CN107557905A - A kind of down jackets anti-static ventilation eider down and preparation method thereof - Google Patents
A kind of down jackets anti-static ventilation eider down and preparation method thereof Download PDFInfo
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- CN107557905A CN107557905A CN201710732753.5A CN201710732753A CN107557905A CN 107557905 A CN107557905 A CN 107557905A CN 201710732753 A CN201710732753 A CN 201710732753A CN 107557905 A CN107557905 A CN 107557905A
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Abstract
The invention discloses a kind of down jackets anti-static ventilation eider down, including 80 110 parts of poultry feather, 12 17 parts of goose down, 35 55 parts of ramee, 8 10 parts of dressing liquid, 47 parts of protein degradation liquid, 0.2 2.3 parts of 0.5 3.5 part, nanometer di-iron trioxide of betaine, 2.2 3.8 parts of alginate fibre spinning solution, 0.1 0.8 parts of sorbierite, 24 parts of water, 15 parts of antistatic additive, has the beneficial effect that:It can make that down jackets antistatic effect is good, gas permeability is strong after mentioned component Raw material processing, and antistatic property persistence is strong;Elasticity is good, and feel is soft, comfortable and easy to wear, and to no skin irritation, and eider down is more soft, frivolous;Proportioning components are reasonable, reduce production cost, have huge economic benefit and social benefit.
Description
Technical field
The present invention relates to textile technology field, specifically a kind of down jackets anti-static ventilation eider down and preparation method thereof.
Background technology
For textile easily because rubbing and sensing generation electrostatic in production and processing and use, caused electric charge is not easy loss,
Electrostatic phenomenon still unobvious in cellulose fibre processing, and the electrostatic interference of protein fibre is just more serious, although wool fibre has
Higher equilibrium moisture regain, but its mass specific resistance reaches highest in natural fiber;The universal relatively low synthetic fibers of regain,
Charge buildup phenomenon is more notable, and the electrification phenomenon of textile material can often cause fiber winding or plugging machine in wool manufacturing production
Part, semi-products or yarn is scared, broken end, Warp opening is unclear during weaving, and fabric folds phenomena such as uneven, influences production
It is smoothed out, in use, the accumulation of electrostatic charge easily causes dust to adhere to, clothes tangle limbs and produce adhesion discomfort textile
Sense;And pH value of blood can be caused to rise, calcium content reduces in blood, calcium content increase, blood glucose rise, Vitamin C content in urine
Decline, wear business suit insulation ground it is up walk when, static electricity on human body's current potential can reach more than 3000V, coat electrostatic potential
More than 8000V is can reach, higher electrostatic pressure can produce electric shock to human body, and cause electronic component to damage;Static discharge can
Cause the accidental explosion of explosive wastewater and electric spark workpiece;Electromagnetic radiation caused by static discharge can be to various electronic equipments, information system
System causes electromagnetic interference, so, it is necessary to carry out antistatic finish to textile.
Prior art such as Authorization Notice No. is the A of CN 107022805 Chinese invention patent, and the invention provides a kind of in situ
The preparation method of polymeric composite conduction/antistatic fibre, it includes, the surface modification of nanometer electricity-conductive powder, antistatic master granule
Prepare, and, antistatic master granule is dried into 2-8 hours in 100-180 DEG C of temperature, antistatic master granule and basic resin cut into slices mixed
Close uniformly, then carry out melt spinning, spinning speed 600-3000m/min, filament spinning component initial pressure 8-16MPa, obtain
In-situ polymerization composite conducting/antistatic fibre, the invention prepare new antistatic fibre using brand-new antistatic mechanism, had
Permanence antistatic function, mechanical performance can reach the standard of general fibre, fully meet various woven requirements, cost with
Antistatic final finishing is suitable, only using a quarter of white conductive fiber, reduces pollution, the invention can expand weaving
The outlet of product, the added value of textile is lifted, although the preparation method antistatic effect is notable, difficulty of processing is big, prepares and requires
Height, it is not easy to promote the use of.
The content of the invention
It is an object of the invention to provide a kind of antistatic effect, gas permeability, a kind of down jackets good to skin compatibility
With anti-static ventilation eider down and preparation method thereof.
The present invention is directed to the problem of being mentioned in above-mentioned technology, and the technical scheme taken is:A kind of down jackets are with antistatic
Gas eider down, including poultry feather 80-110 parts, goose down 12-17 parts, ramee 35-55 parts, dressing liquid 8-10 parts, protein degradation
Liquid 4-7 parts, betaine 0.5-3.5 parts, nanometer di-iron trioxide 0.2-2.3 parts, alginate fibre spinning solution 2.2-3.8
Part, sorbierite 0.1-0.8 parts, water 2-4 parts, antistatic additive 1-5 parts, down jackets can be made antistatic after mentioned component Raw material processing
Effect is good, gas permeability is strong, and antistatic property persistence is strong;Elasticity is good, and feel is soft, and to no skin irritation, compatibility is good, and
Eider down is more soft, frivolous;Proportioning components are reasonable, reduce production cost, have huge economic benefit and social benefit.
A kind of preparation method of down jackets anti-static ventilation eider down, preparation process are:
After weighing poultry feather, goose down mixing by formula ratio, autoclaving is carried out in the environment of 150 DEG C -200 DEG C to it, it is cold
But 4-8 hours are soaked after in alcohol, then are rinsed with clear water, then it are dried in the environment of 80 DEG C -100 DEG C, most
After be ground into powder it is standby;
Ground feather meal is added in dressing liquid to stir, and 1 ~ 1.5h of preliminary drying under 90 DEG C of -95 DEG C of environment, is then existed again
Drying is carried out at a temperature of 120 DEG C -150 DEG C and removes solvent, obtains modified fish oil powder;
Modified fish oil powder is added in protein degradation liquid, sealing is placed in 30 ~ 45min at 90 DEG C -100 DEG C, is then removed with gauze
Residue, obtain feather keratin solution for standby;
Betaine, nanometer di-iron trioxide, alginate fibre spinning solution, sorbierite, water are added by formula ratio to mix
Uniformly, then by ramee cellulose sulfonate solution is processed into through yellow again after dipping by lye, it is rear to add in trimethylammonium second
Ester mixed solution is stirred, and progress wet spinning is then mixed with standby feather protein solution and obtains feather protein viscose;
Spinning is carried out by the way that keratin solution and modified ramee lysate are well mixed, greatly enhances feather fiber
The characteristics such as toughness, tensile strength, fragility, wearability, spinnability, improve productive value and social benefit, the nanometer three of addition
The ventilative of down fiber, electromagnetic radiation resistant, sterilization, mould proof can be strengthened by aoxidizing two iron, alginate fibre, sorbierite and interacting
Etc. performance, non-stimulated to skin, preparation method is simple, is worthy to be popularized.
By obtained feather protein viscose successively carry out solidification processing, pickling, washing drying obtain albumen feather fiber
It is standby;
Obtained albumen feather fiber is impregnated into the antistatic additive by the configuration of certain recipe ratio, obtained after drying and processing anti-quiet
The ventilative albumen feather fiber of electricity, then feather fiber is made into artificial eider down.By adding antiseptic, to possess eider down antistatic, anti-
Tide, ventilative characteristic.
Protein degradation liquid contains urea 4-8 parts, potassium metabisulfite 0.1-0.5 parts, lauryl sodium sulfate 0.02-0.4
Part, water 2-4 parts, by using protein degradation liquid made from suitable proportion make feather powder dissolve to obtain viscosity, rheological characteristic it is preferable
Keratin solution.
Dressing liquid includes silane coupler kh5906-9 parts, acetone soln 55-60 parts, is obtained by silane coupler modified
Dressing liquid, make mixing feather powder that there is excellent hydrophobic performance.
Antistatic additive includes laurate 1-3 parts, butanol 3-7 parts, titanate esters 6-11 parts, water 58-75 parts, catalyst amber
Sour 11-29 parts, active peptides 1-2 parts, antistatic additive and fiber have very strong adhesion, and fabric repeatedly after washing, still has
Excellent antistatic property, antistatic additive preparation method is simple to operate, reaction condition is gentle, environmental protection and energy saving.
The amino acid sequence of active peptides is SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC, by anti-quiet
The active peptides are added in electric agent, make in antistatic additive can better by active peptides from the hole inside and outside down fiber not
Penetrate into disconnectedly inside down fiber, after padding a period of time, it may occur that aggregation, stable is solidified to fibrous inside, close row
Row form complete conductive film, so as to preferably improve the antistatic effect of down fiber.
Compared with prior art, the advantage of the invention is that:
1. carrying out spinning by the way that keratin solution and modified ramee lysate are well mixed, feather is greatly enhanced
The characteristics such as the toughness of fiber, tensile strength, fragility, wearability, spinnability, improve productive value and social benefit;
2. the nanometer di-iron trioxide of addition, alginate fibre, sorbierite, which interact, can strengthen ventilative, the anti-electricity of down fiber
The performance of electromagnetic wave radiation, sterilization, mould proof etc., non-stimulated to skin, preparation method is simple, is worthy to be popularized;
3. amino acid sequence is SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC active peptides, make in antistatic additive
It can constantly be penetrated into better by active peptides from the hole inside and outside down fiber inside down fiber, when padding one section
Between after, it may occur that aggregation, stable is solidified to fibrous inside, and close-packed arrays form complete conductive film, so as to preferably
Improve the antistatic effect of down fiber;
4. proportioning components are reasonable, production cost is reduced, suitable for all kinds of clothes, fabric added value is improved, there is huge warp
Benefit of helping and social benefit.
Embodiment
The present invention program is described further below by embodiment:
Embodiment 1:
A kind of down jackets anti-static ventilation eider down, including poultry feather 80-110 parts, goose down 12-17 parts, ramee 35-55
Part, dressing liquid 8-10 parts, protein degradation liquid 4-7 parts, betaine 0.5-3.5 parts, nanometer di-iron trioxide 0.2-2.3
Part, alginate fibre spinning solution 2.2-3.8 parts, sorbierite 0.1-0.8 parts, water 2-4 parts, antistatic additive 1-5 parts.
A kind of preparation method of down jackets anti-static ventilation eider down, preparation process are:
1)After weighing poultry feather, goose down mixing by formula ratio, autoclaving is carried out in the environment of 150 DEG C -200 DEG C to it,
4-8 hours are soaked after cooling in alcohol, then are rinsed with clear water, then it is dried in the environment of 80 DEG C -100 DEG C,
Finally it is ground into powder standby;
2)Add ground feather meal in dressing liquid to stir, preliminary drying 1-1.5h, Ran Houzai under 90 DEG C of -95 DEG C of environment
Drying is carried out at a temperature of 120 DEG C -150 DEG C and removes solvent, obtains modified fish oil powder, dressing liquid composition is silane coupler
55 parts -60 parts of kh5906-9 parts, acetone soln;
3)Modified fish oil powder is added in protein degradation liquid, sealing is placed in 30-45min at 90 DEG C -100 DEG C, is then gone with gauze
Except residue, feather keratin solution for standby is obtained, protein degradation liquid composition is urea 4-8 parts, potassium metabisulfite 0.1-0.5
Part, lauryl sodium sulfate 0.02-0.4 parts, water 2-4 parts;
4)Betaine, nanometer di-iron trioxide, alginate fibre spinning solution, sorbierite, water are added by formula ratio to mix and stir
Mix uniformly, then ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, it is rear to add trimethylammonium second
Lactone mixed solution is stirred, and progress wet spinning is then mixed with standby feather protein solution and obtains feather protein viscose glue
Silk;
5)Obtained feather protein viscose is successively carried out to solidification processing, pickling, to obtain albumen feather fiber standby for washing drying
With;
6)Obtained albumen feather fiber is impregnated into the antistatic additive by the configuration of certain recipe ratio, resisted after drying and processing
The ventilative albumen feather fiber of electrostatic, then feather fiber is made into artificial eider down.
Antistatic additive includes laurate 1-3 parts, butanol 3-7 parts, titanate esters 6-11 parts, water 58-75 parts, catalyst amber
Sour 11-29 parts, active peptides 1-2 parts, the amino acid sequence of active peptides are
SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC。
Embodiment 2:
A kind of down jackets anti-static ventilation eider down, including 90 parts of poultry feather, 12 parts of goose down, 35 parts of ramee, dressing liquid 8
Part, 4 parts of protein degradation liquid, 0.2 part of 0.5 part, nanometer di-iron trioxide of betaine, 2.2 parts of alginate fibre spinning solution, mountain
0.5 part of pears alcohol, 2 parts of water, 2 parts of antistatic additive.
A kind of most preferably preparation method of down jackets anti-static ventilation eider down, preparation process are:
1)After weighing poultry feather, goose down mixing by formula ratio, autoclaving is carried out in the environment of 165 DEG C to it, after cooling
Soak 5 hours in alcohol, then rinsed with clear water, then it is dried in the environment of 90 DEG C, last grind into powder
Shape is standby;
2)Add ground feather meal in dressing liquid to stir, the preliminary drying 1h under 95 DEG C of environment, then again at 120 DEG C
At a temperature of carry out drying and remove solvent, obtain modified fish oil powder, dressing liquid composition is that silane coupler kh5907 parts, acetone are molten
55 parts of liquid;
3)Modified fish oil powder is added in protein degradation liquid, sealing is placed in 45min at 100 DEG C, then removes residue with gauze, obtains
To feather keratin solution for standby, protein degradation liquid composition is 4 parts of urea, 0.3 part of potassium metabisulfite, lauryl sodium sulfate
0.2 part, 2 parts of water;
4)Betaine, nanometer di-iron trioxide, alginate fibre spinning solution, sorbierite, water are added by formula ratio to mix and stir
Mix uniformly, then ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, it is rear to add trimethylammonium second
Lactone mixed solution is stirred, and progress wet spinning is then mixed with standby feather protein solution and obtains feather protein viscose glue
Silk;
5)Obtained feather protein viscose is successively carried out to solidification processing, pickling, to obtain albumen feather fiber standby for washing drying
With;
6)Obtained albumen feather fiber is impregnated into the antistatic additive by the configuration of certain recipe ratio, resisted after drying and processing
The ventilative albumen feather fiber of electrostatic, then feather fiber is made into artificial eider down.
Antistatic additive includes 2 parts of laurate, 4 parts of butanol, 5 parts of titanate esters, 65 parts of water, 20 parts of catalyst butanedioic acid,
1 part of active peptides, the amino acid sequence of active peptides is SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC.
Embodiment 3:
A kind of down jackets anti-static ventilation eider down, including 100 parts of poultry feather, 14 parts of goose down, 32 parts of ramee, dressing liquid
7 parts, 5 parts of protein degradation liquid, 0.3 part of 0.3 part, nanometer di-iron trioxide of betaine, 2.3 parts of alginate fibre spinning solution,
0.6 part of sorbierite, 3 parts of water, 2.5 parts of antistatic additive.
A kind of most preferably preparation method of down jackets anti-static ventilation eider down, preparation process are:
1)After weighing poultry feather, goose down mixing by formula ratio, autoclaving is carried out in the environment of 168 DEG C to it, after cooling
Soak 6 hours in alcohol, then rinsed with clear water, then it is dried in the environment of 100 DEG C, last grind into powder
Shape is standby;
2)Add ground feather meal in dressing liquid to stir, the preliminary drying 1.5h under 95 DEG C of environment, then again at 130 DEG C
At a temperature of carry out drying and remove solvent, obtain modified fish oil powder, dressing liquid composition is silane coupler kh5908 parts, acetone
60 parts of solution;
3)Modified fish oil powder is added in protein degradation liquid, sealing is placed in 40min at 110 DEG C, then removes residue with gauze, obtains
To feather keratin solution for standby, protein degradation liquid composition is 5 parts of urea, 0.5 part of potassium metabisulfite, lauryl sodium sulfate
0.4 part, 4 parts of water;
4)Betaine, nanometer di-iron trioxide, alginate fibre spinning solution, sorbierite, water are added by formula ratio to mix and stir
Mix uniformly, then ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, it is rear to add trimethylammonium second
Lactone mixed solution is stirred, and progress wet spinning is then mixed with standby feather protein solution and obtains feather protein viscose glue
Silk;
5)Obtained feather protein viscose is successively carried out to solidification processing, pickling, to obtain albumen feather fiber standby for washing drying
With;
6)Obtained albumen feather fiber is impregnated into the antistatic additive by the configuration of certain recipe ratio, resisted after drying and processing
The ventilative albumen feather fiber of electrostatic, then feather fiber is made into artificial eider down.
Antistatic additive includes 3 parts of laurate, 5 parts of butanol, 6 parts of titanate esters, 66 parts of water, 24 parts of catalyst butanedioic acid, lives
2 parts of polypeptide of property, the amino acid sequence of active peptides is SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC.
Routine operation in the operating procedure of the present invention is well known to those skilled in the art, herein without repeating.
Technical scheme is described in detail embodiment described above, it should be understood that it is described above only
For the specific embodiment of the present invention, it is not intended to limit the invention, all any modifications made in the spirit of the present invention,
Supplement or similar fashion replacement etc., should be included in the scope of the protection.
Sequence table
<110>Sea salt sends Mortopl Science and Technology Ltd.
<120>A kind of down jackets anti-static ventilation eider down and preparation method thereof
<160> 1
<170> SIPOSequenceListing 1.0
<210> 1
<211> 35
<212> PRT
<213>Artificial synthesized (Mytilus coruscus)
<400> 1
Ser Cys Ala Cys Arg Cys Lys Ala His Cys Arg Ala Arg Arg Cys Gly
1 5 10 15
Lys Gly Val Ser Val Ala His Arg Gly Arg Cys Ile Tyr Ser Val Cys
20 25 30
Leu Arg Cys
35
Claims (6)
- A kind of 1. down jackets anti-static ventilation eider down, it is characterised in that:Including poultry feather 80-110 parts, goose down 12-17 parts, Ramee 35-55 parts, dressing liquid 8-10 parts, protein degradation liquid 4-7 parts, betaine 0.5-3.5 parts, nanometer three aoxidize Two iron 0.2-2.3 parts, alginate fibre spinning solution 2.2-3.8 parts, sorbierite 0.1-0.8 parts, water 2-4 parts, antistatic additive 1-5 parts.
- A kind of 2. down jackets preparation method of anti-static ventilation eider down, it is characterised in that:The step that described preparation method includes Suddenly it is:1)After weighing poultry feather, goose down mixing by formula ratio, autoclaving is carried out in the environment of 150 DEG C -200 DEG C to it, 4-8 hours are soaked after cooling in alcohol, then are rinsed with clear water, then it is dried in the environment of 80 ° DEG C -100 DEG C, Finally it is ground into powder standby;2)Add ground feather meal in dressing liquid to stir, 1 ~ 1.5h of preliminary drying, Ran Houzai under 90 DEG C of -95 DEG C of environment Drying is carried out at a temperature of 120 DEG C -150 DEG C and removes solvent, obtains modified fish oil powder;3)Modified fish oil powder is added in protein degradation liquid, sealing is placed in 30 ~ 45min at 90 DEG C -100 DEG C, is then gone with gauze Except residue, feather keratin solution for standby is obtained;4)Betaine, nanometer di-iron trioxide, alginate fibre spinning solution, sorbierite, water are added by formula ratio to mix and stir Mix uniformly, then ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, it is rear to add trimethylammonium second Lactone mixed solution is stirred, and progress wet spinning is then mixed with standby feather protein solution and obtains feather protein viscose glue Silk;5)The successively progress coagulating bath processing of obtained feather protein viscose, pickling, washing drying are obtained into albumen feather fiber It is standby;6)Obtained albumen feather fiber is impregnated into antistatic additive, anti-static ventilation albumen feather fibre is obtained after drying and processing Dimension, then feather fiber is made into artificial eider down.
- A kind of 3. preparation method of down jackets anti-static ventilation eider down according to claim 2, it is characterised in that:It is described The protein degradation liquid of step 3 contains urea 4-8 parts, potassium metabisulfite 0.1-0.5 parts, lauryl sodium sulfate 0.02-0.4 Part, water 2-4 parts.
- A kind of 4. preparation method of down jackets anti-static ventilation eider down according to claim 2, it is characterised in that:It is described The dressing liquid of step 2 includes silane coupler kh5906-9 parts, 55 parts -60 parts of acetone soln.
- A kind of 5. preparation method of down jackets anti-static ventilation eider down according to claim 1, it is characterised in that:It is described Antistatic additive includes laurate 1-3 parts, butanol 3-7 parts, titanate esters 6-11 parts, water 58-75 parts, catalyst butanedioic acid 11-29 Part, active peptides 1-2 parts.
- A kind of 6. preparation method of down jackets anti-static ventilation eider down according to claim 5, it is characterised in that:It is described The amino acid sequence of active peptides is SCACRCKAHCRARRCGKGVSVAHRGRCIYSVCLRC.
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