimed in claim 2, it is characterised in that the preparation process of the galangal rhizome extract is：
Galangal extract part is crushed, 40-60 mesh sieves is crossed, obtains powder；By powder and extraction solvent with solid-to-liquid ratio 1：(10-15)
(g/mL) it is well mixed, extracts 1.5-5 hours in 90-100 DEG C, obtain extract solution；By extract solution in 50-60 DEG C, vacuum
3-4 hours are concentrated under conditions of 0.06-0.07MPa, obtain concentrate；Water and petroleum ether are added into concentrate, is extracted, concentration
Liquid is 1 with the volume ratio of water and petroleum ether：(0.5-0.8)：(1-2), collect petroleum ether phase；By petroleum ether mutually in 50-60 DEG C, it is true
5-10 hours are dried under conditions of reciprocal of duty cycle 0.06-0.07MPa, obtain galangal rhizome extract.
4. herbal medicine ball is used in massage as claimed in claim 3, it is characterised in that the galangal extract part is rhizome, flower, fruit
One or more in real, ground cauline leaf.
5. herbal medicine ball is used in massage as claimed in claim 1, it is characterised in that the gauze is that area load has compound particle
Gauze.
6. the preparation method of massage herbal medicine ball as claimed in claim 5, it is characterised in that described compound particle be essential oil/
Polymer composite particle, SiO2Or modified SiO2One kind or composition in/essential oil/polymer composite particle.
7. herbal medicine ball is used in massage as claimed in claim 6, it is characterised in that the preparation of the essential oil/polymer composite particle
Process is：Essential oil and monomer are well mixed, the mass ratio of essential oil and monomer is (0.04-0.07)：1, monomer is metering system
Sour methyl esters and n-butyl acrylate are using mol ratio as 1：The mixture that (1.5-2) is mixed, with 800-1000 revs/min turn
Speed stirring 8-15 minutes；Hexadecane and initiator A IBN are then added, hexadecane is the 2.5-5% of monomer mass, and AIBN is single
The 1.5-4% of weight, is mixed to get oil phase；Allyloxy nonyl phenol ether ammonium sulfate salt is dissolved into deionized water, obtained
Aqueous phase；Under 300-500 revs/min of mixing speed, oil phase is added in aqueous phase, the solid-to-liquid ratio of monomer and deionized water is
(5-8)：10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate salt are the 20-30% of monomer mass；Then with 7000-8000 turn/
The rotating speed stirring 10-20 minutes of minute, obtain emulsion；By emulsion using ultrasonic cell disruptor in ultrasonic power 300-400W
Under conditions of be ultrasonically treated 10-15 minutes after, in 70-75 DEG C react 120-160 minutes；After the completion of reaction, reaction solution is cooled down
To 20-30 DEG C, 20-30 minutes are centrifuged with 7000-9000 revs/min of rotating speed, abandon supernatant, collect bottom precipitation；By bottom
It is deposited in 50-60 DEG C, 10-15 hours is dried under conditions of vacuum 0.06-0.08MPa, obtains the compound grain of essential oil/polymer
Son.
8. the preparation method of massage herbal medicine ball as claimed in claim 6, it is characterised in that the SiO2Or modified SiO2/ essence
The preparation process of oil/polymer composite particle is：By SiO2Or modified SiO2, essential oil and monomer be well mixed, SiO2It is or modified
SiO2, essential oil and monomer mass ratio be (0.012-0.018)：(0.04-0.07)：1, monomer is methyl methacrylate and third
Olefin(e) acid N-butyl is using mol ratio as 1：The mixture that (1.5-2) is mixed, 8-15 is stirred with 800-1000 revs/min of rotating speed
Minute；Hexadecane and initiator A IBN are then added, hexadecane is the 2.5-5% of monomer mass, and AIBN is monomer mass
1.5-4%, it is mixed to get oil phase；Allyloxy nonyl phenol ether ammonium sulfate salt is dissolved into deionized water, obtains aqueous phase；
Under 300-500 revs/min of mixing speed, oil phase is added in aqueous phase, the solid-to-liquid ratio of monomer and deionized water is (5-8)：
10 (g/mL), allyloxy nonyl phenol ether ammonium sulfate salt are the 20-30% of monomer mass；Then with 7000-8000 revs/min
Rotating speed stirs 10-20 minutes, obtains emulsion；Emulsion is used into ultrasonic cell disruptor in ultrasonic power 300-400W condition
After lower supersound process 10-15 minutes, 120-160 minutes are reacted in 70-75 DEG C；After the completion of reaction, reaction solution is cooled to 20-30
DEG C, 20-30 minutes are centrifuged with 7000-9000 revs/min of rotating speed, abandon supernatant, collect bottom precipitation；By bottom precipitation in
50-60 DEG C, 10-15 hours are dried under conditions of vacuum 0.06-0.08MPa, obtain SiO2Or modified SiO2/ essential oil/polymer
Compound particle.
9. the preparation method of massage herbal medicine ball as claimed in claim 8, it is characterised in that the modified SiO2Preparation
Cheng Wei：By SiO2With absolute ethyl alcohol with solid-to-liquid ratio 1：(3-5) (g/mL) is mixed, and adds deionized water, absolute ethyl alcohol and deionization
The volume ratio of water is (10-12)：1, it is well mixed, obtains mixed liquor；Use mass fraction mixed for 20-25wt% ammoniacal liquor regulation
The pH to 9.0 of liquid is closed, Silane coupling reagent KH-570, SiO are added under 200-300 revs/min of stirring action2With KH-570's
Mass ratio is (6-7)：1, react 12-24 hours in 23-25 DEG C；Reaction solution is centrifuged with 4000-5000 revs/min of rotating speed
15-20 minutes, collect bottom precipitation；Bottom precipitation is washed with deionized, the solid-to-liquid ratio of bottom precipitation and deionized water is
1：(300-400) (g/mL), 8-10 hours are dried under conditions of 50-55 DEG C, vacuum 0.07-0.08MPa, are modified
SiO2。
10. prepare the massage method of herbal medicine ball as claimed in any one of claims 1-9 wherein, it is characterised in that including following
Step：
S1 is crushed：Herbal raw material is crushed respectively, crosses 40-60 mesh sieves；
S2 batch mixings：Herbal raw material after sieving is well mixed by formula, obtain compound；
S3 is sterilized：Compound is sterilized 3-5 points under conditions of microwave power 200-240KW, microwave frequency 915-2450MHz
Clock；
S4 is filled：By the compound gauze wrapped after sterilizing, ball body is formed, is then attached with ball handle.
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| CN109846725A (en) * | 2019-01-30 | 2019-06-07 | 东莞市炫墨生物科技有限公司 | Massage emulsion of the microcapsules containing composite essential oil and preparation method thereof |
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Application publication date: 20180119 |