CN107583586A - The ester exchange reaction device of surfactant - Google Patents
The ester exchange reaction device of surfactant Download PDFInfo
- Publication number
- CN107583586A CN107583586A CN201710952322.XA CN201710952322A CN107583586A CN 107583586 A CN107583586 A CN 107583586A CN 201710952322 A CN201710952322 A CN 201710952322A CN 107583586 A CN107583586 A CN 107583586A
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- China
- Prior art keywords
- methyl esters
- containing alcohol
- transesterification reactor
- thick methyl
- settling tank
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Abstract
The invention discloses a kind of ester exchange reaction device of surfactant, including transesterification reactor, the thick methyl esters settling tank of containing alcohol being sequentially connected；Above-mentioned transesterification reactor includes ester exchange reaction kettle, transesterification reactor motor, transesterification reactor rotating shaft, multiple retainer plates, multiple transesterification reactor paddles, multiple dividing plates；The above-mentioned thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank motor of containing alcohol, the thick methyl esters settling tank rotating shaft of containing alcohol, rotating disk, multiple rotary shafts, multiple pivoting leafs.The beneficial effects of the present invention are, pass through more exquisite design, so that operating personnel are produced under relatively simple operation, each technological parameter can be adjusted effectively simultaneously, improve operating flexibility, on the other hand the operating efficiency of each device is high, reduce human cost he, while improve general safety coefficient.
Description
Technical field
The present invention relates to the ester exchange reaction device of a kind of production system, especially surfactant.
Background technology
Surfactant (surfactant), referring to add can make the interface state of its solution system that obvious become occur on a small quantity
The material of change.With fixed hydrophilic lipophilic group, aligned in the surface energy of solution.The molecular structure tool of surfactant
Have amphipathic：One end is hydrophilic radical, and the other end is hydrophobic grouping；Hydrophilic radical is often polar group, such as carboxylic acid, sulfonic acid, sulphur
Acid, amino or amido and its salt, hydroxyl, amide groups, ehter bond etc. can also be used as polar hydrophilic group；And hydrophobic grouping is often non-pole
Property hydrocarbon chain, such as 8 carbon atom above hydrocarbon chains.Surfactant is divided into ionic surfactant (including cation surface activating
Agent and anion surfactant), nonionic surface active agent, amphoteric surfactant, compound surfactant, other tables
Face activating agent etc..
The equipment for producing surfactant, the equipment for especially improving the quality of production and production efficiency, lived for surface
The production of property agent is particularly important.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of ester exchange reaction device of surfactant, having preferably makes
Use effect.
The present invention is achieved through the following technical solutions.
A kind of ester exchange reaction device of surfactant, including transesterification reactor, the thick methyl esters of containing alcohol being sequentially connected
Settling tank；
Above-mentioned transesterification reactor include ester exchange reaction kettle, transesterification reactor motor, transesterification reactor rotating shaft,
Multiple retainer plates, multiple transesterification reactor paddles, multiple dividing plates, the top and bottom difference of above-mentioned ester exchange reaction kettle
Transesterification reactor liquid inlet and transesterification reactor liquid outlet are provided with, above-mentioned transesterification reactor motor is fixed on above-mentioned ester
Above-mentioned transesterification reactor rotating shaft is simultaneously assembled in the top of exchange reaction kettle, and above-mentioned multiple dividing plates are horizontally installed on above-mentioned ester exchange
In reaction kettle body and multiple interconnected spaces are divided into, the transesterification reactor rotating shaft positioned at each space is fixed
Above-mentioned retainer plate is set with, above-mentioned retainer plate outer surface is provided with equally distributed screwed hole, above-mentioned transesterification reactor stirring
One end of leaf is provided with the screw thread bar matched with screwed hole；
The above-mentioned thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank motor of containing alcohol, containing alcohol
Thick methyl esters settling tank rotating shaft, rotating disk, multiple rotary shafts, multiple pivoting leafs, the side wall of the above-mentioned thick methyl esters sedimentation tank body of containing alcohol are set
There are the thick methyl esters settling tank liquid inlet of containing alcohol and containing alcohol glycerine liquid inlet, bottom is provided with the thick methyl esters settling tank liquid outlet of containing alcohol,
The above-mentioned thick methyl esters settling tank motor of containing alcohol is fixed on the top of the thick methyl esters sedimentation tank body of containing alcohol, and the above-mentioned thick methyl esters settling tank of containing alcohol turns
Axle is assemblied in the thick methyl esters settling tank motor of above-mentioned containing alcohol, and above-mentioned rotating disk is vertically fixed on the thick methyl esters settling tank rotating shaft of containing alcohol, multiple
Rotary shaft vertically penetrates above-mentioned rotating disk and is uniformly arranged on the marginal position of above-mentioned rotating disk, and each rotary shaft is provided with multiple
Above-mentioned pivoting leaf.
Further, aforementioned barriers are provided with two, and the transesterification reactor that retainer plate from top to bottom is assembled
The increased number of paddle.
Further, pivoting leaf of above-mentioned rotary shaft or so is arranged alternately.
Beneficial effects of the present invention：
The present invention passes through more exquisite design so that operating personnel are produced under relatively simple operation, simultaneously
Each technological parameter can effectively be adjusted, improve operating flexibility, on the other hand the operating efficiency of each device is high, drop
Low human cost he, while improve general safety coefficient.
Brief description of the drawings
Fig. 1 is the structural representation of transesterification reactor；
Fig. 2 is the structural representation of the thick methyl esters settling tank of containing alcohol.
Embodiment
The present invention is described in further detail below according to drawings and examples.
Reference picture 1- Fig. 2, the present invention, the ester exchange reaction device of surfactant, including the ester exchange being sequentially connected are anti-
Answer the thick methyl esters settling tank of kettle, containing alcohol；
Above-mentioned transesterification reactor includes ester exchange reaction kettle 4-1, transesterification reactor motor 4-2, ester exchange reaction
Kettle rotating shaft 4-3, multiple retainer plate 4-4, multiple transesterification reactor paddle 4-5, multiple dividing plate 4-6, above-mentioned ester exchange reaction
Kettle 4-1 top and bottom is respectively arranged with transesterification reactor liquid inlet 4-7 and transesterification reactor liquid outlet 4-8, on
State ester exchange reaction motor 4-2 and be fixed on above-mentioned ester exchange reaction kettle 4-1 top and assemble above-mentioned transesterification reactor and turn
Axle 4-3, above-mentioned multiple dividing plate 4-6 are horizontally installed in above-mentioned ester exchange reaction kettle 4-1 and are divided into multiple phases interconnection
Logical space, the equal fixed covers of transesterification reactor rotating shaft 4-3 positioned at each space are equipped with above-mentioned retainer plate 4-4, above-mentioned fixation
Circle 4-4 outer surfaces are provided with equally distributed screwed hole, and above-mentioned transesterification reactor paddle 4-5 one end is provided with and screw thread
The screw thread bar of hole matching.
Aforementioned barriers 4-6 is provided with two, and the transesterification reactor stirring that retainer plate 4-4 from top to bottom is assembled
Leaf 4-5 increased number.
Space is divided into multiple by the dividing plate 4-6 of setting, can carry out continuous ester exchange reaction, while the retainer plate 4- set
4 and assembling transesterification reactor paddle 4-5 can carry out transesterification reactor paddle 4-5's as the case may be
Arrangement, improves using flexible.
The above-mentioned thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body 5-1 of containing alcohol, the thick methyl esters settling tank motor 5- of containing alcohol
2nd, the thick methyl esters settling tank rotating shaft 5-3 of containing alcohol, rotating disk 5-4, multiple rotary shaft 5-5, multiple pivoting leaf 5-6, the above-mentioned thick methyl esters of containing alcohol
Sedimentation tank body 5-1 side wall is provided with the thick methyl esters settling tank liquid inlet 5-7 of containing alcohol and containing alcohol glycerine liquid inlet 5-8, and bottom is set
It is equipped with containing alcohol thick methyl esters settling tank liquid outlet 5-9, the above-mentioned thick methyl esters settling tank motor 5-2 of containing alcohol and is fixed on the thick methyl esters sedimentation of containing alcohol
Tank body 5-1 top, the above-mentioned thick methyl esters settling tank rotating shaft 5-3 of containing alcohol are assemblied in the thick methyl esters settling tank motor 5-2 of above-mentioned containing alcohol, on
State rotating disk 5-4 and be vertically fixed on containing alcohol thick methyl esters settling tank rotating shaft 5-3, multiple rotary shaft 5-5 and vertically penetrate above-mentioned rotating disk 5-4 simultaneously
And above-mentioned rotating disk 5-4 marginal position is uniformly arranged on, each rotary shaft 5-5 is provided with multiple above-mentioned pivoting leaf 5-6.
Pivoting leaf 5-6 of above-mentioned rotary shaft or so is arranged alternately.
By setting rotating disk 5-4 and multiple rotary shaft 5-5, it is possible to increase stirring efficiency, improve the sedimentation effect of settling tank
Fruit.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow be familiar with this art
Personage can understand present invention and be carried out, and it is not intended to limit the scope of the present invention.It is all according to the present invention
The equivalent change or modification that Spirit Essence is made, it should all cover within the scope of the present invention.
Claims (3)
- A kind of 1. ester exchange reaction device of surfactant, it is characterised in that including be sequentially connected transesterification reactor, contain The thick methyl esters settling tank of alcohol；The transesterification reactor includes ester exchange reaction kettle, transesterification reactor motor, transesterification reactor rotating shaft, multiple Retainer plate, multiple transesterification reactor paddles, multiple dividing plates, the top and bottom of the ester exchange reaction kettle are set respectively There are transesterification reactor liquid inlet and transesterification reactor liquid outlet, the transesterification reactor motor is fixed on the ester exchange The transesterification reactor rotating shaft is simultaneously assembled in the top of reaction kettle body, and the multiple dividing plate is horizontally installed on the ester exchange reaction In kettle and multiple interconnected spaces are divided into, the fixed suit of transesterification reactor rotating shaft positioned at each space There is the retainer plate, the retainer plate outer surface is provided with equally distributed screwed hole, the transesterification reactor paddle One end is provided with the screw thread bar matched with screwed hole；The thick methyl esters settling tank of containing alcohol includes the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank motor of containing alcohol, the thick first of containing alcohol The rotating shaft of ester settling tank, rotating disk, multiple rotary shafts, multiple pivoting leafs, the side wall of the thick methyl esters sedimentation tank body of containing alcohol, which is provided with, to be contained The thick methyl esters settling tank liquid inlet of alcohol and containing alcohol glycerine liquid inlet, bottom is provided with the thick methyl esters settling tank liquid outlet of containing alcohol, described The thick methyl esters settling tank motor of containing alcohol is fixed on the top of the thick methyl esters sedimentation tank body of containing alcohol, the thick methyl esters settling tank rotating shaft dress of containing alcohol The thick methyl esters settling tank motor of the containing alcohol is fitted over, the rotating disk is vertically fixed on the thick methyl esters settling tank rotating shaft of containing alcohol, multiple rotations Axle vertically penetrates the rotating disk and is uniformly arranged on the marginal position of the rotating disk, and each rotary shaft is provided with multiple described Pivoting leaf.
- 2. the ester exchange reaction device of surfactant according to claim 1, it is characterised in that the dividing plate is provided with Two, and the increased number of transesterification reactor paddle that retainer plate from top to bottom is assembled.
- 3. the ester exchange reaction device of surfactant according to claim 1, it is characterised in that the rotation of the rotary shaft Rotating vane or so is arranged alternately.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710952322.XA CN107583586A (en) | 2017-10-13 | 2017-10-13 | The ester exchange reaction device of surfactant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710952322.XA CN107583586A (en) | 2017-10-13 | 2017-10-13 | The ester exchange reaction device of surfactant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107583586A true CN107583586A (en) | 2018-01-16 |
Family
ID=61054014
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710952322.XA Pending CN107583586A (en) | 2017-10-13 | 2017-10-13 | The ester exchange reaction device of surfactant |
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| JP2009298982A (en) * | 2008-06-17 | 2009-12-24 | Hitachi Zosen Corp | Tank and method for liquid-liquid separation of crude biodiesel fuel from glycerol |
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| CN103785341A (en) * | 2014-01-24 | 2014-05-14 | 广州市凯闻食品发展有限公司 | High-efficiency mixed continuous transesterification reactor |
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| CN106062039A (en) * | 2014-04-30 | 2016-10-26 | 株式会社吴羽 | Polyarylene sulfide production method, and polyarylene sulfide production apparatus |
| CN106731951A (en) * | 2017-01-17 | 2017-05-31 | 湖州光博生物科技有限公司 | A kind of plant glue agitating device |
| CN206404773U (en) * | 2016-12-26 | 2017-08-15 | 苏州高夫高分子材料有限公司 | A kind of novel reaction kettle agitating device |
| CN207324827U (en) * | 2017-10-13 | 2018-05-08 | 安徽天意环保科技有限公司 | The ester exchange reaction device of surfactant |
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2017
- 2017-10-13 CN CN201710952322.XA patent/CN107583586A/en active Pending
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1441837A (en) * | 2000-07-12 | 2003-09-10 | 科金斯公司 | Transesterification process |
| JP2004067937A (en) * | 2002-08-08 | 2004-03-04 | Komatsu Mie Kk | Apparatus for producing fuel alternative for petroleum and its production method |
| JP2008161848A (en) * | 2007-01-04 | 2008-07-17 | Mitsubishi Rayon Co Ltd | Vertical-type multi-blades reaction tank and purification method of (meth)acrylic acid |
| JP2009298982A (en) * | 2008-06-17 | 2009-12-24 | Hitachi Zosen Corp | Tank and method for liquid-liquid separation of crude biodiesel fuel from glycerol |
| CN202530009U (en) * | 2012-04-01 | 2012-11-14 | 山东国邦药业股份有限公司 | D-ethyal ester production system |
| CN102641679A (en) * | 2012-05-21 | 2012-08-22 | 黄更生 | Multi-blade stirring device |
| CN203474763U (en) * | 2012-11-09 | 2014-03-12 | 广州市南洋国际工程技术服务公司 | Continuous ester exchange reactor and device |
| CN103785341A (en) * | 2014-01-24 | 2014-05-14 | 广州市凯闻食品发展有限公司 | High-efficiency mixed continuous transesterification reactor |
| CN106062039A (en) * | 2014-04-30 | 2016-10-26 | 株式会社吴羽 | Polyarylene sulfide production method, and polyarylene sulfide production apparatus |
| CN204395960U (en) * | 2015-01-13 | 2015-06-17 | 迈安德集团有限公司 | A kind of ester exchange reaction device |
| CN206404773U (en) * | 2016-12-26 | 2017-08-15 | 苏州高夫高分子材料有限公司 | A kind of novel reaction kettle agitating device |
| CN106731951A (en) * | 2017-01-17 | 2017-05-31 | 湖州光博生物科技有限公司 | A kind of plant glue agitating device |
| CN207324827U (en) * | 2017-10-13 | 2018-05-08 | 安徽天意环保科技有限公司 | The ester exchange reaction device of surfactant |
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