CN107462589A - Seabed integrated neutron activation analysis system in situ - Google Patents

Seabed integrated neutron activation analysis system in situ Download PDF

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Publication number
CN107462589A
CN107462589A CN201710798939.0A CN201710798939A CN107462589A CN 107462589 A CN107462589 A CN 107462589A CN 201710798939 A CN201710798939 A CN 201710798939A CN 107462589 A CN107462589 A CN 107462589A
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CN
China
Prior art keywords
detector
neutron
neutron source
ray
source
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Pending
Application number
CN201710798939.0A
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Chinese (zh)
Inventor
成毅
庹先国
杨剑波
廖佳威
刘欢
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Chengdu Univeristy of Technology
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Chengdu Univeristy of Technology
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Application filed by Chengdu Univeristy of Technology filed Critical Chengdu Univeristy of Technology
Priority to CN201710798939.0A priority Critical patent/CN107462589A/en
Publication of CN107462589A publication Critical patent/CN107462589A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/005Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using neutrons
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/07Investigating materials by wave or particle radiation secondary emission
    • G01N2223/074Investigating materials by wave or particle radiation secondary emission activation analysis
    • G01N2223/0745Investigating materials by wave or particle radiation secondary emission activation analysis neutron-gamma activation analysis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/60Specific applications or type of materials
    • G01N2223/635Specific applications or type of materials fluids, granulates

Abstract

The invention discloses a kind of seabed integrated neutron activation analysis system in situ, including detector assembly, triumphant wiring cable and control system, the detector assembly is connected by triumphant wiring cable with control system, the detector assembly includes body, is arranged on intrinsic neutron source, detector, and solid is made using C, H high polymer material in division board, the body made of neutron absorber material between neutron source and detector;The neutron source is irradiated for given-ioff neutron to bottom sediment, and bottom sediment is produced prompt gamma ray after neutron activation, and the neutron source outer wall is enclosed with the lead layer shielded to the spontaneous gamma-rays of neutron source;The division board is used to absorb the neutron that neutron source is transmitted directly on detector;The detector is used to collect the wink hair Characteristic γ ray, and the data detected are sent into control system and analyzed and processed.The present invention will not increase the background of detector, and it is simple in construction, intensity is high, without setting detecting window, small, service life length is damaged to detector.

Description

Seabed integrated neutron activation analysis system in situ
Technical field
The present invention relates to a kind of neutron detection device, more particularly to a kind of seabed integrated neutron activation analysis system in situ System.
Background technology
At present, bottom sediment is detected, is generally divided into 2 kinds of methods.First method is directly to sea-bottom deposit Thing is sampled, and then aboard ship either land carries out physics or chemical analysis obtains containing for various bottom sediment elements Amount.Second method is that in situ and measurement in real time is carried out to bottom sediment, and qualitative and quantitative point is then carried out to thalassoxene element Analysis.But first method the step such as need to be sampled sample, process or transport, it is necessary to the time spent it is very long and These steps are pretty troublesome.Therefore the detection to bottom sediment now slowly turns to the 2nd kind of method.Second method avoids completely To steps such as bottom sediment sample, processing, directly bottom sediment can be carried out during surveying vessel navigation Measurement in real time, the content and distribution diagram of element of bottom sediment element can be got in real time.
In the second approach, present use must be X-fluorescence Detection Techniques, referring to Fig. 1, that is, utilize x-ray bombardment seabed Deposit, bottom sediment is produced characteristic X-ray, then detected by detector, qualitatively and quantitatively analyzed.But Because X ray penetration capacity is weak, cause to be easy to produce bottom sediment by Absorption by Sea Water so as to which bottom sediment can not be irradiated Characteristic X-ray or because caused bottom sediment characteristic X-ray can not be detected after Absorption by Sea Water by detector, therefore The content for the bottom sediment element for causing to measure has certain error.In addition, being also due to that X ray penetration capacity is weak, need Will be in seabed inserting tube(X fluorescent probes system and various instruments are protected in seabed)Middle setting detecting window, to weaken Absorption of the inserting tube to X ray.But although detecting window can weaken the absorption to X ray, still there is a certain amount of X ray quilt Sponge, and detecting window is more fragile, it is easy to damaged by bottom sediment, so as to cause the infringement of instrument.Further, since X-ray tube produces the X ray for being, this can increase the background for the X-ray spectrum that detector detects, so as to bottom sediment element Content measurement have a certain impact.
The content of the invention
The purpose of the present invention is that providing one kind solves the above problems, and will not increase the background of detector, and structure letter Single, intensity height, without setting detecting window, small, the seabed integrated neutron activation point in situ of service life length is damaged to detector Analysis system.
To achieve these goals, the technical solution adopted by the present invention is such:A kind of seabed integrated neutron in situ Activation analysis system, including detector assembly, triumphant wiring cable and control system, the detector assembly pass through triumphant wiring cable and control System connection processed, the detector assembly include body, are arranged on intrinsic neutron source, detector, and positioned at neutron source Between detector made of neutron absorber material division board;
Solid is made using C, H high polymer material in the body;
The neutron source is irradiated for launching radioactive source to bottom sediment, and bottom sediment is produced wink after neutron activation Gamma-rays is sent out, and the neutron source outer wall is enclosed with the lead layer shielded to the spontaneous gamma-rays of neutron source;
The division board is used to absorb the neutron that neutron source is transmitted on detector;
The detector is used to collect the wink hair Characteristic γ ray, and the data detected are sent into control system;
The obturator of adjustment center of gravity is additionally provided with body, the obturator is used for the integral level for adjusting detector assembly.
As preferred:The detector is scintillator or semiconductor detector, and the obturator uses Pb or Cu, in described Component is radioactive isotope neutron source, and the material of the division board is10B。
In fact, selection is not limited to above-mentioned material, the detector is scintillator or semiconductor detector, such as NaI (Tl)、LaBr3Deng, the obturator using high-density matters such as Pb or Cu, for adjusting the center of gravity of body, the neutron source is Radioactive isotope neutron source, such as241Am-Be sources,24Na-Be sources etc., its effect is for producing neutron, then to seabed Deposit is irradiated, and bottom sediment is produced prompt gamma ray after neutron activation;The material of the division board is inhaled for neutron The big material in section is received, such as10B, its effect is for absorbing neutron, avoiding damage of the neutron to detector.
As preferred:The body is horizontally disposed cylinder or cuboid.
Compared with prior art, the advantage of the invention is that:The present invention produces neutron using neutron source, and irradiation seabed sinks Product thing is so as to produce Characteristic γ ray, because neutron and gamma-ray penetration capacity ratio X ray are strong, therefore when design not Need special detecting window.Overall construction intensity is high, can more bear the pressure at deep-sea, can realize and deep seafloor is detected.
In addition, seawater can also degraded neutron, so as to increase the reaction cross-section of neutron and bottom sediment, and neutron due to There are the stop of high-performance neutron absorber material, therefore the infringement very little to detector, the service life of the present invention can be improved, due to Neutron does not interfere with detector, so the background for the gamma ray spectrum that detector detects will not be increased.
Solid is made using C, H high polymer material in body of the present invention, can either be thermal neutron moderation of neutrons, moreover it is possible to right The effect that probe portion is protected and supported, therefore the probe portion in device need not be protected using seabed inserting tube Shield.
In addition, the part of detection is all embedded in body made of C, H macromolecule by the present invention, forms integration and set Meter, can very easily be moved.
Brief description of the drawings
Fig. 1 is the structural representation of seabed in-situ investigation device in the prior art;
Fig. 2 is the structural representation of the present invention.
In figure:1st, bottom sediment;2nd, X-ray tube;3rd, power-supply controller of electric;4th, signal processing circuit;5th, detecting window;6th, excite Detection device;7th, X-ray detector;8th, triumphant wiring cable;9th, obturator;10th, body;11st, neutron source;12nd, detector;13rd, every From plate.
Embodiment
Below in conjunction with accompanying drawing, the invention will be further described.
Embodiment 1:Referring to Fig. 1, in the prior art, seabed in situ X-ray diffraction fluorescence measurement sample is continued using this structure more Product excite and detection schematic diagram.As seen from the figure, generally hollow excitation detection gear 6, inside set X-ray tube 2 and X ray Detector 7, bottom open up detecting window 5, and the angle of X-ray tube 2 and horizontal plane is α, and the angle of X-ray detector 7 and horizontal plane is β, X-ray tube 2 connect power-supply controller of electric 3, and X-ray detector 7 connects signal processing circuit 4;The detection method of the present apparatus is:Utilize X-ray bombardment bottom sediment 1, bottom sediment 1 is produced characteristic X-ray, then detected, entering by X-ray detector 7 Row is qualitatively and quantitatively analyzed.But because X ray penetration capacity is weak, cause to be easy to by Absorption by Sea Water so as to which seabed can not be irradiated Deposit 1 produces the characteristic X-ray of bottom sediment 1 or because the caused characteristic X-ray of bottom sediment 1 is by after Absorption by Sea Water It can not be detected by X-ray detector 7, therefore the content for the element of bottom sediment 1 for causing to measure has certain error.This Outside, also it is due to that X ray penetration capacity is weak, it is necessary in seabed inserting tube(To the system of x fluorescent X-rays detector 7 and respectively in seabed Kind instrument is protected)Middle setting detecting window 5, to weaken absorption of the inserting tube to X ray.But although detecting window 5 can weaken to X The absorption of ray, but still there is a certain amount of X ray to be predominantly absorbed, and detecting window 5 compare it is fragile, it is easy to sunk by seabed Product thing 1 damages, so as to cause the infringement of instrument.Further, since X-ray tube produces the X ray for being, this can increase X-ray detection The background for the X-ray spectrum that device 7 detects, so as to be had a certain impact to the content measurement of the element of bottom sediment 1.
Referring to Fig. 2, scheme that the present invention uses for:A kind of seabed integrated neutron activation analysis system in situ, including visit The component of device 12, triumphant wiring cable 8 and control system, the component of detector 12 is surveyed to be connected with control system by triumphant wiring cable 8,
The component of detector 12 includes body 10, the neutron source 11 being arranged in body 10, detector 12, and positioned at neutron Between source 11 and detector 12 made of neutron absorber material division board 13;
Solid is made using C, H high polymer material in the body 10;
The neutron source 11 is irradiated for launching radioactive source to bottom sediment 1, and bottom sediment 1 is produced after neutron activation Raw prompt gamma ray, and the outer wall of the neutron source 11 is enclosed with the lead layer shielded to 11 spontaneous gamma-rays of neutron source;
The division board 13 is used to absorb the neutron that neutron source 11 is transmitted on detector 12;
The detector 12 is used to collect the wink hair Characteristic γ ray, and the data detected are sent into control system;
The obturator 9 of adjustment center of gravity is additionally provided with body 10, the obturator 9 is used for the overall water for adjusting the component of detector 12 It is flat.
Wherein, the detector 12 is scintillator or semiconductor detector 12, such as NaI(Tl), LaBr3 etc., the filling Body 9 uses Pb or Cu, such as241Am-Be sources,24Na-Be sources etc., the neutron source 11 is radioactive isotope neutron source 11, described The material of division board 13 is10B, the body 10 are horizontally disposed cylinder or cuboid.
Detection method of the present invention is that the present invention is carried to the position for needing to detect using ship, will by triumphant wiring cable 8 The component of detector 12 is placed on seabed, is contacted with bottom sediment 1, now opens the component of detector 12 and is detected.
Neutron source 11 launches radioactive source and bottom sediment 1 is excited, and produces prompt gamma ray, and detector 12 detects Arrive, the detector 12 collects wink hair Characteristic γ ray, and by the data detected be sent to control system carry out it is qualitative Quantitative analysis.
Body 10 made of C, H high polymer material during the present invention uses, can not only be slow by fast neutron caused by neutron source 11 It is melted into thermal neutron, moreover it is possible to the effect protected and supported to probe portion, therefore seabed inserting tube is not needed to the spy in device Survey part to be protected, the outer wall of neutron source 11 coats the lead layer that a pair of neutrons carry out slowing down, body made of C, H high polymer material 10 and lead layer, the two is all can be by Moderation of the fast neutrons caused by neutron source 11 into thermal neutron, increase neutron and bottom sediment 1 Reaction cross-section.So body 10 not only acts as the effect of shell protection support, the effect of degraded neutron is also taken into account.
The division board 13 is used to absorb the neutron that neutron source 11 is transmitted on detector 12, therefore to the broken of detector 12 Bad very little, and neutron will not increase the background for the gamma ray spectrum that detector 12 detects.Adjustment center of gravity is additionally provided with body 10 Obturator 9, the obturator 9 is used for the integral level for adjusting the component of detector 12, and is advantageous to entirety of the invention in the seawater Sink, be easy to detect.
The present invention without detecting window 5, and seawater can degraded neutron, so as to increase the reaction cross-section with bottom sediment 1, Detector 12 is hardly influenceed by neutron source 11, adds service life, and probe portion is all embedded in body 10, forms one Bodyization designs, and can very easily move, bottom sediment 1 is detected.

Claims (3)

1. a kind of seabed integrated neutron activation analysis system in situ, including detector assembly, triumphant wiring cable and control system, institute Detector assembly is stated to be connected with control system by triumphant wiring cable, it is characterised in that:
The detector assembly includes body, is arranged on intrinsic neutron source, detector, and positioned at neutron source and detector Between made of neutron absorber material division board;
Solid is made using C, H high polymer material in the body;
The neutron source is irradiated for launching radioactive source to bottom sediment, and bottom sediment is produced wink after neutron activation Gamma-rays is sent out, and the neutron source outer wall is enclosed with the lead layer shielded to the spontaneous gamma-rays of neutron source;
The division board is used to absorb the neutron that neutron source is transmitted on detector;
The detector is used to collect the wink hair Characteristic γ ray, and the data detected are sent into control system;
The obturator of adjustment center of gravity is additionally provided with body, the obturator is used for the integral level for adjusting detector assembly.
2. seabed according to claim 1 integrated neutron activation analysis system in situ, it is characterised in that:The detector For scintillator or semiconductor detector, the obturator uses Pb or Cu, and the neutron source is radioactive isotope neutron source, institute The material for stating division board is10B。
3. seabed according to claim 1 integrated neutron activation analysis system in situ, it is characterised in that:The body is Horizontally disposed cylinder or cuboid.
CN201710798939.0A 2017-09-07 2017-09-07 Seabed integrated neutron activation analysis system in situ Pending CN107462589A (en)

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Application Number Priority Date Filing Date Title
CN201710798939.0A CN107462589A (en) 2017-09-07 2017-09-07 Seabed integrated neutron activation analysis system in situ

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114324430A (en) * 2022-03-07 2022-04-12 合肥金星智控科技股份有限公司 Detection device based on neutron activation

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CN106970428A (en) * 2017-05-02 2017-07-21 成都理工大学 Seabed inserting tube
CN207148004U (en) * 2017-09-07 2018-03-27 成都理工大学 Seabed integrated neutron activation analysis system in situ
CN111257413A (en) * 2020-02-17 2020-06-09 中国海洋大学 Three-dimensional in-situ real-time submarine sediment acoustic section scanning device

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114324430A (en) * 2022-03-07 2022-04-12 合肥金星智控科技股份有限公司 Detection device based on neutron activation
CN114324430B (en) * 2022-03-07 2022-06-17 合肥金星智控科技股份有限公司 Detection device based on neutron activation

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Application publication date: 20171212