CN107503195B - A kind of dyeing waste water dyeing inorganic agent and preparation method thereof - Google Patents
A kind of dyeing waste water dyeing inorganic agent and preparation method thereof Download PDFInfo
- Publication number
- CN107503195B CN107503195B CN201710572576.9A CN201710572576A CN107503195B CN 107503195 B CN107503195 B CN 107503195B CN 201710572576 A CN201710572576 A CN 201710572576A CN 107503195 B CN107503195 B CN 107503195B
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- dyeing
- agent
- waste water
- water
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/30—Nature of the water, waste water, sewage or sludge to be treated from the textile industry
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2305/00—Use of specific compounds during water treatment
- C02F2305/04—Surfactants, used as part of a formulation or alone
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The present invention discloses a kind of dyeing waste water dyeing inorganic agent, raw material including following weight percent: the cleaning agent of 5-10%, the borax of 10-20%, the surfactant of 5-10%, the buffer of 3-5%, the anti-flocculating agent of 5-10%, the dispersing agent MF of 3-5%, the defoaming agent of 0.5-1%, the odium stearate of 10-20%；Surplus is water.Preparation method are as follows: be first diluted with water odium stearate, it is prepared into the aqueous solution that mass concentration is 10~20%, then aqueous solution is transferred in reaction kettle, surfactant is added, it is heated to 65~75 DEG C, cleaning agent and borax are sequentially added, is thoroughly mixed, is cooled to 35~45 DEG C, sequentially add defoaming agent, dispersing agent MF, buffer and anti-flocculating agent, after foam is eliminated naturally, finally plus after water is thoroughly mixed, the dyeing waste water dyeing inorganic agent is obtained.A kind of dyeing waste water dyeing inorganic agent of the present invention, can be improved the reproducibility of dyeing, it is ensured that dyeing quality and cloth cover effect.
Description
Technical field
The present invention relates to techniques of Dyeing Wastewater Treatment fields, and in particular to be a kind of dyeing waste water dyeing inorganic agent and
Preparation method.
Background technique
Dyeing waste water circulating dyeing process is the dyeing of one of innovation, be directly using dyeing waste water entirely as to
The dyeing water of dyeing and weaving object waste water treating agent, surfactant, dyeing used additives and dyestuff is added in dyeing, to complete
To the dyeing of dyeing and weaving object and the recycling of realization dyeing waste water, kill two birds with one stone.In the dyeing course of this technique, need out
Send out dyeing waste water a kind of and dye dedicated inorganic agent, improve the reproducibility of dyeing, it is ensured that dyeing quality and cloth cover effect, this case by
This is generated.
Summary of the invention
The purpose of the present invention is to provide a kind of dyeing waste water dyeing inorganic agents, can be improved the reproducibility of dyeing, really
Protect dyeing quality and cloth cover effect.
In order to achieve the above objectives, solution of the invention is:
A kind of dyeing waste water dyeing inorganic agent, the raw material including following weight percent:
A kind of dyeing waste water dyeing inorganic agent, the raw material including following weight percent:
The cleaning agent is the cleaning agent WFS288 that Shishi Wanfengsheng Bleaching and Dyeing Knitting Co., Ltd. provides.
The surfactant is the surfactant that Shishi Wanfengsheng Bleaching and Dyeing Knitting Co., Ltd. provides.
The buffer is disodium hydrogen phosphate.
The anti-flocculating agent is the anti-flocculating agent DN that Guangdong Demei Fine Chemical Co., Ltd. provides.
The defoaming agent is the defoaming agent that Zhejiang development of evil in febrile disease fine chemistry industry limited liability company provides.
The dyeing waste water dyeing preparation method of inorganic agent, comprising the following steps: will first account for raw material gross weight 10-20%
Odium stearate be diluted with water, be prepared into mass concentration be 10~20% aqueous solution, aqueous solution is then transferred to reaction kettle
In, 65~75 DEG C are heated to, then example sequentially adds the cleaning agent and 10- for accounting for raw material gross weight 5-10% by weight percentage
20% borax, is thoroughly mixed, and is cooled to 35~45 DEG C, then example by weight percentage sequentially adds and accounts for raw material gross weight
The defoaming agent of 0.5-1%, the dispersing agent MF of 3-5%, the buffer of 3-5% and 5-10% anti-flocculating agent, to foam nature
After elimination, finally plus after water is thoroughly mixed, the dyeing waste water dyeing inorganic agent is obtained.
After adopting the above technical scheme, a kind of dyeing waste water dyeing inorganic agent of the present invention, the effect of each raw material are as follows:
1, cleaning agent: cleaning cloth cover greasy dirt；
2, borax: there is softened water and pH value buffer function, cloth cover dirt can also be removed；
3, it surfactant: prevents dyestuff or impurity in dyeing waste water from adhering on the fabric, improves dyeing quality；
4, buffer: pH value in adjustable dye bath, so that dye bath keeps weak basic condition, in favor of dyeing；
5, oil emulsion, coloration, heavy metal ion and the other pollutants in water removal anti-flocculating agent: are removed；
6, dispersing agent MF: it may make that dye shade is bright-coloured, uniform coloring, improve fabric dye uptake；
7, it defoaming agent: quickly defoams；
8, stearic acid sodium: there is emulsification, infiltration, decontamination.
A kind of dyeing waste water dyeing inorganic agent of the present invention, has following distinguishing feature: (1) can be effectively prevented waste water
Impurity, residual dye adhere on the fabric again, and reduce the coloration in dyeing waste water；(2) there is certain buffer function, make
PH value in dye bath keeps stability；(3) reproducibility of dyeing is improved, it is ensured that dyeing quality and cloth cover effect.Therefore, of the invention
There is wide application value in dyeing waste water dyeing.
Specific embodiment
In order to further explain the technical solution of the present invention, being explained in detail below by specific embodiment the present invention
It states.
1, it prepares:
Being related to cleaning agent in following embodiment is the cleaning agent that Shishi Wanfengsheng Bleaching and Dyeing Knitting Co., Ltd. provides
WFS288, surfactant are the surfactant that Shishi Wanfengsheng Bleaching and Dyeing Knitting Co., Ltd. provides, and buffer is phosphoric acid
Disodium hydrogen, anti-flocculating agent are the anti-flocculating agent DN that Guangdong Demei Fine Chemical Co., Ltd. provides, and defoaming agent is Zhejiang biography
Change the defoaming agent that fine chemistry industry limited liability company provides.
Embodiment 1
A kind of dyeing waste water dyeing inorganic agent, prepares the following steps are included: will first account for the hard of raw material gross weight 15%
Resin acid sodium is diluted with water, and is prepared into the aqueous solution that mass concentration is 10%, then aqueous solution is transferred in reaction kettle, addition accounts for
The surfactant of raw material gross weight 10%, is heated to 70 DEG C, then example by weight percentage sequentially adds and accounts for raw material gross weight
10% cleaning agent and 20% borax, be thoroughly mixed, be cooled to 40 DEG C, then example by weight percentage is sequentially added and accounted for
The defoaming agent of raw material gross weight 1%, 4% dispersing agent MF, 5% buffer and 8% anti-flocculating agent, disappear naturally to foam
After removing, finally plus after water is thoroughly mixed, the dyeing waste water dyeing inorganic agent is obtained.In above-mentioned preparation method, initially
Water used in dilution stearic acid sodium and the total amount for being finally stirred water used account for the 27% of raw material gross weight.
Embodiment 2
A kind of dyeing waste water dyeing inorganic agent, prepares the following steps are included: will first account for the hard of raw material gross weight 10%
Resin acid sodium is diluted with water, and is prepared into the aqueous solution that mass concentration is 10%, then aqueous solution is transferred in reaction kettle, addition accounts for
The surfactant of raw material gross weight 5%, is heated to 70 DEG C, then example by weight percentage sequentially adds and accounts for raw material gross weight 5%
Cleaning agent and 10% borax, be thoroughly mixed, be cooled to 40 DEG C, then example by weight percentage sequentially adds and accounts for raw material
The defoaming agent of total weight 0.5%, 5% dispersing agent MF, 3% buffer and 10% anti-flocculating agent, disappear naturally to foam
After removing, finally plus after water is thoroughly mixed, the dyeing waste water dyeing inorganic agent is obtained.In above-mentioned preparation method, initially
Water used in dilution stearic acid sodium and the total amount for being finally stirred water used account for the 51.5% of raw material gross weight.
Embodiment 3
A kind of dyeing waste water dyeing inorganic agent, prepares the following steps are included: will first account for the hard of raw material gross weight 20%
Resin acid sodium is diluted with water, and is prepared into the aqueous solution that mass concentration is 10%, then aqueous solution is transferred in reaction kettle, addition accounts for
The surfactant of raw material gross weight 8%, is heated to 70 DEG C, then example by weight percentage sequentially adds and accounts for raw material gross weight 8%
Cleaning agent and 15% borax, be thoroughly mixed, be cooled to 40 DEG C, then example by weight percentage sequentially adds and accounts for raw material
The defoaming agent of total weight 0.8%, 3% dispersing agent MF, 4% buffer and 5% anti-flocculating agent, eliminated naturally to foam
Afterwards, finally plus after water is thoroughly mixed, the dyeing waste water dyeing inorganic agent is obtained.It is initially dilute in above-mentioned preparation method
The total amount released water used in stearic acid sodium and be finally stirred water used accounts for the 36.2% of raw material gross weight.
2, application method:
According to technique bath raio=1: 8 are put into dacron to be dyed into overflow dyeing machine, dyeing waste water are added, then to dye
Dyeing waste water dyeing inorganic agent, surfactant, dyeing used additives are added in dyeing waste water in color machine, according to dyeing needs
Dyestuff is added, after being warming up to 110 DEG C with the speed of 1.5 DEG C/min, overflow dyeing machine heat preservation operating 15 minutes, reusable heat exchanger was with 2
DEG C/speed of min is cooled to 70 DEG C, to the direct cloth outputting that do not wash cloth after good color, the dyeing of dacron is completed in dehydration.
3, compared with the dyeing effect of traditional dyeing process
Table 1 uses the dyeing quality contrast table of dyeing and traditional handicraft of the invention
From table 1 it follows that dyeing waste water dyeing of the invention to be applied to the dyer of dyeing waste water with inorganic agent
Helpful to the stability of dyeing in skill, the reproducibility of dyeing is high, and dyeing quality and cloth cover effect are good.
Above-described embodiment and non-limiting product form and style of the invention, the ordinary skill people of any technical field
The appropriate changes or modifications that member does it, all should be regarded as not departing from patent category of the invention.
Claims (2)
1. a kind of dyeing waste water dyeing inorganic agent, it is characterised in that: be made of the raw material of following weight percent:
The cleaning agent is cleaning agent WFS288, and the buffer is disodium hydrogen phosphate, and the anti-flocculating agent is anti-flocculating agent DN.
2. a kind of dyeing waste water dyeing inorganic agent according to claim 1, it is characterised in that: by following weight percent
Raw material composition:
The cleaning agent is cleaning agent WFS288, and the buffer is disodium hydrogen phosphate, and the anti-flocculating agent is anti-flocculating agent DN.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710572576.9A CN107503195B (en) | 2017-07-12 | 2017-07-12 | A kind of dyeing waste water dyeing inorganic agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710572576.9A CN107503195B (en) | 2017-07-12 | 2017-07-12 | A kind of dyeing waste water dyeing inorganic agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107503195A CN107503195A (en) | 2017-12-22 |
| CN107503195B true CN107503195B (en) | 2019-03-19 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710572576.9A Active CN107503195B (en) | 2017-07-12 | 2017-07-12 | A kind of dyeing waste water dyeing inorganic agent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113047069A (en) * | 2021-03-24 | 2021-06-29 | 广东溢达纺织有限公司 | Cleaning method for fabric mercerizing after-treatment |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101709554A (en) * | 2009-08-18 | 2010-05-19 | 石狮市万峰盛漂染织造有限公司 | Surfactant for woven fabric dye-bath retreat process and preparation method thereof |
| CN102250493A (en) * | 2011-06-09 | 2011-11-23 | 天津德凯化工股份有限公司 | Blue alkali resistant active dye |
| CN103243588A (en) * | 2013-06-08 | 2013-08-14 | 武汉纺织大学 | Method for dyeing terylene textile at high temperature and under high pressure |
| CN104233856A (en) * | 2014-08-20 | 2014-12-24 | 张家港市大新毛纺有限公司 | Dyeing composition for wool and polyester blended fabric |
-
2017
- 2017-07-12 CN CN201710572576.9A patent/CN107503195B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101709554A (en) * | 2009-08-18 | 2010-05-19 | 石狮市万峰盛漂染织造有限公司 | Surfactant for woven fabric dye-bath retreat process and preparation method thereof |
| CN102250493A (en) * | 2011-06-09 | 2011-11-23 | 天津德凯化工股份有限公司 | Blue alkali resistant active dye |
| CN103243588A (en) * | 2013-06-08 | 2013-08-14 | 武汉纺织大学 | Method for dyeing terylene textile at high temperature and under high pressure |
| CN104233856A (en) * | 2014-08-20 | 2014-12-24 | 张家港市大新毛纺有限公司 | Dyeing composition for wool and polyester blended fabric |
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| CN107503195A (en) | 2017-12-22 |
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