CN107503171A - A kind of colouring method of Acrylic Fiber - Google Patents

A kind of colouring method of Acrylic Fiber Download PDF

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Publication number
CN107503171A
CN107503171A CN201710928076.4A CN201710928076A CN107503171A CN 107503171 A CN107503171 A CN 107503171A CN 201710928076 A CN201710928076 A CN 201710928076A CN 107503171 A CN107503171 A CN 107503171A
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CN
China
Prior art keywords
levelling agent
warming
acrylic fibers
acrylic
dyestuff
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710928076.4A
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Chinese (zh)
Inventor
夏铁
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WUXI SHILEAD BLEACHING AND DYEING CO Ltd
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WUXI SHILEAD BLEACHING AND DYEING CO Ltd
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Priority to CN201710928076.4A priority Critical patent/CN107503171A/en
Publication of CN107503171A publication Critical patent/CN107503171A/en
Withdrawn legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/0032Determining dye recipes and dyeing parameters; Colour matching or monitoring
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/445Use of auxiliary substances before, during or after dyeing or printing
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/70Material containing nitrile groups

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Coloring (AREA)

Abstract

The invention provides a kind of colouring method of Acrylic Fiber, and it can not be tested after solving the problems, such as existing Acrylic Fiber dyeing by antiallergy.It comprises the following steps:Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;Step 2: opening impregnating mangle, Acrylic Fiber, water inlet are added, it is warming up to 70 DEG C and plays dye, first adds acrylic fibers levelling agent, the model RX8202 of the acrylic fibers levelling agent, dyestuff is added, the concentration of the dyestuff is less than 0.1%, is then warming up to 85 DEG C with 0.33 DEG C/min ~ 0.5 DEG C/min speed;Step 3: being warming up to 95 DEG C ~ 98 DEG C with 0.5 DEG C/min ~ 1 DEG C/min speed, 20min ~ 30min is incubated, is sampled, detection;Step 4: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying.

Description

A kind of colouring method of Acrylic Fiber
Technical field
The present invention relates to chemical fibre colouring art, specially a kind of colouring method of Acrylic Fiber.
Background technology
Acrylic fibers are that polyacrylonitrile or acrylonitrile content are more than 85%(Mass percent)Acrylonitrile copolymer made of synthesize Fiber, it has excellent performance, because its property is close to wool, therefore has the title of " synthetic wool ".When to acrylic fibres dyeing, lead to Acrylic fibers levelling agent can be often added, and the model 1227 of now widely used acrylic fibers levelling agent, its dyeing course are as follows:First survey Determine the saturation value of yarn, determine 1227 dosage, then 70 DEG C rise dye, first add levelling agent 1227, add dyestuff, then with (2~3)DEG C/min speed is warming up to 85 DEG C, then is warming up to 1 DEG C/min speed(90~92)DEG C, insulation, now in dye vat Yarn start to inhale dyestuff colouring, wait inhale it is clear after, be warming up to 98 DEG C with 1 DEG C/min speed, sampled after being incubated 40min.But Due to 1227 addition so that Acrylic Fiber can not be tested by antiallergy, influence the safety in utilization of yarn.Therefore, having must A kind of new acrylic fibres dyeing technique is developed, Acrylic Fiber is met antiallergy requirement as defined in standard.
The content of the invention
In view of the above-mentioned problems, the invention provides a kind of colouring method of Acrylic Fiber, it can solve existing Acrylic Fiber The problem of can not being tested after dyeing by antiallergy, it thereby may be ensured that the safety in utilization of yarn.
Its technical scheme is such:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to 85 DEG C;
Step 3: heating, is incubated, sample, detection;
Step 4: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is less than 0.1%, it is warming up to described 85 DEG C with 0.33 DEG C/min ~ 0.5 DEG C/min speed;In the step 3, with 0.5 DEG C/min ~ 1 DEG C/min speed is warming up to 95 DEG C ~ 98 DEG C, it is incubated 20min ~ 30min.
It is further characterized by:
In the step 2, the concentration of the acrylic fibers levelling agent is 2.5% ~ 4%.
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to the first temperature;
Step 3: being warming up to second temperature, it is incubated;
Step 4: being warming up to the 3rd temperature, it is incubated, samples, detection;
Step 5: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is 0.1% ~ 0.5%, first temperature is 80 DEG C, and programming rate is 1 DEG C/min;In the step 3, the second temperature is 92 DEG C, is risen Warm speed is 0.33 DEG C/min ~ 0.5 DEG C/min, is incubated 10min ~ 20min;In the step 4, the 3rd temperature is 95 DEG C, programming rate is 0.33 DEG C/min ~ 0.5 DEG C/min, is incubated 30min ~ 40min.
It is further characterized by:
In the step 2, the concentration of the acrylic fibers levelling agent is 1.5% ~ 2.5%.
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to 85 DEG C;
Step 3: heating, is incubated, sample, detection;
Step 4: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is 0.5% ~ 2.5%, then it is warming up to described 85 DEG C with 1 DEG C/min speed;In the step 3, with 0.33 DEG C/min ~ 0.5 DEG C/min Speed be warming up to 95 DEG C, be incubated 50min ~ 60min.
It is further characterized by:
In the step 2, the concentration of the acrylic fibers levelling agent is 0.5% ~ 1.5%.
The beneficial effects of the invention are as follows:
The inventive method is dyed using acrylic fibers levelling agent RX8202 instead of traditional acrylic fibers levelling agent 1227 to Acrylic Fiber, So that the yarn after dyeing can be tested by antiallergy, the safety in utilization of yarn is ensured that.
Embodiment
Embodiment one:Dye light color(The concentration of dyestuff i.e. used is less than 0.1%), method is as follows:
A kind of colouring method of Acrylic Fiber of the present invention, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 2.5%;Add Dyestuff, the concentration of dyestuff is 0.08%, is then warming up to 85 DEG C with 0.33 DEG C/min speed;
Step 3: being warming up to 95 DEG C with 0.5 DEG C/min speed, 20min is incubated, is sampled, detection;
Step 4: being cooled to 40 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment two:Dye light color(The concentration of dyestuff i.e. used is less than 0.1%), method is as follows:
A kind of colouring method of Acrylic Fiber of the present invention, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 4%;Add dye Material, the concentration of dyestuff is 0.06%, is then warming up to 85 DEG C with 0.5 DEG C/min speed;
Step 3: being warming up to 98 DEG C with 1 DEG C/min speed, 30min is incubated, is sampled, detection;
Step 4: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment three:Dye light color(The concentration of dyestuff i.e. used is less than 0.1%), method is as follows:
A kind of colouring method of Acrylic Fiber of the present invention, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 3.3%;Add Dyestuff, the concentration of dyestuff is 0.07%, is then warming up to 85 DEG C with 0.4 DEG C/min speed;
Step 3: being warming up to 97 DEG C with 0.75 DEG C/min speed, 25min is incubated, is sampled, detection;
Step 4: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Example IV:Color in dye(The concentration of dyestuff i.e. used is 0.1% ~ 0.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 1.5%;Add Dyestuff, the concentration of dyestuff is 0.1%, is then warming up to 80 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 92 DEG C with 0.33 DEG C/min speed, 10min is incubated;
Step 4: being warming up to 95 DEG C with 0.33 DEG C/min speed, 30min is incubated, is sampled, detection;
Step 5: being cooled to 40 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment five:Color in dye(The concentration of dyestuff i.e. used is 0.1% ~ 0.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 2.5%;Add Dyestuff, the concentration of dyestuff is 0.5%, is then warming up to 80 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 92 DEG C with 0.5 DEG C/min speed, 20min is incubated;
Step 4: being warming up to 95 DEG C with 0.5 DEG C/min speed, 40min is incubated, is sampled, detection;
Step 5: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment six:Color in dye(The concentration of dyestuff i.e. used is 0.1% ~ 0.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 2%;Add dye Material, the concentration of dyestuff is 0.3%, is then warming up to 80 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 92 DEG C with 0.4 DEG C/min speed, 15min is incubated;
Step 4: being warming up to 95 DEG C with 0.4 DEG C/min speed, 35min is incubated, is sampled, detection;
Step 5: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment seven:Dye is dark(The concentration of dyestuff i.e. used is 0.5% ~ 2.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 0.5%;Add Dyestuff, the concentration of dyestuff is 0.6%, is then warming up to 85 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 95 DEG C with 0.33 DEG C/min speed, 50min is incubated, is sampled, detection;
Step 4: being cooled to 40 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment eight:Dye is dark(The concentration of dyestuff i.e. used is 0.5% ~ 2.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 1.5%;Add Dyestuff, the concentration of dyestuff is 2.5%, is then warming up to 85 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 95 DEG C with 0.5 DEG C/min speed, 60min is incubated, is sampled, detection;
Step 4: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.
Embodiment nine:Dye is dark(The concentration of dyestuff i.e. used is 0.5% ~ 2.5%), method is as follows:
A kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first add acrylic fibers levelling agent, it is By the model RX8202 of Xing Rong auxiliary agents Co., Ltd of Jiangyin City purchase acrylic fibers levelling agent, addition concentration is 1%;Add dye Material, the concentration of dyestuff is 1.5%, is then warming up to 85 DEG C with 1 DEG C/min speed;
Step 3: being warming up to 95 DEG C with 0.4 DEG C/min speed, 55min is incubated, is sampled, detection;
Step 4: being cooled to 50 DEG C of progress soft treatments, then yarn goes out cylinder, dehydration, drying.

Claims (6)

1. a kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to 85 DEG C;
Step 3: heating, is incubated, sample, detection;
Step 4: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is less than 0.1%, it is warming up to described 85 DEG C with 0.33 DEG C/min ~ 0.5 DEG C/min speed;In the step 3, with 0.5 DEG C/min ~ 1 DEG C/min speed is warming up to 95 DEG C ~ 98 DEG C, it is incubated 20min ~ 30min.
A kind of 2. colouring method of Acrylic Fiber according to claim 1, it is characterised in that:It is described in the step 2 The concentration of acrylic fibers levelling agent is 2.5% ~ 4%.
3. a kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to the first temperature;
Step 3: being warming up to second temperature, it is incubated;
Step 4: being warming up to the 3rd temperature, it is incubated, samples, detection;
Step 5: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is 0.1% ~ 0.5%, first temperature is 80 DEG C, and programming rate is 1 DEG C/min;In the step 3, the second temperature is 92 DEG C, is risen Warm speed is 0.33 DEG C/min ~ 0.5 DEG C/min, is incubated 10min ~ 20min;In the step 4, the 3rd temperature is 95 DEG C, programming rate is 0.33 DEG C/min ~ 0.5 DEG C/min, is incubated 30min ~ 40min.
A kind of 4. colouring method of Acrylic Fiber according to claim 3, it is characterised in that:It is described in the step 2 The concentration of acrylic fibers levelling agent is 1.5% ~ 2.5%.
5. a kind of colouring method of Acrylic Fiber, it comprises the following steps:
Step 1: determining the saturation value of yarn, the dosage of acrylic fibers levelling agent is determined;
Step 2: opening impregnating mangle, Acrylic Fiber is added, water inlet, 70 DEG C is warming up to and plays dye, first adds acrylic fibers levelling agent, then add Enter dyestuff, then heat to 85 DEG C;
Step 3: heating, is incubated, sample, detection;
Step 4: being cooled to 40 DEG C ~ 50 DEG C progress soft treatments, then yarn goes out cylinder, dehydration, drying;
It is characterized in that:In the step 2, the model RX8202 of the acrylic fibers levelling agent, the concentration of the dyestuff is 0.5% ~ 2.5%, then it is warming up to described 85 DEG C with 1 DEG C/min speed;In the step 3, with 0.33 DEG C/min ~ 0.5 DEG C/min Speed be warming up to 95 DEG C, be incubated 50min ~ 60min.
A kind of 6. colouring method of Acrylic Fiber according to claim 5, it is characterised in that:It is described in the step 2 The concentration of acrylic fibers levelling agent is 0.5% ~ 1.5%.
CN201710928076.4A 2017-10-09 2017-10-09 A kind of colouring method of Acrylic Fiber Withdrawn CN107503171A (en)

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CN201710928076.4A CN107503171A (en) 2017-10-09 2017-10-09 A kind of colouring method of Acrylic Fiber

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Application Number Priority Date Filing Date Title
CN201710928076.4A CN107503171A (en) 2017-10-09 2017-10-09 A kind of colouring method of Acrylic Fiber

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106049112A (en) * 2016-07-25 2016-10-26 浙江中昕染整有限公司 Purple dyeing method of acrylon
CN106223064A (en) * 2016-07-25 2016-12-14 浙江中昕染整有限公司 A kind of pink colouring method of acrylon

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106049112A (en) * 2016-07-25 2016-10-26 浙江中昕染整有限公司 Purple dyeing method of acrylon
CN106223064A (en) * 2016-07-25 2016-12-14 浙江中昕染整有限公司 A kind of pink colouring method of acrylon

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Application publication date: 20171222