CN107561461A - A kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor - Google Patents

A kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor Download PDF

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Publication number
CN107561461A
CN107561461A CN201710585191.6A CN201710585191A CN107561461A CN 107561461 A CN107561461 A CN 107561461A CN 201710585191 A CN201710585191 A CN 201710585191A CN 107561461 A CN107561461 A CN 107561461A
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China
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magnetoresistive transducer
excitation coil
magnetic
field
magnetic permeability
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王超
白瑞峰
崔自强
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Tianjin University
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Tianjin University
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Abstract

The present invention relates to a kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor, detected for being pointed to high magnetic permeability catalyst identification in the multiphase flow system of pillars field areas with distributed mutually, magnetoresistive transducer and electro-magnetic screen layer, excitation coil and magnetoresistive transducer are placed in inside electro-magnetic screen layer including M excitation coil, N;Each excitation coil has individually excitation passage;Excitation coil is arranged on the same section outside pillars field areas;Each pair of magnetoresistive transducer is also arranged herein on same section, and excitation coil is arranged in from magnetoresistive transducer on different circumference, and each pair magnetoresistive transducer is respectively positioned on inside some excitation coil;Each pair magnetoresistive transducer can detect the magnetic field size of object field radially and tangentially.

Description

A kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor
Technical field
The invention belongs to the heterogeneous fluid imaging field of fluidization technology, more particularly to magnetic conductivity electricity tomography fills Put.
Background technology
Fluidization technology has very high heat transfer and mass-transfer efficiency and the ability of a large amount of processing particles, extensive use The gasification of burning, coal in solid fuel and coking, the conveying of solid material, the gas in Chemical Manufacture, solid catalysis reaction, The field such as dry materials, heating and cooling, petroleum cracking, metallurgy, environmental protection, and its application field is also constantly expanding.
The identification of multiphase fluid mapper process multiphase is most important, and the especially identification of solid-phase catalyst and the monitoring of distribution can Effectively avoid the abnormal fluidized state such as bulla, slugging and channel, improve production efficiency, instruct the designing of fluid bed, industry amplification And optimization.The raising of solid loading is advantageous to improve the volume utilization of reactor, so as to improve reaction rate and production concentration, Can also there is the traditional measurement side such as situations such as local granule accumulation, conducting probe, Pitot tube, optical fiber probe, ultrasonic probe simultaneously Method all cisco unity malfunctions easily damage.
In conventional gas-liquid is solid three-phase fluid bed, gas phase is generally air, hydrogen etc., and liquid phase is water or oil, and solid phase is to urge Agent.Gas phase, liquid phase do not have magnetic conductivity typically, and catalyst per se with high magnetic permeability or can make it by modified mode With high magnetic permeability, solid phase is substantially distinguished from gas-liquid two-phase on magnetic conductivity.The electromagnetic chromatography imaging technique sensitive to magnetic conductivity (Electromagnetic Tomography, abbreviation EMT) has the characteristics of radiationless, to be suitable for opaque tube wall and fluid can Realize mutually identification and the distribution measuring of solid-phase catalyst, and its temporal resolution is up to Millisecond, fully meet fluid bed compared with Measurement request under the conditions of high apparent gas phase and liquid velocity.
Traditional EMT uses coil stimulating Coil Detector mode, and measuring coil sensitivity is directly proportional to frequency, and improves Frequency, application of the technology on large scale fluid bed can be limited again.Simultaneously because the size of coil is not easy the very little designed, this Limit the number and accuracy of detection of excitation detection coil.
Traditional EMT is based primarily upon vortex principle, and point of electrical conductivity is obtained by the induced-current (secondary field information) of coil Cloth, and then the differentiation for the phase realized, secondary field field strength are relatively weak so that EMT accuracy of detection is severely limited, in order to improve The induced-current of coil brings serious test and cost consumption, it is necessary to improve the amplitude and frequency of excitation field for exciting circuit.
The content of the invention
The purpose of the present invention is overcome the shortcomings of in prior art, there is provided one kind is used for high magnetic permeability in multiphase flow system and urged Agent identifies and the high sensitivity of distributed mutually detection, good reliability sensor.The technical scheme that the present invention takes is:
A kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor, for being pointed to the multiphase flow of pillars field areas The identification of high magnetic permeability catalyst detects with distributed mutually in system, including M excitation coil, N are to magnetoresistive transducer and electromagnetic shielding Layer, excitation coil and magnetoresistive transducer are placed in inside electro-magnetic screen layer;Each excitation coil has individually excitation passage;Swash Coil configuration is encouraged on the same section outside pillars field areas;Each pair of magnetoresistive transducer is also arranged same section herein On, excitation coil is arranged in from magnetoresistive transducer on different circumference, and each pair magnetoresistive transducer is respectively positioned on some excitation coil It is internal;Each pair magnetoresistive transducer can detect the magnetic field size of object field radially and tangentially.
Brief description of the drawings
Fig. 1 is electromagnetic chromatographic imaging system structural representation
Fig. 2 illustrates the structure of electromagnetic chromatographic imaging system.In figure, 1 represents outer layer electro-magnetic screen layer;2 represent pipeline;3 Excitation coil is represented, shares 8 excitation coils in Fig. 2, it is expansible in real system, if the number of excitation coil is M;4 tables Show the magnetoresistive transducer of two kinds of different placement directions, each two is one group, respectively has one group in the center of each coil, its is quick Sense direction of principal axis is mutually perpendicular to, and is respectively used to measure magnetic field intensity axially and radially.
5 expression thing field areas.8 pairs, i.e. 16 magnetoresistive transducers are illustrated in Fig. 2, it is actual expansible, if magnetoresistive transducer Number be N pairs.
Fig. 3 electromagnetic chromatographic imaging system Sensor Design sectional views
In figure, 1:Electromagnetism magnetic masking layer 2:Pipeline 3:Excitation coil 4:Magnetoresistive transducer 5:Object field region.
Fig. 4 illustrates magnetoresistive transducer sensitivity direction of principal axis
5 expression thing field areas in figure, 8 and 9 be a pair of magnetoresistive transducers, measures the tangential and radial magnetic field of the position respectively Intensity.
Fig. 5 employs the structural representation of one embodiment of the electromagnetic chromatographic imaging system of sensor of the invention
Embodiment
The present invention devises fluidization electromagnetic chromatographic magnetoresistive transducer array, for being pointed to pillars field areas The identification of high magnetic permeability catalyst detects with distributed mutually in multiphase flow system.Magnetic approach is directly detected by magnetic resistance, magnetic can be obtained Conductance is distributed, and realizes that magnetic conductivity distribution parameter measurement is imaged with magnetic conductivity.Magnetoresistive transducer, detection sensitivity are not excited exciting field The influence of frequency, substantially increases the scope of application, simultaneously because it has, high sensitivity, good reliability, measurement range be wide, anti-evil The advantages that bad environment, small volume, is more and more favored.Introduce magnetoresistive transducer, because its size is small, generally 5mm with It is interior, the direct detection radially and tangentially in magnetic field can be achieved, increase test point number, improve the detection sensitivity of system, simultaneously Reduce the demand to driving frequency.The EMT technologies that magnetic conductivity distribution is rebuild are designed, it is solid by magnetic conductivity distribution situation, identification Phase information simultaneously obtains its distributed image, and then to realize mutually identification and distribution parameter measurement with permeability substance.
Distribution of Magnetic Field can be changed when high magnetic permeability catalyst is placed in magnetic field space, magnetic field line density at high magnetic permeability material Greatly, while solid-phase catalyst can also produce faradic secondary field.Traditional EMT is using coil as field sensing component, mainly Principle based on vortex secondary field.Magnetic conductivity distribution can be directly obtained using magnetic resistance detection primary field, so as to obtain solid phase identification With distribution.The field strength of primary field will be significantly larger than faradic secondary field, and the use of magnetoresistive transducer can improve accuracy of detection, Hardware design limitation and cost are reduced simultaneously.
Because other coils can also influence the distribution in magnetic field near eddy current effect;But magnetic resistance as field sensing component just Be not in such case, this reduces the difficulty of image reconstruction.
Magnetoresistance refers to the phenomenon that the resistance value of some metals or semiconductor changes and changed with externally-applied magnetic field.This Invention make use of high sensitivity characteristic of the magnetic resistance to magnetic field, directly detects magnetic field intensity with it, overcomes traditional EMT Coil Detectors The problem of sensitivity is low under low frequency condition.
Electromagnetic chromatographic sensor is designed using magnetoresistive array, and magnetoresistive transducer can be divided into normal magnetic resistance (Ordinary Magneto resistance, OMR), giant magnetoresistance (Giant Magneto resistance, GMR), super huge magnetic Hinder (Colossal Magneto resistance, CMR), incorgruous magnetic resistance (Anisotropic magneto resistance, AMR), tunnel magneto-resistance effect (Tunnel Magneto resistance, TMR), the change of normal magnetic resistance resistance is typically smaller than 5%, Super giant magnetoresistance phase transition temperature is relatively low, and incorgruous magnetic resistance is adapted to weak magnetic measurement, considers accuracy of detection and excitation field scope GMR It is applied to the system with TMR.
Electromagnetic chromatographic sensor as shown in Figure 3, every group of magnetoresistive transducer are devised in order to improve detection sensitivity Sensitive direction of principal axis as shown in figure 4, detect object field radially and tangentially magnetic field, radial magnetic field a+bi, tangential magnetic field strength c respectively + di, then the magnetic field is x+yi by Vector modulation.
Illustrated with reference to the application scenarios of sensor of the invention.
In order to improve field strength and sensitivity, using symmetrical enhancing cycle motivation strategy, for shown in Fig. 3, note is as shown in the figure The three excitation coil of position is #1, and counterclockwise is followed successively by #2 to #M (M is even number, and coil is symmetrically placed). Identical alternating current, and two excitation coils are applied to excitation coil #1 and its symmetrical slot # M/2+1 excitation coils respectively first Caused magnetic direction is identical, and EMT systems scan the output signal of each magnetoresistive transducer successively;Then it is right successively in such a manner Coil #2, #3 ..., #M/2 and its symmetrical drive coil apply excitation, and measure magnetoresistive transducer output respectively, until completing complete Portion measures, and by radial direction and the Vector modulation x+yi of tangential magnetic resistance, finally gives its modulus value composition measured value vector U (P × 1).
Gathered data are utilized to obtain sensitivity matrix S (P × Q), wherein P is independent measurement number, and Q is pixel, is swashed It is M to encourage coil number, and the magnetoresistive transducer number of reception is N pairs, then independent measurement number P is M × N.
Sensitivity matrix inearized model is established, and it is normalized, U is that AVHRR NDVI value is vectorial in U=Sg formulas, S It is sensitivity matrix, g is the gray value vectors for representing the relative change of material magnetic conductivity.Unknown quantity g can be solved by known U. It is ill-condition matrix, using S but sensitivity matrix S is not square formationTInstead of inverse matrix.Build object function gμ=(STS+μI)- 1STU, wherein, I is unit matrix, and μ is regularization parameter, (STS+μI)-1STIt is the optimization weight of sensitivity field for regularization process Build matrix.It is imaged by the gray value in each pixel.

Claims (1)

  1. A kind of 1. high magnetic permeability catalyst fluidized bed electricity imaging sensor, for being pointed to the heterogeneous fluid of pillars field areas The identification of high magnetic permeability catalyst detects with distributed mutually in system, including M excitation coil, N be to magnetoresistive transducer and electro-magnetic screen layer, Excitation coil and magnetoresistive transducer are placed in inside electro-magnetic screen layer.Each excitation coil has individually excitation passage;Excitation Coil configuration is on the same section outside pillars field areas;Each pair of magnetoresistive transducer is also arranged herein on same section, Excitation coil is arranged in from magnetoresistive transducer on different circumference, and each pair magnetoresistive transducer is respectively positioned in some excitation coil Portion;Each pair magnetoresistive transducer can detect the magnetic field size of object field radially and tangentially.
CN201710585191.6A 2017-07-18 2017-07-18 A kind of high magnetic permeability catalyst fluidized bed electricity imaging sensor Pending CN107561461A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109557144A (en) * 2018-12-17 2019-04-02 天津大学 A kind of integrated capacitive/electromagnetic double-mode state layer analysis imaging sensor
CN111157396A (en) * 2020-01-16 2020-05-15 天津大学 Observation visual angle adjustable solid combustion reactor

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070268016A1 (en) * 2006-05-16 2007-11-22 Cheng-Chung Chi Apparatus for detecting magnetic signals and signals of electric tunneling
CN101566639A (en) * 2009-06-05 2009-10-28 天津大学 Molten steel flow-speed measurement method and device based on electromagnetic tomography
CN102271577A (en) * 2008-12-30 2011-12-07 皇家飞利浦电子股份有限公司 Method and system for magnetic induction tomography
CN102428381A (en) * 2009-03-17 2012-04-25 Lg伊诺特有限公司 System for signal detection of specimen using magnetic resistance sensor and detecting method of the same
CN104655656A (en) * 2014-12-05 2015-05-27 广州丰谱信息技术有限公司 Detection imaging method and detection imaging device based on broadband magnetic wave transmission model parameter identification

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070268016A1 (en) * 2006-05-16 2007-11-22 Cheng-Chung Chi Apparatus for detecting magnetic signals and signals of electric tunneling
CN102271577A (en) * 2008-12-30 2011-12-07 皇家飞利浦电子股份有限公司 Method and system for magnetic induction tomography
CN102428381A (en) * 2009-03-17 2012-04-25 Lg伊诺特有限公司 System for signal detection of specimen using magnetic resistance sensor and detecting method of the same
CN101566639A (en) * 2009-06-05 2009-10-28 天津大学 Molten steel flow-speed measurement method and device based on electromagnetic tomography
CN104655656A (en) * 2014-12-05 2015-05-27 广州丰谱信息技术有限公司 Detection imaging method and detection imaging device based on broadband magnetic wave transmission model parameter identification

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109557144A (en) * 2018-12-17 2019-04-02 天津大学 A kind of integrated capacitive/electromagnetic double-mode state layer analysis imaging sensor
CN111157396A (en) * 2020-01-16 2020-05-15 天津大学 Observation visual angle adjustable solid combustion reactor

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Application publication date: 20180109