CN107496929A - Oleosin glue and preparation method thereof - Google Patents
Oleosin glue and preparation method thereof Download PDFInfo
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- CN107496929A CN107496929A CN201710877687.0A CN201710877687A CN107496929A CN 107496929 A CN107496929 A CN 107496929A CN 201710877687 A CN201710877687 A CN 201710877687A CN 107496929 A CN107496929 A CN 107496929A
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- oleosin
- glue
- pollen
- heating
- resin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/44—Oils, fats or waxes according to two or more groups of A61K47/02-A61K47/42; Natural or modified natural oils, fats or waxes, e.g. castor oil, polyethoxylated castor oil, montan wax, lignite, shellac, rosin, beeswax or lanolin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/32—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/46—Ingredients of undetermined constitution or reaction products thereof, e.g. skin, bone, milk, cotton fibre, eggshell, oxgall or plant extracts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8117—Homopolymers or copolymers of aromatic olefines, e.g. polystyrene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/70—Web, sheet or filament bases ; Films; Fibres of the matrix type containing drug
- A61K9/7023—Transdermal patches and similar drug-containing composite devices, e.g. cataplasms
- A61K9/703—Transdermal patches and similar drug-containing composite devices, e.g. cataplasms characterised by shape or structure; Details concerning release liner or backing; Refillable patches; User-activated patches
- A61K9/7038—Transdermal patches of the drug-in-adhesive type, i.e. comprising drug in the skin-adhesive layer
- A61K9/7076—Transdermal patches of the drug-in-adhesive type, i.e. comprising drug in the skin-adhesive layer the adhesive comprising ingredients of undetermined constitution or reaction products thereof, e.g. rosin or other plant resins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicinal Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Birds (AREA)
- Botany (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Insects & Arthropods (AREA)
- Zoology (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Preparation (AREA)
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Abstract
The present invention relates to a kind of oleosin glue and preparation method thereof.The oleosin glue of the present invention, grease is used, for substrate, to be merged with beeswax, pollen by adding rubber and resin, finished product is made in reaction.Beneficial effects of the present invention are：Oleosin glue of the invention is nontoxic, has no irritating odor, and is adapted to use in cosmetics and medicine；Easily realize the raising of drug effect, no sensitization；Preferable stability, winter resistance and heat resistance are kept for a long time.Because the present invention adds rubber and resin after grease is mixed with beeswax, pollen, viscosity is not only increased so that grease is preferably merged with beeswax, pollen, also causes finished product to have more preferable stability, winter resistance and heat resistance.
Description
Technical field
The present invention relates to a kind of protein adhesive, and in particular to a kind of oleosin glue and preparation method thereof.
Background technology
Plaster, plaster is commonly called as, is to refine medicinal material, edible vegetable oil and red lead into creme, spreads onto in framed back material
Manufactured external preparation.In traditional plaster production, oil and pellet are added in pharmaceutical compositions, cream is decocted into pot, is applied to paper
Or turn into plaster on cloth.This way is adapted to small-scale production, can not meet the needs of large-scale production.With chemical engineering industry
, there is the adhesive of medical of many asepsis environment-protectings in development, and plaster glue is exactly one kind therein, and it is by science detection and for a long time
Facts have proved nontoxic, health environment-friendly, and enter the large-scale production of modern procedural style, to supply and promote plaster
The modernization of adhesion production, scale.
Plaster glue is one kind of PUR, is the important component for making plaster, to increase the viscosity of plaster, simultaneously
And in plaster pharmaceutical compositions carrier.It is sprayed on non-woven fabrics and is carried out with plaster flush coater after addition pharmaceutical compositions in plaster glue
Spraying, has finally become plaster by the processing of plaster forming machine.It is general add pharmaceutical compositions be traditional Chinese medicine powder, essential oil of traditional Chinese medicine or
Chinese medical extract, but added drug ingedient accounting is less, PUR accounting more than more than 70%, cause made of plaster drug effect compared with
It is low.
The content of the invention
In order to solve the problems, such as that prior art is present, the invention provides a kind of oleosin glue and preparation method thereof, system
Oleosin glue there are stable components, it is nontoxic, have no irritating odor, without sensitization the features such as.
It is an object of the present invention to provide a kind of oleosin glue.
According to the oleosin glue of the specific embodiment of the invention, the oleosin glue is prepared by following raw material, described
Raw materials by weight includes：Grease 10-50%；Beeswax 10-30%；Pollen 1-5%；Rubber 10-30% and resin 10-
30%.
According to the oleosin glue of the specific embodiment of the invention, wherein, the grease is that vegetable oil, essential oil or Chinese medicine carry
Oil refining.
According to the oleosin glue of the specific embodiment of the invention, wherein, the vegetable oil is tea-seed oil.
According to the oleosin glue of the specific embodiment of the invention, wherein, the essential oil is Rosa Damascana.
According to the oleosin glue of the specific embodiment of the invention, wherein, the pollen is pollen pini.
Pollen pini, it is pinaceae plant masson pine, Chinese pine or the dry pollen for belonging to several plants together.It is sweet, it is warm-natured；Return liver,
The spleen channel；With astringing to arrest bleeding, the effect of eliminating dampness and astringing sores；It is dripping for traumatism and bleeding, eczema, impetigo, skin erosion, pus.
According to the oleosin glue of the specific embodiment of the invention, wherein, the resin is rosin resin, Petropols
And/or terpene resin；The rubber is SBS (SBS) or styrene-isoamyl two
Alkene-styrene block copolymer (SIS).
Another object of the present invention is to provide a kind of preparation method of oleosin glue.
According to the preparation method of the oleosin glue of the specific embodiment of the invention, the described method comprises the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and melting is to well mixed and react to obtain just
Secondary mixture；
(2) rubber is added in the mixture obtained to step (1), then heating and melting is to well mixed and react to obtain two
Secondary mixture；
(3) resin is added in the mixture obtained to step (2), then heating and melting is to well mixed and react to obtain oil
Lipoprotein glue.
According to the preparation method of the oleosin glue of the specific embodiment of the invention, in step (1), the heating and melting
Temperature is 160-200 DEG C.
According to the preparation method of the oleosin glue of the specific embodiment of the invention, in step (1), the heating and melting
Temperature is 180 DEG C.
It is described in step (2) and step (3) according to the preparation method of the oleosin glue of the specific embodiment of the invention
The temperature of heating and melting is 180-250 DEG C.
PUR is divided into rubber-type and EVA types, PUR composition in oleosin glue of the invention (including rubber and tree
Fat) belong to the PUR of rubber-type.
Traditional PUR is made of raw materials such as resin, tackifier, viscosity modifier and antioxidants.Wherein, viscosify
Agent is one of main auxiliary agent of PUR.If the cohesive force having at a certain temperature when only being melted with basic resin, works as temperature
After degree declines, just it is difficult to paper is soaked and permeated, loses cementitiousness, be unable to reach bond effect；Add tackifier
Can improves the mobility of colloid and the wetability to adherend, improves adhesive property, reaches required adhesion strength.Viscosity
Conditioning agent is also one of main auxiliary agent of PUR.It is mobility, the regulation setting rate for increasing colloid that it, which is acted on, to reach fast
The purpose that speed is firmly bonded, otherwise melt viscosity spend it is big, can not or be not easy to flow, it is difficult to penetrate into signature, cannot
It is firmly bonded.Add the low viscosity modifier of softening point, it is possible to permeated when reaching cohesive, glue to obtain firm purpose.One
As select paraffin, microwax.Synthetic wax (PE or PP), Buddhist support wax etc..Appropriate antioxidant is added, is to prevent EVA from heating
The premature aging of glue.Because colloid temperature drift meeting oxidation Decomposition in melting, adding antioxidant can ensure in hot conditions
Under, adhesive property does not change.Also need to mix some suitable cold belts according to the difference of temperature, area in addition to several raw materials more than
The cold-resistance agent of temperature or the antiheat agent for being adapted to tropical temperature.
The present invention is only with grease 10-50%；Beeswax 10-30%；Pollen 1-5%；Rubber 10-30% and resin 10-
30% is prepared, and rubber and resin only account for 20%-60%, if ointment is made, can also add medicinal powder thereto, then rubber and tree
The ratio of ointment shared by fat will be less.
Beneficial effects of the present invention are：
(1) oleosin glue of the invention is nontoxic, has no irritating odor, and is suitably used in cosmetics and medicine；This is
Because the present invention is using the grease beneficial to human body, pure natural beeswax and pollen, and nonpoisonous and tasteless rubber and resin work
For raw material, the content of the natural component in the composition of oleosin glue is improved to the full extent.
(2) plaster is prepared using the oleosin glue of the present invention, easily realizes the raising of drug effect, no sensitization；This be because
For the oleosin glue of the present invention, the content of drug ingedient in plaster can be improved, is reduced such as PURs such as rubber and resins
Composition, the content below 60% of PUR composition in the present invention, and the content of traditional PUR composition is more than 70%；Effectively
The content of functional component is improved, reduces sensitization rate.
(3) oleosin glue of the invention keeps preferable stability, winter resistance and heat resistance for a long time.Because
The present invention adds rubber and resin after grease is mixed with beeswax, pollen, not only increases viscosity so that grease and honeybee
Wax, pollen are preferably merged, and also cause finished product to have more preferable stability, winter resistance and heat resistance.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below
Detailed description.Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned
Other embodiment, belong to the scope that the present invention is protected.
Embodiment 1
A kind of oleosin glue, is prepared by following raw material, included by weight percentage：Tea-seed oil 50%；Beeswax 10%；Flower
Powder 1%；SIS (SBS) 20% and Petropols 19%.
Its preparation method, comprise the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and keeping temperature be 200 DEG C melted to
It is well mixed and reacts to obtain first mixture；
(2) rubber is added in the mixture obtained to step (1), then simultaneously keeping temperature is melted to mixed for 250 DEG C for heating
Close uniformly and react and obtain secondary mixture；
(3) resin is added in the mixture obtained to step (2), then simultaneously keeping temperature is melted to mixed for 250 DEG C for heating
Close uniformly and react and obtain oleosin glue.
Embodiment 2
A kind of oleosin glue, is prepared by following raw material, included by weight percentage：Rosa Damascana 10%；Beeswax 25%；
Pollen 5%；SBS (SIS) 30% and terpene resin 30%.
Its preparation method, comprise the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and keeping temperature be 160 DEG C melted to
It is well mixed and reacts to obtain first mixture；
(2) rubber is added in the mixture obtained to step (1), then simultaneously keeping temperature is melted to mixed for 180 DEG C for heating
Close uniformly and react and obtain secondary mixture；
(3) resin is added in the mixture obtained to step (2), then simultaneously keeping temperature is melted to mixed for 180 DEG C for heating
Close uniformly and react and obtain oleosin glue.
Embodiment 3
A kind of oleosin glue, is prepared by following raw material, included by weight percentage：Chinese medicine lard oil 20%；Beeswax
30%；Pollen pini 2%；Rubber 24% and rosin resin 24%.
Its preparation method, comprise the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and keeping temperature be 180 DEG C melted to
It is well mixed and reacts to obtain first mixture；
(2) rubber is added in the mixture obtained to step (1), then simultaneously keeping temperature is melted to mixed for 200 DEG C for heating
Close uniformly and react and obtain secondary mixture；
(3) resin is added in the mixture obtained to step (2), then simultaneously keeping temperature is melted to mixed for 200 DEG C for heating
Close uniformly and react and obtain oleosin glue.
Embodiment 4
A kind of oleosin glue, is prepared by following raw material, included by weight percentage：Traditional Chinese medicine powder 20%, Chinese medicine lard oil
20%；Beeswax 30%；Pollen pini 2%；Rubber 14% and rosin resin 14%.
Its preparation method, comprise the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and keeping temperature be 180 DEG C melted to
It is well mixed and reacts to obtain first mixture；
(2) rubber is added in the mixture obtained to step (1), then simultaneously keeping temperature is melted to mixed for 200 DEG C for heating
Close uniformly and react and obtain secondary mixture；
(3) resin is added in the mixture obtained to step (2), then simultaneously keeping temperature is melted to mixed for 200 DEG C for heating
Close uniformly and react and obtain oleosin glue.
In example 4, the materials such as available amino end acid, protein powder, sodium hyaluronate are gone back and substitute traditional Chinese medicine powder, applied to cosmetics
And pharmaceuticals industry.
Finished product obtained by embodiment 1-4 is detected, detection method and testing result such as table 1.
The testing result of table 1
Open hour are the complete fixed line time of adhesive.
As can be seen from the above table, the finished product obtained by embodiment 1-4 is yellowish-brown, the specification of finished product be 15cm ×
25cm × 3cm, and be detection impurity, illustrating the preparation method of the oleosin glue of the present invention can produce in enormous quantities, technique
It is stable；The softening point of finished product is between 50-80 DEG C, and viscosity is 1200mpas/120-200 °, and the open hour are in 30-
100s, show that the quality of finished of the present invention is preferable, modest viscosity, the open hour are longer.
The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any
Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all be contained
Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of oleosin glue, it is characterised in that the oleosin glue is prepared by following raw material, the raw material by weight hundred
Ratio is divided to include：Grease 10-50%；Beeswax 10-30%；Pollen 1-5%；Rubber 10-30% and resin 10-30%.
2. oleosin glue according to claim 1, it is characterised in that the grease is that vegetable oil, essential oil or Chinese medicine carry
Oil refining.
3. oleosin glue according to claim 2, it is characterised in that the vegetable oil is tea-seed oil.
4. oleosin glue according to claim 2, it is characterised in that the essential oil is Rosa Damascana.
5. oleosin glue according to claim 1, it is characterised in that the pollen is pollen pini.
6. oleosin glue according to claim 1, it is characterised in that the resin be rosin resin, Petropols and/
Or terpene resin；The rubber is that SBS or styrene-isoprene-phenylethene are embedding
Section copolymer.
7. prepare the method for the oleosin glue described in claim 1, it is characterised in that the described method comprises the following steps：
(1) grease, beeswax, pollen are weighed by proportioning and mixed, then heating and melting is to well mixed and react and mixed for the first time
Compound；
(2) rubber is added in the mixture obtained to step (1), then heating and melting is to well mixed and react to obtain secondary mixed
Compound；
(3) resin is added in the mixture obtained to step (2), then heating and melting is to well mixed and react to obtain grease egg
White glue.
8. the preparation method of oleosin glue according to claim 7, it is characterised in that in step (1), the heating is melted
The temperature of change is 160-200 DEG C.
9. the preparation method of oleosin glue according to claim 8, it is characterised in that in step (1), the heating is melted
The temperature of change is 180 DEG C.
10. the preparation method of oleosin glue according to claim 7, it is characterised in that in step (2) and step (3),
The temperature of the heating and melting is 180-250 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710877687.0A CN107496929A (en) | 2017-09-25 | 2017-09-25 | Oleosin glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710877687.0A CN107496929A (en) | 2017-09-25 | 2017-09-25 | Oleosin glue and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107496929A true CN107496929A (en) | 2017-12-22 |
Family
ID=60698783
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710877687.0A Pending CN107496929A (en) | 2017-09-25 | 2017-09-25 | Oleosin glue and preparation method thereof |
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| Country | Link |
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| CN (1) | CN107496929A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109430877A (en) * | 2018-11-12 | 2019-03-08 | 上海朴方生物科技有限公司 | A kind of grease lozenge and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60258296A (en) * | 1984-06-05 | 1985-12-20 | Tomoji Tanaka | Method for heating greenhouse or body by formed fuel mixure |
| CN102093831A (en) * | 2009-12-15 | 2011-06-15 | 上海中药制药技术有限公司 | Hot-melt pressure-sensitive adhesive and preparation method and application thereof |
| CN102727421A (en) * | 2011-04-13 | 2012-10-17 | 上海中药制药技术有限公司 | Resin ointment with high drug release, and preparation method and application thereof |
| CN103540281A (en) * | 2013-10-21 | 2014-01-29 | 广东东方树脂有限公司 | Quickly-cured rubber-type hot melt adhesive |
-
2017
- 2017-09-25 CN CN201710877687.0A patent/CN107496929A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60258296A (en) * | 1984-06-05 | 1985-12-20 | Tomoji Tanaka | Method for heating greenhouse or body by formed fuel mixure |
| CN102093831A (en) * | 2009-12-15 | 2011-06-15 | 上海中药制药技术有限公司 | Hot-melt pressure-sensitive adhesive and preparation method and application thereof |
| CN102727421A (en) * | 2011-04-13 | 2012-10-17 | 上海中药制药技术有限公司 | Resin ointment with high drug release, and preparation method and application thereof |
| CN103540281A (en) * | 2013-10-21 | 2014-01-29 | 广东东方树脂有限公司 | Quickly-cured rubber-type hot melt adhesive |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109430877A (en) * | 2018-11-12 | 2019-03-08 | 上海朴方生物科技有限公司 | A kind of grease lozenge and preparation method thereof |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171222 |
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