CN107502977A - A kind of preparation method of high-quality textile fabric - Google Patents
A kind of preparation method of high-quality textile fabric Download PDFInfo
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- CN107502977A CN107502977A CN201710879603.7A CN201710879603A CN107502977A CN 107502977 A CN107502977 A CN 107502977A CN 201710879603 A CN201710879603 A CN 201710879603A CN 107502977 A CN107502977 A CN 107502977A
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- textile fabric
- preparation
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
Abstract
The invention discloses a kind of preparation method of high-quality textile fabric, comprise the following steps：（1）Compounded mix preparation,（2）It is prepared by fiber.The present invention has carried out rational Optimal improvements to the preparation method of textile fabric and handled, under the common mating reaction of each step, final obtained textile fabric has relatively low density, and with characteristics such as good insulation, sound insulation, fire-retardant, intensity, and can strengthens body immunity, good health-care effect is played, integrated quality is high, has good application value.
Description
Technical field
The invention belongs to textile technology field, and in particular to a kind of preparation method of high-quality textile fabric.
Background technology
Textile fabric using high polymer material as raw material is widely used in the fabric of the textiles such as clothes, bedding,
But there is the problems such as function is single, textile property is bad, service life is not high, category homogeneity more in existing such textile fabric
Seriously, the market competitiveness is reduced, therefore for more preferable enterprise benefit, it is necessary to be carried out not to textile fiber material quality
Disconnected improvement.
The content of the invention
The purpose of the present invention is to be directed to the problem of existing, there is provided a kind of preparation method of high-quality textile fabric.
The present invention is achieved by the following technical solutions：
A kind of preparation method of high-quality textile fabric, comprises the following steps：
（1）It is prepared by compounded mix：
A. by loess stone and stone needle by weight 3：1 carries out weighing mixing, is put into jointly in pulverizer and carries out pulverization process, complete
It is standby that mixed powder is obtained after；
B. the mixed powder operated obtained by a is put into hydrochloric acid solution after 20 ~ 25min of immersion treatment and taken out, then placed into
Take out, finally spend standby after clear water rinses one time after 10 ~ 15min of immersion treatment in sodium hydroxide solution；
C. the mixed powder after b is handled will be operated to be put into calcining furnace, it is 400 ~ 450 DEG C that heating, which keeps the temperature in calcining furnace,
Taken out after 40 ~ 45min of calcination processing standby；
D. the mixed powder after c is handled will be operated to be put into modification liquid, filtered out after being stirred continuously 1 ~ 2h of immersion treatment, then put
Enter into drying box 30 ~ 40min of drying process take out compounded mix is standby；Each composition and its right in described modification liquid
The parts by weight are answered to be：15 ~ 20 parts of silane couplers, 4 ~ 7 parts of neopelexes, 2 ~ 4 parts of zinc stearates, 120 ~ 140 parts of water；
After carrying out silane coupled modification to mixed powder, scattered compatibility of the mixed powder in resin matrix is enhanced, this powdery is filled out
The addition of material not give only a variety of new functional characteristics of textile fabric, enhance the mechanical characteristics such as its intensity again；
（2）It is prepared by fiber：
A. by step（1）Obtained compounded mix is added to be well mixed in polyester resin after that master batch is made is standby；
B., the resin raw material that master batch made from operation a can be formed to textile fabric with other is mixed, and it is total then to add its
The foaming agent of quality 0.05 ~ 0.15%, the premix after being well mixed, after finally carrying out melting extrusion, wire-drawing shape to premix
Get product fiber.
Further, step（1）The granular size of mixed powder is 400 ~ 500 mesh after pulverization process described in operation a.
Further, step（1）The mass fraction for operating hydrochloric acid in the hydrochloric acid solution described in b is 3 ~ 4%.
Further, step（1）The mass fraction for operating sodium hydroxide in the sodium hydroxide solution described in b is 5 ~ 6%.
Further, step（1）It is 50 ~ 55 that heating, which keeps the temperature of modification liquid, when operating immersion treatment described in d
℃。
Further, step（1）It is 75 ~ 80 DEG C that heating, which keeps the temperature in drying box, when operating drying process described in d.
Further, step（2）The mass ratio for operating the compounded mix described in a and polyester resin is 1：4~5.
Further, step（2）Master batch described in operation b accounts for the 20 ~ 23% of premix gross mass.
Further, step（2）The foaming agent operated described in b is azodicarbonamide.
Existing most textile fabrics do not have special function affect, and the characteristic such as its intensity is not still high, also need into
The enhancing of one step, the present invention have carried out rational improvement on the basis of a large amount of practices to the preparation method of existing textile fabric,
Effectively improve its synthesis and use quality, improve its use value.A kind of special match somebody with somebody is with the addition of in the preparation of textile fabric
The compounded mix of system, specifically it is made up of loess stone and stone needle compounding, loess stone and stone needle are respectively provided with good permanent infrared emission
Characteristic, after two kinds of composition compounding uses, the optical wavelength of transmitting is 5 ~ 20 μm, and the emissivity of normal direction is more than 90%, can be effective
Promote blood circulation of human body, accelerate metabolism, strengthen body immunity, while loess stone and stone needle are again with negative well
Plasma diffusing W,Mo characteristic, it can further improve human body constitution, loess stone and stone needle have good vibrant characteristic again in addition, are stirring
When mixing motion phase mutual friction, ultrasonic wave can be produced, the present invention with the addition of blowing agent component again in prepared by follow-up fiber, this production
Raw ultrasonic wave energy promotes the refinement of follow-up foaming bubble, and beneficial to the growing amount of closure bubble, and improve the equal of its distribution
Even property, and then the qualities such as the insulation of textile fabric, noise reduction are enhanced, and the density and quality of textile fabric are reduced well,
Improve textile property.
The present invention has advantages below compared with prior art：
The present invention has carried out rational Optimal improvements to the preparation method of textile fabric and handled, in the common mating reaction of each step
Under, final obtained textile fabric has relatively low density, and has the characteristics such as good insulation, sound insulation, fire-retardant, intensity, again
Body immunity can be strengthened, play good health-care effect, integrated quality is high, has good application value.
Embodiment
Embodiment 1
A kind of preparation method of high-quality textile fabric, comprises the following steps：
（1）It is prepared by compounded mix：
A. by loess stone and stone needle by weight 3：1 carries out weighing mixing, is put into jointly in pulverizer and carries out pulverization process, complete
It is standby that mixed powder is obtained after；
B. the mixed powder operated obtained by a is put into hydrochloric acid solution after immersion treatment 20min and taken out, then place into hydrogen-oxygen
Change in sodium solution and taken out after immersion treatment 10min, finally spent standby after clear water rinses one time；
C. the mixed powder after b is handled will be operated to be put into calcining furnace, it is 400 DEG C that heating, which keeps the temperature in calcining furnace, calcining
Taken out after processing 40min standby；
D. the mixed powder after c is handled will be operated to be put into modification liquid, filter out, place into after being stirred continuously immersion treatment 1h
In to drying box drying process 30min take out compounded mix is standby；Each composition and its corresponding weight in described modification liquid
Measuring part is：15 parts of silane couplers, 4 parts of neopelexes, 2 parts of zinc stearates, 120 parts of water；
（2）It is prepared by fiber：
A. by step（1）Obtained compounded mix is added to be well mixed in polyester resin after that master batch is made is standby；
B., the resin raw material that master batch made from operation a can be formed to textile fabric with other is mixed, and it is total then to add its
The foaming agent of quality 0.05%, the premix after being well mixed, produced after finally carrying out melting extrusion, wire-drawing shape to premix
Finished fiber.
Further, step（1）The granular size of mixed powder is 400 mesh after pulverization process described in operation a.
Further, step（1）The mass fraction for operating hydrochloric acid in the hydrochloric acid solution described in b is 3%.
Further, step（1）The mass fraction for operating sodium hydroxide in the sodium hydroxide solution described in b is 5%.
Further, step（1）It is 50 DEG C that heating, which keeps the temperature of modification liquid, when operating immersion treatment described in d.
Further, step（1）It is 75 DEG C that heating, which keeps the temperature in drying box, when operating drying process described in d.
Further, step（2）The mass ratio for operating the compounded mix described in a and polyester resin is 1：4.
Further, step（2）Master batch described in operation b accounts for the 20% of premix gross mass.
Further, step（2）The foaming agent operated described in b is azodicarbonamide.
Embodiment 2
A kind of preparation method of high-quality textile fabric, comprises the following steps：
（1）It is prepared by compounded mix：
A. by loess stone and stone needle by weight 3：1 carries out weighing mixing, is put into jointly in pulverizer and carries out pulverization process, complete
It is standby that mixed powder is obtained after；
B. the mixed powder operated obtained by a is put into hydrochloric acid solution after immersion treatment 23min and taken out, then place into hydrogen-oxygen
Change in sodium solution and taken out after immersion treatment 13min, finally spent standby after clear water rinses one time；
C. the mixed powder after b is handled will be operated to be put into calcining furnace, it is 420 DEG C that heating, which keeps the temperature in calcining furnace, calcining
Taken out after processing 43min standby；
D. the mixed powder after c is handled will be operated to be put into modification liquid, filtered out after being stirred continuously immersion treatment 1.5h, then put
Enter into drying box drying process 35min take out compounded mix is standby；Each composition and its correspondingly in described modification liquid
Parts by weight are：18 parts of silane couplers, 6 parts of neopelexes, 3 parts of zinc stearates, 130 parts of water；
（2）It is prepared by fiber：
A. by step（1）Obtained compounded mix is added to be well mixed in polyester resin after that master batch is made is standby；
B., the resin raw material that master batch made from operation a can be formed to textile fabric with other is mixed, and it is total then to add its
The foaming agent of quality 0.1%, the premix after being well mixed, produced into after finally carrying out melting extrusion, wire-drawing shape to premix
Product fiber.
Further, step（1）The granular size of mixed powder is 450 mesh after pulverization process described in operation a.
Further, step（1）The mass fraction for operating hydrochloric acid in the hydrochloric acid solution described in b is 3.5%.
Further, step（1）The mass fraction for operating sodium hydroxide in the sodium hydroxide solution described in b is 5.5%.
Further, step（1）It is 52 DEG C that heating, which keeps the temperature of modification liquid, when operating immersion treatment described in d.
Further, step（1）It is 78 DEG C that heating, which keeps the temperature in drying box, when operating drying process described in d.
Further, step（2）The mass ratio for operating the compounded mix described in a and polyester resin is 1：4.5.
Further, step（2）Master batch described in operation b accounts for the 22% of premix gross mass.
Further, step（2）The foaming agent operated described in b is azodicarbonamide.
Embodiment 3
A kind of preparation method of high-quality textile fabric, comprises the following steps：
（1）It is prepared by compounded mix：
A. by loess stone and stone needle by weight 3：1 carries out weighing mixing, is put into jointly in pulverizer and carries out pulverization process, complete
It is standby that mixed powder is obtained after；
B. the mixed powder operated obtained by a is put into hydrochloric acid solution after immersion treatment 25min and taken out, then place into hydrogen-oxygen
Change in sodium solution and taken out after immersion treatment 15min, finally spent standby after clear water rinses one time；
C. the mixed powder after b is handled will be operated to be put into calcining furnace, it is 450 DEG C that heating, which keeps the temperature in calcining furnace, calcining
Taken out after processing 45min standby；
D. the mixed powder after c is handled will be operated to be put into modification liquid, filter out, place into after being stirred continuously immersion treatment 2h
In to drying box drying process 40min take out compounded mix is standby；Each composition and its corresponding weight in described modification liquid
Measuring part is：20 parts of silane couplers, 7 parts of neopelexes, 4 parts of zinc stearates, 140 parts of water；
（2）It is prepared by fiber：
A. by step（1）Obtained compounded mix is added to be well mixed in polyester resin after that master batch is made is standby；
B., the resin raw material that master batch made from operation a can be formed to textile fabric with other is mixed, and it is total then to add its
The foaming agent of quality 0.15%, the premix after being well mixed, produced after finally carrying out melting extrusion, wire-drawing shape to premix
Finished fiber.
Further, step（1）The granular size of mixed powder is 500 mesh after pulverization process described in operation a.
Further, step（1）The mass fraction for operating hydrochloric acid in the hydrochloric acid solution described in b is 4%.
Further, step（1）The mass fraction for operating sodium hydroxide in the sodium hydroxide solution described in b is 6%.
Further, step（1）It is 55 DEG C that heating, which keeps the temperature of modification liquid, when operating immersion treatment described in d.
Further, step（1）It is 80 DEG C that heating, which keeps the temperature in drying box, when operating drying process described in d.
Further, step（2）The mass ratio for operating the compounded mix described in a and polyester resin is 1：5.
Further, step（2）Master batch described in operation b accounts for the 23% of premix gross mass.
Further, step（2）The foaming agent operated described in b is azodicarbonamide.
Comparative example 1
This comparative example 1 compared with Example 2, saves step（2）Blowing agent component in fiber preparation manipulation b, in addition
Method and step all same.
Comparative example 2
This comparative example 2 compared with Example 2, in step（1）In compounded mix preparation manipulation a, stone needle material composition is saved,
Only use a kind of composition of loess stone, method and step all same in addition.
Comparative example 3
This comparative example 3 compared with Example 2, saves step（1）Compounded mix operates d processing, side in addition in preparing
Method step all same.
Control group
Existing commercially available polyester resin class textile fabric.
In order to contrast effect of the present invention, to above-described embodiment 2, comparative example 1, comparative example 2, comparative example 3,
Textile fabric obtained by control group carries out performance test, and specific correction data is as shown in table 1 below：
Table 1
| Antibacterial ability（%） | Negative ion concentration yield | Thermal conductivity factor（W/mk） | Modulus of elasticity（cN/dtex） | |
| Embodiment 2 | ≥99 | 4600 | 0.019 | 57.3 |
| Comparative example 1 | ≥99 | 4550 | 0.030 | 53.8 |
| Comparative example 2 | ≥97 | 3200 | 0.025 | 50.4 |
| Comparative example 3 | ≥99 | 4570 | 0.023 | 49.2 |
| Control group | / | / | 0.032 | 42.6 |
Note：Antibacterial ability described in upper table 1 is measured to Candida albicans, staphylococcus aureus, Escherichia coli and lung
The synthesis antibacterial ability of the scorching white bacterium of Cray；Described negative ion concentration yield is tested with reference to TTC.F024-2007；“/”
Indicate without.
The integrated quality of textile fabric produced by the present invention is good it can be seen from upper table 1, and use value is high, great market
Competitiveness.
Claims (9)
1. a kind of preparation method of high-quality textile fabric, it is characterised in that comprise the following steps：
（1）It is prepared by compounded mix：
A. by loess stone and stone needle by weight 3：1 carries out weighing mixing, is put into jointly in pulverizer and carries out pulverization process, complete
It is standby that mixed powder is obtained after；
B. the mixed powder operated obtained by a is put into hydrochloric acid solution after 20 ~ 25min of immersion treatment and taken out, then placed into
Take out, finally spend standby after clear water rinses one time after 10 ~ 15min of immersion treatment in sodium hydroxide solution；
C. the mixed powder after b is handled will be operated to be put into calcining furnace, it is 400 ~ 450 DEG C that heating, which keeps the temperature in calcining furnace,
Taken out after 40 ~ 45min of calcination processing standby；
D. the mixed powder after c is handled will be operated to be put into modification liquid, filtered out after being stirred continuously 1 ~ 2h of immersion treatment, then put
Enter into drying box 30 ~ 40min of drying process take out compounded mix is standby；Each composition and its right in described modification liquid
The parts by weight are answered to be：15 ~ 20 parts of silane couplers, 4 ~ 7 parts of neopelexes, 2 ~ 4 parts of zinc stearates, 120 ~ 140 parts of water；
（2）It is prepared by fiber：
A. by step（1）Obtained compounded mix is added to be well mixed in polyester resin after that master batch is made is standby；
B., the resin raw material that master batch made from operation a can be formed to textile fabric with other is mixed, and it is total then to add its
The foaming agent of quality 0.05 ~ 0.15%, the premix after being well mixed, after finally carrying out melting extrusion, wire-drawing shape to premix
Get product fiber.
A kind of 2. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（1）Operate a
Described in pulverization process after the granular size of mixed powder be 400 ~ 500 mesh.
A kind of 3. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（1）Operate b
Described in hydrochloric acid solution in hydrochloric acid mass fraction be 3 ~ 4%.
A kind of 4. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（1）Operate b
Described in sodium hydroxide solution in sodium hydroxide mass fraction be 5 ~ 6%.
A kind of 5. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（1）Operate d
Described in immersion treatment when heating keep modification liquid temperature be 50 ~ 55 DEG C.
A kind of 6. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（1）Operate d
Described in drying process when heating keep drying box in temperature be 75 ~ 80 DEG C.
A kind of 7. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（2）Operate a
Described in compounded mix and polyester resin mass ratio be 1：4~5.
A kind of 8. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（2）Operate b
Described in master batch account for the 20 ~ 23% of premix gross mass.
A kind of 9. preparation method of high-quality textile fabric according to claim 1, it is characterised in that step（2）Operate b
Described in foaming agent be azodicarbonamide.
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| CN201710879603.7A CN107502977A (en) | 2017-09-26 | 2017-09-26 | A kind of preparation method of high-quality textile fabric |
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| CN201710879603.7A CN107502977A (en) | 2017-09-26 | 2017-09-26 | A kind of preparation method of high-quality textile fabric |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108385192A (en) * | 2018-02-24 | 2018-08-10 | 中科纺织研究院（青岛）有限公司 | A kind of stone needle nylon fibre |
| CN108755244A (en) * | 2018-06-22 | 2018-11-06 | 安徽索亚装饰材料有限公司 | A kind of preparation method of high-quality PVC foam wallpaper |
| CN109306636A (en) * | 2018-10-17 | 2019-02-05 | 马鞍山市康辉纸箱纸品有限公司 | A kind of processing method that waste and old wrapping paper enhancing recycles |
| CN109487368A (en) * | 2018-10-30 | 2019-03-19 | 中科纺织研究院（青岛）有限公司 | A kind of stone needle polyester fabric and preparation method thereof |
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| CN104911746A (en) * | 2015-06-03 | 2015-09-16 | 东华大学 | Polyester fiber with functions of storing energy and adjusting temperature and preparation method thereof |
| CN105671678A (en) * | 2016-03-27 | 2016-06-15 | 吴正锋 | Preparation method of antibacterial anti-radiation copper-modified polyester composite fiber |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108385192A (en) * | 2018-02-24 | 2018-08-10 | 中科纺织研究院（青岛）有限公司 | A kind of stone needle nylon fibre |
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| CN109306636A (en) * | 2018-10-17 | 2019-02-05 | 马鞍山市康辉纸箱纸品有限公司 | A kind of processing method that waste and old wrapping paper enhancing recycles |
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