CN107502056A - A kind of stamp-pad ink and preparation method thereof - Google Patents
A kind of stamp-pad ink and preparation method thereof Download PDFInfo
- Publication number
- CN107502056A CN107502056A CN201710725693.4A CN201710725693A CN107502056A CN 107502056 A CN107502056 A CN 107502056A CN 201710725693 A CN201710725693 A CN 201710725693A CN 107502056 A CN107502056 A CN 107502056A
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- Prior art keywords
- stamp
- pad ink
- parts
- ink according
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of stamp-pad ink and preparation method thereof, the stamp-pad ink includes the raw material of following parts by weight：5~15 parts of water soluble polymer, 1~3 part of food coloring, 80~93 parts of saturated alcohols, 0.5~3 part of antioxidant；One or more of the saturated alcohols in ethanol, isopropanol, n-butanol, glycerine.The stamp-pad ink of the present invention is used as bridging agent using water soluble polymer, using the marking that the stamp-pad ink is formed in skin surface adhesion-tight, be not easy to rub flower, easily clean.
Description
Technical field
It is more particularly to a kind of available for human body and animal skin the present invention relates to a kind of seal stamp-pad ink and preparation method thereof
Seal stamp-pad ink and preparation method thereof.
Background technology
Stamp-pad ink can be capped in the material such as paper and skin as a kind of seal oil by seal.It is applicable on skin
Stamp-pad ink be mainly used in two aspect, human body skin is on the one hand can be applied to, particularly in the field such as large-scale museum and recreation ground
Institute, the stamp-pad ink covered on visitor's arm can substitute admission ticket both to facilitate the multiple disengaging of visitor, and can avoids as authority is entered
The phenomenon of the more people of one ticket；On the other hand animal skin is can be applied to, is closed particularly in Slaughter tache quarantine and examination as inspection
Case marker will, play an important roll in the supervision of the Product quality and safeties such as livestock and poultry.Stamp-pad ink applied to these two aspects, which needs to have, matches somebody with somebody
Fang Jiankang, easily colour, be in bright colors, firm coloration the features such as, while can be rinsed well again with water, not cutaneous U.S.
See and healthy.
Application No. CN201110241392.7 and CN201210072406.1 patent individually disclose a kind of hog on hook
Affix one's seal with red stamp-pad ink and a kind of meat detection stamp stamp-pad ink, the stamp-pad ink disclosed in two patents be difficult in actual applications by
Pigment in stamp-pad ink is delivered on animal skin from ink pad, and after stamp-pad ink air-dries in skin surface, pigment is in skin table
The attachment fastness in face is limited, easily rubs flower, causes stamp imprint to be difficult to recognize, can not examine, and is unsuitable for applying in human body and moving
On thing skin.
The content of the invention
The invention provides a kind of stamp-pad ink and preparation method thereof, with least solve in the prior art stamp-pad ink in skin surface shape
Into marking attachment fastness it is limited, easily rub the problem of colored.
The invention provides a kind of stamp-pad ink, include the raw material of following parts by weight：5~15 parts of water soluble polymer, eat color
1~3 part of element, 80~93 parts of saturated alcohols, 0.5~3 part of antioxidant；The saturated alcohols are selected from ethanol, isopropanol, n-butanol, sweet
One or more in oil.
Further, the water soluble polymer be selected from polyvinylpyrrolidone, carboxymethyl cellulose, polyacrylamide,
One or more in hydrolyzed polyacrylamide, polyethylene glycol.
Further, the water soluble polymer is polyvinylpyrrolidone, the polyvinylpyrrolidonemolecules molecules amount
For 5000~50000.
Further, the stamp-pad ink includes the raw material of following parts by weight：5~15 parts of water soluble polymer, food coloring 1~
3 parts, 60~80 parts of ethanol, 2~4 parts of glycerine, 10~20 parts of n-butanol, 0.5~3 part of antioxidant.
Further, the food coloring is selected from famille rose, lemon yellow, amaranth, alkermes, beta carotene, red yeast rice
One or more in red.
Further, one or more of the antioxidant in ascorbic acid, citric acid, vitamin E.
Further, the stamp-pad ink also includes 0.1~1 part of fluorchrome.
Further, the fluorchrome is in rhodamine B, acid rhodamine B, rhodamine 6G, Rhodamine 123
It is one or more.
It is to provide a kind of preparation method of above-mentioned stamp-pad ink, it is characterised in that the preparation side another mesh of the present invention
Method comprises the following steps：
Step 1：Take food coloring to add in saturated alcohols, be mixed evenly and be heated to 30~100 DEG C to food coloring
It is completely dissolved；
Step 2：Polyvinylpyrrolidone and antioxidant are added into the solution obtained by step 1, stirring and dissolving, is cooled to
10~30 DEG C, filtering, obtain stamp-pad ink.
Further, heating-up temperature is 70~90 DEG C in the step 1.
The present invention compared with prior art, has the advantages that：
1. present invention employs water soluble polymer as binder, the viscosity having in itself using water soluble polymer,
The food coloring in stamp-pad ink can be more preferably bonded, the transmission effect that food coloring is transferred to animal skin from ink pad is improved, makes
Stamp-pad ink is easy to colour；
2. the present invention makes stamp-pad ink after air drying, water soluble polymer therein being capable of shape by using water soluble polymer
Into polymeric membrane, food coloring is fixed therein, and is bonded in skin surface, improves adhesion-tight of the marking in skin surface
Degree, there is the characteristics of firm coloration；
3. the constitutive material toxicity of stamp-pad ink of the present invention is relatively low, suitable for human body skin and animal products skin；
4. the main component in the present invention using water soluble polymer as stamp-pad ink the formed marking after solidification, it is not necessary to
During the marking, using water soluble polymer it is soluble in water the characteristics of, can use water rinse remove, skin is not caused to damage.
Embodiment
In order that those skilled in the art more fully understand the present invention program, below by the skill in the embodiment of the present invention
Art scheme is clearly and completely described, it is clear that and described embodiment is only the embodiment of a present invention part, without
It is whole embodiments.
Unless otherwise specified, the material proportion used in the embodiment of the present invention and reference examples, percentage are weight
Unit, used water soluble polymer are pharmaceutical grade, and saturated alcohols, food coloring are food-grade.
Embodiment 1
The embodiment of the present invention 1 is by 5 parts of polyvinylpyrrolidone, carmine 1 part, 80 parts of ethanol, 2 parts of glycerine, n-butanol 11
1 part of part, vitamin E composition, wherein, polyvinylpyrrolidonemolecules molecules amount is 30000~45000.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：In the mixed solution for taking carmine addition ethanol, glycerine and n-butanol, it is mixed evenly and is heated to
70 DEG C are completely dissolved to famille rose；
Step 2：Polyvinylpyrrolidone and vitamin E are added into the solution obtained by step 1, stirring and dissolving, is cooled to
25 DEG C, filtering, obtain the stamp-pad ink of the embodiment of the present invention 1.
Embodiment 2
The embodiment of the present invention 1 is by 10 parts of polyvinylpyrrolidone, carmine 2 parts, 70 parts of ethanol, 3 parts of glycerine, n-butanol
1 part of 13.5 parts, vitamin E composition, wherein, polyvinylpyrrolidonemolecules molecules amount is 30000~45000.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：In the mixed solution for taking carmine addition ethanol, glycerine and n-butanol, it is mixed evenly and is heated to
80 DEG C are completely dissolved to famille rose；
Step 2：Polyvinylpyrrolidone and vitamin E are added into the solution obtained by step 1, stirring and dissolving, is cooled to
20 DEG C, filtering, obtain the stamp-pad ink of the embodiment of the present invention 2.
Embodiment 3
The embodiment of the present invention 1 is by 15 parts of polyvinylpyrrolidone, carmine 3 parts, 60 parts of ethanol, 4 parts of glycerine, n-butanol 15
0.5 part of part, ascorbic acid composition, wherein, polyvinylpyrrolidonemolecules molecules amount is 30000~45000.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：In the mixed solution for taking carmine addition ethanol, glycerine and n-butanol, it is mixed evenly and is heated to
90 DEG C are completely dissolved to famille rose；
Step 2：Polyvinylpyrrolidone and vitamin E are added into the solution obtained by step 1, stirring and dissolving, is cooled to
20 DEG C, filtering, obtain the stamp-pad ink of the embodiment of the present invention 3.
Embodiment 4
The embodiment of the present invention 1 by 15 parts of polyacrylamide, carmine 3 parts, 60 parts of ethanol, 4 parts of glycerine, 15 parts of n-butanol,
0.5 part of 0.5 part of ascorbic acid, Rhodamine 123 composition, wherein, the molecular weight of polyacrylamide is 10000~20000.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：Take carmine and Rhodamine 123 to add in the mixed solution of ethanol, glycerine and n-butanol, mix equal
It is even and be heated to 90 DEG C and be completely dissolved to famille rose；
Step 2：Polyvinylpyrrolidone and vitamin E are added into the solution obtained by step 1, stirring and dissolving, is cooled to
20 DEG C, filtering, obtain the stamp-pad ink of the embodiment of the present invention 3.
Embodiment 5
The embodiment of the present invention 1 is by 15 parts of polyvinylpyrrolidone, 3 parts of alkermes, 60 parts of ethanol, 4 parts of glycerine, n-butanol
0.5 part of 15 parts, ascorbic acid composition, wherein, polyvinylpyrrolidonemolecules molecules amount is 10000~25000.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：Take alkermes to add in the mixed solution of ethanol, glycerine and n-butanol, be mixed evenly and heat
It is completely dissolved to 90 DEG C to famille rose；
Step 2：Polyvinylpyrrolidone and vitamin E are added into the solution obtained by step 1, stirring and dissolving, is cooled to
20 DEG C, filtering, obtain the stamp-pad ink of the embodiment of the present invention 3.
Reference examples 1
The embodiment of the present invention 1 is by 0.5 part of carmine 3 parts, 60 parts of ethanol, 4 parts of glycerine, 15 parts of n-butanol, ascorbic acid group
Into.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：In the mixed solution for taking carmine addition ethanol, glycerine and n-butanol, it is mixed evenly and is heated to
90 DEG C are completely dissolved to famille rose；
Step 2：Vitamin E is added into the solution obtained by step 1, stirring and dissolving, 20 DEG C is cooled to, filtering, obtains this
The stamp-pad ink of invention reference examples 1.
Reference examples 2
The embodiment of the present invention 1 is by 15 parts of polyvinylpyrrolidone, carmine 3 parts, 60 parts of ethanol, 4 parts of glycerine, n-butanol 15
0.5 part of part, ascorbic acid composition.
The preparation method of the embodiment of the present invention 1 comprises the following steps：
Step 1：In the mixed solution for taking carmine addition ethanol, glycerine and n-butanol, it is mixed evenly and is heated to
90 DEG C are completely dissolved to famille rose；
Step 2：Add polyvinylpyrrolidone and vitamin E into the solution obtained by step 1, direct mistake after stirring and dissolving
Filter, obtains the stamp-pad ink of reference examples 2 of the present invention.
For the attachment fastness of investigation stamp-pad ink provided by the present invention, the stamp-pad ink of Example 1~5 and reference examples 1~2 passes through print
Chapter carries out physical property detection, measure knot in pigskin upper press cover, the natural air drying at spaciousness, the marking formed after being solidified to stamp-pad ink
Fruit is as shown in the table.
| Title | Imprinting status when just covering | Imprinting status after air-drying | 278nm ultraviolets irradiate |
| Embodiment 1 | Color is uniform, is in bright colors | Surfacing is smooth, is not easily stripped | It is unchanged |
| Embodiment 2 | Color is uniform, is in bright colors | Surfacing is smooth, is not easily stripped | It is unchanged |
| Embodiment 3 | Color is uniform, is in bright colors | Surfacing is smooth, is not easily stripped | It is unchanged |
| Embodiment 4 | Color is uniform, is in bright colors | Surfacing is smooth, is not easily stripped | There is green fluorescence |
| Embodiment 5 | Color is uniform, is in bright colors | Surfacing is smooth, is not easily stripped | It is unchanged |
| Reference examples 1 | Color is uniform, color is thin | Rough surface, fade | It is unchanged |
| Reference examples 2 | Irregular colour, it is in bright colors | Rough surface has slight crack, is not easily stripped | It is unchanged |
As shown above, by adding polyvinylpyrrolidone and polyacrylamide wherein in embodiments of the invention 1~5
Deng water-soluble organic macromolecule material, make stamp-pad ink that there is viscosity in itself, when being affixed one's seal, can stablize and carry food coloring,
Ensure that the marking color to be formed is uniform, vivid.Meanwhile the marking of embodiment 1~5 is after air drying, water soluble organic polymer material
Material can condense, and form the smooth polymeric membrane of surfacing, food coloring is formed and protected, prevents food coloring from coming off.And not
The reference examples 1 of water-soluble organic macromolecule material are added, when being affixed one's seal, the food coloring amount of carrying is less, and color is thin,
And after the marking air-dries, food coloring lacks polymeric membrane protection, causes the easy skin surface ablation of food coloring.And compare
Example 2 filters when temperature is higher to cool again, causes have solid precipitation in mimeograph, causes mimeograph system uneven, forms face in the marking
Color is uneven, and the marking air-dry after can form shaggy polymeric membrane.
In addition, by adding fluorescent dyes rhodamine 123 in example 4, the marking for forming mimeograph is ultraviolet in 278nm
Fluorescence is produced under the irradiation of line, further increases the anti-counterfeit recognition ability of the marking, staff is only needed simple irradiation just
The marking true and false is can confirm that, reduces identification difficulty.
Particularly, the embodiment of the present invention uses less toxic raw material, materials health, and is substituted using full alcoholic solvent in conventional stamp-pad ink
Moisture content, improve the lipophilicity of stamp-pad ink and the rate of drying on skin.Stamp-pad ink in the embodiment of the present invention, which also has, to be produced into
The characteristics of this is low, raw material is easy to get, technique is simple.
Finally it should be noted that the above embodiments are merely illustrative of the technical scheme of the present invention and are not intended to be limiting thereof, to the greatest extent
The present invention is described in detail with reference to above-described embodiment for pipe, it should be understood by a person of ordinary skill in the art that technology
Still the embodiment of the present invention can be modified after reading present specification by personnel or equivalent substitution, but this
A little modifications are changed within all without departing from the present patent application accompanying claims protection domain.
Claims (10)
1. a kind of stamp-pad ink, it is characterised in that the stamp-pad ink includes the raw material of following parts by weight：5~15 parts of water soluble polymer, food
With 1~3 part of pigment, 80~93 parts of saturated alcohols, 0.5~3 part of antioxidant；The saturated alcohols are selected from ethanol, isopropanol, positive fourth
One or more in alcohol, glycerine.
2. stamp-pad ink according to claim 1, it is characterised in that the water soluble polymer be selected from polyvinylpyrrolidone,
One or more in carboxymethyl cellulose, polyacrylamide, hydrolyzed polyacrylamide, polyethylene glycol.
3. stamp-pad ink according to claim 2, it is characterised in that the water soluble polymer is polyvinylpyrrolidone, institute
Polyvinylpyrrolidonemolecules molecules amount is stated as 5000~50000.
4. stamp-pad ink according to claim 1, it is characterised in that the stamp-pad ink includes the raw material of following parts by weight：It is water-soluble
5~15 parts of macromolecule, 1~3 part of food coloring, 60~80 parts of ethanol, 2~4 parts of glycerine, 10~20 parts of n-butanol, antioxidant
0.5~3 part.
5. stamp-pad ink according to claim 1, it is characterised in that the food coloring is selected from famille rose, lemon yellow, three-coloured amaranth
One or more in red, alkermes, beta carotene, Monascus color.
6. stamp-pad ink according to claim 1, it is characterised in that the antioxidant is selected from ascorbic acid, citric acid, dimension life
One or more in plain E.
7. stamp-pad ink according to claim 1, it is characterised in that the stamp-pad ink also includes 0.1~1 part of fluorchrome.
8. stamp-pad ink according to claim 7, it is characterised in that the fluorchrome be selected from rhodamine B, acid rhodamine B,
One or more in rhodamine 6G, Rhodamine 123.
9. a kind of preparation method of stamp-pad ink as claimed in claim 1, it is characterised in that the preparation method comprises the following steps：
Step 1：Take food coloring to add in saturated polyol, be mixed evenly and be heated to 30~100 DEG C to food coloring
It is completely dissolved；
Step 2：Polyvinylpyrrolidone and antioxidant, stirring and dissolving are added into the solution obtained by step 1, it is cooled to 10~
30 DEG C, filtering, obtain stamp-pad ink.
10. the preparation method of stamp-pad ink according to claim 9, it is characterised in that heating-up temperature is 70~90 in the step 1
℃。
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| CN201710725693.4A CN107502056B (en) | 2017-08-22 | 2017-08-22 | Stamp-pad ink and preparation method thereof |
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| CN107502056B CN107502056B (en) | 2021-03-23 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113337153A (en) * | 2021-06-18 | 2021-09-03 | 浙江科力印业新技术发展有限公司 | Environment-friendly second-drying glass stamp-pad ink and preparation method thereof |
| CN116376349A (en) * | 2023-04-11 | 2023-07-04 | 北京国印网安科技有限公司 | Stamp-pad ink based on high molecular crosslinking and preparation method thereof |
| CN118027745A (en) * | 2024-02-19 | 2024-05-14 | 东莞市唐德医疗科技有限公司 | Ethyl violet composite medical skin marker ink and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113337153A (en) * | 2021-06-18 | 2021-09-03 | 浙江科力印业新技术发展有限公司 | Environment-friendly second-drying glass stamp-pad ink and preparation method thereof |
| CN116376349A (en) * | 2023-04-11 | 2023-07-04 | 北京国印网安科技有限公司 | Stamp-pad ink based on high molecular crosslinking and preparation method thereof |
| CN116376349B (en) * | 2023-04-11 | 2024-02-02 | 北京国印网安科技有限公司 | Stamp-pad ink based on high molecular crosslinking and preparation method thereof |
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