CN107503183A - A kind of dyeing of wear-resisting color blend polyester cloth - Google Patents
A kind of dyeing of wear-resisting color blend polyester cloth Download PDFInfo
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- CN107503183A CN107503183A CN201710843812.6A CN201710843812A CN107503183A CN 107503183 A CN107503183 A CN 107503183A CN 201710843812 A CN201710843812 A CN 201710843812A CN 107503183 A CN107503183 A CN 107503183A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/655—Compounds containing ammonium groups
- D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
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Abstract
The present invention relates to fabric processing technology field, more particularly to a kind of dyeing of wear-resisting color blend polyester cloth, including step S1：Blend polyester cloth preheats pad dyeing；Prepare pad dyeing preparation；Step S2：The hot color development of far infrared；Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing and stripping treatment is carried out 23 seconds to blend polyester design on fabric surface；Step S4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, handles 20min；Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, using softening agent impregnation, keeping temperature is 40 DEG C, handles 10 15min；Step S6：Padding type coating；And step S7：High temperature is dried；140 DEG C of keeping temperature dries 2 3min to cloth.
Description
Technical field
The present invention relates to fabric processing technology field, more particularly to a kind of dyeing of wear-resisting color blend polyester cloth.
Background technology
At present, the conventional fabric of in the market weaving face fabric mostly using cotton, terylene, cotton synthetic fibre and regenerated celulose fibre as
Main, although these fabrics can meet people's demand substantially, there is also some shortcomings.For example dacron has well resistance to
It is hot, but its hygroscopicity is poor, and electrostatic phenomenon is serious, is a kind of hard-packed hydrophobic fibre mainly due to polyester fiber,
Without specific dye radical in molecule, lack hydrophily, expanded level is low in water, and certain difficulty is brought to dyeing.
In recent years, continuing to bring out with tencel, multi-component fibre compound fabric application is more extensive, such as terylene and sheep
The fiber mixed fabrics such as hair, silk, vinegar fibre, spandex are due to the advantages of having gathered various fibers so that fabric has unique wind
Lattice, it is more and more popular with consumers.But there is upper dye green low, easy damaged, levelling in multicomponent blend fabric in dyeing process
Property poor, the problems such as color fastness is low, in order that easily colouring is uniform for blend fabric, it usually needs adding substantial amounts of salt promotees dye, increase
The difficulty of sewage disposal, damages to environment.
The content of the invention
It is an object of the invention to provide a kind of dyeing of wear-resisting color blend polyester cloth, solves yarn weaved fabric colouring
Rate is low, uneven, the not strong technical problem of color fastness of painting.
In order to solve the above-mentioned technical problem, the invention provides technical scheme to be：A kind of wear-resisting color blend polyester cloth
Dyeing, including step are as follows：
Step S1：Blend polyester cloth preheats pad dyeing；Pad dyeing preparation is prepared, pad dyeing preparation is put into staining bath carries out pre-add
Heat, 80-105 DEG C of holding 2-3min is preheated to, the staining bath pad dyeing is entered under the traction that blend polyester cloth is passed through into deflector roll；
Step S2：The hot color development of far infrared；Blend polyester cloth after preheating pad dyeing carries out carrying out heat into far-infrared baking oven
Color development, temperature control keep 2-3min at 210-235 DEG C；
Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing pair
Blend polyester design on fabric surface carries out the stripping treatment 2-3 seconds；
Step 4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, processing
20min；
Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, at softening agent dipping
Reason, keeping temperature are 40 DEG C, handle 10-15min；
Step S6：Padding type coating；Blend polyester cloth is imported in the coating solution of temperature≤30 DEG C and carry out padding type painting
Layer processing；And
Step S7：High temperature is dried；140 DEG C of keeping temperature dries 2-3min to cloth.
Further, the making of the pad dyeing preparation in the step S1 includes：In the mixed of cobaltous sulfate, ferrous sulfate and glauber salt
Powder is closed, adds deionized water mixing, heating water temperature stirs 0.5-1.5h to 30-55 DEG C, obtains preliminary preparation；Preliminary
Glycerine is added in preparation to be well mixed, and adds oxydiphthalic, AEO, trimethylolpropane, second
Anilide and disodium ethylene diamine tetraacetate mix, and are heated to 40-65 DEG C, handle 1.5-4h, obtain mix preparation；And
Catalyst, modifying agent, diffusant and surfactant are added in mix preparation to mix, and maintain the temperature at 25-40
DEG C, and ultrasonic reaction 0.5-2h is used, obtain final pad dyeing preparation.
Further, the catalyst is transglutaminase.
Further, the modifying agent is by chitosan and 2,3- epoxypropyltrimethylchloride chlorides composition.
Further, the diffusant is sodium metnylene bis-naphthalene sulfonate.
Further, the surfactant is cationic surfactant.
Further, the once washing in step S3 uses common cold water flush；And secondary washing uses normal temperature alkaline water
Dilution takes cloth padding type to carry out surface stripping treatment, and is subject to 1-3pa pick-ups.
Further, the alkaline rinsing solution is that MSA forms with the modulation of 30% solid content liquid caustic soda, wherein, MSA dosages are 2-
8g/L, liquid caustic soda dosage are 8-20g/L.
Further, in step S7,1-3pa pressure is subject to cloth；And the coating solution is that four surface-actives help
Agent, include nonionic modified polydimethylsiloxane emulsion, anion aliphatic polyester polyacids esters polyurethane dispersing liquid, non-
Inclined anion aliphatic polyester polyurethane dispersion liquid and water-based aliphatic polyester polyurethane dispersion liquid.
Further, the coating solution fitting method is：By nonionic modified polydimethylsiloxane emulsion be added to it is cloudy from
It is sufficiently mixed in sub- aliphatic polyester polyacids esters polyurethane dispersing liquid, by non-anion aliphatic polyester polyurethane dispersion liquid partially
It is added in water-based aliphatic polyester polyurethane dispersion liquid and is sufficiently mixed, two after being sufficiently mixed kind material mixes again, and
Less than 30 DEG C are maintained the temperature at, stirs 3-5min.
Beneficial effects of the present invention are：The present invention, as catalyst, can not only make terylene interspersion using transglutaminase
Network structure is formed in material, playing improves molecular functional effect, avoids cloth in dyeing course because damage causes to contaminate
Color effect is deteriorated, and improves rate of dyeing and reduces dyeing temperature.Add chitosan amount of money 2,3- epoxypropyl trimethylammonium chlorides
Ammonium more improves the binding strength of blend polyester cloth, so as to improve dye-uptake, realizes low salt dyeing；Diffusant uses methylene
Base sodium dinaphthalenesulfonate makes dyeing more it is possible to prevente effectively from diffusion of the blend polyester cloth molecular structure obstruction dyestuff in cloth
Uniformly；Cationic surfactant improves the flexibility, antistatic behaviour and bactericidal properties of blend polyester cloth.
Further, by the improvement to technique, improve to realize keeping the same of color fastness to dyeing and postfinishing process
When with good levelling effect.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the flow chart of the dyeing of the wear-resisting color blend polyester cloth of the present invention.
In figure：Step S1, step S2, step S3, step S4, step S5, step S6, step S7.
Embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These accompanying drawings are simplified schematic diagram, only with
Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant with the present invention.
Embodiment 1：
As shown in figure 1, the invention provides a kind of dyeing of wear-resisting color blend polyester cloth, including step are as follows：
Step S1：Blend polyester cloth preheats pad dyeing；Pad dyeing preparation is prepared, pad dyeing preparation is put into staining bath carries out pre-add
Heat, 80 DEG C of holding 3min are preheated to, the staining bath pad dyeing is entered under the traction that blend polyester cloth is passed through into deflector roll；
Step S2：The hot color development of far infrared；Blend polyester cloth after preheating pad dyeing carries out carrying out heat into far-infrared baking oven
Color development, temperature control keep 3min at 210- DEG C；
Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing pair
Blend polyester design on fabric surface carries out stripping treatment 3 seconds；
Step S4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, place
Manage 20min；
Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, at softening agent dipping
Reason, keeping temperature are 40 DEG C, handle 10min；
Step S6：Padding type coating；Blend polyester cloth is imported in the coating solution that temperature is 30 DEG C and carries out padding type painting
Layer processing；And
Step S7：High temperature is dried；140 DEG C of keeping temperature dries 3min to cloth.
Specifically, the making of the pad dyeing preparation in the step S1 includes：Take 0.5 part of cobaltous sulfate, 1 part of ferrous sulfate and member
Bright 0.5 part of powder, 10 parts of deionized waters are added, in the case where temperature is 25 DEG C, stir 0.5h.Obtain preliminary preparation；In preliminary preparation
It is well mixed to add 3 parts of glycerine, adds 3 parts of oxydiphthalic, 2 parts of AEO, trimethylolpropane 3
2 parts of part, 4 parts of antifebrin and disodium ethylene diamine tetraacetate mixings, are heated to 45 DEG C, handle 2h, obtain mix preparation；
And 1 part of catalyst transglutaminase, 2 parts of modifying agent chitosan and 2,3- glycidyl front threes are added in mix preparation
4 parts of 3 parts of ammonium chloride, 2 parts of diffusant sodium metnylene bis-naphthalene sulfonate and surfactant mixings, maintain the temperature at 30 DEG C,
And ultrasonic reaction 1.5h is used, obtains final pad dyeing preparation.
The catalyst is transglutaminase.Using transglutaminase as catalyst, terylene interspersion can not only be made
Network structure is formed in material, playing improves molecular functional effect, avoids cloth in dyeing course because damage causes to contaminate
Color effect is deteriorated, and improves rate of dyeing and reduces dyeing temperature.
The modifying agent is made up of chitosan and 2,3- epoxypropyltrimethylchloride chlorides.On the one hand because chitosan is in acid
In the property aqueous solution can and H+With reference to and there is good water solubility, on the other hand, in chitosan molecule introduce quaternary ammonium salt knot
Structure, it can be made to obtain good water solubility, and can be applied in larger pH range；In addition chitosan is in alkaline bar
The reactivity worth of nucleophilic addition occurs under part with blend polyester cloth, so as to improve the binding strength with polyester fiber, so as to real
Dye-uptake is now improved, realizes low salt dyeing.
The diffusant is sodium metnylene bis-naphthalene sulfonate.It is avoided that blend polyester cloth molecular structure hinders dyestuff in cloth
In diffusion, not only improve dye-uptake, level-dyeing property and color fastness, moreover it is possible to reduce the strength damage of fabric.
The surfactant is cationic surfactant.The surfactant is quaternary surfactant, is carried
The high flexibility of blend polyester cloth, antistatic behaviour, anti-yellowing property and bactericidal properties.
Once washing in step S3 uses common cold water flush；And secondary washing uses normal temperature alkalescence rinsing solution pair
Cloth takes padding type to carry out surface stripping treatment, and is subject to 3pa pick-ups.
The alkaline rinsing solution is that MSA and 30% solid content liquid caustic soda are modulated and formed, wherein, MSA dosages are 6g/L, liquid caustic soda
Dosage is 12g/L.
In step S7,3pa pressure is subject to cloth；And the coating solution is four surface-active auxiliary agents, is included
Nonionic modified polydimethylsiloxane emulsion, anion aliphatic polyester polyacids esters polyurethane dispersing liquid, non-inclined anion
Aliphatic polyester polyurethane dispersion liquid and water-based aliphatic polyester polyurethane dispersion liquid.
The coating solution fitting method is：Nonionic modified polydimethylsiloxane emulsion is added to anion aliphatic
It is sufficiently mixed in polyester polyacids esters polyurethane dispersing liquid, non-anion aliphatic polyester polyurethane dispersion liquid partially is added to water
It is sufficiently mixed in property aliphatic polyester polyurethane dispersion liquid, two after being sufficiently mixed kind material mixes again, and keeping temperature
Below 25 DEG C, 5min is stirred.Coating aid improves the smoothness of design on fabric surface, reduces the skin friction resistance of cloth, with
Improve colorfastness to rubbing.
Embodiment 2
The invention provides a kind of dyeing of wear-resisting color blend polyester cloth, including step are as follows：
Step S1：Blend polyester cloth preheats pad dyeing；Pad dyeing preparation is prepared, pad dyeing preparation is put into staining bath carries out pre-add
Heat, 105 DEG C of holding 2min are preheated to, the staining bath pad dyeing is entered under the traction that blend polyester cloth is passed through into deflector roll；
Step S2：The hot color development of far infrared；Blend polyester cloth after preheating pad dyeing carries out carrying out heat into far-infrared baking oven
Color development, temperature control keep 2min at 235 DEG C；
Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing pair
Blend polyester design on fabric surface carries out stripping treatment 2 seconds；
Step S4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, place
Manage 20min；
Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, at softening agent dipping
Reason, keeping temperature are 40 DEG C, handle 10min；
Step S6：Padding type coating；Blend polyester cloth is imported in the coating solution of 20 DEG C of temperature and carry out padding type coating
Processing；And
Step S7：High temperature is dried；140 DEG C of keeping temperature dries 3min to cloth.
Specifically, the making of the pad dyeing preparation in the step S1 includes：Take 1 part of cobaltous sulfate, 1.5 parts of ferrous sulfate and member
Bright 0.8 part of powder, 10 parts of deionized waters are added, in the case where temperature is 38 DEG C, stir 1h.Obtain preliminary preparation；Add in preliminary preparation
It is well mixed to enter 4 parts of glycerine, adds 4 parts of oxydiphthalic, 3 parts of AEO, trimethylolpropane 4
4 parts of part, 3 parts of antifebrin and disodium ethylene diamine tetraacetate mixings, are heated to 50 DEG C, handle 2.5h, obtain mixing system
Agent；And 2 parts of catalyst transglutaminase, 1 part of modifying agent chitosan and 2,3- glycidyl are added in mix preparation
5 parts of 3 parts of trimethyl ammonium chloride, 3 parts of diffusant sodium metnylene bis-naphthalene sulfonate and surfactant mixings, are maintained the temperature at
32 DEG C, and ultrasonic reaction 1.2h is used, obtain final pad dyeing preparation.
The catalyst is transglutaminase.Using transglutaminase as catalyst, terylene interspersion can not only be made
Network structure is formed in material, playing improves molecular functional effect, avoids cloth in dyeing course because damage causes to contaminate
Color effect is deteriorated, and improves rate of dyeing and reduces dyeing temperature.
The modifying agent is made up of chitosan and 2,3- epoxypropyltrimethylchloride chlorides.On the one hand because chitosan is in acid
In the property aqueous solution can and H+With reference to and there is good water solubility, on the other hand, in chitosan molecule introduce quaternary ammonium salt knot
Structure, it can be made to obtain good water solubility, and can be applied in larger pH range；In addition chitosan is in alkaline bar
The reactivity worth of nucleophilic addition occurs under part with blend polyester cloth, so as to improve the binding strength with polyester fiber, so as to real
Dye-uptake is now improved, realizes low salt dyeing.
The diffusant is sodium metnylene bis-naphthalene sulfonate.It is avoided that blend polyester cloth molecular structure hinders dyestuff in cloth
In diffusion, not only improve dye-uptake, level-dyeing property and color fastness, moreover it is possible to reduce the strength damage of fabric.
The surfactant is cationic surfactant.The surfactant is quaternary surfactant, is carried
The high flexibility of blend polyester cloth, antistatic behaviour, anti-yellowing property and bactericidal properties.
Once washing in step S3 uses common cold water flush；And secondary washing uses normal temperature alkalescence rinsing solution pair
Cloth takes padding type to carry out surface stripping treatment, and is subject to 3pa pick-ups.
The alkaline rinsing solution is that MSA and 30% solid content liquid caustic soda are modulated and formed, wherein, MSA dosages are 8g/L, liquid caustic soda
Dosage is 20g/L.
In step S7,3pa pressure is subject to cloth；And the coating solution is four surface-active auxiliary agents, is included
Nonionic modified polydimethylsiloxane emulsion, anion aliphatic polyester polyacids esters polyurethane dispersing liquid, non-inclined anion
Aliphatic polyester polyurethane dispersion liquid and water-based aliphatic polyester polyurethane dispersion liquid.
The coating solution fitting method is：Nonionic modified polydimethylsiloxane emulsion is added to anion aliphatic
It is sufficiently mixed in polyester polyacids esters polyurethane dispersing liquid, non-anion aliphatic polyester polyurethane dispersion liquid partially is added to water
It is sufficiently mixed in property aliphatic polyester polyurethane dispersion liquid, two after being sufficiently mixed kind material mixes again, and keeping temperature
At 28 DEG C, 5min is stirred.Coating aid improves the smoothness of design on fabric surface, reduces the skin friction resistance of cloth, to improve
Colorfastness to rubbing.
Embodiment 3
The invention provides a kind of dyeing of wear-resisting color blend polyester cloth, including step are as follows：
Step S1：Blend polyester cloth preheats pad dyeing；Pad dyeing preparation is prepared, pad dyeing preparation is put into staining bath carries out pre-add
Heat, 100 DEG C of holding 3min are preheated to, the staining bath pad dyeing is entered under the traction that blend polyester cloth is passed through into deflector roll；
Step S2：The hot color development of far infrared；Blend polyester cloth after preheating pad dyeing carries out carrying out heat into far-infrared baking oven
Color development, temperature control keep 2.5min at 220 DEG C；
Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing pair
Blend polyester design on fabric surface carries out stripping treatment 2 seconds；
Step S4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, place
Manage 20min；
Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, at softening agent dipping
Reason, keeping temperature are 40 DEG C, handle 10min；
Step S6：Padding type coating；Blend polyester cloth is imported in the coating solution of 25 DEG C of temperature and carry out padding type coating
Processing；And
Step S7：High temperature is dried；140 DEG C of keeping temperature dries 2.5min to cloth.
Specifically, the making of the pad dyeing preparation in the step S1 includes：Take 1.5 parts of cobaltous sulfate, 1 part of ferrous sulfate and member
Bright 0.5 part of powder, 10 parts of deionized waters are added, in the case where temperature is 45 DEG C, stir 0.8h.Obtain preliminary preparation；In preliminary preparation
It is well mixed to add 4 parts of glycerine, adds 4 parts of oxydiphthalic, 4 parts of AEO, trimethylolpropane 3
4 parts of part, 4 parts of antifebrin and disodium ethylene diamine tetraacetate mixings, are heated to 50 DEG C, handle 3h, obtain mix preparation；
And 0.5 part of catalyst transglutaminase, 3 parts of modifying agent chitosan and 2,3- glycidyl three are added in mix preparation
4 parts of 3 parts of ammonio methacrylate, 2 parts of diffusant sodium metnylene bis-naphthalene sulfonate and surfactant mixings, maintain the temperature at 40
DEG C, and ultrasonic reaction 2h is used, obtain final pad dyeing preparation.
The catalyst is transglutaminase.Using transglutaminase as catalyst, terylene interspersion can not only be made
Network structure is formed in material, playing improves molecular functional effect, avoids cloth in dyeing course because damage causes to contaminate
Color effect is deteriorated, and improves rate of dyeing and reduces dyeing temperature.
The modifying agent is made up of chitosan and 2,3- epoxypropyltrimethylchloride chlorides.On the one hand because chitosan is in acid
In the property aqueous solution can and H+With reference to and there is good water solubility, on the other hand, in chitosan molecule introduce quaternary ammonium salt knot
Structure, it can be made to obtain good water solubility, and can be applied in larger pH range；In addition chitosan is in alkaline bar
The reactivity worth of nucleophilic addition occurs under part with blend polyester cloth, so as to improve the binding strength with polyester fiber, so as to real
Dye-uptake is now improved, realizes low salt dyeing.
The diffusant is sodium metnylene bis-naphthalene sulfonate.It is avoided that blend polyester cloth molecular structure hinders dyestuff in cloth
In diffusion, not only improve dye-uptake, level-dyeing property and color fastness, moreover it is possible to reduce the strength damage of fabric.
The surfactant is cationic surfactant.The surfactant is quaternary surfactant, is carried
The high flexibility of blend polyester cloth, antistatic behaviour, anti-yellowing property and bactericidal properties.
Once washing in step S3 uses common cold water flush；And secondary washing uses normal temperature alkalescence rinsing solution pair
Cloth takes padding type to carry out surface stripping treatment, and is subject to 2pa pick-ups.
The alkaline rinsing solution is that MSA and 30% solid content liquid caustic soda are modulated and formed, wherein, MSA dosages are 6g/L, liquid caustic soda
Dosage is 20g/L.
In step S7,2pa pressure is subject to cloth；And the coating solution is four surface-active auxiliary agents, is included
Nonionic modified polydimethylsiloxane emulsion, anion aliphatic polyester polyacids esters polyurethane dispersing liquid, non-inclined anion
Aliphatic polyester polyurethane dispersion liquid and water-based aliphatic polyester polyurethane dispersion liquid.
The coating solution fitting method is：Nonionic modified polydimethylsiloxane emulsion is added to anion aliphatic
It is sufficiently mixed in polyester polyacids esters polyurethane dispersing liquid, non-anion aliphatic polyester polyurethane dispersion liquid partially is added to water
It is sufficiently mixed in property aliphatic polyester polyurethane dispersion liquid, two after being sufficiently mixed kind material mixes again, and keeping temperature
Below 30 DEG C, 5min is stirred.Coating aid improves the smoothness of design on fabric surface, reduces the skin friction resistance of cloth, with
Improve colorfastness to rubbing.
It is complete by above-mentioned description, relevant staff using the above-mentioned desirable embodiment according to the present invention as enlightenment
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to determines its technical scope according to right.
Claims (10)
1. a kind of dyeing of wear-resisting color blend polyester cloth, it is characterised in that as follows including step：
Step S1：Blend polyester cloth preheats pad dyeing；Pad dyeing preparation is prepared, pad dyeing preparation is put into staining bath and preheated, in advance
80-105 DEG C of holding 2-3min is heated to, the staining bath pad dyeing is entered under the traction that blend polyester cloth is passed through into deflector roll；
Step S2：The hot color development of far infrared；Blend polyester cloth after preheating pad dyeing carries out hot color development into far-infrared baking oven,
Temperature control keeps 2-3min at 210-235 DEG C；
Step S3：Wash stripping treatment；A washing cooling high temperature blend polyester cloth is carried out, then carries out secondary washing to terylene
Yarn weaved fabric surface carries out the stripping treatment 2-3 seconds；
Step S4：Fixation treatment；Blend polyester cloth is immersed in aldehyde-free colour stabilizer solution, keeping temperature is 45 DEG C, processing
20min；
Step S5：Soft treatment；After blend polyester cloth after fixation is carried out into low temperature drying, using softening agent impregnation,
Keeping temperature is 40 DEG C, handles 10-15min；
Step S6：Padding type coating；Blend polyester cloth is imported in the coating solution of temperature≤30 DEG C and carried out at padding type coating
Reason；And
Step S7：High temperature is dried；140 DEG C of keeping temperature dries 2-3min to cloth.
2. the dyeing of wear-resisting color blend polyester cloth according to claim 1, it is characterised in that in the step S1
The making of pad dyeing preparation include：
In the mixed-powder of cobaltous sulfate, ferrous sulfate and glauber salt, deionized water mixing is added, heats water temperature to 30-55 DEG C, and
0.5-1.5h is stirred, obtains preliminary preparation；
Glycerine is added in preliminary preparation to be well mixed, and adds oxydiphthalic, AEO, three hydroxyl first
Base propane, antifebrin and disodium ethylene diamine tetraacetate mix, and are heated to 40-65 DEG C, handle 1.5-4h, are mixed
Preparation；And
Catalyst, modifying agent, diffusant and surfactant are added in mix preparation to mix, and maintain the temperature at 25-
40 DEG C, and ultrasonic reaction 0.5-2h is used, obtain final pad dyeing preparation.
3. the dyeing of wear-resisting color blend polyester cloth according to claim 2, it is characterised in that the catalyst is
Transglutaminase.
4. the dyeing of wear-resisting color blend polyester cloth according to claim 2, it is characterised in that the modifying agent by
Chitosan and 2,3- epoxypropyltrimethylchloride chlorides composition.
5. the dyeing of wear-resisting color blend polyester cloth according to claim 2, it is characterised in that the diffusant is
Sodium metnylene bis-naphthalene sulfonate.
6. the dyeing of wear-resisting color blend polyester cloth according to claim 2, it is characterised in that the surface-active
Agent is cationic surfactant.
7. the dyeing of wear-resisting color blend polyester cloth according to claim 1, it is characterised in that one in step S3
Secondary washing uses common cold water flush；And
Secondary washing takes cloth padding type to carry out surface stripping treatment using normal temperature alkalescence rinsing solution, and is subject to 1-3pa
Pick-up.
8. the dyeing of wear-resisting color blend polyester cloth according to claim 7, it is characterised in that the alkalescence washing
Solution is that MSA forms with the modulation of 30% solid content liquid caustic soda, wherein, MSA dosages are 2-8g/L, and liquid caustic soda dosage is 8-20g/L.
9. the dyeing of wear-resisting color blend polyester cloth according to claim 1, it is characterised in that right in step S7
Cloth is subject to 1-3pa pressure；And
The coating solution is four surface-active auxiliary agents, includes nonionic modified polydimethylsiloxane emulsion, anion resin
Fat adoption ester polyacids esters polyurethane dispersing liquid, non-anion aliphatic polyester polyurethane dispersion liquid and water-based aliphatic polyester partially
Polyurethane dispersing liquid.
10. the dyeing of wear-resisting color blend polyester cloth according to claim 9, it is characterised in that：The coating solution
Fitting method is：Nonionic modified polydimethylsiloxane emulsion is added to anion aliphatic polyester polyacids esters polyurethane
It is sufficiently mixed in dispersion liquid, non-anion aliphatic polyester polyurethane dispersion liquid partially is added to water-based aliphatic polyester polyurethane
It is sufficiently mixed in dispersion liquid, two after being sufficiently mixed kind material mixes again, and maintains the temperature at less than 30 DEG C, stirs 3-
5min。
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| CN201710843812.6A CN107503183A (en) | 2017-09-19 | 2017-09-19 | A kind of dyeing of wear-resisting color blend polyester cloth |
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| CN101225603A (en) * | 2007-11-30 | 2008-07-23 | 东华大学 | Darkening washing method for improving color depth of wool color fabric by using transglutaminase |
| CN106758408A (en) * | 2016-12-20 | 2017-05-31 | 长兴宝诺纺织科技有限公司 | A kind of blend polyester dyeing fabric liquid and preparation method thereof |
| CN106758377A (en) * | 2016-12-20 | 2017-05-31 | 长兴宝诺纺织科技有限公司 | A kind of blend polyester dyeing fabric liquid |
| CN106811894A (en) * | 2017-01-22 | 2017-06-09 | 华懋（厦门）新材料科技股份有限公司 | It is a kind of to improve terylene ribbon colour fastness to rubbing and the uneven technique of dyeing |
| CN106835757A (en) * | 2017-04-21 | 2017-06-13 | 长兴宝诺纺织科技有限公司 | A kind of blend polyester dyeing fabric technique |
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2017
- 2017-09-19 CN CN201710843812.6A patent/CN107503183A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101225603A (en) * | 2007-11-30 | 2008-07-23 | 东华大学 | Darkening washing method for improving color depth of wool color fabric by using transglutaminase |
| CN106758408A (en) * | 2016-12-20 | 2017-05-31 | 长兴宝诺纺织科技有限公司 | A kind of blend polyester dyeing fabric liquid and preparation method thereof |
| CN106758377A (en) * | 2016-12-20 | 2017-05-31 | 长兴宝诺纺织科技有限公司 | A kind of blend polyester dyeing fabric liquid |
| CN106811894A (en) * | 2017-01-22 | 2017-06-09 | 华懋（厦门）新材料科技股份有限公司 | It is a kind of to improve terylene ribbon colour fastness to rubbing and the uneven technique of dyeing |
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