CN107595646B - French stripe sticker and preparation method thereof - Google Patents
French stripe sticker and preparation method thereof Download PDFInfo
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- CN107595646B CN107595646B CN201710771524.4A CN201710771524A CN107595646B CN 107595646 B CN107595646 B CN 107595646B CN 201710771524 A CN201710771524 A CN 201710771524A CN 107595646 B CN107595646 B CN 107595646B
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Abstract
The invention discloses a stature stripe sticker and a preparation method thereof, wherein the stature stripe sticker is composed of an elastic non-woven fabric, a hydrogel layer and an embossing film, wherein the hydrogel layer comprises glycerol, sodium polyacrylate, benzyl alcohol, ethylhexyl glycerol, tocopherol, aluminum glycinate, EDTA disodium, methyl hydroxybenzoate, water, tartaric acid, color paste, povidone and carbomer, and the preparation method comprises the following steps: (1) adding sodium polyacrylate, benzyl alcohol and the like into glycerol to obtain an oil phase mixture for later use; (2) adding tartaric acid, color paste and the like into water to obtain a water phase mixture for later use; (3) pouring the mixture of the oil phase and the water phase in the steps (1) and (2) into a vacuum stirring barrel, vacuumizing and stirring, and discharging; (4) coating and rolling; (5) curing the semi-finished product; (6) die cutting and packaging to obtain the finished product. The statuary line sticker provided by the invention is simple in structure and convenient to manufacture, is pasted at the mouth corner when in use, has good pasting degree with the face, can fade fine lines, preserve moisture and nourish, is attractive in shape, is repaired and compact, and can be continuously used for more than 4 hours.
Description
Technical Field
The invention relates to the technical field of skin care products, in particular to a stature stripe sticker and a preparation method thereof.
Background
Skin is the largest organ of the human body, and aging is caused by aging, so that people pay more attention to facial skin care along with the improvement of life quality. With the increase of human age, the differentiation of skin cells is slower, the dermis is gradually thinned, the fat cells under the dermis begin to shrink, and the skin tissue becomes looser and looser. When the skin loses elasticity, the skin does not recover after being squeezed, and thus, the skin sags and wrinkles are generated.
All the fishtail lines, fine lines and caudad eyes are caused by uneven collapse of the epidermis layer of the skin. The skin is composed of three layers: the epidermis, dermis, and subcutaneous fat, respectively, the dermis contains collagen, elastin, and other fibers that form the skeleton supporting the skin. These elements also make the skin smooth and youthful, and are also vulnerable to UVA, UVB, which is a long-wave uv (380-. Wrinkle resistant dermatologists indicate: shallow small wrinkles, bags under the eyes may appear around 25 years old; the forehead wrinkles deepen and increase around the age of 30, and the external canthus has fishtail lines and upper and lower eyelid skins have wrinkles of different degrees; the nasolabial sulcus deepens when the patient is aged 40 years, fine wrinkles appear at the corners of the mouth, and neck wrinkles appear; under 50 years old, the eye bags deepen and appear with lower eyelid lines, and the upper and lower lips also appear with wrinkles; the elasticity of the whole face is reduced and the wrinkles of the face are deepened by the age of 60. The statutory veins are two veins extending from the side of the nasal alar part, and are typical skin surface depression caused by skin tissue aging.
The reasons for generating the statutory marks mainly include: (1) aging and relaxing the skin; (2) the expression is too rich; (3) air pollution, radiation of computer and mobile phone and irregular daily work and rest; (4) the sleeping posture is not proper. At present, the method for eliminating the statute line mainly comprises a surgical method and an injection method. The surgical method improves the statute lines by pulling the skin, but the face is always tight, the expression is unnatural and the face is easy to recover; the injection method promotes the growth of collagen by injecting autologous cells, thereby reducing wrinkles, and although the effect is remarkable, the safety is low because of individual differences and practitioner level differences. The obvious statutory veins often make the user look serious, old and unappealing, and make the user feel difficult to be close to the system. There is no effective and feasible method for removing the grain of the statute.
Disclosure of Invention
In order to solve the above problems, it is an object of the present invention to provide a statute line sticker capable of weakening and eliminating statute lines; the second purpose of the invention is to provide a preparation method of the stature line sticker; it is a further object of the present invention to provide a hydrogel.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a law pattern subsides, includes that elasticity non-woven fabrics 1, hydrogel layer 2, pearlized membrane 3 preface laminating in proper order, elasticity non-woven fabrics 1 covers hydrogel layer 2 completely, pearlized membrane 3 covers hydrogel layer 2 completely.
Preferably, the area of the elastic nonwoven fabric 1 is larger than the area of the hydrogel layer 2; further preferably, the edges of the elastic nonwoven 1 are wider than the hydrogel by 1-2mm, so that the hydrogel can be prevented from overflowing the elastic nonwoven. Preferably, the pearlescent film 3 is completely attached to the hydrogel layer 2.
Preferably, the order grain paste is arranged to extend upwards in a narrow oblique manner with a wide lower part and a narrow upper part, and one side of the order grain paste close to the nose wing is matched with the nose wing and the mouth corner for forming, referring to fig. 2, the order grain paste 11 is arc-shaped and is inwards sunken near the nose wing, so that the order grain paste 11 can bypass the nose wing and is completely jointed with the cheek. The law pattern sticker 12 protrudes outwards and is attached to the positions below the nasal alar part and above the mouth corner, so that the law pattern sticker is better attached to the face; in addition, the stature stripe sticker 12 protrudes outwards and then extends towards the bottom of the stature stripe sticker, so that an inwards concave stuffing shape is formed between the stature stripe sticker and the bottom of the stature stripe sticker, and the mouth corner can be just avoided. The bottom of the other side of the stature stripe sticker protrudes outwards, so that the stature stripe sticker is favorable for meeting the shape of a cheek and further being attached to the face, the fixity of the stature stripe sticker is improved, and the stature stripe sticker is prevented from being tilted and even falling off in the using process; more importantly, the part also has the function of lifting upwards, and is beneficial to massaging and lifting the cheek muscles by the stature strip.
Preferably, the hydrogel layer 2 comprises the following raw materials in weight ratio: 10-30% of glycerol, 1-10% of sodium polyacrylate, 0.1-1% of benzyl alcohol, 0.01-0.08% of ethylhexyl glycerol, 0.01-0.05% of tocopherol, 0.1-0.5% of aluminum glycinate, 0.1-0.5% of EDTA disodium, 0.1-0.3% of methylparaben, 0.1-0.5% of tartaric acid, 0.01-0.05% of color paste, 0.5-5% of povidone, 1-5% of carbomer and the balance of water.
Preferably, the elastic nonwoven has an elongation of 10% to 100%.
Preferably, the thickness of the elastic non-woven fabric (1) is 300-600 μm, the thickness of the hydrogel layer (2) is 300-800 μm, and the thickness of the pearlized film (3) is 80-150 μm.
Preferably, the pearlized film 3 is PP, PE, release paper, or the like.
Preferably, the statute line sticker comprises two stickers, one sticker on the left and the right.
The preparation method of the stature stripe sticker comprises the following steps:
(1) adding sodium polyacrylate, benzyl alcohol, ethylhexyl glycerol, tocopherol, aluminum glycinate, disodium EDTA and methyl hydroxybenzoate into glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding tartaric acid, color paste, povidone and carbomer into water, and stirring and mixing uniformly in a dispersion machine to obtain a water phase mixture for later use;
(3) pouring the oil phase mixture obtained in the step (1) and the water phase mixture obtained in the step (2) into a vacuum stirring barrel, covering the stirring barrel tightly, starting stirring, vacuumizing to-0.05 to-0.01 kpa, stopping vacuumizing, continuously stirring, and discharging to obtain hydrogel;
(4) the coating machine is provided with an elastic non-woven fabric and a pearlized film, wherein the elastic non-woven fabric is a lower layer, and the embossed film is an upper layer; adjusting the coating thickness according to the specified gram weight of the product, adopting a paper core according to the width after coating, and rolling according to a rolling unit;
(5) winding to obtain a semi-finished product, and placing the semi-finished product in a curing chamber for curing;
(6) and (5) after curing, die cutting and packaging to obtain a finished product.
Preferably, the stirring speed of the vacuum stirring barrel in the step (3) is 110-130 r/min, and the stirring time is continued for 5-10min after the vacuumizing is stopped.
Preferably, the indoor temperature range of the curing chamber in the step (5) is 20-35 ℃; the curing time is 24-48 h.
The hydrogel comprises the following raw materials in parts by weight: 10-30% of glycerol, 1-10% of sodium polyacrylate, 0.1-1% of benzyl alcohol, 0.01-0.08% of ethylhexyl glycerol, 0.01-0.05% of tocopherol, 0.1-0.5% of aluminum glycinate, 0.1-0.5% of EDTA disodium, 0.1-0.3% of methylparaben, 0.1-0.5% of tartaric acid, 0.01-0.05% of color paste, 0.5-5% of povidone, 1-5% of carbomer and the balance of water.
The invention has the beneficial effects that:
1. compared with the traditional operation and injection wrinkle removal, the statue line patch provided by the invention is simple in structure, convenient to manufacture and convenient to carry;
2. the statue line sticker provided by the invention has good fitting degree with the face when in use, is used for repairing and tightening, can guide muscles to lift upwards, and plays a role in massaging the muscles around the statue line and promoting the absorption of contents through the movement of the face;
3. the facial mask is used for the grains of the statute, is attached to the corners of the mouth, can fade fine grains, moisturize and nourish the skin, has beautiful shape, is attached to the skin, and can be continuously used for more than 4 hours.
Drawings
FIG. 1 is a cross-sectional view of a statute applique of the present invention;
FIG. 2 is a top view of the statute applique of the present invention.
Detailed Description
Example 1
A hydrogel prepared by the steps of:
(1) adding 2% of sodium polyacrylate, 0.4% of benzyl alcohol, 0.01% of ethylhexyl glycerol, 0.01% of tocopherol (vitamin E), 0.1% of aluminum glycinate, 0.1% of disodium EDTA and 0.1% of methyl hydroxybenzoate into 23.28% of glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding 0.1% of tartaric acid, 0.01% of color paste, 0.5% of povidone and 1% of carbomer into 72.39% of water, and uniformly stirring and mixing in a dispersion machine to obtain an aqueous phase mixture for later use;
(3) and (3) pouring the mixture of the oil phase and the water phase in the steps (1) and (2) into a vacuum stirring barrel, covering the stirring barrel tightly, starting stirring for 120r/min, vacuumizing to-0.075 kpa, stopping vacuumizing, continuously stirring for 7min, and discharging to obtain the oil-water-based composite material.
Example 2
A hydrogel prepared by the steps of:
(1) adding 4% of sodium polyacrylate, 0.6% of benzyl alcohol, 0.03% of ethylhexyl glycerol, 0.03% of tocopherol (vitamin E), 0.3% of aluminum glycinate, 0.3% of disodium EDTA and 0.2% of methyl hydroxybenzoate into 20.54% of glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding 0.3% of tartaric acid, 0.03% of color paste, 3% of povidone and 3% of carbomer into 67.67% of water, and uniformly stirring and mixing in a dispersion machine to obtain an aqueous phase mixture for later use;
(3) and (3) pouring the mixture of the oil phase and the water phase in the steps (1) and (2) into a vacuum stirring barrel, covering the stirring barrel tightly and starting stirring, wherein the stirring speed is 110r/min, vacuumizing is stopped after-0.05 kpa is achieved, and discharging after the stirring is continued for 5min to obtain the oil-water-based organic silicon oil.
Example 3
A hydrogel prepared by the steps of:
(1) adding 6% of sodium polyacrylate, 0.8% of benzyl alcohol, 0.05% of ethylhexyl glycerol, 0.05% of tocopherol (vitamin E), 0.5% of aluminum glycinate, 0.5% of disodium EDTA and 0.3% of methyl hydroxybenzoate into 17.8% of glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding 0.5% of tartaric acid, 0.05% of color paste, 5% of povidone and 5% of carbomer into 63.45% of water, and uniformly stirring and mixing in a dispersion machine to obtain an aqueous phase mixture for later use;
(3) and (3) pouring the mixture of the oil phase and the water phase in the steps (1) and (2) into a vacuum stirring barrel, covering the stirring barrel tightly, starting stirring for 130r/min, vacuumizing to-0.01 kpa, stopping vacuumizing, continuously stirring for 10min, and discharging to obtain the oil-water-based composite material.
Example 4
A hydrogel prepared by the steps of:
(1) adding 5% of sodium polyacrylate, 0.45% of benzyl alcohol, 0.04% of ethylhexyl glycerol, 0.01% of tocopherol (vitamin E), 0.2% of aluminum glycinate, 0.2% of disodium EDTA and 0.1% of methyl hydroxybenzoate into 20% of glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding 0.2% of tartaric acid, 0.01% of color paste, 1% of povidone and 2% of carbomer into 70.79% of water, and uniformly stirring and mixing in a dispersion machine to obtain an aqueous phase mixture for later use;
(3) and (3) pouring the mixture of the oil phase and the water phase in the steps (1) and (2) into a vacuum stirring barrel, covering the stirring barrel tightly and starting stirring, wherein the stirring speed is 120r/min, vacuumizing is stopped after-0.08 kpa is achieved, and discharging is carried out after continuous stirring is carried out for 6 min.
Example 5
A stature line sticker comprises an elastic non-woven fabric 1, a hydrogel layer 2 and a pearlized film 3 which are sequentially attached, wherein the elastic non-woven fabric 1 completely covers the hydrogel layer 2, and the pearlized film 3 completely covers the hydrogel layer 2; wherein the edge of the elastic non-woven fabric 1 is wider than 1mm of the hydrogel, and the pearlized film 3 is completely attached to the hydrogel layer 2; the hydrogel layer was coated from the hydrogel of example 4.
The elastic nonwoven fabric had an elongation of 50%, the thickness of the elastic nonwoven fabric 1 was 450 μm, the thickness of the hydrogel layer 2 was 450 μm, and the thickness of the pearlescent film 3 was 130 μm.
The law line pastes and sets up to the narrow oblique upwards extension in lower part width upper portion, and the one side that the law line pasted and is close to the alar nasal wing cooperates the alar nasal wing and the shaping of mouth angle, refers to fig. 2, and law line pastes 11 is circular-arc, and its department that is close to the alar nasal wing is inwards sunken, makes law line paste 11 can bypass the alar nasal wing and laminate completely in the cheek. The order grain paster 12 protrudes outwards and is attached to the part below the nasal wing and above the corner of the mouth, so that the order grain paster can be better attached to the face; in addition, the stature stripe sticker 12 protrudes outwards and then extends towards the bottom of the stature stripe sticker, so that an inwards concave stuffing shape is formed between the stature stripe sticker and the bottom of the stature stripe sticker, and the mouth corner can be just avoided. The bottom of the other side of the stature stripe sticker protrudes outwards, so that the stature stripe sticker is favorable for meeting the shape of a cheek and further being attached to the face, the fixity of the stature stripe sticker is improved, and the stature stripe sticker is prevented from being tilted and even falling off in the using process; more importantly, the part also has the function of lifting upwards, and is beneficial to massaging and lifting the cheek muscles by the stature strip.
The preparation method of the stature stripe sticker comprises the following steps:
(1) the coating machine is provided with an elastic non-woven fabric and a pearlized film, wherein the elastic non-woven fabric is a lower layer, and the embossed film is an upper layer; adjusting the coating thickness according to the specified gram weight of the product, namely 3.0-4.0 grams, adopting a paper core according to the width after coating, and rolling by taking 5kg of colloid as a rolling unit;
(2) rolling to obtain a semi-finished product, moving the semi-finished product into a curing chamber, arranging the semi-finished product in order, adjusting the indoor humidity range to be 20-35 ℃, and starting curing for 24 hours;
(3) and (5) after curing, die cutting and packaging to obtain a finished product.
Example 6
A stature line sticker comprises an elastic non-woven fabric 1, a hydrogel layer 2 and a pearlized film 3 which are sequentially attached, wherein the elastic non-woven fabric 1 completely covers the hydrogel layer 2, and the pearlized film 3 completely covers the hydrogel layer 2; wherein the edge of the elastic non-woven fabric 1 is wider than 1.2mm of the hydrogel, and the pearlized film 3 is completely attached to the hydrogel layer 2; the hydrogel layer was coated from the hydrogel of example 4. The elastic nonwoven fabric had an elongation of 20%, the thickness of the elastic nonwoven fabric 1 was 500 μm, the thickness of the hydrogel layer 2 was 600 μm, and the thickness of the pearlescent film 3 was 150 μm. The shape of the stature band was the same as that of example 5.
Example 7
A stature line sticker comprises an elastic non-woven fabric 1, a hydrogel layer 2 and a pearlized film 3 which are sequentially attached, wherein the elastic non-woven fabric 1 completely covers the hydrogel layer 2, and the pearlized film 3 completely covers the hydrogel layer 2; wherein the edge of the elastic non-woven fabric 1 is wider than 1mm of the hydrogel, and the pearlized film 3 is completely attached to the hydrogel layer 2; the hydrogel layer was coated from the hydrogel of example 4. The elastic nonwoven fabric had an elongation of 70%, the thickness of the elastic nonwoven fabric 1 was 550 μm, the thickness of the hydrogel layer 2 was 800 μm, and the thickness of the pearlescent film 3 was 135 μm. The shape of the stature band was the same as that of example 5.
Effect implementation
To further illustrate the beneficial effects of the present invention, the following evaluation effect experiments were performed on the statute lines obtained in examples 1 to 7 and the commercially available medical youthful lines-soothing patches:
randomly selecting volunteers within the age of 28-38, performing blind test in 8 groups, cleaning faces of 1 st-8 groups of volunteers, standing still for 10min until the skin temperature and humidity are balanced with the environment, respectively taking 5 groups of samples, and sticking the samples to the corners of the mouth and the nasal wings for 4 hours. The evaluation indexes include appearance, touch feeling, skin moistening feeling, allergy, water replenishing effect and fine line relaxing and fading effect, each index is set to be 1-5 points according to the using feeling, and the higher the score is, the better the effect is.
TABLE 1 sensory evaluation table of the statutory prints obtained in EXAMPLES-4 and the commercially available medical-flower facial-smoothing print sticker
As can be seen from the above table, compared with the standard grain stickers obtained in examples 2 to 7 and the commercially available medical flower standard grain stickers, the sensory evaluation obtained in example 1 is better, and the standard grain effect obtained in example 7 is also better, which indicates that the comprehensive use of examples 1 and 7 is more beneficial to moisturizing and relieving and fading fine grains.
Claims (5)
1. The stature stripe sticker is characterized by comprising an elastic non-woven fabric (1), a hydrogel layer (2) and a pearlized film (3) which are sequentially pasted, wherein the elastic non-woven fabric (1) completely covers the hydrogel layer (2), and the pearlized film (3) completely covers the hydrogel layer (2); the order grain paste is arranged to be wide at the lower part and narrow at the upper part, the order grain paste extends upwards in a narrow and oblique mode, one side, close to the nose wing, of the order grain paste is formed by matching the shape of the nose wing and the shape of the mouth corner, and the bottom of the other side of the order grain paste protrudes outwards; the hydrogel layer (2) comprises the following raw materials in percentage by weight: 10-30% of glycerol, 1-10% of sodium polyacrylate, 0.1-1% of benzyl alcohol, 0.01-0.08% of ethylhexyl glycerol, 0.01-0.05% of tocopherol, 0.1-0.5% of aluminum glycinate, 0.1-0.5% of EDTA disodium, 0.1-0.3% of methylparaben, 0.1-0.5% of tartaric acid, 0.01-0.05% of color paste, 0.5-5% of povidone, 1-5% of carbomer and the balance of water; the thickness of the elastic non-woven fabric (1) is 300-600 microns, the thickness of the hydrogel layer (2) is 300-800 microns, and the thickness of the pearlized film (3) is 80-150 microns; the elongation of the elastic non-woven fabric is 10% -100%.
2. The ream wrap of claim 1, wherein said ream wrap comprises two wraps, one on each of the left and right wraps.
3. A method of making the french mark applique of any of the preceding claims comprising the steps of:
(1) adding sodium polyacrylate, benzyl alcohol, ethylhexyl glycerol, tocopherol, aluminum glycinate, disodium EDTA and methyl hydroxybenzoate into glycerol, and uniformly stirring in a dispersion machine to obtain an oil phase mixture for later use;
(2) adding tartaric acid, color paste, povidone and carbomer into water, and stirring and mixing uniformly in a dispersion machine to obtain a water phase mixture for later use;
(3) pouring the oil phase mixture obtained in the step (1) and the water phase mixture obtained in the step (2) into a vacuum stirring barrel, covering the stirring barrel tightly, starting stirring, vacuumizing to-0.05 to-0.01 kpa, stopping vacuumizing, continuously stirring, and discharging to obtain hydrogel;
(4) the coating machine is provided with an elastic non-woven fabric and a pearlized film, wherein the elastic non-woven fabric is a lower layer, and the embossed film is an upper layer; adjusting the coating thickness according to the specified gram weight of the product, adopting a paper core according to the width after coating, and rolling according to a rolling unit;
(5) winding to obtain a semi-finished product, and placing the semi-finished product in a curing chamber for curing;
(6) and (5) after curing, die cutting and packaging to obtain a finished product.
4. The method for preparing the French frieze sticker according to claim 3, wherein the stirring speed of the vacuum stirring barrel in the step (3) is 110-130 r/min, and the stirring time is continued for 5-10min after the vacuumizing is stopped.
5. The method for preparing the French frieze sticker according to claim 3, wherein the indoor temperature of the curing chamber in the step (5) is in the range of 20-35 ℃; the curing time is 24-48 h.
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| DE102021116255A1 (en) | 2021-06-23 | 2022-12-29 | Hybrid Reality GmbH | PROCESS FOR MAKING A UTENSIL COMPRISING SEVERAL UTENSIL ELEMENTS |
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| CN112120965A (en) * | 2020-09-28 | 2020-12-25 | 江门市新时代外用制剂有限公司 | Water-oil double-phase wrinkle-removing and anti-aging hydrogel patch and preparation method thereof |
| CN112370374B (en) * | 2020-11-20 | 2023-02-10 | 江门市新时代外用制剂有限公司 | High-elastic hydrogel plaster |
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