CN107473344A - A kind of lobster pond is special to remove algae bactericidal purifying composite - Google Patents
A kind of lobster pond is special to remove algae bactericidal purifying composite Download PDFInfo
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- CN107473344A CN107473344A CN201710634030.1A CN201710634030A CN107473344A CN 107473344 A CN107473344 A CN 107473344A CN 201710634030 A CN201710634030 A CN 201710634030A CN 107473344 A CN107473344 A CN 107473344A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/50—Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
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- A—HUMAN NECESSITIES
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
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- A—HUMAN NECESSITIES
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- A01N59/16—Heavy metals; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- C02F1/00—Treatment of water, waste water, or sewage
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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Abstract
Algae bactericidal purifying composite is removed the invention discloses a kind of lobster pond is special, and its raw material includes sterilization filler, except algae filler, lysozyme, polymetaphosphate sodium, hexa, sulfamic acid, SODIUM PERCARBONATE, carbamide percarbonate, ZnOw, nano titanium oxide, sodium-based montmorillonite, calgon, silver nitrate, copper sulphate, zinc nitrate, graphene oxide, gelatin, PLA, dichloromethane, glycerine, methanol, butyl acetate, potassium dihydrogen phosphate, sodium tetraborate, dodecyl phenenyl sulfate and deionized water.The lobster pond composite material special of the present invention can carry out kill to the algae in pond, and have excellent bactericidal property, and the release of germ killing drugs is efficiently high-quality.
Description
Technical field
The present invention relates to the technical field of disinfection material, more particularly to a kind of lobster pond is special removes algae bactericidal purifying
Composite.
Background technology
With being continuously increased for China's pond culture area, the ecologic structure of aquaculture itself and traditional breeding way
Defect so that many outstanding problems be present in culture fishery, although lobster to the strong adaptability of environment, with its demand
Increase, the cultivation density more and more higher in single pond, also worse and worse, Water Eutrophication is increasingly severe for water quality, existing skill
The material toxicity removed algae and sterilized in art is too big, can not adapt to the demand in actual breeding process, so it is a kind of to need exploitation badly
Lobster pond is special to remove algae bactericidal purifying composite to solve the problems of the prior art.
The content of the invention
To solve technical problem present in background technology, the present invention proposes that a kind of lobster pond is special and removes algae bactericidal purifying
Composite, kill can be carried out to the algae in pond, and there is excellent bactericidal property, and the release of germ killing drugs is efficient
It is high-quality.
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize filler 20-50 parts, except algae filler 15-25 parts, lysozyme 2-5 parts, polymetaphosphate sodium 2-6 parts, hexa 3-5
Part, sulfamic acid 1-3 parts, SODIUM PERCARBONATE 2-5 parts, carbamide percarbonate 3-6 parts, ZnOw 4-8 parts, nano titanium oxide 2-
6 parts, sodium-based montmorillonite 1-4 parts, calgon 2-6 parts, silver nitrate 1-5 parts, copper sulphate 3-6 parts, zinc nitrate 2-5 parts, oxidation
Graphene 4-8 parts, gelatin 2-5 parts, PLA 4-8 parts, dichloromethane 3-5 parts, glycerine 1-4 parts, methanol 3-5 parts, acetic acid fourth
Ester 2-5 parts, potassium dihydrogen phosphate 1-6 parts, sodium tetraborate 4-8 parts, dodecyl phenenyl sulfate 3-6 parts, deionized water 15-35 parts.
Preferably, sterilize the raw material of filler includes by weight:Oyster shell whiting 5-15 parts, CNT 8-16 parts, quality point
Sodium chloride solution 4-8 parts that hydrochloric acid 3-6 parts that number is 0.1-0.3%, substance withdrawl syndrome are 0.1-0.3mol/L, Nano Silver 2-
5 parts, butyl titanate 1-4 parts, neopelex 3-5 parts, polyvinyl pyrrolidone 2-6 parts, copper chloride 4-8 parts.
Preferably, sterilization filler is prepared by following technique:Oyster shell whiting and CNT are calcined, then cooled, in
Mass fraction is to be soaked in 0.1-0.3% hydrochloric acid, is washed, and is calcined after drying in Muffle furnace, grinding sieving, is cooled to room
Temperature, add sodium chloride solution, Nano Silver, butyl titanate, DBSA that substance withdrawl syndrome is 0.1-0.3mol/L
Sodium and polyvinyl pyrrolidone are well mixed, and stirring, are subsequently added into copper chloride and are well mixed, and are heated up, and insulation, are followed by stirring for, and are filtered,
Cleaning, dry, be cooled to room temperature and obtain sterilizing filler.
Preferably, sterilization filler is prepared by following technique:Oyster shell whiting and CNT are calcined into 1- in 500-600 DEG C
3h, be then cooled to 70-80 DEG C, in mass fraction be 0.1-0.3% hydrochloric acid in soak 0.5-1.5h, wash, dry after
1-3h is calcined in 1050-1150 DEG C in Muffle furnace, ground 80-120 mesh sieves, is cooled to room temperature, adding substance withdrawl syndrome is
0.1-0.3mol/L sodium chloride solution, Nano Silver, butyl titanate, neopelex and polyvinyl pyrrolidone mixing is
It is even, 10-30min is stirred in 650-850r/min rotating speeds, copper chloride is subsequently added into and is well mixed, is warming up to 120-140 DEG C, insulation
15-35 DEG C, 0.5-1.5h then is stirred in 1250-1550r/min rotating speeds, is filtered, cleaning, in 55-65 DEG C of dry 5-7h, cooling
Obtain sterilizing filler to room temperature.
Preferably, except the raw material of algae filler includes by weight:Sodium hydroxide 4-9 parts, sodium carbonate 5-15 parts, magnesium nitrate 2-
8 parts, aluminum nitrate 1-4 parts, magnetite powder 3-6 parts, aluminum oxide 2-4 parts, zeolite 1-4 parts, bentonite 2-6 parts, silane coupler KH-
550 4-8 parts.
Preferably, except algae filler is prepared by following technique:Sodium hydroxide, sodium carbonate and water are well mixed, stirred
Obtain material a;Magnesium nitrate, aluminum nitrate and water are well mixed, stirring obtains material b;Magnetite powder, material a and material b are mixed
Uniform, regulation pH is closed, then heats up, is incubated, Chen Hua, is washed to neutrality, dry, be cooled to room temperature, then adds aluminum oxide, boiling
Stone and bentonite are well mixed, and then grinding sieving, is subsequently added into silane resin acceptor kh-550 and is well mixed, and are stirred,
Then dry, be then cooled to room temperature and obtain removing algae filler.
Preferably, except algae filler is prepared by following technique:Sodium hydroxide, sodium carbonate and water are well mixed, in
450-650r/min rotating speeds stirring 1-3h obtains material a;Magnesium nitrate, aluminum nitrate and water are well mixed, in 850-1050r/min
Rotating speed stirring 20-40min obtains material b;Magnetite powder, material a and material b are well mixed, adjust pH to 10-11, then
80-90 DEG C is warming up to, 3-5h is incubated, Chen Hua 10-14h, is washed to neutrality, in 50-70 DEG C of dry 3-5h, is cooled to room temperature, so
Add aluminum oxide, zeolite and bentonite afterwards to be well mixed, then ground 30-50 mesh sieves, are subsequently added into silane coupled
Agent KH-550 is well mixed, and 20-40min is stirred in 650-850r/min rotating speeds, then cold then in 80-120 DEG C of dry 7-9h
But obtain removing algae filler to room temperature.
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, its raw material include sterilization filler,
Except algae filler, lysozyme, polymetaphosphate sodium, hexa, sulfamic acid, SODIUM PERCARBONATE, carbamide percarbonate, zinc oxide
Whisker, nano titanium oxide, sodium-based montmorillonite, calgon, silver nitrate, copper sulphate, zinc nitrate, graphene oxide, gelatin,
PLA, dichloromethane, glycerine, methanol, butyl acetate, potassium dihydrogen phosphate, sodium tetraborate, dodecyl phenenyl sulfate and go
Ionized water.Wherein, filler is sterilized by the way that oyster shell whiting and CNT are calcined, and is then cooled, is soaked in hydrochloric acid, washed, is done
Calcined after dry in Muffle furnace, grinding sieving, be cooled to room temperature, add sodium chloride solution, Nano Silver, butyl titanate, dodecane
Base benzene sulfonic acid sodium salt and polyvinyl pyrrolidone are well mixed, and stirring, are subsequently added into copper chloride and are well mixed, and are heated up, and insulation, are then stirred
Mix, filter, clean, dry, be cooled to room temperature and obtain sterilizing filler, it is used as porous absorption base using oyster shell whiting and CNT
Material, sterilization is used as using sodium chloride solution, Nano Silver, butyl titanate, neopelex, polyvinyl pyrrolidone and copper chloride
Material, bactericidal property can be effectively improved by the sterilization filler obtained after mixing, it not only itself has bactericidal property, and it is more
Pore structure can also for the present invention lobster pond it is special remove algae bactericidal purifying composite in other raw bactericidal materials attachment is provided
Site, further increase the sustained release performance of sterilization material so that bactericidal effect is more preferable.
Wherein, except algae filler is by the way that sodium hydroxide, sodium carbonate and water are well mixed, stirring obtains material a;By nitric acid
Magnesium, aluminum nitrate and water are well mixed, and stirring obtains material b;Magnetite powder, material a and material b are well mixed, pH is adjusted, connects
Heating, is incubated, Chen Hua, is washed to neutrality, dries, is cooled to room temperature, it is equal then to add aluminum oxide, zeolite and bentonite mixing
Even, then grinding sieving, is subsequently added into silane resin acceptor kh-550 and is well mixed, and stirs, then dries, then cold
But obtain removing algae filler to room temperature, using aluminum oxide, zeolite and bentonite as base-material, using sodium hydroxide and sodium carbonate as algae removal
Auxiliary agent, and being modified in the presence of silane resin acceptor kh-550, obtain except algae filler is applied in the present invention, not only this
Body can be removed to algae, suppress the growth of algae, moreover it is possible to special except algae bactericidal purifying is compound for lobster pond of the present invention
Material provides abundant attachment site, effectively increases sterilization adsorption effect, optimizes the environment of lobster cultivating pool.The present invention
Lobster pond composite material special can carry out kill to the algae in pond, and there is excellent bactericidal property, and sterilization
The release of medicine is efficiently high-quality.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair
It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair
In bright protection domain.
In embodiment, sterilize filler parts by weight can be 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, 45 parts, 50
Part;Except algae filler parts by weight can be 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25
Part;The parts by weight of lysozyme can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of polymetaphosphate sodium
It can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts;The parts by weight of hexa can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;
The parts by weight of sulfamic acid can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts;The parts by weight of SODIUM PERCARBONATE can be 2 parts, 2.5
Part, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of carbamide percarbonate can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts,
5.5 parts, 6 parts;The parts by weight of ZnOw can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8
Part;The parts by weight of nano titanium oxide can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts;The parts by weight of sodium-based montmorillonite can be 1 part,
1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts;The parts by weight of calgon can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts;Nitre
The parts by weight of sour silver can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts;The parts by weight of copper sulphate can be 3 parts, 3.5 parts, 4 parts, 4.5
Part, 5 parts, 5.5 parts, 6 parts;The parts by weight of zinc nitrate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;Aoxidize stone
The parts by weight of black alkene can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;The parts by weight of gelatin can
Think 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of PLA can be 4 parts, 4.5 parts, 5 parts, 5.5
Part, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;The parts by weight of dichloromethane can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The third three
The parts by weight of alcohol can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts;The parts by weight of methanol can be 3 parts, 3.5
Part, 4 parts, 4.5 parts, 5 parts;The parts by weight of butyl acetate can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;Phosphoric acid
The parts by weight of potassium dihydrogen can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts;Four
The parts by weight of Boratex can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;Detergent alkylate sulphur
The parts by weight of sour sodium can be 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts;The parts by weight of deionized water can be 15
Part, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts, 30
Part, 31 parts, 32 parts, 33 parts, 34 parts, 35 parts.
Embodiment 1
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize 35 parts of filler, except 20 parts of algae filler, 3.5 parts of lysozyme, 4 parts of polymetaphosphate sodium, 4 parts of hexa, amino sulphur
2 parts of acid, 3.5 parts of SODIUM PERCARBONATE, 4.5 parts of carbamide percarbonate, 6 parts of ZnOw, 4 parts of nano titanium oxide, sodium-based montmorillonite
2.5 parts, 4 parts of calgon, 3 parts of silver nitrate, 4.5 parts of copper sulphate, 3.5 parts of zinc nitrate, 6 parts of graphene oxide, gelatin 3.5
Part, 6 parts of PLA, 4 parts of dichloromethane, 2.5 parts of glycerine, 4 parts of methanol, 3.5 parts of butyl acetate, 3.5 parts of potassium dihydrogen phosphate, four
6 parts of Boratex, 4.5 parts of dodecyl phenenyl sulfate, 25 parts of deionized water.
Sterilization filler is prepared by following technique:By weight by 10 parts of oyster shell whitings and 12 parts of CNTs in 550 DEG C
2h is calcined, is then cooled to 75 DEG C, soaks 1h in the hydrochloric acid that 4.5 parts of mass fractions are 0.2%, is washed, in Muffle after drying
2h is calcined in 1100 DEG C in stove, ground 100 mesh sieve, is cooled to room temperature, adds the chlorine that 6 parts of substance withdrawl syndromes are 0.2mol/L
It is equal to change sodium solution, 3.5 parts of Nano Silvers, 2.5 parts of butyl titanates, 4 parts of neopelexes and 4 parts of polyvinyl pyrrolidone mixing
It is even, 20min is stirred in 750r/min rotating speeds, 6 parts of copper chlorides is subsequently added into and is well mixed, is warming up to 130 DEG C, 25 DEG C is incubated, connects
And stir 1h in 1400r/min rotating speeds, filter, cleaning, in 60 DEG C of dry 6h, be cooled to room temperature and obtain sterilizing filler.
Except algae filler is prepared by following technique:6.5 parts of sodium hydroxides, 10 parts of sodium carbonate and water are mixed by weight
Uniformly, material a is obtained in 550r/min rotating speeds stirring 2h;5 parts of magnesium nitrates, 2.5 parts of aluminum nitrates and water are well mixed, in
950r/min rotating speeds stirring 30min obtains material b;4.5 parts of magnetite powders, material a and material b are well mixed, regulation pH to
10.5,85 DEG C are then warming up to, 4h is incubated, Chen Hua 12h, is washed to neutrality, in 60 DEG C of dry 4h, is cooled to room temperature, Ran Houjia
Enter 3 parts of aluminum oxide, 2.5 parts of zeolites and 4 parts of bentonite to be well mixed, then ground 40 mesh sieve, is subsequently added into 6 parts of silicon
Alkane coupling agent KH-550 is well mixed, and is stirred 30min in 750r/min rotating speeds, then in 100 DEG C of dry 8h, is then cooled to room
Temperature obtains removing algae filler.
Embodiment 2
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize 20 parts of filler, except 25 parts of algae filler, 2 parts of lysozyme, 6 parts of polymetaphosphate sodium, 3 parts of hexa, sulfamic acid 3
It is part, 2 parts of SODIUM PERCARBONATE, 6 parts of carbamide percarbonate, 4 parts of ZnOw, 6 parts of nano titanium oxide, 1 part of sodium-based montmorillonite, six inclined
6 parts of sodium phosphate, 1 part of silver nitrate, 6 parts of copper sulphate, 2 parts of zinc nitrate, 8 parts of graphene oxide, 2 parts of gelatin, 8 parts of PLA, dichloro
3 parts of methane, 4 parts of glycerine, 3 parts of methanol, 5 parts of butyl acetate, 1 part of potassium dihydrogen phosphate, 8 parts of sodium tetraborate, detergent alkylate sulphur
Sour 3 parts of sodium, 35 parts of deionized water.
Sterilization filler is prepared by following technique:5 parts of oyster shell whitings and 16 parts of CNTs are forged in 500 DEG C by weight
3h is burnt, is then cooled to 70 DEG C, soaks 1.5h in the hydrochloric acid that 6 parts of mass fractions are 0.1%, is washed, in Muffle furnace after drying
In 3h are calcined in 1050 DEG C, ground 80 mesh sieve is cooled to room temperature, adds the chlorination that 8 parts of substance withdrawl syndromes are 0.1mol/L
Sodium solution, 5 parts of Nano Silvers, 1 part of butyl titanate, 5 parts of neopelexes and 2 parts of polyvinyl pyrrolidones are well mixed, in
850r/min rotating speeds stir 10min, are subsequently added into 8 parts of copper chlorides and are well mixed, and are warming up to 120 DEG C, are incubated 35 DEG C, then in
1250r/min rotating speeds stir 1.5h, filter, cleaning, in 55 DEG C of dry 7h, are cooled to room temperature and obtain sterilizing filler.
Except algae filler is prepared by following technique:4 parts of sodium hydroxides, 15 parts of sodium carbonate and water are mixed by weight equal
It is even, obtain material a in 450r/min rotating speeds stirring 3h;2 parts of magnesium nitrates, 4 parts of aluminum nitrates and water are well mixed, in 850r/min
Rotating speed stirring 40min obtains material b;3 parts of magnetite powders, material a and material b are well mixed, pH to 11 is adjusted, then heats up
To 80 DEG C, 5h is incubated, Chen Hua 10h, neutrality is washed to, in 70 DEG C of dry 3h, is cooled to room temperature, then add 4 parts of aluminum oxide, 1
Part zeolite and 6 parts of bentonite are well mixed, and then ground 30 mesh sieve, is subsequently added into 8 parts of silane resin acceptor kh-550s
It is well mixed, 40min is stirred in 650r/min rotating speeds, then in 80 DEG C of dry 9h, room temperature is then cooled to and obtains removing algae filler.
Embodiment 3
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize 50 parts of filler, except 15 parts of algae filler, 5 parts of lysozyme, 2 parts of polymetaphosphate sodium, 5 parts of hexa, sulfamic acid 1
It is part, 5 parts of SODIUM PERCARBONATE, 3 parts of carbamide percarbonate, 8 parts of ZnOw, 2 parts of nano titanium oxide, 4 parts of sodium-based montmorillonite, six inclined
2 parts of sodium phosphate, 5 parts of silver nitrate, 3 parts of copper sulphate, 5 parts of zinc nitrate, 4 parts of graphene oxide, 5 parts of gelatin, 4 parts of PLA, dichloro
5 parts of methane, 1 part of glycerine, 5 parts of methanol, 2 parts of butyl acetate, 6 parts of potassium dihydrogen phosphate, 4 parts of sodium tetraborate, detergent alkylate sulphur
Sour 6 parts of sodium, 15 parts of deionized water.
Sterilization filler is prepared by following technique:15 parts of oyster shell whitings and 8 parts of CNTs are forged in 600 DEG C by weight
1h is burnt, is then cooled to 80 DEG C, soaks 0.5h in the hydrochloric acid that 3 parts of mass fractions are 0.3%, is washed, in Muffle furnace after drying
In 1h are calcined in 1150 DEG C, ground 120 mesh sieve is cooled to room temperature, adds the chlorination that 4 parts of substance withdrawl syndromes are 0.3mol/L
Sodium solution, 2 parts of Nano Silvers, 4 parts of butyl titanates, 3 parts of neopelexes and 6 parts of polyvinyl pyrrolidones are well mixed, in
650r/min rotating speeds stir 30min, are subsequently added into 4 parts of copper chlorides and are well mixed, and are warming up to 140 DEG C, are incubated 15 DEG C, then in
1550r/min rotating speeds stir 0.5h, filter, cleaning, in 65 DEG C of dry 5h, are cooled to room temperature and obtain sterilizing filler.
Except algae filler is prepared by following technique:9 parts of sodium hydroxides, 5 parts of sodium carbonate and water are mixed by weight equal
It is even, obtain material a in 650r/min rotating speeds stirring 1h;8 parts of magnesium nitrates, 1 part of aluminum nitrate and water are well mixed, in 1050r/
Min rotating speeds stirring 20min obtains material b;6 parts of magnetite powders, material a and material b are well mixed, adjust pH to 10, then
90 DEG C are warming up to, 3h is incubated, Chen Hua 14h, is washed to neutrality, in 50 DEG C of dry 5h, is cooled to room temperature, then adds 2 parts of oxidations
Aluminium, 4 parts of zeolites and 2 parts of bentonite are well mixed, then ground 50 mesh sieve, are subsequently added into 4 parts of silane coupler KH-
550 is well mixed, stirs 20min in 850r/min rotating speeds, then in 120 DEG C of dry 7h, is then cooled to room temperature and obtains removing algae
Filler.
Embodiment 4
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize 25 parts of filler, except 22 parts of algae filler, 3 parts of lysozyme, 5 parts of polymetaphosphate sodium, 3.5 parts of hexa, amino sulphur
2.5 parts of acid, 3 parts of SODIUM PERCARBONATE, 5 parts of carbamide percarbonate, 5 parts of ZnOw, 5 parts of nano titanium oxide, sodium-based montmorillonite 2
Part, 5 parts of calgon, 2 parts of silver nitrate, 5 parts of copper sulphate, 3 parts of zinc nitrate, 7 parts of graphene oxide, 3 parts of gelatin, PLA 7
Part, 3.5 parts of dichloromethane, 3 parts of glycerine, 3.5 parts of methanol, 4 parts of butyl acetate, 2 parts of potassium dihydrogen phosphate, 7 parts of sodium tetraborate, ten
4 parts of dialkyl benzene sodium sulphate, 32 parts of deionized water.
Sterilization filler is prepared by following technique:8 parts of oyster shell whitings and 15 parts of CNTs are forged in 520 DEG C by weight
2.5h is burnt, is then cooled to 72 DEG C, soaks 1.2h in the hydrochloric acid that 5 parts of mass fractions are 0.15%, is washed, in Muffle after drying
2.5h is calcined in 1080 DEG C in stove, ground 85 mesh sieve, is cooled to room temperature, it is 0.15mol/L's to add 7 parts of substance withdrawl syndromes
Sodium chloride solution, 4 parts of Nano Silvers, 2 parts of butyl titanates, 4.5 parts of neopelexes and 3 parts of polyvinyl pyrrolidone mixing are equal
It is even, 15min is stirred in 820r/min rotating speeds, 7 parts of copper chlorides is subsequently added into and is well mixed, is warming up to 125 DEG C, 32 DEG C is incubated, connects
And stir 1.2h in 1280r/min rotating speeds, filter, cleaning, in 58 DEG C of dry 6.5h, be cooled to room temperature and obtain sterilizing filler.
Except algae filler is prepared by following technique:5 parts of sodium hydroxides, 12 parts of sodium carbonate and water are mixed by weight equal
It is even, obtain material a in 480r/min rotating speeds stirring 2.5h;3 parts of magnesium nitrates, 3 parts of aluminum nitrates and water are well mixed, in 880r/
Min rotating speeds stirring 35min obtains material b;4 parts of magnetite powders, material a and material b are well mixed, pH to 11.8 is adjusted, connects
And be warming up to 82 DEG C, be incubated 4.5h, Chen Hua 11h, be washed to neutrality, in 65 DEG C of dry 3.5h, be cooled to room temperature, then add
3.5 parts of aluminum oxide, 2 parts of zeolites and 5 parts of bentonite are well mixed, then ground 35 mesh sieve, are subsequently added into 7 parts of silane
Coupling agent KH-550 is well mixed, and is stirred 35min in 680r/min rotating speeds, then in 85 DEG C of dry 8.5h, is then cooled to room
Temperature obtains removing algae filler.
Embodiment 5
A kind of lobster pond proposed by the present invention is special to remove algae bactericidal purifying composite, and its raw material includes by weight:
Sterilize 45 parts of filler, except 18 parts of algae filler, 4 parts of lysozyme, 3 parts of polymetaphosphate sodium, 4.5 parts of hexa, amino sulphur
1.5 parts of acid, 4 parts of SODIUM PERCARBONATE, 4 parts of carbamide percarbonate, 7 parts of ZnOw, 3 parts of nano titanium oxide, sodium-based montmorillonite 3
Part, 3 parts of calgon, 4 parts of silver nitrate, 4 parts of copper sulphate, 4 parts of zinc nitrate, 5 parts of graphene oxide, 4 parts of gelatin, PLA 5
Part, 4.5 parts of dichloromethane, 2 parts of glycerine, 4.5 parts of methanol, 3 parts of butyl acetate, 5 parts of potassium dihydrogen phosphate, 5 parts of sodium tetraborate, ten
5 parts of dialkyl benzene sodium sulphate, 18 parts of deionized water.
Sterilization filler is prepared by following technique:12 parts of oyster shell whitings and 9 parts of CNTs are forged in 580 DEG C by weight
1.5h is burnt, is then cooled to 78 DEG C, soaks 0.8h in the hydrochloric acid that 4 parts of mass fractions are 0.25%, is washed, in Muffle after drying
1.5h is calcined in 1120 DEG C in stove, ground 115 mesh sieve, is cooled to room temperature, it is 0.25mol/L to add 5 parts of substance withdrawl syndromes
Sodium chloride solution, 3 parts of Nano Silvers, 3 parts of butyl titanates, 3.5 parts of neopelexes and the mixing of 5 parts of polyvinyl pyrrolidones
Uniformly, 25min is stirred in 680r/min rotating speeds, is subsequently added into 5 parts of copper chlorides and is well mixed, be warming up to 135 DEG C, be incubated 18 DEG C,
Then 0.8h is stirred in 1520r/min rotating speeds, filtered, cleaning, in 62 DEG C of dry 5.5h, be cooled to room temperature and obtain sterilizing filler.
Except algae filler is prepared by following technique:8 parts of sodium hydroxides, 8 parts of sodium carbonate and water are mixed by weight equal
It is even, obtain material a in 620r/min rotating speeds stirring 1.5h;7 parts of magnesium nitrates, 2 parts of aluminum nitrates and water are well mixed, in 1020r/
Min rotating speeds stirring 25min obtains material b;5 parts of magnetite powders, material a and material b are well mixed, pH to 10.2 is adjusted, connects
And be warming up to 88 DEG C, be incubated 3.5h, Chen Hua 13h, be washed to neutrality, in 55 DEG C of dry 4.5h, be cooled to room temperature, then add
2.5 parts of aluminum oxide, 3 parts of zeolites and 3 parts of bentonite are well mixed, then ground 45 mesh sieve, are subsequently added into 5 parts of silane
Coupling agent KH-550 is well mixed, and is stirred 25min in 820r/min rotating speeds, then in 115 DEG C of dry 7.5h, is then cooled to room
Temperature obtains removing algae filler.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (7)
1. a kind of lobster pond is special to remove algae bactericidal purifying composite, it is characterised in that its raw material includes by weight:Sterilization
Filler 20-50 parts, except algae filler 15-25 parts, lysozyme 2-5 parts, polymetaphosphate sodium 2-6 parts, hexa 3-5 parts,
Sulfamic acid 1-3 parts, SODIUM PERCARBONATE 2-5 parts, carbamide percarbonate 3-6 parts, ZnOw 4-8 parts, nano titanium oxide 2-6
Part, sodium-based montmorillonite 1-4 parts, calgon 2-6 parts, silver nitrate 1-5 parts, copper sulphate 3-6 parts, zinc nitrate 2-5 parts, oxidation stone
Black alkene 4-8 parts, gelatin 2-5 parts, PLA 4-8 parts, dichloromethane 3-5 parts, glycerine 1-4 parts, methanol 3-5 parts, butyl acetate
2-5 parts, potassium dihydrogen phosphate 1-6 parts, sodium tetraborate 4-8 parts, dodecyl phenenyl sulfate 3-6 parts, deionized water 15-35 parts.
2. lobster pond according to claim 1 is special to remove algae bactericidal purifying composite, it is characterised in that sterilization filler
Raw material include by weight:Oyster shell whiting 5-15 parts, CNT 8-16 parts, the hydrochloric acid 3-6 that mass fraction is 0.1-0.3%
Part, sodium chloride solution 4-8 parts that substance withdrawl syndrome is 0.1-0.3mol/L, Nano Silver 2-5 parts, butyl titanate 1-4 parts, 12
Sodium alkyl benzene sulfonate 3-5 parts, polyvinyl pyrrolidone 2-6 parts, copper chloride 4-8 parts.
3. lobster pond according to claim 1 or 2 is special to remove algae bactericidal purifying composite, it is characterised in that sterilization
Filler is prepared by following technique:Oyster shell whiting and CNT are calcined, then cooled, in mass fraction be 0.1-0.3%
Hydrochloric acid in soak, wash, calcined after drying in Muffle furnace, grinding sieving, be cooled to room temperature, adding substance withdrawl syndrome is
0.1-0.3mol/L sodium chloride solution, Nano Silver, butyl titanate, neopelex and polyvinyl pyrrolidone mixing is
It is even, stirring, it is subsequently added into copper chloride and is well mixed, heat up, insulation, be followed by stirring for, filter, clean, dries, be cooled to room temperature and obtain
To sterilization filler.
4. lobster pond according to claim any one of 1-3 is special to remove algae bactericidal purifying composite, it is characterised in that
Sterilization filler is prepared by following technique:Oyster shell whiting and CNT are calcined into 1-3h in 500-600 DEG C, are then cooled to
70-80 DEG C, in mass fraction be 0.1-0.3% hydrochloric acid in soak 0.5-1.5h, wash, dry after in Muffle furnace in
1050-1150 DEG C of calcining 1-3h, ground 80-120 mesh sieves are cooled to room temperature, and addition substance withdrawl syndrome is 0.1-0.3mol/
L sodium chloride solution, Nano Silver, butyl titanate, neopelex and polyvinyl pyrrolidone is well mixed, in 650-
850r/min rotating speeds stir 10-30min, are subsequently added into copper chloride and are well mixed, and are warming up to 120-140 DEG C, are incubated 15-35 DEG C,
Then 0.5-1.5h is stirred in 1250-1550r/min rotating speeds, filtered, cleaning, in 55-65 DEG C of dry 5-7h, be cooled to room temperature and obtain
To sterilization filler.
5. lobster pond according to claim any one of 1-4 is special to remove algae bactericidal purifying composite, it is characterised in that
Except the raw material of algae filler includes by weight:Sodium hydroxide 4-9 parts, sodium carbonate 5-15 parts, magnesium nitrate 2-8 parts, aluminum nitrate 1-4
Part, magnetite powder 3-6 parts, aluminum oxide 2-4 parts, zeolite 1-4 parts, bentonite 2-6 parts, silane resin acceptor kh-550 4-8 parts.
6. lobster pond according to claim any one of 1-5 is special to remove algae bactericidal purifying composite, it is characterised in that
Except algae filler is prepared by following technique:Sodium hydroxide, sodium carbonate and water are well mixed, stirring obtains material a;By nitric acid
Magnesium, aluminum nitrate and water are well mixed, and stirring obtains material b;Magnetite powder, material a and material b are well mixed, pH is adjusted, connects
Heating, is incubated, Chen Hua, is washed to neutrality, dries, is cooled to room temperature, it is equal then to add aluminum oxide, zeolite and bentonite mixing
Even, then grinding sieving, is subsequently added into silane resin acceptor kh-550 and is well mixed, and stirs, then dries, then cold
But obtain removing algae filler to room temperature.
7. lobster pond according to claim any one of 1-6 is special to remove algae bactericidal purifying composite, it is characterised in that
Except algae filler is prepared by following technique:Sodium hydroxide, sodium carbonate and water are well mixed, stirred in 450-650r/min rotating speeds
Mix 1-3h and obtain material a;Magnesium nitrate, aluminum nitrate and water are well mixed, obtained in 850-1050r/min rotating speeds stirring 20-40min
To material b;Magnetite powder, material a and material b are well mixed, adjust pH to 10-11, is then warming up to 80-90 DEG C, insulation
3-5h, Chen Hua 10-14h, are washed to neutrality, in 50-70 DEG C of dry 3-5h, are cooled to room temperature, then add aluminum oxide, zeolite and
Bentonite is well mixed, and then ground 30-50 mesh sieves, are subsequently added into silane resin acceptor kh-550 and are well mixed, in
650-850r/min rotating speeds stir 20-40min, then in 80-120 DEG C of dry 7-9h, are then cooled to room temperature and obtain except algae is filled out
Material.
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CN108117116A (en) * | 2017-12-29 | 2018-06-05 | 安徽阳城化工科技有限公司 | A kind of water treatment composite material of high antibacterial efficiency and sustained release performance |
CN108164009A (en) * | 2017-12-29 | 2018-06-15 | 安徽阳城化工科技有限公司 | A kind of antibacterial water treatment composite material |
CN108178206A (en) * | 2017-12-29 | 2018-06-19 | 安徽阳城化工科技有限公司 | A kind of high slow release water treatment composite material |
CN108557908A (en) * | 2017-12-29 | 2018-09-21 | 安徽阳城化工科技有限公司 | A kind of water treatment composite material and preparation method |
CN109266192A (en) * | 2018-09-11 | 2019-01-25 | 合肥绿普包装材料有限公司 | A kind of preparation method of long-life anion wallpaper |
CN109266192B (en) * | 2018-09-11 | 2020-11-13 | 山东光明园迪儿童家具科技有限公司 | Preparation method of long-life negative ion wallpaper |
WO2021245466A1 (en) | 2020-06-05 | 2021-12-09 | Lysterra Llc | Formulation for purifying reservoirs from cyanobacteria and green algae |
WO2021245465A1 (en) | 2020-06-05 | 2021-12-09 | Lysterra Llc | Composition for purifying reservoirs from cyanobacteria and green algae |
CN115595007A (en) * | 2022-10-28 | 2023-01-13 | 传质新材料有限公司(Cn) | Composite multifunctional wall material for disinfection and sterilization and preparation method and application thereof |
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