CN107473718A - 一种耐久香味陶瓷制品及其制备方法 - Google Patents

一种耐久香味陶瓷制品及其制备方法 Download PDF

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CN107473718A
CN107473718A CN201710867302.2A CN201710867302A CN107473718A CN 107473718 A CN107473718 A CN 107473718A CN 201710867302 A CN201710867302 A CN 201710867302A CN 107473718 A CN107473718 A CN 107473718A
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闵海龙
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Suzhou Porcelain Gas Epoch Cleaning Equipment Co Ltd
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Abstract

本发明公开了一种耐久香味陶瓷制品，以高铝细粉作为主原料，添加了粉煤灰、贝壳粉等廉价易得原料，不仅降低了对环境的污染，还大大降低了成本，废玻璃的加入，在烧结过程中形成玻璃心，起到粘合剂的作用，提高陶瓷表面的光滑性能、抗裂、抗冲击性能，熏香、麦饭石粉、白釉球等通过施釉在陶瓷表面，提高了陶瓷的香味及香味的耐久性，熏香具有助眠和驱蚊效果，促进人体睡眠；制备方法简单，成本低，环保无毒，不会产生污染环境的有害物质。

Description

一种耐久香味陶瓷制品及其制备方法
技术领域
本发明涉及陶瓷制品技术领域，特别是一种耐久香味陶瓷制品及其制备方法。
背景技术
陶瓷在我国具有悠久的使用历史，如今在全时间范围内广泛使用，日用陶瓷制品已成为人们日常生活不可或缺的一部分，形形色色的餐具、茶具、各类洁具等随处可见，这些陶瓷不仅美观大方、造型多样，而且还具有易清洗、耐温、耐磨耐腐蚀等优点，深受消费者喜欢，然而陶瓷制品普遍存在性脆、不耐冲击、韧性差、生产能耗大、成本高等缺点，在运输过程中容易破损；现有的陶瓷制品大都是具备摆放艺术观赏性和盛放物品功能性，现有的陶瓷制品大都不具有熏香功能或者熏香不持久等问题。
发明内容
发明目的：为了解决上述问题，本发明的目的在于提供一种耐久香味陶瓷制品及其制备方法。
发明内容：一种耐久香味陶瓷制品，包括以下重量份的组分：高铝细粉30-50份、长石粉20-30份、粉煤灰40-50份、石英粉20-30份、废玻璃8-12份、麦饭石粉10-20份、贝壳粉8-12份、白釉球30-40份、熏香料5-10份。
优选地，所述的高铝细粉为铝矿石经高温煅烧后所得，其中氧化铝含量大于80％，100-200目。
优选地，所述的熏香料包括以下重量份的组分：薰衣草30-50份、艾草35-55份、橙皮20-30份、冰片30-40份、茶叶渣10-20份、石菖蒲20-30份、高锰酸钾5-10份、迷迭香精油20-30份。
优选地，所述的熏香料制备方法为将薰衣草、艾草、橙皮、冰片、石菖蒲、高锰酸钾、茶叶渣混合研磨成300-400目细粉后加入迷迭香精油混合均匀即得。
优选地，所述的耐久香味陶瓷制品制备方法，包括以下方法步骤：
(1)制备贝壳粉，将贝壳于400-600℃条件下进行一次煅烧1-3h，冷却至室温后进行一次研磨分散均匀后再于600-800℃进行二次煅烧1-3h，冷却至室温进行二次研磨分散，直至贝壳粉粒径为300-400目；
(2)称取配方量的高铝细粉、长石粉、粉煤灰、石英粉、贝壳粉、废玻璃，放入球磨罐中，并加入物料总重量40-50％的去离子水和占总重量1.5-2.5％的水玻璃后密封，启动球磨机，球磨8-12h；
(3)将步骤(2)球磨后的浆料过300-400目过滤网，得浆料备用；
(4)将步骤(3)制备的浆料用磁选机进行磁选除铁，使浆料中铁的含量≤0.2％，将浆料加到成型机中干燥成型得到坯体，将坯体放入烧结炉内烧结成型，炉内温度为800-1000℃，烧结时间为4-6h，冷却至常温后打磨刨光备用；
(5)将配方量的白釉球、麦饭石粉和熏香混合加到球磨机中湿法球磨，加入物料总量30-40％的去离子水，球磨后浆料过300目筛，去除杂质和粗颗粒，得到细浆料，再施釉于步骤(4)打磨刨光的陶瓷表面，在700-800℃烧结3-4h即得。
优选地，所述的步骤(1)中贝壳粉制备方法中一次煅烧气氛为氩气，二次煅烧气氛为氧气。
优选地，所述的步骤(1)中贝壳粉制备方法中一次研磨分散时搅拌速度为400-600r/min，二次研磨分散时搅拌速度为600-800r/min。
本发明的有益效果在于：本发明的一种耐久香味陶瓷制品，以高铝细粉作为主原料，添加了粉煤灰、贝壳粉等廉价易得原料，不仅降低了对环境的污染，还大大降低了成本，废玻璃的加入，在烧结过程中形成玻璃心，起到粘合剂的作用，提高陶瓷表面的光滑性能、抗裂、抗冲击性能，熏香、麦饭石粉、白釉球等通过施釉在陶瓷表面，提高了陶瓷的香味及香味的耐久性，熏香具有助眠和驱蚊效果，促进人体睡眠；制备方法简单，成本低，环保无毒，不会产生污染环境的有害物质。
具体实施方式
为了更清楚地说明本申请实施例或现有技术中的技术方案，下面将对实施例作简单地介绍，对于本领域普通技术人员来讲，在不付出创造性劳动的前提下，还可以根据这些实施例获得其他的实施例。
表1为本发明实施例所述的耐久香味陶瓷制品组成成分表；表2为本发明实施例所述的熏香成本表。
表1.实施例所述的耐久香味陶瓷制品成分(单位：份)
实施例1 实施例2 实施例3
高铝细粉 30 50 40
长石粉 20 30 25
粉煤灰 40 50 45
石英粉 20 30 25
废玻璃 8 12 10
麦饭石粉 10 20 15
贝壳粉 8 12 10
白釉球 30 40 35
熏香料 5 10 8
表2.实施例所述的熏香成分(单位：份)
实施例1 实施例2 实施例3
薰衣草 30 50 40
艾草 35 55 45
橙皮 20 30 25
冰片 30 40 35
茶叶渣 10 20 15
石菖蒲 20 30 25
高锰酸钾 5 10 8
迷迭香精油 20 30 25
实施例1
一种耐久香味陶瓷制品，所述的高铝细粉为铝矿石经高温煅烧后所得，其中氧化铝含量大于80％，100目。
所述的熏香料制备方法为将薰衣草、艾草、橙皮、冰片、石菖蒲、高锰酸钾、茶叶渣混合研磨成300目细粉后加入迷迭香精油混合均匀即得。
所述的耐久香味陶瓷制品制备方法，包括以下方法步骤：
(1)制备贝壳粉，将贝壳于400℃条件下进行一次煅烧1h，冷却至室温后进行一次研磨分散均匀后再于600℃进行二次煅烧1h，冷却至室温进行二次研磨分散，直至贝壳粉粒径为300目；
(2)称取配方量的高铝细粉、长石粉、粉煤灰、石英粉、贝壳粉、废玻璃，放入球磨罐中，并加入物料总重量40％的去离子水和占总重量1.5％的水玻璃后密封，启动球磨机，球磨8h；
(3)将步骤(2)球磨后的浆料过300目过滤网，得浆料备用；
(4)将步骤(3)制备的浆料用磁选机进行磁选除铁，使浆料中铁的含量≤0.2％，将浆料加到成型机中干燥成型得到坯体，将坯体放入烧结炉内烧结成型，炉内温度为800℃，烧结时间为4h，冷却至常温后打磨刨光备用；
(5)将配方量的白釉球、麦饭石粉和熏香混合加到球磨机中湿法球磨，加入物料总量30％的去离子水，球磨后浆料过300目筛，去除杂质和粗颗粒，得到细浆料，再施釉于步骤(4)打磨刨光的陶瓷表面，在700℃烧结3h即得。
所述的步骤(1)中贝壳粉制备方法中一次煅烧气氛为氩气，二次煅烧气氛为氧气。
所述的步骤(1)中贝壳粉制备方法中一次研磨分散时搅拌速度为400r/min，二次研磨分散时搅拌速度为600r/min。
实施例2
一种耐久香味陶瓷制品，所述的高铝细粉为铝矿石经高温煅烧后所得，其中氧化铝含量大于80％，200目。
所述的熏香料制备方法为将薰衣草、艾草、橙皮、冰片、石菖蒲、高锰酸钾、茶叶渣混合研磨成400目细粉后加入迷迭香精油混合均匀即得。
所述的耐久香味陶瓷制品制备方法，包括以下方法步骤：
(1)制备贝壳粉，将贝壳于600℃条件下进行一次煅烧3h，冷却至室温后进行一次研磨分散均匀后再于800℃进行二次煅烧3h，冷却至室温进行二次研磨分散，直至贝壳粉粒径为400目；
(2)称取配方量的高铝细粉、长石粉、粉煤灰、石英粉、贝壳粉、废玻璃，放入球磨罐中，并加入物料总重量50％的去离子水和占总重量2.5％的水玻璃后密封，启动球磨机，球磨12h；
(3)将步骤(2)球磨后的浆料过400目过滤网，得浆料备用；
(4)将步骤(3)制备的浆料用磁选机进行磁选除铁，使浆料中铁的含量≤0.2％，将浆料加到成型机中干燥成型得到坯体，将坯体放入烧结炉内烧结成型，炉内温度为1000℃，烧结时间为6h，冷却至常温后打磨刨光备用；
(5)将配方量的白釉球、麦饭石粉和熏香混合加到球磨机中湿法球磨，加入物料总量40％的去离子水，球磨后浆料过300目筛，去除杂质和粗颗粒，得到细浆料，再施釉于步骤(4)打磨刨光的陶瓷表面，在800℃烧结4h即得。
所述的步骤(1)中贝壳粉制备方法中一次煅烧气氛为氩气，二次煅烧气氛为氧气。
所述的步骤(1)中贝壳粉制备方法中一次研磨分散时搅拌速度为600r/min，二次研磨分散时搅拌速度为800r/min。
实施例3
一种耐久香味陶瓷制品，所述的高铝细粉为铝矿石经高温煅烧后所得，其中氧化铝含量大于80％，150目。
所述的熏香料制备方法为将薰衣草、艾草、橙皮、冰片、石菖蒲、高锰酸钾、茶叶渣混合研磨成350目细粉后加入迷迭香精油混合均匀即得。
所述的耐久香味陶瓷制品制备方法，包括以下方法步骤：
(1)制备贝壳粉，将贝壳于500℃条件下进行一次煅烧2h，冷却至室温后进行一次研磨分散均匀后再于700℃进行二次煅烧2h，冷却至室温进行二次研磨分散，直至贝壳粉粒径为350目；
(2)称取配方量的高铝细粉、长石粉、粉煤灰、石英粉、贝壳粉、废玻璃，放入球磨罐中，并加入物料总重量45％的去离子水和占总重量2％的水玻璃后密封，启动球磨机，球磨10h；
(3)将步骤(2)球磨后的浆料过350目过滤网，得浆料备用；
(4)将步骤(3)制备的浆料用磁选机进行磁选除铁，使浆料中铁的含量≤0.2％，将浆料加到成型机中干燥成型得到坯体，将坯体放入烧结炉内烧结成型，炉内温度为900℃，烧结时间为5h，冷却至常温后打磨刨光备用；
(5)将配方量的白釉球、麦饭石粉和熏香混合加到球磨机中湿法球磨，加入物料总量35％的去离子水，球磨后浆料过300目筛，去除杂质和粗颗粒，得到细浆料，再施釉于步骤(4)打磨刨光的陶瓷表面，在750℃烧结3.5h即得。
所述的步骤(1)中贝壳粉制备方法中一次煅烧气氛为氩气，二次煅烧气氛为氧气。
所述的步骤(1)中贝壳粉制备方法中一次研磨分散时搅拌速度为500r/min，二次研磨分散时搅拌速度为700r/min。
以上实施例仅用以说明本发明的优选技术方案，应当指出，对于本技术领域的普通技术人员而言，在不脱离本发明原理的前提下，所做出的若干改进或等同替换，均视为本发明的保护范围，仍应涵盖在本发明的权利要求范围中。

Claims (7)

1.一种耐久香味陶瓷制品，其特征在于，包括以下重量份的组分：高铝细粉30-50份、长石粉20-30份、粉煤灰40-50份、石英粉20-30份、废玻璃8-12份、麦饭石粉10-20份、贝壳粉8-12份、白釉球30-40份、熏香料5-10份。
2.根据权利要求1所述的一种耐久香味陶瓷制品，其特征在于，所述的高铝细粉为铝矿石经高温煅烧后所得，其中氧化铝含量大于80%，100-200目。
3.根据权利要求1所述的一种耐久香味陶瓷制品，其特征在于，所述的熏香料包括以下重量份的组分：薰衣草30-50份、艾草35-55份、橙皮20-30份、冰片30-40份、茶叶渣10-20份、石菖蒲20-30份、高锰酸钾5-10份、迷迭香精油20-30份。
4.根据权利要求3所述的一种耐久香味陶瓷制品，其特征在于，所述的熏香料制备方法为将薰衣草、艾草、橙皮、冰片、石菖蒲、高锰酸钾、茶叶渣混合研磨成300-400目细粉后加入迷迭香精油混合均匀即得。
5.一种根据权利要求1所述的耐久香味陶瓷制品的制备方法，其特征在于，包括以下方法步骤：
（1）制备贝壳粉，将贝壳于400-600℃条件下进行一次煅烧1-3h，冷却至室温后进行一次研磨分散均匀后再于600-800℃进行二次煅烧1-3h，冷却至室温进行二次研磨分散，直至贝壳粉粒径为300-400目；
（2）称取配方量的高铝细粉、长石粉、粉煤灰、石英粉、贝壳粉、废玻璃，放入球磨罐中，并加入物料总重量40-50%的去离子水和占总重量1.5-2.5%的水玻璃后密封，启动球磨机，球磨8-12h；
（3）将步骤（2）球磨后的浆料过300-400目过滤网，得浆料备用；
（4）将步骤（3）制备的浆料用磁选机进行磁选除铁，使浆料中铁的含量≤0.2%，将浆料加到成型机中干燥成型得到坯体，将坯体放入烧结炉内烧结成型，炉内温度为800-1000℃，烧结时间为4-6h，冷却至常温后打磨刨光备用；
（5）将配方量的白釉球、麦饭石粉和熏香混合加到球磨机中湿法球磨，加入物料总量30-40%的去离子水，球磨后浆料过300目筛，去除杂质和粗颗粒，得到细浆料，再施釉于步骤（4）打磨刨光的陶瓷表面，在700-800℃烧结3-4h即得。
6.根据权利要求5所述的一种耐久香味陶瓷制品的制备方法，其特征在于，所述的步骤（1）中贝壳粉制备方法中一次煅烧气氛为氩气，二次煅烧气氛为氧气。
7.根据权利要求5所述的一种耐久香味陶瓷制品的制备方法，其特征在于，所述的步骤（1）中贝壳粉制备方法中一次研磨分散时搅拌速度为400-600r/min，二次研磨分散时搅拌速度为600-800r/min。
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CN114213009A (zh) * 2021-12-30 2022-03-22 李晓倩 一种利用废弃贝壳制备的陶瓷釉料及其制备方法

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