CN107474570A - A kind of degradable disponsable tableware and preparation method thereof - Google Patents
A kind of degradable disponsable tableware and preparation method thereof Download PDFInfo
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- CN107474570A CN107474570A CN201710751760.XA CN201710751760A CN107474570A CN 107474570 A CN107474570 A CN 107474570A CN 201710751760 A CN201710751760 A CN 201710751760A CN 107474570 A CN107474570 A CN 107474570A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L97/00—Compositions of lignin-containing materials
- C08L97/02—Lignocellulosic material, e.g. wood, straw or bagasse
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2397/00—Characterised by the use of lignin-containing materials
- C08J2397/02—Lignocellulosic material, e.g. wood, straw or bagasse
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2403/00—Characterised by the use of starch, amylose or amylopectin or of their derivatives or degradation products
- C08J2403/02—Starch; Degradation products thereof, e.g. dextrin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/06—Biodegradable
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Abstract
The invention belongs to disposable tableware field, more particularly to a kind of degradable disponsable tableware and preparation method thereof.The present invention uses the fully natural green raw materials such as composite stalk powder, oyster shell whiting, composite starch, composite fibre slurry, using peach gum as binder, bamboo green grass or young crops is added to lift the tough and tensile degree of tableware, Thallus Laminariae (Thallus Eckloniae) extract is sprayed in tableware surface, with isolation oil, water, make tableware more robust, finally give a kind of pure natural raw material of use, without chemical composition, tough and tensile durable degradable disponsable tableware.
Description
Technical field
The invention belongs to disposable tableware field, more particularly to a kind of degradable disponsable tableware and preparation method thereof.
Background technology
The disposable tableware demand in China is huge, is mostly plastic products or paper products.The plastics system of industrialized production
Product are largely difficult to degrade, and Heavy environmental pollution is also resulted in while fossil energy is consumed;Paper products can bring forest again
The problems such as felling, film difficult degradation, water resource waste, and cost is higher.
At present, the degradable dinner set in China is mainly prepared by raw material of starch, and environment protecting tableware is prepared using stalk
Have the advantages that utilization ratio is high, easily reclaim.A kind of table ware made of stalk disclosed in Chinese Patent Application No. 98124818.7, by straw
Stalk, urea-formaldehyde moulding powder, filler or calcium stearate (or flour) are prepared by stirring, mixing, extrusion forming, and the tableware is in light weight, anti-
Pressure, processing technology is simple, but causes toughness insufficient because lacking adhesive, frangible;Chinese Patent Application No. 99115359.6 is public
Opened a kind of method that degradable dinner set is produced using plant haulm and fruit shell as raw material, the tableware be first by plant haulm and
Adhesive is added after the processing of fruit shell and is mixed, adds plaster mold drying after forming, then be made through surface coating drying, finished product
Degradation property it is good, it is nontoxic, but the forming method of raw material determines that product strength is bad, and processing technology is complicated;In
State's number of patent application 01127386.0 discloses a kind of once-used degradeable tableware and its manufacture method, tableware by degradable major ingredient,
Refined after adhesive, filler mashing mixing through vacuum pugmill, normal temperature shaped by fluid pressure, drying and processing, surface spraying interleaving agent
Be made, tableware rigidity is high and can be adjusted by matching adjustment, and degradation property and toughness are preferable, but its using corn flour and
Bletilla striata powder makees adhesive, and toughness of products is bad after drying, and the interleaving agent such as water-based polyurethane used in product has poison gas before curing
Body discharges;Chinese Patent Application No. 01108832.X discloses one kind and eaten by easily degradable disposable made of primary raw material of starch
Tool, the 70%-90% of tableware is starch, then is aided with a small amount of stalk fibre, vegetable oil and additive, through once hot-forming, into
The coating of surface waterproofing glue is carried out after type, the tableware mainly turns into starch, and therefore degradation property is good, and cost is low, nontoxic, tasteless, but
Itself primary disadvantage is that solidification after starch present fragility cause product tensile strength poor, it is broken.
The content of the invention
In order to solve above-mentioned technical problem present in prior art, the present invention provide a kind of degradable disponsable tableware and
Its preparation method, it is achieved particular by following art scheme:
A kind of degradable disponsable tableware, it is prepared by the raw material of following parts by weight:Composite stalk powder 35-45 parts, shellfish
Shell powder 10-15 parts, composite starch 25-30 parts, composite fibre slurry 20-25, Thallus Laminariae (Thallus Eckloniae) extract 8-10 parts, peach gum 20-25 parts, bamboo are blue or green
2-3 parts.
It is preferred that it is prepared by the raw material of following parts by weight:40 parts of composite stalk powder, 12.5 parts of oyster shell whiting, composite starch
27.5 parts, composite fibre slurry 22.5,9 parts of Thallus Laminariae (Thallus Eckloniae) extract, 22.5 parts of peach gum, blue or green 2.5 parts of bamboo.
The composite stalk powder, be by powdered rice hulls, bagasse powder, milled powders of cornstalk, maize cob meal, Honeysuckle bine powder, according to
8:6:4:3:1 weight ratio mixes.
The composite starch, it is by tapioca, cornstarch, farina, according to 2:3:2 weight than mixing and
Into.
Composite fibre slurry, be reed fiber is starched, flax fiber slurry, wood fibre slurry, according to 2:3:5 weight ratio
Mix.
The preparation method of the degradable disponsable tableware, comprises the following steps:
(1) it is composite stalk powder, oyster shell whiting, composite starch difference is finely ground, cross 80 mesh sieves;
(2) composite stalk powder is put into high temperature and high speed mixer, adds oyster shell whiting, after being well mixed, by composite starch
Three parts each are equally divided into composite fibre slurry, adds portion every time, the two is alternately added, until adding, is mixed after cooling
Condensating fiber powder;
(3) by the blue or green hammer pine of bamboo, it is shredded into thread, is dried after being rinsed repeatedly with 0.1mol/L NaOH solution;
(4) peach gum is fully soaked with the 4-6 times of water measured, is heated to 90 DEG C -100 DEG C, is stirred well to form glue;
(5) the bamboo green grass or young crops after composite fibre powder, rinsing is added in peach gum, fills into composite fibre powder 10%-35% water,
Obtain mixture of raw material;
(6) mixture of raw material is molded with moulding press, taken out after shaping;
(7) Thallus Laminariae (Thallus Eckloniae) extract is fully dissolved in strong alkali solution, solution ph to 7.2-8.0 is adjusted with acid, to shaping
Degradable disponsable tableware surface afterwards is uniformly sprayed, and is produced.
The molding, its molding temperature are 80-120 DEG C, molding pressure 180-200MPa.
The step (7), strong alkali solution are ph=13 NaOH solutions, and acid is 0.1mol/L HCl solution.
Compared with prior art, the technique effect of the invention is embodied in:
The present invention is using fully natural green raw materials such as composite stalk powder, oyster shell whiting, composite starch, composite fibre slurries, with peach
Glue is binder, adds bamboo green grass or young crops to lift the tough and tensile degree of tableware, and Thallus Laminariae (Thallus Eckloniae) extract is sprayed in tableware surface, to completely cut off oil, water,
Make tableware more robust, finally given a kind of using pure natural raw material, without chemical composition, tough and tensile durable degradable disponsable
Tableware.
Embodiment
Limited with reference to specific embodiment technical scheme is further, but claimed
Scope is not only limited to made description.
Embodiment 1
(1) composite stalk powder 40kg, oyster shell whiting 12.5kg, composite starch 27.5kg, composite fibre slurry 22.5kg, sea are weighed
Band extract 9kg, peach gum 22.5kg, bamboo green grass or young crops 2.5kg
(2) it is composite stalk powder, oyster shell whiting, composite starch difference is finely ground, cross 80 mesh sieves;
(3) composite stalk powder is put into high temperature and high speed mixer, adds oyster shell whiting, after being well mixed, by composite starch
Three parts each are equally divided into composite fibre slurry, adds portion every time, the two is alternately added, until adding, is mixed after cooling
Condensating fiber powder;
(4) by the blue or green hammer pine of bamboo, it is shredded into thread, is dried after being rinsed repeatedly with 0.1mol/L NaOH solution;
(5) peach gum is fully soaked with the water of 5 times of amounts, is heated to 95 DEG C, is stirred well to form glue;
(6) the bamboo green grass or young crops after composite fibre powder, rinsing is added in peach gum, fills into the water of composite fibre powder 22.5%, obtain
To mixture of raw material;
(7) mixture of raw material is molded with moulding press, taken out after shaping, its molding temperature is 100 DEG C, molding pressure
Power is 190MPa;
(8) Thallus Laminariae (Thallus Eckloniae) extract is fully dissolved in ph=13 NaOH solution, it is molten with 0.1mol/L HCl solution adjustment
Liquid ph to 7.6, the degradable disponsable tableware surface after shaping is uniformly sprayed, produced.
The composite stalk powder, be by powdered rice hulls, bagasse powder, milled powders of cornstalk, maize cob meal, Honeysuckle bine powder, according to
8:6:4:3:1 weight ratio mixes.
The composite starch, it is by tapioca, cornstarch, farina, according to 2:3:2 weight than mixing and
Into.
Composite fibre slurry, be reed fiber is starched, flax fiber slurry, wood fibre slurry, according to 2:3:5 weight ratio
Mix.
Embodiment 2
(1) composite stalk powder 35kg, oyster shell whiting 10kg, composite starch 25kg, composite fibre slurry 20kg, sea-tangle extraction are weighed
Thing 8kg, peach gum 20kg, bamboo green grass or young crops 2kg
(2) it is composite stalk powder, oyster shell whiting, composite starch difference is finely ground, cross 80 mesh sieves;
(3) composite stalk powder is put into high temperature and high speed mixer, adds oyster shell whiting, after being well mixed, by composite starch
Three parts each are equally divided into composite fibre slurry, adds portion every time, the two is alternately added, until adding, is mixed after cooling
Condensating fiber powder;
(4) by the blue or green hammer pine of bamboo, it is shredded into thread, is dried after being rinsed repeatedly with 0.1mol/L NaOH solution;
(5) peach gum is fully soaked with the water of 5 times of amounts, is heated to 90 DEG C, is stirred well to form glue;
(6) the bamboo green grass or young crops after composite fibre powder, rinsing is added in peach gum, fills into the water of composite fibre powder 10%, obtain
Mixture of raw material;
(7) mixture of raw material is molded with moulding press, taken out after shaping, its molding temperature is 80 DEG C, molding pressure
Power is 180MPa;
(8) Thallus Laminariae (Thallus Eckloniae) extract is fully dissolved in ph=13 NaOH solution, it is molten with 0.1mol/L HCl solution adjustment
Liquid ph to 7.6, the degradable disponsable tableware surface after shaping is uniformly sprayed, produced.
The composite stalk powder, be by powdered rice hulls, bagasse powder, milled powders of cornstalk, maize cob meal, Honeysuckle bine powder, according to
8:6:4:3:1 weight ratio mixes.
The composite starch, it is by tapioca, cornstarch, farina, according to 2:3:2 weight than mixing and
Into.
Composite fibre slurry, be reed fiber is starched, flax fiber slurry, wood fibre slurry, according to 2:3:5 weight ratio
Mix.
Embodiment 3
(1) composite stalk powder 45kg, oyster shell whiting 15kg, composite starch 30kg, composite fibre slurry 25kg, sea-tangle extraction are weighed
Thing 10kg, peach gum 25kg, bamboo green grass or young crops 3kg
(2) it is composite stalk powder, oyster shell whiting, composite starch difference is finely ground, cross 80 mesh sieves;
(3) composite stalk powder is put into high temperature and high speed mixer, adds oyster shell whiting, after being well mixed, by composite starch
Three parts each are equally divided into composite fibre slurry, adds portion every time, the two is alternately added, until adding, is mixed after cooling
Condensating fiber powder;
(4) by the blue or green hammer pine of bamboo, it is shredded into thread, is dried after being rinsed repeatedly with 0.1mol/L NaOH solution;
(5) peach gum is fully soaked with the water of 5 times of amounts, is heated to 95 DEG C, is stirred well to form glue;
(6) the bamboo green grass or young crops after composite fibre powder, rinsing is added in peach gum, fills into the water of composite fibre powder 35%, obtain
Mixture of raw material;
(7) mixture of raw material is molded with moulding press, taken out after shaping, its molding temperature is 120 DEG C, molding pressure
Power is 200MPa;
(8) Thallus Laminariae (Thallus Eckloniae) extract is fully dissolved in ph=13 NaOH solution, it is molten with 0.1mol/L HCl solution adjustment
Liquid ph to 7.6, the degradable disponsable tableware surface after shaping is uniformly sprayed, produced.
The composite stalk powder, be by powdered rice hulls, bagasse powder, milled powders of cornstalk, maize cob meal, Honeysuckle bine powder, according to
8:6:4:3:1 weight ratio mixes.
The composite starch, it is by tapioca, cornstarch, farina, according to 2:3:2 weight than mixing and
Into.
Composite fibre slurry, be reed fiber is starched, flax fiber slurry, wood fibre slurry, according to 2:3:5 weight ratio
Mix.
Comparative example 1
(1) by the wheat stalk powder 400g of 60 mesh, PLA (PLA) 150g of 100 mesh, cornstarch 250g, 300 purposes
Talcum powder 80g, KH-550w1mL and water 119mL stir and evenly mix standby;
(2) by mould be warming up to 180 DEG C it is constant, adjust upper and lower mould hot pressing when stable headway be 1mm, 20g compounds are put
Enter in the mould of constant temperature, pressurize 30s, goes out mold forming under 30 tons of pressure;
(3) it is molded tableware inner surface after trimming and carries out ethyl cellulose waterproof coating processing, drying, sterilization, obtains
Table ware made of stalk finished product.
Embodiment 1-3, comparative example 1, the durability of commercially available papery disposable tableware and degradation time are contrasted:
The degraded, it is during degradable disponsable tableware is placed into the soil, treats that its is degradable, records the time.
Contrast understands that the degradable disponsable tableware that the present invention obtains is more tough and tensile more durable than papery disposable tableware, but its
Time required for natural degradation increased;The degradable disponsable tableware that the present invention obtains, rigidity is with breakdown strength with adding
The degradable disponsable tableware for having entered biological plastics PLA is more or less the same, but degradation time has great lifting.
Finally it is pointed out that above example is only the more representational example of the present invention.Obviously, technology of the invention
Scheme is not limited to above-described embodiment, can also there is many deformations.One of ordinary skill in the art can be from disclosed by the invention
All deformations that content is directly exported or associated, are considered as protection scope of the present invention.
Claims (8)
1. a kind of degradable disponsable tableware, it is characterised in that be prepared by the raw material of following parts by weight:Composite stalk powder
35-45 parts, oyster shell whiting 10-15 parts, composite starch 25-30 parts, composite fibre slurry 20-25 parts, Thallus Laminariae (Thallus Eckloniae) extract 8-10 parts, peach gum
20-25 parts, bamboo green grass or young crops 2-3 parts.
2. degradable disponsable tableware according to claim 1, it is characterised in that by the raw material preparation of following parts by weight
Into:40 parts of composite stalk powder, 12.5 parts of oyster shell whiting, 27.5 parts of composite starch, composite fibre slurry 22.5,9 parts of Thallus Laminariae (Thallus Eckloniae) extract, peach
22.5 parts of glue, bamboo are blue or green 2.5 parts.
3. degradable disponsable tableware according to claim 1 or 2, it is characterised in that the composite stalk powder, be by rice
Shell powder, bagasse powder, milled powders of cornstalk, maize cob meal, Honeysuckle bine powder, according to 8:6:4:3:1 weight ratio mixes.
4. degradable disponsable tableware according to claim 1 or 2, it is characterised in that the composite starch, be by cassava
Starch, cornstarch, farina, according to 2:3:2 weight ratio mixes.
5. degradable disponsable tableware according to claim 1 or 2, it is characterised in that the composite fibre slurry, is by reed
Reed fiber pulp, flax fiber slurry, wood fibre slurry, according to 2:3:5 weight ratio mixes.
6. a kind of preparation method for preparing the degradable disponsable tableware described in claim 1 or 2, it is characterised in that including such as
Lower step:
(1) it is composite stalk powder, oyster shell whiting, composite starch difference is finely ground, cross 80 mesh sieves;
(2) composite stalk powder is put into high temperature and high speed mixer, adds oyster shell whiting, after being well mixed, by composite starch and again
Condensating fiber slurry is each equally divided into three parts, adds portion every time, and the two is alternately added, until adding, it is fine that mixing is obtained after cooling
Tie up powder;
(3) by the blue or green hammer pine of bamboo, it is shredded into thread, is dried after being rinsed repeatedly with 0.1mol/L NaOH solution;
(4) peach gum is fully soaked with the 4-6 times of water measured, is heated to 90 DEG C -100 DEG C, is stirred well to form glue;
(5) the bamboo green grass or young crops after composite fibre powder, rinsing is added in peach gum, fills into composite fibre powder 10%-35% water, obtain
Mixture of raw material;
(6) mixture of raw material is molded with moulding press, taken out after shaping;
(7) Thallus Laminariae (Thallus Eckloniae) extract is fully dissolved in strong alkali solution, solution ph to 7.2-8.0 is adjusted with acid, after shaping
Degradable disponsable tableware surface is uniformly sprayed, and is produced.
7. the preparation method of degradable disponsable tableware according to claim 6, it is characterised in that the molding, its mould
It is 80-120 DEG C to press temperature, molding pressure 180-200MPa.
8. the preparation method of degradable disponsable tableware according to claim 6, it is characterised in that the step (7), by force
Alkaline solution is ph=13 NaOH solution, and acid is 0.1mol/L HCl solution.
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Cited By (5)
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---|---|---|---|---|
CN109747017A (en) * | 2019-01-17 | 2019-05-14 | 吕旭光 | A kind of disposable tableware and manufacture craft with maize leaves production |
CN110577753A (en) * | 2019-10-18 | 2019-12-17 | 廖思凤 | Method for manufacturing degradable disposable tableware by using jasmine |
CN113201227A (en) * | 2021-04-20 | 2021-08-03 | 广州市鹏铖纸业有限公司 | Preparation method and application of environment-friendly material taking bagasse as base material |
CN115304825A (en) * | 2022-06-20 | 2022-11-08 | 贵州省玉态康环保餐具有限公司 | Raw material formula for producing disposable tableware by recycling straw and production method thereof |
CN116082714A (en) * | 2023-02-27 | 2023-05-09 | 浙江喜恒科技新材料有限公司 | Degradable tableware and preparation method |
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CN105920050A (en) * | 2016-06-16 | 2016-09-07 | 广东海洋大学 | Preparation method and application of kelp extract for effectively reducing uric acid |
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CN1380361A (en) * | 2001-04-12 | 2002-11-20 | 上海长洁卫生保健制品有限公司 | Degradable disposable tableware |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109747017A (en) * | 2019-01-17 | 2019-05-14 | 吕旭光 | A kind of disposable tableware and manufacture craft with maize leaves production |
CN110577753A (en) * | 2019-10-18 | 2019-12-17 | 廖思凤 | Method for manufacturing degradable disposable tableware by using jasmine |
CN113201227A (en) * | 2021-04-20 | 2021-08-03 | 广州市鹏铖纸业有限公司 | Preparation method and application of environment-friendly material taking bagasse as base material |
CN113201227B (en) * | 2021-04-20 | 2022-08-05 | 广州市鹏铖纸业有限公司 | Preparation method and application of environment-friendly material taking bagasse as base material |
CN115304825A (en) * | 2022-06-20 | 2022-11-08 | 贵州省玉态康环保餐具有限公司 | Raw material formula for producing disposable tableware by recycling straw and production method thereof |
CN116082714A (en) * | 2023-02-27 | 2023-05-09 | 浙江喜恒科技新材料有限公司 | Degradable tableware and preparation method |
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Application publication date: 20171215 |