CN107496239A - A kind of fragrant plant eats the preparation method of lip gloss - Google Patents
A kind of fragrant plant eats the preparation method of lip gloss Download PDFInfo
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- CN107496239A CN107496239A CN201710813284.XA CN201710813284A CN107496239A CN 107496239 A CN107496239 A CN 107496239A CN 201710813284 A CN201710813284 A CN 201710813284A CN 107496239 A CN107496239 A CN 107496239A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The present invention relates to the preparation method that a kind of fragrant plant eats lip gloss, belong to cosmetic technical field.In order to overcome the toxicity of the pigment in lipstick in the prior art larger, easily there is the dry and cracked phenomenon of lip after use, the present invention provides the preparation method that a kind of fragrant plant eats lip gloss, it is the raw material based on fragrant plant, aromatic plant extract is obtained by way of the auxiliary distillation of suitable Microwave Extraction, lilac extract is obtained by supercritical extract, then aromatic plant extract and lilac extract are merged and in vegetable wax, the green auxiliary material such as avocado oil is mixed with to obtain the edible lip gloss of fragrant plant, the product can effectively prevent that the lip of user is dry and cracked, it is and safe and non-toxic, it is adapted to women long-term use of liking to be beautiful.
Description
Technical field
The present invention relates to the preparation method that a kind of fragrant plant eats lip gloss, belong to cosmetic technical field.
Background technology
Lipstick is to make lip ruddy glossy, reaches moist, protection lip, and increasing facial aesthetic feeling and amendment lip outline has
The product of effect is set off, is one of indispensable cosmetics of women, the sexy, charming of women can be showed;But lipstick because
It is applied on lip, so inevitably swallow in abdomen, and existing lipstick is all containing some harmful things
Matter, therefore under accumulating over a long period, the lipstick swallowed among human body necessarily produce harm to the health of body.
The main component of lipstick is pigment, surfactant, base starting material in the prior art(Grease wax etc.)And essence
Formed etc. auxiliary material.Composition and ratio is usually that wax class accounts for 20% ~ 25%, and oil and grease account for 65% to 70%, and pigment and pigment account for
10%, surfactant accounts for 5%(It is or following).But presently commercially available lipstick, certain safety issue be present.First, addition
The synthetic wax of the natural constituent such as wax, mostly ceresine, spermaceti, microwax, atoleine, although this ensure that lipstick can be into
Type, to the cold heat a kind of not dissolving deformation, but be also injury in practice for human body lip easily, not only cause lip dry and cracked de-
Skin, if after imprudence is had in belly, it can even more produce healthy hidden danger;For example in terms of pigment, what commercially available lipstick added is work
Industry pigment, although color is beautiful, consequence dare not be contemplated after eating
Chinese patent application 201610018884.2 discloses a kind of colored edible lipstick, and it includes following component:2-3
The coconut oil of part, the extra virgin avocado oil of 2-3 parts, the candelila wax of 1-3 parts, the supercritical extract pomegranate of 0.5-1.5 parts
The day of seed oil, the edible pigment of 1-1.5 parts, the sweet osmanthus wax of 0.5-1 parts, the plant saualane of 0.5-1 parts and 0.5-1 parts
Right vitamin E, any synthetic fragrance is not added with, possesses more preferable smell, all raw materials are natural material, right after eating
Human body fanout free region, and lipstick gloss naturally, lip feel is very soft, and the raw material used is all all-natural product, can be with
For eating.
The content of the invention
Easily occur that lip is dry and cracked to be showed in order to overcome the toxicity of the pigment in lipstick in the prior art larger, after use
As the present invention provides the preparation method that a kind of fragrant plant eats lip gloss, and it is the raw material based on fragrant plant, passes through conjunction
The mode of suitable Microwave Extraction auxiliary distillation obtains aromatic plant extract, and lilac extract is obtained by supercritical extract,
Then aromatic plant extract and lilac extract are merged and is mixed with to obtain virtue in the green auxiliary material such as vegetable wax, avocado oil
Fragrant plant edible food lip gloss, the product can effectively prevent that the lip of user is dry and cracked, and safe and non-toxic, be adapted to women length of liking to be beautiful
Phase uses.
The present invention is achieved through the following technical solutions above-mentioned technique effect:
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio:0.8-1.6:4-8 ratio is mixed to prepare aromatic plant powder, and it is added to aromatic plant powder
The purified water of 5 times of volumes of quality, is placed in Microwave Extraction device, and it is 350W-500W to control Microwave Extraction power, continuous extraction
Extract solution is transferred in boiler after 15-25min, computer heating control distillation kettle temperature is 55-69 DEG C, and distillation pot inner pressure is
2-3Kpa, continuous still 1-1.5h, temperature is increased to 150-160 DEG C, distillates fragrant plant oil-water mixture, by fragrant plant
Oil-water mixture is by condensing tube condensation, and the inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, is then passed through
Oil water separator is separated, and obtains including the aromatic plant extract of essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 24-28MPa to set extraction kettle pressure, and temperature is 35-55 DEG C, extraction time 2-4h;
Supercritical carbon dioxide fluid dissolved with extract successively enters separating still I and separating still II through pressure-reducing valve, sets separating still I
Pressure is 6-8MPa, and temperature is 44-48 DEG C, collects extract I;It is 4-5MPa, temperature 32-34 to set the pressure of separating still II
DEG C, collect extract II;Combining extraction liquid I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
Thing extract solution 4-5 parts, lilac extract 6-8 parts, 3-5 part vegetable waxs, 2-4 part sweet osmanthus waxes, 3-5 part avocado oils, 1.5-2.5 part coconut palms
Seed oil, 2-3 part red beet powder, vegetable wax is heated into 60 DEG C -78 DEG C dissolves it, adds aromatic plant extract, fourth thereto
Fragrant flower extract, vegetable wax, avocado oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould
It can obtain fragrant plant and eat lip gloss.
Preferably, the step 1)Thyme powder, lavender powder and giant knotweed powder mass ratio are 1 in middle aromatic plant powder:
1.2:6.
Preferably, the step 1)Middle Microwave Extraction power is 450W, extraction time 20min.
Preferably, the step 1)Middle vapo(u)rizing temperature is 62 DEG C, distillation time 1h.
Preferably, the mass ratio of cloves pollen and entrainer is 1 in the step 2):4-6.
Preferably, the step 2)Middle extraction kettle pressure is 26MPa, and temperature is 45 DEG C, separated when extraction time is 3h
The active ingredient of obtained lilac is maximum.
Preferably, the step 2)The pressure of middle setting separating still I is 7MPa, and temperature is 46 DEG C;Separating still II is set to press
Power is 4.5MPa, and temperature is 33 DEG C.
Fragrant plant of the present invention is eaten in lip gloss formula:
1st, set cured:Candelila wax is natural plants wax, also known as candy lira wax, the yellowish glossy waxy solid in angle, there is aroma
Taste, the crisp and hard total quality such as vegetalitas wax, its ductility, pigment-dispersing, peel.While lipstick gloss is certainly
So, lip feel is very soft.
2nd, sweet osmanthus wax:Sweet osmanthus wax derives from the plant wax that itself is contained in sweet osmanthus valve, is the by-product for extracting the former essence of sweet osmanthus
Product, petal wax is come out by complete purification among extraction process, has special moisturizing effect to skin of lip.
3rd, avocado oil:Avocado oil is adapted to the crowd of dry skin, aging to use.Skin damages caused by sunlight or weather
Wound, for example be dehydrated or used when malnutritive, effect is very good.It also has the function of making skin regeneration and softening skin tissue.
Avocado oil is easily absorbed by deep tissues, can effectively softening skin tissue, skin moisturization are obvious.
4th, coconut oil:Coconut oil can use what beauty anti-aging, have very strong oxidation resistance, human body can be helped to prevent freedom
The generation of base.Oral administration and externally all can skin care, adjust smegma, improve the dry skin quality of the universe, smooth away wrinkles, acne and scalp
Bits.Allergy skin quality can strengthen skin adaptability, lip of releiving cracking, Exposure to Sunlight, frostbite, diaper rash and gingivitis.Skin can be protected
Not by uv damage.
5th, Geranium Essential:The major function of Geranium Essential is to stimulate circulation, and makes the skin of lip more red
Moisten vibrant, make the glossy exquisiteness of skin.
The present invention has following technical advantage relative to prior art:
1)The present invention use fragrant plant to extract active component from lilac for primary raw material extraction aromatic oil, and auxiliary with
Other such as avocado oils, vegetable wax plant origin material, its is safe and non-toxic, long-term use of thing toxic action.
2)It can effectively lower during the preparation-obtained lipstick use of the present invention or avoid user from producing lip and do
Phenomena such as splitting, its compliance is strong, and audient's degree is high, can carry out popularization and application.
3)For red beet powder of the present invention as pigment substitute, its is safe and non-toxic, and length of holding time, and does not take off
Color, it is adapted to use in lipstick production.
Embodiment
The present invention is further described below by way of specific embodiment, but the embodiment does not limit this hair in any way
The scope of bright patent protection.
A kind of 1 fragrant plant of embodiment eats the preparation method of lip gloss
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio:0.8:4 ratio is mixed to prepare aromatic plant powder, and 5 times of its quality is added to aromatic plant powder
The purified water of volume, it is placed in Microwave Extraction device, it is 350W to control Microwave Extraction power, will extraction after continuous extraction 15min
Liquid is transferred in boiler, and computer heating control distillation kettle temperature is 55 DEG C, and distillation pot inner pressure is 2Kpa, continuous still 1h, is incited somebody to action
Temperature is increased to 150 DEG C, distillates fragrant plant oil-water mixture, cold by fragrant plant oil-water mixture by condensing tube condensation
The inlet temperature of solidifying pipe is 150 DEG C, and outlet temperature is 70 DEG C, is then separated it by oil water separator, comprising
The aromatic plant extract of essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 24MPa to set extraction kettle pressure, and temperature is 35 DEG C, extraction time 2h;Dissolved with extraction
The supercritical carbon dioxide fluid for going out thing successively enters separating still I and separating still II through pressure-reducing valve, and the setting pressure of separating still I is
6MPa, temperature are 44 DEG C, collect extract I;It is 4MPa to set the pressure of separating still II, and temperature is 32 DEG C, collects extract II;Close
And extract I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
4 parts of thing extract solution, 6 parts of lilac extract, 3 parts of vegetable waxs, 2 parts of sweet osmanthus waxes, 3 parts of avocado oils, 1.5 portions of coconut oil, 2 parts of red beets
Powder, vegetable wax is heated into 60 DEG C dissolves it, adds aromatic plant extract, lilac extract, vegetable wax, avocado thereto
Oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould and can obtain fragrant plant and eat
Lip gloss.
A kind of 2 fragrant plant of embodiment eats the preparation method of lip gloss
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio: 1.6:8 ratio is mixed to prepare aromatic plant powder, and its quality 5 is added to aromatic plant powder
The purified water of times volume, is placed in Microwave Extraction device, and it is 500W to control Microwave Extraction power, it is continuous extract 25min after will carry
Liquid is taken to be transferred in boiler, computer heating control distillation kettle temperature is 69 DEG C, and distillation pot inner pressure is 3Kpa, continuous still
1.5h, is increased to 160 DEG C by temperature, distillates fragrant plant oil-water mixture, and fragrant plant oil-water mixture is passed through into condenser pipe
Condensation, the inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, and then it is separated by oil water separator, is obtained
To the aromatic plant extract comprising essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 28MPa to set extraction kettle pressure, and temperature is 55 DEG C, extraction time 4h;Dissolved with extraction
The supercritical carbon dioxide fluid for going out thing successively enters separating still I and separating still II through pressure-reducing valve, and the setting pressure of separating still I is
8MPa, temperature are 48 DEG C, collect extract I;It is 5MPa to set the pressure of separating still II, and temperature is 34 DEG C, collects extract II;Close
And extract I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
5 parts of thing extract solution, 8 parts of lilac extract, 5 parts of vegetable waxs, 4 parts of sweet osmanthus waxes, 5 parts of avocado oils, 2.5 portions of coconut oil, 3 parts red
Sugar beet powder, vegetable wax is heated into 78 DEG C dissolves it, adds aromatic plant extract, lilac extract, vegetable wax, crocodile thereto
Pear oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature retrogressing mould and can obtain fragrant plant food
Use lip gloss.
A kind of 3 fragrant plant of embodiment eats the preparation method of lip gloss
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio:1.2:6 ratio is mixed to prepare aromatic plant powder, and 5 times of its quality is added to aromatic plant powder
The purified water of volume, it is placed in Microwave Extraction device, it is 450W to control Microwave Extraction power, will extraction after continuous extraction 20min
Liquid is transferred in boiler, and computer heating control distillation kettle temperature is 62 DEG C, and distillation pot inner pressure is 2.5Kpa, continuous still
1.5h, is increased to 155 DEG C by temperature, distillates fragrant plant oil-water mixture, and fragrant plant oil-water mixture is passed through into condenser pipe
Condensation, the inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, and then it is separated by oil water separator, is obtained
To the aromatic plant extract comprising essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 26MPa to set extraction kettle pressure, and temperature is 45 DEG C, extraction time 3h;Dissolved with extraction
The supercritical carbon dioxide fluid for going out thing successively enters separating still I and separating still II through pressure-reducing valve, and the setting pressure of separating still I is
7MPa, temperature are 46 DEG C, collect extract I;It is 4.5MPa to set the pressure of separating still II, and temperature is 33 DEG C, collects extract II;
Combining extraction liquid I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
4.5 parts of thing extract solution, 7 parts of lilac extract, 4 parts of vegetable waxs, 3 parts of sweet osmanthus waxes, 4 parts of avocado oils, 2 portions of coconut oil, 2.5 parts of red sweet teas
Vegetable powder, vegetable wax is heated into 69 DEG C dissolves it, adds aromatic plant extract, lilac extract, vegetable wax, avocado thereto
Oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould and can obtain fragrant plant and eat
Lip gloss.
A kind of 4 fragrant plant of embodiment eats the preparation method of lip gloss
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio: 1.6:4 ratio is mixed to prepare aromatic plant powder, and its quality 5 is added to aromatic plant powder
The purified water of times volume, is placed in Microwave Extraction device, and it is 500W to control Microwave Extraction power, it is continuous extract 15min after will carry
Liquid is taken to be transferred in boiler, computer heating control distillation kettle temperature is 69 DEG C, and distillation pot inner pressure is 2Kpa, continuous still
1.5h, is increased to 150 DEG C by temperature, distillates fragrant plant oil-water mixture, and fragrant plant oil-water mixture is passed through into condenser pipe
Condensation, the inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, and then it is separated by oil water separator, is obtained
To the aromatic plant extract comprising essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 28MPa to set extraction kettle pressure, and temperature is 35 DEG C, extraction time 4h;Dissolved with extraction
The supercritical carbon dioxide fluid for going out thing successively enters separating still I and separating still II through pressure-reducing valve, and the setting pressure of separating still I is
6MPa, temperature are 48 DEG C, collect extract I;It is 4MPa to set the pressure of separating still II, and temperature is 34 DEG C, collects extract II;Close
And extract I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
4 parts of thing extract solution, 8 parts of lilac extract, 3 parts of vegetable waxs, 2 parts of sweet osmanthus waxes, 5 parts of avocado oils, 1.5 portions of coconut oil, 3 parts of red sweet teas
Vegetable powder, vegetable wax is heated into 60 DEG C dissolves it, adds aromatic plant extract, lilac extract, vegetable wax, avocado thereto
Oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould and can obtain fragrant plant and eat
Lip gloss.
A kind of 5 fragrant plant of embodiment eats the preparation method of lip gloss
A kind of fragrant plant eats the preparation method of lip gloss, and it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio:0.8:8 ratio is mixed to prepare aromatic plant powder, and its quality 5 is added to aromatic plant powder
The purified water of times volume, is placed in Microwave Extraction device, and it is 350W to control Microwave Extraction power, it is continuous extract 25min after will carry
Liquid is taken to be transferred in boiler, computer heating control distillation kettle temperature is 55 DEG C, and distillation pot inner pressure is 3Kpa, continuous still 1h,
Temperature is increased to 160 DEG C, distillates fragrant plant oil-water mixture, by fragrant plant oil-water mixture by condensing tube condensation,
The inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, and then it is separated by oil water separator, is wrapped
Aromatic plant extract containing essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 24MPa to set extraction kettle pressure, and temperature is 55 DEG C, extraction time 2h;Dissolved with extraction
The supercritical carbon dioxide fluid for going out thing successively enters separating still I and separating still II through pressure-reducing valve, and the setting pressure of separating still I is
8MPa, temperature are 44 DEG C, collect extract I;It is 5MPa to set the pressure of separating still II, and temperature is 32 DEG C, collects extract II;Close
And extract I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
5 parts of thing extract solution, 6 parts of lilac extract, 5 parts of vegetable waxs, 4 parts of sweet osmanthus waxes, 3 parts of avocado oils, 2.5 portions of coconut oil, 2 parts of red sweet teas
Vegetable powder, vegetable wax is heated into 78 DEG C dissolves it, adds aromatic plant extract, lilac extract, vegetable wax, avocado thereto
Oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould and can obtain fragrant plant and eat
Lip gloss.
6 fragrant plant of the present invention of embodiment eats therapeutic effect of the lip gloss to cheilitis
400 patients of this group.Clinical diagnosis is cheilitis, except acute severe contact cheilitis.Not used in medical first 2 weeks
What oral or external medication, and can medication and further consultation person on request.
Research object is chronic cheilitis patient 400 in this experiment, and female 198 is male 202;Age 13~42
Year, first attack 180, recurrent exerbation 220;The course of disease 2 weeks~6 months.It is randomly divided into 2 groups, each 26.Control
It is local in lip mucous membrane and disease damage that group applies commercially available Chinese medicine anti-anaphylaxis musclemoistening paste outside, daily 2 times.2nd group of Chinese medicine applies implementation of the present invention outside
The edible lip gloss of fragrant plant that example 3 is prepared is local in lip mucous membrane and disease damage, daily 2 times.
Efficacy determination:Recovery from illness:Pain symptom disappearance of itching is felt, lip mucosa lesions all disappear;It is effective:Dry and chap
Most of healing is split, pain bleeding is clearly better;Take a turn for the better:Dry and chap part is healed, subjective symptoms take a favorable turn;
It is invalid:Dry and chap is most of without healing, subjective symptoms is without being clearly better.
Group | Recovery from illness | It is effective | Take a turn for the better | It is invalid | It is efficient |
Treatment group | 132 | 37 | 25 | 6 | 97% |
Control group | 65 | 54 | 15 | 66 | 67% |
It is to have anti-harelip, anti-drying that experimental result, which shows that fragrant plant of the present invention eats lip gloss, moistens lip and simultaneously controls
Treat the Chinese herbal medicine lip-stick of cheilitis effect.Curative effect is improved, patient is comfortable on after smearing, alleviates local symptom, and be not easy to pollute
Clothes, patient is easy to carry, and its therapeutic effect is significantly better than existing Chinese medicine lip gloss.
7 fragrant plant of the present invention of embodiment eats its mouse oral acute toxicity testing of lip gloss
According to Huo Enfa, from Kunming kind healthy mice 40,4 groups are randomly divided into, every group 10, male and female half and half.Average weight
Female mice (19.4 ± 1.6) g.Male mice (18.5 ± 1.5) g.Virtue of the laboratory sample prepared by according to the embodiment of the present invention 1
Fragrant plant lip gloss, set dosage is 21.5,10.0,4.64,2.15g/ (kgbw), after an orally administration tested material, see
Examine animal poisoning reaction and death condition in two weeks.
Its mouse oral acute toxicity testing experimental result is shown:Each group mouse is showed no abnormal response within the observation period, raw
Length is all right, and no dead generation, female mice end weight is (27.4 ± 2.8) g, and male mouse end weight is (28.9 ± 1.1) g, LD50>
21.5g/(kg·bw);According to acute toxicity grading criteria.Fragrant plant of the present invention eats lip gloss and belongs to nontoxic level material, can be with
Reach edible rank.
Claims (7)
1. a kind of fragrant plant eats the preparation method of lip gloss, it specifically includes following step:
1)It is prepared by aromatic plant extract:Thyme, lavender and giant knotweed are respectively crushed into powder, according to thyme powder, smoke clothing
Grass meal is 1 with giant knotweed powder mass ratio:0.8-1.6:4-8 ratio is mixed to prepare aromatic plant powder, and it is added to aromatic plant powder
The purified water of 5 times of volumes of quality, is placed in Microwave Extraction device, and it is 350W-500W to control Microwave Extraction power, continuous extraction
Extract solution is transferred in boiler after 15-25min, computer heating control distillation kettle temperature is 55-69 DEG C, and distillation pot inner pressure is
2-3Kpa, continuous still 1-1.5h, temperature is increased to 150-160 DEG C, distillates fragrant plant oil-water mixture, by fragrant plant
Oil-water mixture is by condensing tube condensation, and the inlet temperature of condenser pipe is 150 DEG C, and outlet temperature is 70 DEG C, is then passed through
Oil water separator is separated, and obtains including the aromatic plant extract of essential oil;
2)Lilac extracts active ingredients:It will be cleaned after lilac stalk and cross 20 mesh sieves after being ground into cloves pollen after drying, will
Cloves pollen is prepared by mixing into extraction solution with the ethanol of entrainer 95%;Extraction solution is placed in extraction kettle, into extraction kettle
Supercritical carbon dioxide fluid is inputted, it is 24-28MPa to set extraction kettle pressure, and temperature is 35-55 DEG C, extraction time 2-4h;
Supercritical carbon dioxide fluid dissolved with extract successively enters separating still I and separating still II through pressure-reducing valve, sets separating still I
Pressure is 6-8MPa, and temperature is 44-48 DEG C, collects extract I;It is 4-5MPa, temperature 32-34 to set the pressure of separating still II
DEG C, collect extract II;Combining extraction liquid I and extract II obtain lilac extract;
3)Fragrant plant eats lip gloss and prepared:Fragrant plant, which is prepared, according to following ratio of weight and number eats lip gloss:Fragrance is planted
Thing extract solution 4-5 parts, lilac extract 6-8 parts, 3-5 part vegetable waxs, 2-4 part sweet osmanthus waxes, 3-5 part avocado oils, 1.5-2.5 part coconut palms
Seed oil, 2-3 part red beet powder, vegetable wax is heated into 60 DEG C -78 DEG C dissolves it, adds aromatic plant extract, fourth thereto
Fragrant flower extract, vegetable wax, avocado oil, coconut oil and red beet powder, stir after-pouring, are cooled to room temperature and retreat mould
It can obtain fragrant plant and eat lip gloss.
2. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that the step 1)In
Thyme powder, lavender powder and giant knotweed powder mass ratio are 1 in aromatic plant powder:1.2:6.
3. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that the step 1)In
Microwave Extraction power is 450W, extraction time 20min.
4. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that the step 1)In
Vapo(u)rizing temperature is 62 DEG C, distillation time 1h.
5. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that in the step 2)
The mass ratio of cloves pollen and entrainer is 1:4-6.
6. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that the step 2)In
Extraction kettle pressure is 26MPa, and temperature is 45 DEG C, extraction time 3h.
7. fragrant plant according to claim 1 eats the preparation method of lip gloss, it is characterised in that, the step 2)
The pressure of middle setting separating still I is 7MPa, and temperature is 46 DEG C;It is 4.5MPa to set the pressure of separating still II, and temperature is 33 DEG C.
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