CN107488701A - The method of quality control of no added facial mask and its application and the packing method of no added facial mask - Google Patents

The method of quality control of no added facial mask and its application and the packing method of no added facial mask Download PDF

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Publication number
CN107488701A
CN107488701A CN201710844561.3A CN201710844561A CN107488701A CN 107488701 A CN107488701 A CN 107488701A CN 201710844561 A CN201710844561 A CN 201710844561A CN 107488701 A CN107488701 A CN 107488701A
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added
facial mask
quality control
transparent
nutrient solution
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Inventor
邓必彪
杨志喜
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Guangzhou's No Added Cosmetics Co Ltd
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Guangzhou's No Added Cosmetics Co Ltd
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Priority to CN201710844561.3A priority Critical patent/CN107488701A/en
Priority to PCT/CN2017/109787 priority patent/WO2019051965A1/en
Publication of CN107488701A publication Critical patent/CN107488701A/en
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12QMEASURING OR TESTING PROCESSES INVOLVING ENZYMES, NUCLEIC ACIDS OR MICROORGANISMS; COMPOSITIONS OR TEST PAPERS THEREFOR; PROCESSES OF PREPARING SUCH COMPOSITIONS; CONDITION-RESPONSIVE CONTROL IN MICROBIOLOGICAL OR ENZYMOLOGICAL PROCESSES
    • C12Q1/00Measuring or testing processes involving enzymes, nucleic acids or microorganisms; Compositions therefor; Processes of preparing such compositions
    • C12Q1/02Measuring or testing processes involving enzymes, nucleic acids or microorganisms; Compositions therefor; Processes of preparing such compositions involving viable microorganisms
    • C12Q1/04Determining presence or kind of microorganism; Use of selective media for testing antibiotics or bacteriocides; Compositions containing a chemical indicator therefor
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/20Bacteria; Culture media therefor

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  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • General Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Biochemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • General Health & Medical Sciences (AREA)
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Abstract

The invention provides a kind of method of quality control of no added facial mask and its application and the packing method of no added facial mask, it is related to facial mask production field, the method for quality control of the no added facial mask, comprises the following steps:No added nutrient solution is sealed in transparent packaging substrate, then carries out Bacteria Culture, outward appearance detection is carried out to the no added nutrient solution in transparent packaging substrate afterwards.The product being contaminated by bacterial can be effectively rejected using the method for quality control, so as to alleviate the technical problem that the product being contaminated by bacterial can not be effectively removed after no added facial mask of the prior art seals.

Description

The method of quality control of no added facial mask and its application and the bag of no added facial mask Dress method
Technical field
The present invention relates to the technical field of facial mask production, more particularly, to a kind of quality control side of no added facial mask Method and its application and the packing method of no added facial mask.
Background technology
The formula of facial treatment mask product has raw material of industry addition, such as artificial color, artificial essence, mineral oil, petroleum Surfactant, alcohol, preservative, heavy metal and hormone etc..These additives have potential hazard to the skin of people, when long Between use the chronic injury that skin can be caused profound.
With the raising of quality of life, requirement of the people to consumer safety is more and more stronger.The end of the eighties in last century Phase, Japanese cosmetic industry start not adding the chemical composition for the effect of being irritating to the skin as far as possible;The initial stage nineties, one, Japan Cosmetics group releases completely no added cosmetics first, starts the beginning of no added cosmetics.So-called " no added ", refers to There is no the composition that addition forms sensitive infringement to skin during production and selling, " color is dirty to avoid the occurrence of " perfume pollutes " Dye " " oily pollution ", is damaged to consumer's body.Including bactericide, preservative, acidifying preventing agent, artificial perfume, artificial color 102 kinds of compositions including element, grease and interfacial agent etc. are defined as " adding ingredient ".Therefore, " no added " is equivalent more The synonym of safety, more effective facial mask.The prerequisite several features of " no added " product:Preservative free, without bactericide, Without petroleum surfactant, perfume-free, non-mineral oil and it is fully sealed.
The appearance of " no added ", it is to answer mankind's life to beautiful, healthy, safety pursuit.Moreover, huge market demand Huge market potential is provided to " no added " product.Nowadays, " no added " with it is organic, natural, not only being embodied in In cosmetic, also as a kind of thought spirit, life various aspects are penetrated into.
But no added product is not because the inside has any preservative, bactericide and without petroleum surfactant etc., very Easy breed bacteria, in encapsulation, no added nutrient solution once will make it that product is apt to deteriorate by germ contamination.It is and current No added skin-protection product be mainly directly packaged in opaque polybag, then just sold.If like this Some bacteriums in no added nutrient solution be present can not directly observe, and can not more be detected and will be contaminated by bacterial Product removes, so as to cause contaminated no added facial mask storage time one length to be easy to occur qualitative change influence product quality and Use.
In view of this, it is special to propose the present invention.
The content of the invention
The first object of the present invention is to provide a kind of method of quality control of no added facial mask, utilizes the quality control Method can effectively reject the product being contaminated by bacterial, and can not have so as to alleviate after no added facial mask of the prior art seals Effect removes the technical problem for the product being contaminated by bacterial.
The second object of the present invention is that provide a kind of method of quality control of above-mentioned no added facial mask adds in preparation nothing Add the purposes in facial mask.
The third object of the present invention is to provide a kind of packing method of no added facial mask, wrapped using this method Dress, it is easy to whether there is product rotten identify before using facial mask.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme:
A kind of method of quality control of no added facial mask, comprises the following steps:No added nutrient solution is sealed in transparent In packing material, Bacteria Culture is then carried out, outward appearance detection is carried out to the no added nutrient solution in transparent packaging substrate afterwards.
Further, the temperature of Bacteria Culture is 35-40 DEG C, and incubation time is 3-30 days.
Further, the temperature of Bacteria Culture is 35-39 DEG C, and incubation time is 5-25 days.
Further, the temperature of Bacteria Culture is 36-38 DEG C, and incubation time is 12-20 days.
Further, aseptically no added nutrient solution is sealed in transparent packaging substrate.
Further, no added nutrient solution is sealed in transparent packaging substrate under 40-95 DEG C of environment.
Further, the transparent packaging substrate is transparent packing bag.
Further, the transparent packing bag is transparent packing bag, the transparent packing bag or PET materials of PP materials of PE materials The transparent packing bag of matter.
A kind of purposes of method of quality control of above-mentioned no added facial mask in no added facial mask is prepared.
A kind of packing method of no added facial mask, using the method for quality control of above-mentioned no added facial mask to being sealed in No added nutrient solution in transparent packaging substrate is detected, and detection certified products progress outer packing is operated and produces the no added shield Skin film.
Compared with the prior art, the present invention has the advantages that:
In method of quality control provided by the invention, no added nutrient solution is sealed in a transparent packaging substrate first, so Carry out Bacteria Culture again afterwards, carry out outward appearance detection afterwards, the project of detection mainly has:Whether no added nutrient solution changes colour, and nothing adds Whether impurity, mildew, stain or crystallization are had in Ensure Liquid liquid, and whether transparent packaging substrate has the bag that rises.In above process, carry out thin After bacterium culture, if bacterium in nutrient solution be present, after cultivating bacterial reproduction, directly observe transparent packaging substrate and can determine whether Whether go out in no added nutrient solution has bacterium.Color change when no added nutrient solution, there is mildew or transparent packaging substrate hair Raw bulge or the bag that rises then illustrate that the no added nutrient solution in the transparent packaging substrate has been contaminated.So as to remove it is contaminated not Certified products, ensure that the quality of the product of sale is relatively reliable.
The step of Bacteria Culture is innovatively employed in the method for quality control is for detecting the no added battalion sealed Whether nutrient solution is contaminated by bacterial, so as to effectively increase the quality of the no added facial mask of sale.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the present invention.It is unreceipted specific in embodiment Condition person, the condition suggested according to normal condition or manufacturer are carried out.Agents useful for same or the unreceipted production firm person of instrument, it is The conventional products that can be obtained by commercially available purchase.
A kind of method of quality control of no added facial mask, comprises the following steps:No added nutrient solution is sealed in transparent In packing material, Bacteria Culture is then carried out, outward appearance detection is carried out to the no added nutrient solution in transparent packaging substrate afterwards.
In method of quality control provided by the invention, no added nutrient solution is sealed in a transparent packaging substrate first, so Carry out Bacteria Culture again afterwards, in this case, if bacterium in nutrient solution be present, after cultivating bacterial reproduction, directly see Examining transparent packaging substrate can judge whether there is bacterium in no added nutrient solution.Color change, appearance when no added nutrient solution Bulge occurs for mildew or transparent packaging substrate or the bag that rises then illustrates that the no added nutrient solution in the transparent packaging substrate has been contaminated.From And contaminated defective work can be removed, ensure that the quality of the product of sale is relatively reliable.
The step of Bacteria Culture is innovatively employed in the method for quality control is for detecting the no added battalion sealed Whether nutrient solution is contaminated by bacterial, so as to effectively increase the quality of the no added facial mask of sale.
No added nutrient solution in the present invention is sealed and after the Bacteria Culture of suitable condition, by manually to transparent bag Dress thing is very detected, and observes the distribution of color in transparent packaging substrate, if impurity, mildew, stain or crystallization occur, together When phenomena such as whether transparent packaging substrate generates bulge or rise bag can be observed.If there is these phenomenons, illustrate transparent wrapper There is germ contamination in thing, by breeding the bacterium colony of different colours is presented, or bacterial metabolism produces gas and caused in bacterium Bright packing material bulge or the bag that rises, now directly destroy problematic transparent packaging substrate, forbid carrying out the packing and selling of next step. So as to avoid consumer from buying contaminated no added facial mask.
Due to also changing original packing method in the present invention, i.e., no added nutrient solution is sealed in transparent packaging substrate It is interior, for consumers, it is also easier to judge facial mask with the presence or absence of problem.Traditional facial mask, especially face Film is typically all to be directly packaged in opaque polybag, if there is pollution in sealing, at all can not before use Distinguish the quality of facial mask.And it is of the invention, can intuitively it be judged very much by situation about observing in transparent packaging substrate before use With the presence or absence of pollution or rotten, the quality guarantee of product is substantially increased, makes consumer safe to use.
As the preferred embodiment of the present invention, the temperature of Bacteria Culture is 35-40 DEG C, and incubation time is 3-30 days.Profit The product that Bacteria Culture can detect to be contaminated by bacterial in a short time is carried out with this method.
In above-mentioned preferred embodiment, the typical but non-limiting temperature of Bacteria Culture is, for example,:35℃、36℃、 37 DEG C, 38 DEG C, 39 DEG C or 35 DEG C;Incubation time is typical but non-limiting to be, for example,:3 days, 4 days, 5 days, 6 days, 7 days, 8 days, 9 My god, 10 days, 11 days, 12 days, 13 days, 14 days, 15 days, 16 days, 17 days, 18 days, 19 days, 20 days, 21 days, 22 days, 23 days, 24 My god, 25 days, 26 days, 27 days, 28 days, 29 days or 30 days.
As the preferred embodiment of the present invention, the temperature of Bacteria Culture is 35-39 DEG C, and incubation time is 5-25 days.Make For further preferred embodiment of the present invention, the temperature of Bacteria Culture is 36-38 DEG C, and incubation time is 12-20 days.By excellent Change cultivation temperature and incubation time, can while defective work is effectively differentiated quality inspection efficiency.
As the preferred embodiment of the present invention, no added nutrient solution is aseptically sealed in transparent packaging substrate It is interior.As further preferred embodiment of the present invention, no added nutrient solution is sealed in transparent wrapper under 40-95 DEG C of environment In thing.By aseptically being sealed, it is possible to reduce into the quantity of the bacterium in transparent packing bag, improve product Accepted product percentage.
Above-mentioned aseptic condition also including high-cleanness, high production environment and carried out using aseptic filler it is filling, wherein noble and unsullied The production environment of cleanliness is preferably within 10,000 grades.
As the preferred embodiment of the present invention, the transparent packaging substrate is transparent packing bag.Using transparent packing bag both The color of the no added nutrient solution in transparent packing bag can be easily observed, bag feelings that rise of transparent packing bag can be observed again Condition, so as to accurately and effectively judge the quality of product.
As the preferred embodiment of the present invention, the transparent packing bag is the transparent packing bag of PE materials, PP materials The transparent packing bag of transparent packing bag or PET materials.The transparent packing bag of PE materials, the transparent packing bag of PP materials or PET materials The transparent packing bag of matter is durable in use, can bear high temperature, be not susceptible to qualitative change.
The second aspect of the invention provides a kind of method of quality control of above-mentioned no added facial mask and added in preparation nothing Add the purposes in facial mask.
A kind of packing method of no added facial mask of the third aspect of the invention, utilizes the matter of above-mentioned no added facial mask Amount control method is detected to the no added nutrient solution being sealed in transparent packaging substrate, and detection certified products are carried out into outer packing behaviour Produce the no added facial mask.
Using the no added facial mask arrived of above-mentioned packing method, it is divided into inner packing and outer packing, interior bag in packaging structure Dress as transparent packaging substrate, opaque packaging bag of the outer packing preferably with printed patterns.Two layers inside and outside whole packaging formation Packaging structure, because inner packing is transparent packaging substrate, now, if bacterium in no added nutrient solution be present, by cultivating, carefully After bacterium breeding, inner bag is directly observed, if inner bag has color, impurity, mildew, stain, crystallization or the bag that rises, that very possible appearance Bacterium, contaminated, product can not be sold.Meanwhile even if opaque outer packaging bag in transit by broken Damage, no added nutrient solution in transparent packaging substrate also will not ingress of air and the external world, so as to ensure that the health of facial mask and peace Entirely.
Below in conjunction with embodiment 1-16 and comparative example 1, the present invention will be further described in detail.
Embodiment 1
The present embodiment is a kind of method of quality control of no added facial treatment mask, is comprised the following steps:First by the film of facial mask Piece is placed in the transparent packing bag of PE materials, then no added nutrient solution is sealed in the transparent wrapper of PE materials under 60 DEG C of environment In bag, Bacteria Culture is then carried out at 37 DEG C, incubation time is 3 days, afterwards to the no added nutrient solution in transparent packaging substrate Color, whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in no added nutrient solution Survey.
Embodiment 2
The present embodiment is a kind of method of quality control of no added skin care hand film, is comprised the following steps:First by the film of hand film Piece is placed in the transparent packing bag of PP materials, then no added nutrient solution is sealed in the transparent wrapper of PP materials under 50 DEG C of environment In bag, Bacteria Culture is then carried out at 35 DEG C, incubation time is 28 days, afterwards to the no added nutrient solution in transparent packaging substrate Color, whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in no added nutrient solution Survey.
Embodiment 3
The present embodiment is a kind of method of quality control of no added skin care pin film, is comprised the following steps:First by the film of pin film Piece is placed in the transparent packing bag of PET materials, then no added nutrient solution is sealed in the transparent bag of PET materials under 70 DEG C of environment In pack, Bacteria Culture is then carried out at 36 DEG C, incubation time is 25 days, afterwards to the no added nutrition in transparent packaging substrate Whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in the color of liquid, no added nutrient solution Survey.
Embodiment 4
The present embodiment is a kind of method of quality control of no added skin care eye mask, is comprised the following steps:First by the film of eye mask Piece is placed in the transparent packing bag of PET materials, then no added nutrient solution is sealed in the transparent bag of PET materials under 80 DEG C of environment In pack, Bacteria Culture is then carried out at 38 DEG C, incubation time is 20 days, afterwards to the no added nutrition in transparent packaging substrate Whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in the color of liquid, no added nutrient solution Survey.
Embodiment 5
The present embodiment is a kind of method of quality control of no added facial treatment mask, is comprised the following steps:First by the film of facial mask Piece is placed in the transparent packing bag of PE materials, then no added nutrient solution is sealed in the transparent wrapper of PE materials under 90 DEG C of environment In bag, Bacteria Culture is then carried out at 40 DEG C, incubation time is 5 days, afterwards to the no added nutrient solution in transparent packaging substrate Color, whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in no added nutrient solution Survey.
Embodiment 6
The present embodiment is a kind of method of quality control of no added facial treatment mask, is comprised the following steps:First by the film of facial mask Piece is placed in the transparent packing bag of PET materials, then no added nutrient solution is sealed in the transparent bag of PET materials under 45 DEG C of environment In pack, Bacteria Culture is then carried out at 39 DEG C, incubation time is 12 days, afterwards to the no added nutrition in transparent packaging substrate Whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in the color of liquid, no added nutrient solution Survey.
Embodiment 7
The present embodiment is a kind of method of quality control of no added facial treatment mask, is comprised the following steps:First by the film of facial mask Piece is placed in the transparent packing bag of PE materials, then no added nutrient solution is sealed in the transparent wrapper of PE materials under 75 DEG C of environment In bag, Bacteria Culture is then carried out at 37 DEG C, incubation time is 10 days, afterwards to the no added nutrient solution in transparent packaging substrate Color, whether have impurity, stain, mildew or crystallization and transparent packing bag whether there is the bag that rises and examined in no added nutrient solution Survey.
With the method for quality control of the no added facial mask provided in embodiment 1-7, respectively sealing 10000 is no added respectively Facial mask, then outward appearance detection is carried out respectively, and testing result is listed in table 1.
The embodiment 1-7 of table 1 testing result
Inspection project Color Impurity Stain Mildew Crystallization Rise bag
Embodiment 1 1 1 1 0 0 0
Embodiment 2 1 1 1 1 0 0
Embodiment 3 0 1 2 0 0 1
Embodiment 4 2 1 0 2 0 1
Embodiment 5 1 0 1 0 1 1
Embodiment 6 2 0 1 0 0 2
Embodiment 7 0 1 1 2 0 0
Embodiment 8-15 provides a kind of method of quality control of no added facial treatment mask respectively, and use is same as Example 1 The step of carry out and with being with the face pack prescription in embodiment 1, preparation technology, method for packing all same, difference, implement Incubation time is different during Bacteria Culture in example 8-15, and the incubation time in embodiment 8-15 is respectively:6 days, 9 days, 12 My god, 15 days, 18 days, 21 days, 24 days and 27 days.Respectively with the no added facial mask provided in embodiment 1 and embodiment 8-15 Method of quality control respectively 10000 no added facial masks of sealing, then carry out outward appearance detection respectively, what is be detected does not conform to product Quantity is listed in table 2.
The testing result of the embodiment 1 of table 2 and embodiment 8-15
As shown in Table 2, when using different incubation times, the quantity of the defective work detected is different, works as culture After number of days reaches 12 days, with the increase of cultivated days, the quantity for the defective work being capable of detecting when is basically unchanged, and therefore, is Balanced production efficiency simultaneously reaches the standard of quality inspection, and cultivated days are preferably selected 12-20 days.
Embodiment 16
The present embodiment is a kind of packing method of no added facial treatment mask, the method for quality control provided using embodiment 1 Carry out quality screening after, by detect it is qualified after product carry out outer packing.
Comparative example 1
This comparative example is a kind of packing method of no added facial treatment mask, is comprised the following steps:No added nutrient solution is existed It is sealed under 60 DEG C of environment in traditional opaque outer packaging bag.
Storage preserves experiment:Each 10000 of the facial treatment mask product obtained in embodiment 16 and comparative example 1 is placed in identical In the environment of, room temperature storage 12 months, open packaging and carry out the quantity that outward appearance detection records problematic facial treatment mask product, inspection Survey result and be listed in table 3.
The storage experimental result of the embodiment 16 of table 3 and comparative example 1
As shown in Table 3, selected using method of quality control provided by the invention, it is qualified after product can for a long time Original quality is kept, for the product sold after traditional directly packaging, improves the quality for the product that dispatches from the factory.
Although illustrate and describing the present invention with specific embodiment, but will be appreciated that without departing substantially from the present invention's Many other change and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims Including belonging to all such changes and modifications in the scope of the invention.

Claims (10)

1. a kind of method of quality control of no added facial mask, it is characterised in that comprise the following steps:No added nutrition is liquid-tight It is encapsulated in transparent packaging substrate, then carries out Bacteria Culture, outward appearance inspection is carried out to the no added nutrient solution in transparent packaging substrate afterwards Survey.
2. the method for quality control of no added facial mask according to claim 1, it is characterised in that the temperature of Bacteria Culture For 35-40 DEG C, incubation time is 3-30 days.
3. the method for quality control of no added facial mask according to claim 1, it is characterised in that the temperature of Bacteria Culture For 35-39 DEG C, incubation time is 5-25 days.
4. the method for quality control of no added facial mask according to claim 1, it is characterised in that the temperature of Bacteria Culture For 36-38 DEG C, incubation time is 12-20 days.
5. the method for quality control of the no added facial mask according to claim any one of 1-4, it is characterised in that sterile Under the conditions of no added nutrient solution is sealed in transparent packaging substrate.
6. the method for quality control of no added facial mask according to claim 5, it is characterised in that in 40-95 DEG C of environment It is lower that no added nutrient solution is sealed in transparent packaging substrate.
7. the method for quality control of the no added facial mask according to claim any one of 1-4, it is characterised in that described Bright packing material is transparent packing bag.
8. the method for quality control of no added facial mask according to claim 7, it is characterised in that the transparent packing bag For the transparent packing bag of the transparent packing bag of PE materials, the transparent packing bag of PP materials or PET materials.
9. a kind of method of quality control of the no added facial mask described in any one of claim 1-8 is preparing no added facial mask In purposes.
10. a kind of packing method of no added facial mask, it is characterised in that added using the nothing described in claim any one of 1-8 Add the method for quality control of facial mask to detect the no added nutrient solution being sealed in transparent packaging substrate, certified products will be detected Progress outer packing, which operates, produces the no added facial mask.
CN201710844561.3A 2017-09-15 2017-09-15 The method of quality control of no added facial mask and its application and the packing method of no added facial mask Pending CN107488701A (en)

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CN201710844561.3A CN107488701A (en) 2017-09-15 2017-09-15 The method of quality control of no added facial mask and its application and the packing method of no added facial mask
PCT/CN2017/109787 WO2019051965A1 (en) 2017-09-15 2017-11-07 Quality control method for additive-free skin-care mask and application thereof, and method for packaging additive-free skin-care mask

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Application publication date: 20171219