CN107468597A - One plant tea bran shampoo and preparation method thereof - Google Patents
One plant tea bran shampoo and preparation method thereof Download PDFInfo
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- CN107468597A CN107468597A CN201710930285.2A CN201710930285A CN107468597A CN 107468597 A CN107468597 A CN 107468597A CN 201710930285 A CN201710930285 A CN 201710930285A CN 107468597 A CN107468597 A CN 107468597A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a plant tea bran shampoo, it is made up of the raw material of following percentage by weight：Tea bran extract 2.5 3%, plant fermented liquid 25 30%, surfactant 15 20%, fat agent 1 1.5% is assigned, chelating agent 0.5 0.8%, vitamin 0.3 0.5%, essence 0.2 0.3%, surplus is water；And provide its preparation method.Contain tea bran extract in the shampoo of the present invention, Tea Saponin therein and a variety of surfactants coordinate, and have stronger cleaning capacity to scalp, pore, the dirt of hair surface, grease；The soybean carrot zymotic fluid obtained by the fermentation process of the present invention, rich in the nutrition such as several amino acids and vitamin, is more easy to be absorbed by scalp；Also contain biotin and folic acid, contribute to amino acid to utilize, promote hair keratin fiber to be formed；The hair washing liquid energy strengthens the toughness of hair, disconnected question topic is had clear improvement, moreover it is possible to prevent and treat alopecia.
Description
Technical field
The invention belongs to cleaning chemical products technical field, in particular it relates to plant tea bran shampoo and preparation method thereof.
Background technology
The structure of hair divides three parts：Epidermis, cortical layer, medullary substance layer, epidermis account for the 10% of hair, are hairs
Coat, enemy initiate protective effect.Cortical layer accounts for the 80% of hair, is the chief component of hair, is made up of keratin
Threadiness, hair dyeing, hair-waving are worked in this layer.Medullary substance layer accounts for the 10% of hair, and nutrition is mainly washed away from scalp
Material supplies natural on-off cycles of hair growth.
People are beautiful in order to pursue, and increasingly paying attention to hair can be big to the overall beautification function of people, the beautiful hair style of fashion
It is big to change external image and makings, often to hair scald dye during cutting ＆ styling, the chemical composition in high temperature, hair dye is correct
The epidermis and cortical layer of hair cause damage, and make the nutrition leak of hair.The reason for being damaged to hair also has harmful in air
Gas componant, dust and ultraviolet irradiation.With advancing age, the nutrition supply ability of hair is reduced, battalion also occurs
Support the problem of supply is insufficient.Above mentioned problem can cause a variety of hair problems, and such as hair quality is deteriorated, break hair, alopecia.
Shampoo is a kind of hair products with functions such as anti-dandruff, treatment oil function and hair dyeings.Containing more in shampoo
Kind composition, the comprehensive function of these compositions can play the function of cleaning scalp and hair.Current shampoo pursue hair it is submissive,
Anti-dandruff, it is easy to make hair it is greasy, it is dirty, collapse, be easy to make again hair coarse, do, disperse, repairing performance it is poor.Also have now
The shampoo of a variety of trophic functions, the hair washing as disclosed in publication number CN1258496A, CN103550132A, CN106852766A etc.
Product, a variety of nutrition can be provided for hair, there is multiple-effect effect, resolution question topic can not be solved, although some contains plant
Extract, because preparation method is unreasonable, plant nutrient ingredient can not be absorbed by scalp, supply hair.
The content of the invention
First purpose of the present invention is to overcome drawbacks described above, there is provided a plant tea bran shampoo, the shampoo have
Clean, trophism, contain various plants amino acid and vitamin in shampoo, provide nutrient for scalp and hair, strengthen head
The toughness of keratin fiber is sent out, disconnected hair, alopecia problem can be obviously improved.
Second object of the present invention is to provide the preparation method of above-mentioned shampoo.
The purpose of the present invention implements by the following technical programs：
One plant tea bran shampoo, is made up of the raw material of following percentage by weight：
Further, the preparation method of the tea bran extract is：Tea seed cake is crushed, adds tea seed cake powder weight 8-10
In water again, 85-90 DEG C is heated to, keeps 3-4h, is filtered, flocculant precipitation is added in filtrate, takes supernatant liquid filtering, concentration,
To compound moisture content below 60%, the 95vt% ethanol of 3-4 times of compound weight after concentration is added, is stirred, with activity
After charcoal absorption, 24h is stood, gained supernatant concentration, drying, is produced.
Further, the plant fermented liquid is soybean-carrot zymotic fluid.
Further, the preparation method of the soybean-carrot zymotic fluid is：Soybean 15-20 parts, Hu are weighed by weight
Radish 5-10 parts, soybean are cooked, and are pounded pureed, carrot stripping and slicing, are boiled to without hard-core, be pounded pureed, soybean mud and mashed carrot mix
Close, add soybean mud and the water of 6-8 times of mashed carrot gross weight, access soybean mud and the saccharomycete of mashed carrot gross weight 2%, in
32-33 DEG C of fermentation 8d, stirring twice, is filtered after fermentation ends daily in fermentation process, filtrate sterilizing, after charcoal absorption,
24h is stood, gained supernatant is soybean-carrot zymotic fluid.
Further, carrot is cooked with sodium acid carbonate containing 0.1wt%, the ascorbic water of 0.01wt%.
Further, the anion surfactant includes ammonium lauryl sulfate, lauryl sodium sulfate, dodecane
Three or more in base dimethyl amine second lactone, DDAO and Dodecyl Glucoside.
Further, the tax fat agent includes olive oil, higher alcohol and/or lanolin；
The chelating agent includes EDTA and/or EDTA-2Na.
Further, the vitamin includes biotin and folic acid.
Preferably, the shampoo is made up of the raw material of following percentage by weight：It is tea bran extract 2.7%, big
Beans-carrot zymotic fluid 30%, lauryl sodium sulfate 12%, dodecyl-dimethyl amine second lactone 3%, Dodecyl Glucoside
3%th, olive oil 1.2%, EDTA-2Na0.6%, biotin 0.3%, folic acid 0.2%, essence 0.2%, water 46.8%.
The preparation method of above-mentioned tea bran shampoo, plant fermented liquid and water are mixed, are heated to more than 95 DEG C, add tea bran
Extract, surfactant, fat agent, chelating agent, vitamin and essence are assigned, continue to be heated to more than 95 DEG C, be uniformly mixed,
Produced after cooling.
Tea bran is a blob of slag of the tea seed after oil expression, contains abundant Tea Saponin.Contain in the tea bran extract of the present invention
Tea Saponin, it is a kind of natural nonionic surface active agent, has and good the function such as emulsify, disperse, foaming, moistening.
It is containing soybean-carrot zymotic fluid in place of the important innovations of the present invention.Soybean is rich in protein, and protein contains
Amount is not only high, and quality is good, the soy proteinaceous amino acid composition ratio that relatively human body needs, is readily absorbed by.
Carrot carrot is rich in carbohydrate, protein, fat, volatile oil, carrotene, vitamin A, vitamin B1, vitamin B2, cyanine
The nutritional ingredients such as element, calcium, iron.The present invention accesses after soybean, carrot curing saccharomycete, shaking table hair is carried out under constant temperature
The preparation method of ferment, compared with prior art middle plant extraction liquid, amino acid, vitamin in soybean of the invention-carrot zymotic fluid
Species is more rich, is more easy to be absorbed by scalp, ultimately forms keratin fiber, makes hair more flexible, not easily broken hair.
Surfactant is as cleaning ingredients, using their infiltration, emulsification and peptizaiton by dirt from hair, scalp
Middle removing.
That assigns fat agent act as making hair smooth submissive.
Chelating agent act as reducing deposition of the calcium ions and magnesium ions on hair.
Contain biotin and folic acid in the shampoo of the present invention.Biotin (biotin, biotin) is protein normal generation
Thank to indispensable material.Utilization of the folic acid to protein and amino acid plays an important roll.Biotin and folic acid can promote head
Send out the synthesis of azelon, moreover it is possible to anti-alopecia-stopping.
The invention has the advantages that：
(1) tea bran extract is contained in shampoo of the invention, Tea Saponin therein and a variety of surfactants coordinate, right
Scalp, pore, the dirt of hair surface, grease have stronger cleaning capacity；
(2) soybean-carrot zymotic fluid obtained by the fermentation process of the present invention, rich in several amino acids and vitamin
Deng nutrition, it is more easy to be absorbed by scalp；
(3) also contain biotin and folic acid, contribute to amino acid to utilize, promote hair keratin fiber to be formed；
(4) toughness of hair washing liquid energy enhancing hair, disconnected question topic is had clear improvement, moreover it is possible to prevent and treat alopecia.
Embodiment
The preferred embodiments of the present invention are illustrated below, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Biotin in the embodiment of the present invention is purchased from Hangzhou Fuyang Kexing Biochemical Co., Ltd., and folic acid is abundant purchased from Xi'an
Magnificent bio tech ltd.
Embodiment 1
One plant tea bran shampoo, preparation method are as follows：
(1) preparation of tea bran extract
Tea seed cake 50kg is weighed, adds 450kg deionized waters, is heated to 85-90 DEG C, keeps 4h.Mistake after the completion of heat extraction
Filter, polyaluminium sulfate is added into filtrate and carries out flocculation sediment, flocculant adds according to 50mg/L filtrates, precipitates more than 6h.On
Clear liquid heating is concentrated into moisture content below 60%, adds the 95vt% ethanol of 4 times of concentrate feed weight, stirs, use activated carbon
Adsorption bleaching, 24h is stood, supernatant concentration, drying, produces tea bran extract.
(2) preparation of soybean-carrot zymotic fluid
Weigh soybean 18kg, carrot 8kg.Soybean is cooked, is pounded pureed.Carrot stripping and slicing, with bicarbonate containing 0.1wt%
The ascorbic deionization boiling of sodium, 0.01wt% is pounded pureed to without hard-core.Soybean mud and mashed carrot are mixed, add mud
The deionized water that 7 times of gross weight, the saccharomycete of access mud gross weight 2%, ferment 8d in 32-33 DEG C, is stirred daily in fermentation process
Mix twice, filtered after fermentation ends, filtrate is heated to boiling and sterilized.Then adsorbed with activated carbon, stand 24h, on
Clear liquid is soybean-carrot zymotic fluid.
(3) preparation of shampoo
Soybean-carrot zymotic fluid 30kg, deionized water 46.8kg is mixed, is heated to more than 95 DEG C, adds 2.7kg tea
Bran extract, lauryl sodium sulfate 12kg, dodecyl-dimethyl amine second lactone 3kg, Dodecyl Glucoside 3kg, olive oil
1.2kg, EDTA-2Na 0.6kg, biotin 0.3kg, folic acid 0.2kg, essence 0.2kg, continue to be heated to more than 95 DEG C, stir,
It is sufficiently mixed uniformly, is produced after cooling.
Embodiment 2
The present embodiment is substantially the same manner as Example 1, and difference is, in step (3), the dosage of the application each component is：Greatly
Beans-carrot zymotic fluid 28kg, deionized water 51.6kg, tea bran extract 3kg, lauryl sodium sulfate 11kg, dodecyl two
Methyl amine second lactone 2kg, Dodecyl Glucoside 2kg, olive oil 1kg, EDTA-2Na 0.8kg, biotin 0.2kg, folic acid
0.1kg, essence 0.3kg.
Embodiment 3
The present embodiment is substantially the same manner as Example 1, and difference is, in step (3), the dosage of the application each component is：Greatly
Beans-carrot zymotic fluid 25kg, deionized water 49.9kg, tea bran extract 2.5kg, lauryl sodium sulfate 14kg, dodecyl
Dimethyl amine second lactone 3kg, Dodecyl Glucoside 3kg, olive oil 1.5kg, EDTA-2Na 0.5kg, biotin 0.2kg, folic acid
0.2kg, essence 0.2kg.
Embodiment 4
One plant tea bran shampoo, preparation method are as follows：
(1) preparation of tea bran extract
Tea seed cake 50kg is weighed, adds 400kg deionized waters, is heated to 85-90 DEG C, keeps 3h.Mistake after the completion of heat extraction
Filter, polyaluminium sulfate is added into filtrate and carries out flocculation sediment, flocculant adds according to 50mg/L filtrates, precipitates more than 6h.On
Clear liquid heating is concentrated into moisture content below 60%, adds the 95vt% ethanol of 3 times of concentrate feed weight, stirs, use activated carbon
Adsorption bleaching, 24h is stood, supernatant concentration, drying, produces tea bran extract.
(2) preparation of soybean-carrot zymotic fluid
Weigh soybean 15kg, carrot 10kg.Soybean is cooked, is pounded pureed.Carrot stripping and slicing, with carbonic acid containing 0.1wt%
The ascorbic deionization boiling of hydrogen sodium, 0.01wt% is pounded pureed to without hard-core.Soybean mud and mashed carrot are mixed, added
The deionized water that 6 times of mud gross weight, the saccharomycete of access mud gross weight 2%, ferment 8d in 32-33 DEG C, in fermentation process daily
Stirring twice, is filtered, filtrate is heated to boiling and sterilized after fermentation ends.Then adsorbed with activated carbon, stand 24h,
Supernatant is soybean-carrot zymotic fluid.
(3) preparation of shampoo
Soybean-carrot zymotic fluid 28kg, deionized water 51.6kg is mixed, is heated to more than 95 DEG C, adds 3kg tea brans
Extract, lauryl sodium sulfate 11kg, dodecyl-dimethyl amine second lactone 2kg, Dodecyl Glucoside 2kg, olive oil
1kg, EDTA-2Na 0.8kg, biotin 0.2kg, folic acid 0.1kg, essence 0.3kg, continue to be heated to more than 95 DEG C, stirring, fill
Divide and be well mixed, produced after cooling.
Embodiment 5
One plant tea bran shampoo, preparation method are as follows：
(1) preparation of tea bran extract
Tea seed cake 50kg is weighed, adds 500kg deionized waters, is heated to 85-90 DEG C, keeps 4h.Mistake after the completion of heat extraction
Filter, polyaluminium sulfate is added into filtrate and carries out flocculation sediment, flocculant adds according to 50mg/L filtrates, precipitates more than 6h.On
Clear liquid heating is concentrated into moisture content below 60%, adds the 95vt% ethanol of 4 times of concentrate feed weight, stirs, use activated carbon
Adsorption bleaching, 24h is stood, supernatant concentration, drying, produces tea bran extract.
(2) preparation of soybean-carrot zymotic fluid
Weigh soybean 20kg, carrot 5kg.Soybean is cooked, is pounded pureed.Carrot stripping and slicing, with bicarbonate containing 0.1wt%
The ascorbic deionization boiling of sodium, 0.01wt% is pounded pureed to without hard-core.Soybean mud and mashed carrot are mixed, add mud
The deionized water that 8 times of gross weight, the saccharomycete of access mud gross weight 2%, ferment 8d in 32-33 DEG C, is stirred daily in fermentation process
Mix twice, filtered after fermentation ends, filtrate is heated to boiling and sterilized.Then adsorbed with activated carbon, stand 24h, on
Clear liquid is soybean-carrot zymotic fluid.
(3) preparation of shampoo
Soybean-carrot zymotic fluid 25kg, deionized water 49.9kg is mixed, is heated to more than 95 DEG C, adds 2.5kg tea
Bran extract, lauryl sodium sulfate 14kg, dodecyl-dimethyl amine second lactone 3kg, Dodecyl Glucoside 3kg, olive oil
1.5kg, EDTA-2Na 0.5kg, biotin 0.2kg, folic acid 0.2kg, essence 0.2kg, continue to be heated to more than 95 DEG C, stir,
It is sufficiently mixed uniformly, is produced after cooling.
Shampoo effect test
1st, subjects
100, be women, and the age between 25-40 year, has disconnected question and inscribed.
2nd, test method
100 women are randomly divided into 5 groups, and every group of 20 people, numbering is test group 1-5, respectively using the embodiment of the present invention
1-5 shampoo, had one's hair wash according to usually custom.
Using effect is divided into 4 grades, and standard is as follows：
Well：Disconnected hair reduces more than 80%；
Effectively：Disconnected hair reduces 50-80%；
Typically：Disconnected hair reduces 20-50%；
It is invalid：Disconnected hair reduces less than 20%.
Using effect is counted after 1 month, the results are shown in Table 1.
The using effect of table 1
As shown in Table 1, the shampoo of the embodiment of the present invention is effective to disconnected question topic, wherein the shampoo of embodiment 1
Using effect is best, and for rate of good up to 65%, that is, the disconnected hair of user for having 65% reduces more than 80%.In addition, after 1 month, use
The alopecia problem of person also has improvement.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic.All essences in the present invention
God any modification, equivalent substitution and improvements made etc., should be included in the scope of the protection with principle.
Claims (10)
- A 1. plant tea bran shampoo, it is characterised in that be made up of the raw material of following percentage by weight：
- 2. tea bran shampoo according to claim 1, it is characterised in that the preparation method of the tea bran extract is：Will Tea seed cake crushes, and adds in the water of 8-10 times of tea seed cake powder weight, is heated to 85-90 DEG C, keeps 3-4h, filters, and adds in filtrate Enter flocculant precipitation, take supernatant liquid filtering, concentrate, to compound moisture content below 60%, add compound weight 3-4 after concentration 95vt% ethanol again, stirs, and after charcoal absorption, stands 24h, gained supernatant concentration, drying, produces.
- 3. tea bran shampoo according to claim 1, it is characterised in that the plant fermented liquid is soybean-carrot fermentation Liquid.
- 4. tea bran shampoo according to claim 3, it is characterised in that the preparation method of the soybean-carrot zymotic fluid For：Soybean 15-20 parts, carrot 5-10 parts are weighed by weight, soybean is cooked, and is pounded pureed, carrot stripping and slicing, is boiled to without hard-core, Be pounded pureed, soybean mud and mashed carrot mixing add soybean mud and the water of 6-8 times of mashed carrot gross weight, access soybean mud with The saccharomycete of mashed carrot gross weight 2%, ferment 8d in 32-33 DEG C, is stirred daily in fermentation process twice, mistake after fermentation ends Filter, filtrate sterilizing, after charcoal absorption, 24h is stood, gained supernatant is soybean-carrot zymotic fluid.
- 5. tea bran shampoo according to claim 4, it is characterised in that carrot sodium acid carbonate containing 0.1wt%, The ascorbic water of 0.01wt% is cooked.
- 6. tea bran shampoo according to claim 1, it is characterised in that the anion surfactant includes dodecane Base ammonium sulfate, lauryl sodium sulfate, dodecyl-dimethyl amine second lactone, DDAO and dodecyl Three or more in glucosides.
- 7. tea bran shampoo according to claim 1, it is characterised in that the tax fat agent include olive oil, higher alcohol and/ Or lanolin；The chelating agent includes EDTA and/or EDTA-2Na.
- 8. tea bran shampoo according to claim 1, it is characterised in that the vitamin includes biotin and folic acid.
- 9. the tea bran shampoo according to claim any one of 1-8, it is characterised in that the shampoo is by following weight hundred Divide the raw material composition of ratio：Tea bran extract 2.7%, soybean-carrot zymotic fluid 30%, lauryl sodium sulfate 12%, dodecane Base dimethyl amine second lactone 3%, Dodecyl Glucoside 3%, olive oil 1.2%, EDTA-2Na 0.6%, biotin 0.3%, leaf Acid 0.2%, essence 0.2%, water 46.8%.
- 10. the preparation method of the tea bran shampoo described in claim any one of 1-9, it is characterised in that by plant fermented liquid and Water mixes, and is heated to more than 95 DEG C, adds tea bran extract, surfactant, assigns fat agent, chelating agent, vitamin and essence, after It is continuous to be heated to more than 95 DEG C, it is uniformly mixed, is produced after cooling.
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