CN107460034A - Giving off a strong fragrance rapeseed oil and preparation method thereof - Google Patents

Giving off a strong fragrance rapeseed oil and preparation method thereof Download PDF

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CN107460034A
CN107460034A CN201710805922.3A CN201710805922A CN107460034A CN 107460034 A CN107460034 A CN 107460034A CN 201710805922 A CN201710805922 A CN 201710805922A CN 107460034 A CN107460034 A CN 107460034A
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rapeseed oil
rapeseed
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giving
temperature
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张海龙
杜静
舒楠
伍贤进
龚任
杨凡
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Huaihua University
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Fats And Perfumes (AREA)

Abstract

本发明涉及一种浓香菜籽油及其制备方法,所述制备方法包括如下步骤:首先将菜籽进行除杂处理,得到干净的菜籽;将茶叶和/或茶叶籽果皮经过超微粉碎处理,然后过筛,再加入软水后进行超声处理,然后过滤并收集滤液;将所述菜籽采用雾化着水设备对其进行着所述滤液;将所述菜籽放置于调质塔中,进行润菜籽处理;将所述产物放入滚筒炒籽机中进行炒籽;将所述产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油。本发明的浓香菜籽油的制备方法,在生产出的风味浓郁、口感爽滑的浓香菜籽油同时,又能使采用传统炒籽工艺生产的浓香菜籽油不含苯并芘或者含量不超国标,使浓香菜籽油天然、绿色、健康。The invention relates to a strong fragrant rapeseed oil and a preparation method thereof. The preparation method comprises the following steps: first, the rapeseed is subjected to impurity removal treatment to obtain clean rapeseed; the tea leaves and/or tea seed peels are subjected to ultrafine grinding treatment, then sieve, then add soft water and perform ultrasonic treatment, then filter and collect the filtrate; use the rapeseed to carry out the filtrate by atomizing water equipment; place the rapeseed in a conditioning tower , carry out rapeseed treatment; put the product into a drum seed frying machine to fry seeds; press the product and then centrifuge, then filter and collect the filtrate to obtain fragrant rapeseed oil. The preparation method of the fragrant rapeseed oil of the present invention can produce the fragrant rapeseed oil with strong flavor and smooth mouthfeel, and can make the fragrant rapeseed oil produced by the traditional frying process free of benzopyrene Or the content does not exceed the national standard, so that the fragrant rapeseed oil is natural, green and healthy.

Description

浓香菜籽油及其制备方法Fragrant rapeseed oil and preparation method thereof

技术领域technical field

本发明属于食品油脂加工技术领域,具体涉及一种浓香菜籽油及其制备方法。The invention belongs to the technical field of food oil processing, and in particular relates to a strong-flavored rapeseed oil and a preparation method thereof.

背景技术Background technique

随着人民生活水平的不断提高,居民的消费观念发生了巨大变化,由以前食用清淡无味的菜籽色拉油转变到食用具有传统浓郁香味的浓香菜籽油,其特有的浓香菜籽油风味—浓郁芳香,口感爽滑,被我国的湖南、湖北、云南、贵州和四川等地区居民所喜爱。With the continuous improvement of people's living standards, great changes have taken place in residents' consumption concepts. They have changed from eating bland and tasteless rapeseed salad oil to eating fragrant rapeseed oil with traditional strong fragrance. Its unique fragrant rapeseed oil Flavor - strong aroma, smooth taste, loved by residents in Hunan, Hubei, Yunnan, Guizhou and Sichuan.

浓香菜籽油风味的产生,主要是菜籽在高温条件下,发生美拉德反应和油脂氧化反应,生成醛、醇、酮和杂环类等小分子气味物质且使油脂颜色加深,加工工艺对浓香菜籽油风味影响显著,经高温蒸炒、压榨获得的预榨毛油中杂环类物质种类和相对含量明显高于其它菜籽油。温度越高,炒制时间越长,获得风味物质也就越多,但随之也会产生致癌物苯并芘。The flavor of fragrant rapeseed oil is mainly due to the Maillard reaction and oil oxidation reaction of rapeseed under high temperature conditions, which generate small molecular odor substances such as aldehydes, alcohols, ketones and heterocyclics, and deepen the color of the oil. Processing The process has a significant impact on the flavor of Luzhou-flavored rapeseed oil, and the types and relative contents of heterocyclic substances in pre-pressed crude oil obtained by high-temperature steaming, frying and pressing are significantly higher than those in other rapeseed oils. The higher the temperature, the longer the frying time, and the more flavor substances will be obtained, but the carcinogen benzopyrene will also be produced.

苯并芘,又名3,4-苯并芘,是世界公认的三大致癌物(亚硝胺、黄曲霉毒素和苯并芘)之一,多项研究表明,苯并芘可以诱导白血病、肺癌、肝癌和乳腺癌的发生,由于苯并芘具有较强的亲脂特性,可通过加工、运输、贮存等途径进入油脂食品。食用植物油中苯并芘的形成机理研究尚未取得较大进展,还不清楚在食用植物油中产生的原因。Benzopyrene, also known as 3,4-benzopyrene, is one of the three major carcinogens (nitrosamines, aflatoxins and benzopyrene) recognized in the world. Many studies have shown that benzopyrene can induce leukemia, The occurrence of lung cancer, liver cancer and breast cancer, because benzopyrene has strong lipophilic properties, can enter oily food through processing, transportation, storage and other ways. The research on the formation mechanism of benzopyrene in edible vegetable oil has not yet made great progress, and the reason for the formation of benzopyrene in edible vegetable oil is still unclear.

目前关于浓香菜籽油专利都集中于其制油和精炼工艺,很少关注在继承传统高温炒籽工艺的同时降低苯并芘含量,保留儿时浓香菜籽油风味。比如:专利申请号201610797438.6一种浓香菜籽油的加工方法和专利申请号201610773485.7中,采用了脱胶、碱炼、脱色、脱臭等工艺处理浓香菜籽油,经过上述工艺处理浓香菜籽油风味和营养物质已大部分流失,专利申请号201210477466.1浓香菜籽油的制取方法,采用低温炒籽工艺,温度在140℃~145℃,这种炒籽工艺制取的浓香菜籽油风味不醇厚,香味较淡,《农产品加工》2011年第1期中,张谦益等学者在《浓香菜籽油制取精制工艺实践》中指出炒籽温度理想值在180℃~200℃之间。专利申请号201510360202.1一种浓香菜籽油的制备方法,为了使制得的浓香菜籽油风味醇厚,采用了高温惰性气体进行加热烘干及干燥处理,此方法生产成本高,且易产生苯并芘,不适合工业化生产。At present, the patents on Luzhou-flavored rapeseed oil are all focused on its oil production and refining process, and little attention has been paid to reducing the content of benzopyrene while inheriting the traditional high-temperature frying process, and retaining the flavor of Luzhou-flavored rapeseed oil in childhood. For example: Patent Application No. 201610797438.6, a processing method of fragrant rapeseed oil and patent application No. 201610773485.7, adopt degumming, alkali refining, decolorization, deodorization and other processes to process fragrant rapeseed oil, and process fragrant rapeseed through the above process Most of the flavor and nutrients of the oil have been lost. Patent Application No. 201210477466.1 The preparation method of Luzhou-flavored rapeseed oil adopts a low-temperature frying process with a temperature of 140°C to 145°C. The Luzhou-flavored rapeseed produced by this frying process The flavor of the oil is not mellow, and the fragrance is relatively light. In the first issue of "Agricultural Products Processing" in 2011, Zhang Qianyi and other scholars pointed out that the ideal temperature for frying seeds is between 180°C and 200°C . Patent Application No. 201510360202.1 A preparation method of Luzhou-flavored rapeseed oil. In order to make the prepared Luzhou-flavored rapeseed oil mellow, a high-temperature inert gas is used for heating, drying and drying treatment. This method has high production costs and is easy to produce Benzopyrene is not suitable for industrial production.

发明内容Contents of the invention

本发明的一个目的在于提出一种浓香菜籽油的制备方法。One object of the present invention is to propose a kind of preparation method of fragrant rapeseed oil.

本发明的浓香菜籽油的制备方法,包括如下步骤:S101:首先将菜籽进行除杂处理,得到干净的菜籽;S102:将茶叶和/或茶叶籽果皮经过超微粉碎处理,然后过筛,再按照料液比为1g:(4mL~8mL)加入软水后进行超声处理,然后过滤并收集滤液;S103:将所述步骤S101得到的菜籽采用雾化着水设备对其进行着所述滤液;S104:将所述步骤S103得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为28℃~30℃,时间为8h~10h;S105:将所述步骤S104得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为180℃~200℃后,进行炒籽;S106:将所述步骤S105得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油。The preparation method of the fragrant rapeseed oil of the present invention comprises the following steps: S101: firstly remove impurities from the rapeseed to obtain clean rapeseed; S102: subject the tea leaves and/or tea seed peels to superfine grinding, and then Sieve, then according to the material-liquid ratio of 1g: (4mL-8mL) add soft water and perform ultrasonic treatment, then filter and collect the filtrate; S103: use atomization watering equipment to treat the rapeseed obtained in the step S101 The filtrate; S104: place the rapeseed obtained in the step S103 in a conditioning tower, and carry out the treatment of the rapeseed; wherein, the temperature of the rapeseed is 28°C-30°C, and the time is 8h-10h; S105: the The product obtained in the step S104 is put into a drum seed frying machine, and then the temperature of the seed frying machine is adjusted to 180°C-200°C, and then the seeds are fried; S106: after pressing the product obtained in the step S105 Centrifuge, then filter and collect the filtrate to obtain fragrant rapeseed oil.

本发明的浓香菜籽油的制备方法,利用废弃的茶叶籽果皮为茶浸提液的原料,对茶叶籽果皮进行回收利用,变废为宝,提升茶叶种植户的收入。由于茶叶和茶叶籽果皮具有多酚、黄酮等生理活性物质,能在高温条件下抑制苯并芘的生成,所以采用浓香制油工艺(高温炒籽)生产出的风味浓郁、口感爽滑的浓香菜籽油同时,又能使采用传统炒籽工艺生产的浓香菜籽油不含苯并芘或者含量不超国标,使浓香菜籽油天然、绿色、健康。The preparation method of the fragrant rapeseed oil of the present invention uses discarded tea seed peel as a raw material of tea extract, recycles the tea seed peel, turns waste into wealth, and increases the income of tea growers. Because tea leaves and tea seed peels contain physiologically active substances such as polyphenols and flavonoids, which can inhibit the formation of benzopyrene under high temperature conditions, the tea with strong flavor and smooth taste is produced by the Luzhou-flavored oil-making process (high-temperature fried seeds) At the same time, the fragrant rapeseed oil can make the fragrant rapeseed oil produced by the traditional frying process not contain benzopyrene or the content does not exceed the national standard, making the fragrant rapeseed oil natural, green and healthy.

本发明的另一个目的在于提出浓香菜籽油的另一种制备方法。Another object of the present invention is to propose another preparation method of fragrant rapeseed oil.

所述浓香菜籽油的制备方法包括如下步骤:S101:首先将菜籽进行除杂处理,得到干净的菜籽;S102:将茶叶和/或茶叶籽果皮置于浸提罐中,然后加入水进行加热浸提,然后过滤并收集滤液;其中,料液比为1:(2~6),浸提温度为40℃~60℃,浸提时间为2h~3h,然后过滤并收集滤液;S103:将所述步骤S101得到的菜籽采用雾化着水设备对其进行着所述滤液;S104:将所述步骤S103得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为28℃~30℃,时间为8h~10h;S105:将所述步骤S104得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为180℃~200℃后,进行炒籽;S106:将所述步骤S105得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油。The preparation method of the fragrant rapeseed oil includes the following steps: S101: firstly remove impurities from the rapeseed to obtain clean rapeseed; S102: put tea leaves and/or tea seed peels in an extraction tank, and then add Heat the water for leaching, then filter and collect the filtrate; wherein, the ratio of solid to liquid is 1:(2-6), the leaching temperature is 40°C-60°C, the leaching time is 2h-3h, then filter and collect the filtrate; S103: Applying the filtrate to the rapeseed obtained in the step S101 using an atomized watering device; S104: placing the rapeseed obtained in the step S103 in a conditioning tower for moistening the rapeseed; wherein , the temperature of moistening rapeseed is 28°C-30°C, and the time is 8h-10h; S105: Put the product obtained in the step S104 into the drum seed frying machine, and then adjust the temperature of the seed frying machine to 180°C-200°C After ℃, fry the seeds; S106: press the product obtained in the step S105, centrifuge, then filter and collect the filtrate to obtain the fragrant rapeseed oil.

另外,本发明的浓香菜籽油的制备方法,还可以具有如下附加的技术特征:In addition, the preparation method of fragrant rapeseed oil of the present invention can also have the following additional technical features:

进一步地,在所述步骤S106中,采用螺旋榨油机进行压榨处理。Further, in the step S106, a screw oil press is used for pressing.

进一步地,在所述步骤S101中,所述除杂处理包括如下步骤:采用振动筛去杂,然后用比重去石机除石。Further, in the step S101, the impurity removal treatment includes the following steps: using a vibrating sieve to remove impurities, and then using a specific gravity stone remover to remove stones.

进一步地,在所述步骤S105中,炒籽时间为30min~60min。Further, in the step S105, the time for frying the seeds is 30 minutes to 60 minutes.

进一步地,所述步骤S103得到的所述菜籽的水分为10%~12%。Further, the moisture content of the rapeseed obtained in the step S103 is 10%-12%.

进一步地,在所述步骤S102中,超声温度为30℃~50℃,超声时间为30min~60min,超声功率为200W~250W。Further, in the step S102, the ultrasonic temperature is 30°C-50°C, the ultrasonic time is 30min-60min, and the ultrasonic power is 200W-250W.

进一步地,所述步骤S101中的菜籽与所述步骤S102中的茶叶和/或茶叶籽果皮的重量比为500:1。Further, the weight ratio of the rapeseed in the step S101 to the tea leaves and/or tea seed peels in the step S102 is 500:1.

本发明的另一个目的在于提出所述的方法制备的浓香菜籽油。Another object of the present invention is to propose the fragrant rapeseed oil prepared by said method.

本发明的附加方面和优点将在下面的描述中部分给出,部分将从下面的描述中变得明显,或通过本发明的实践了解到。Additional aspects and advantages of the invention will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention.

具体实施方式detailed description

下面详细描述本发明的实施例,所述实施例是示例性的,旨在用于解释本发明,而不能理解为对本发明的限制。Embodiments of the present invention are described in detail below, and the embodiments are exemplary and intended to explain the present invention, but should not be construed as limiting the present invention.

实施例1Example 1

实施例1提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 1 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先采用振动筛去杂,然后用比重去石机除石,得到干净的菜籽。(1) First use a vibrating sieve to remove impurities, and then use a specific gravity stoner to remove stones to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮经过超微粉碎处理,然后过筛,再按照料液比为1g:4mL加入软水后进行超声处理,然后过滤并收集滤液,超声温度为50℃,超声时间为30min,超声功率为250W。其中,所述步骤(1)中的菜籽与所述步骤(2)中的茶叶和/或茶叶籽果皮的重量比为500:1。(2) Ultrafine pulverize the tea leaves and/or tea seed peels, then sieve, add soft water according to the solid-liquid ratio of 1g: 4mL, and then perform ultrasonic treatment, then filter and collect the filtrate. The ultrasonic temperature is 50°C. The time is 30min, and the ultrasonic power is 250W. Wherein, the weight ratio of the rapeseed in the step (1) to the tea leaves and/or tea seed peels in the step (2) is 500:1.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液,最终得到水分为10%的菜籽。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by means of atomizing watering equipment, and finally the rapeseed with a water content of 10% is obtained.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为30℃,时间为8h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 30° C., and the time is 8 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为200℃后,进行炒籽,炒籽时间为30min。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 200° C., and then fry the seeds for 30 minutes.

(6)采用螺旋榨油机将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量2.3μg/kg。(6) The product obtained in the step (5) was squeezed by a screw press and then centrifuged, then filtered and the filtrate was collected to obtain Luzhou-flavored rapeseed oil with a benzopyrene content of 2.3 μg/kg.

实施例2Example 2

实施例2提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 2 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先采用振动筛去杂,然后用比重去石机除石,得到干净的菜籽。(1) First use a vibrating sieve to remove impurities, and then use a specific gravity stoner to remove stones to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮经过超微粉碎处理,然后过筛,再按照料液比为1g:8mL加入软水后进行超声处理,然后过滤并收集滤液,超声温度为30℃,超声时间为60min,超声功率为200W。其中,所述步骤(1)中的菜籽与所述步骤(2)中的茶叶和/或茶叶籽果皮的重量比为500:1。(2) Ultrafine pulverize the tea leaves and/or tea seed peels, then sieve, add soft water according to the solid-liquid ratio of 1g: 8mL, and then perform ultrasonic treatment, then filter and collect the filtrate, the ultrasonic temperature is 30°C, ultrasonic The time is 60min, and the ultrasonic power is 200W. Wherein, the weight ratio of the rapeseed in the step (1) to the tea leaves and/or tea seed peels in the step (2) is 500:1.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液,最终得到水分为12%的菜籽。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by means of an atomized watering device, and finally the rapeseed with a water content of 12% is obtained.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为28℃,时间为10h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 28° C., and the time is 10 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为180℃后,进行炒籽,炒籽时间为60min。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 180° C., and then fry the seeds for 60 minutes.

(6)采用螺旋榨油机将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量1.5μg/kg。(6) Press the product obtained in the step (5) by using a screw press, centrifuge, then filter and collect the filtrate to obtain Luzhou-flavored rapeseed oil with a benzopyrene content of 1.5 μg/kg.

实施例3Example 3

实施例3提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 3 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先采用振动筛去杂,然后用比重去石机除石,得到干净的菜籽。(1) First use a vibrating sieve to remove impurities, and then use a specific gravity stoner to remove stones to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮经过超微粉碎处理,然后过筛,再按照料液比为1g:6mL加入软水后进行超声处理,然后过滤并收集滤液,超声温度为40℃,超声时间为45min,超声功率为225W。(2) Ultrafine pulverize the tea leaves and/or tea seed peels, then sieve, add soft water according to the solid-liquid ratio of 1g: 6mL, and then perform ultrasonic treatment, then filter and collect the filtrate, the ultrasonic temperature is 40°C, ultrasonic The time is 45min, and the ultrasonic power is 225W.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液,最终得到水分为11%的菜籽。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by means of an atomized watering device, and finally the rapeseed with a water content of 11% is obtained.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为29℃,时间为9h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 29° C., and the time is 9 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为190℃后,进行炒籽,炒籽时间为45min。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 190° C., and then fry the seeds for 45 minutes.

(6)采用螺旋榨油机将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量1.6μg/kg。(6) The product obtained in the step (5) was squeezed by a screw press and then centrifuged, then filtered and the filtrate was collected to obtain Luzhou-flavored rapeseed oil with a benzopyrene content of 1.6 μg/kg.

实施例4Example 4

实施例4提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 4 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先将菜籽进行除杂处理,得到干净的菜籽。(1) Firstly, the rapeseed is subjected to impurity removal treatment to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮置于浸提罐中,然后加入水进行加热浸提,然后过滤并收集滤液;其中,料液比为1:2,浸提温度为60℃,浸提时间为2h,然后过滤并收集滤液。(2) Put tea leaves and/or tea seed peels in an extraction tank, then add water for heating and extraction, then filter and collect the filtrate; wherein, the ratio of solid to liquid is 1:2, the extraction temperature is 60°C, and the extraction temperature is 60°C. The extraction time was 2h, then filtered and the filtrate was collected.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by using an atomization watering device.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为30℃,时间为8h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 30° C., and the time is 8 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为200℃后,进行炒籽。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 200° C., and then fry the seeds.

(6)将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量2.0μg/kg。(6) Pressing the product obtained in step (5) and then centrifuging, then filtering and collecting the filtrate to obtain fragrant rapeseed oil with a benzopyrene content of 2.0 μg/kg.

实施例5Example 5

实施例5提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 5 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先将菜籽进行除杂处理,得到干净的菜籽。(1) Firstly, the rapeseed is subjected to impurity removal treatment to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮置于浸提罐中,然后加入水进行加热浸提,然后过滤并收集滤液;其中,料液比为1:6,浸提温度为40℃,浸提时间为3h,然后过滤并收集滤液。(2) Put the tea leaves and/or tea seed peels in an extraction tank, then add water for heating and extraction, then filter and collect the filtrate; wherein, the ratio of solid to liquid is 1:6, the extraction temperature is 40°C, and the extraction temperature is 40°C. The extraction time was 3h, then filtered and the filtrate was collected.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by using an atomization watering device.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为28℃,时间为10h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 28° C., and the time is 10 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为180℃后,进行炒籽。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 180° C., and then fry the seeds.

(6)将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量1.8μg/kg。(6) The product obtained in the step (5) was squeezed and then centrifuged, then filtered and the filtrate was collected to obtain fragrant rapeseed oil with a benzopyrene content of 1.8 μg/kg.

实施例6Example 6

实施例6提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 6 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)首先将菜籽进行除杂处理,得到干净的菜籽。(1) Firstly, the rapeseed is subjected to impurity removal treatment to obtain clean rapeseed.

(2)将茶叶和/或茶叶籽果皮置于浸提罐中,然后加入水进行加热浸提,然后过滤并收集滤液;其中,料液比为1:4,浸提温度为50℃,浸提时间为2.5h,然后过滤并收集滤液。(2) Put the tea leaves and/or tea seed peels in an extraction tank, then add water for heating and extraction, then filter and collect the filtrate; wherein, the ratio of solid to liquid is 1:4, the extraction temperature is 50°C, and the extraction temperature is 50°C. The extraction time was 2.5h, then filtered and the filtrate was collected.

(3)将所述步骤(1)得到的菜籽采用雾化着水设备对其进行着所述滤液。(3) The rapeseed obtained in the step (1) is subjected to the filtrate by using an atomization watering device.

(4)将所述步骤(3)得到的菜籽放置于调质塔中,进行润菜籽处理;其中,润菜籽温度为29℃,时间为9h。(4) The rapeseed obtained in the step (3) is placed in a tempering tower, and the rapeseed is moistened; wherein, the temperature of the rapeseed is 29° C., and the time is 9 hours.

(5)将所述步骤(4)得到的产物放入滚筒炒籽机中,然后调节所述炒籽机的温度为190℃后,进行炒籽。(5) Put the product obtained in the step (4) into a drum seed frying machine, then adjust the temperature of the seed frying machine to 190° C., and then fry the seeds.

(6)将所述步骤(5)得到的产物进行压榨处理后离心分离,然后过滤并收集滤液,得到浓香菜籽油,苯并芘含量2.2μg/kg。(6) Centrifuge the product obtained in the step (5) after pressing, then filter and collect the filtrate to obtain fragrant rapeseed oil with a benzopyrene content of 2.2 μg/kg.

实施例7Example 7

实施例7提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 7 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)选取菜籽水分含量7.5%,经过振动筛去杂、比重去石机除石等工艺,得到干净的500kg菜籽。(1) Select the rapeseed with a moisture content of 7.5%, and obtain 500 kg of clean rapeseed through processes such as vibrating sieve to remove impurities and specific gravity stoner to remove stone.

(2)称取木姜叶柯甜茶茶叶1kg放置于浸提罐中在料液比1:6,浸提温度60℃,浸提时间2h的条件下浸提并收集滤液。(2) Weigh 1 kg of the leaves of Ketian tea leaves and place them in an extraction tank for extraction under the conditions of a solid-to-liquid ratio of 1:6, an extraction temperature of 60°C, and an extraction time of 2 hours, and collect the filtrate.

(3)采用雾化着水设备,对菜籽进行着木姜叶柯甜茶茶叶浸提水溶液,要求菜籽着水后水分控制在11%,着水后的菜籽放置于调质塔中,进行润菜籽处理,润菜籽时间:在温度30℃条件下,需要9h。(3) Using atomized watering equipment, the rapeseeds are subjected to the aqueous extract of Mujiangye Ketian tea. It is required that the water content of the rapeseeds be controlled at 11%. Rapeseed treatment, time to moisten rapeseed: 9 hours at a temperature of 30°C.

(4)将润菜籽后的原料输送到滚筒炒籽机,控制炒籽温度190℃,炒籽时间30min后用刮板输送机输送到螺旋榨油机进压榨处理后低温离心,得到浓香菜籽油,苯并芘含量1.5μg/kg。(4) Transport the raw materials after moistening the rapeseed to the drum seed frying machine, control the frying temperature at 190°C, and use the scraper conveyor to transport the seed to the screw oil press after 30 minutes of frying time, then press and centrifuge at low temperature to obtain a strong aroma Rapeseed oil, benzopyrene content 1.5μg/kg.

实施例8Example 8

实施例8提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 8 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)选取菜籽水分含量7%,经过振动筛去杂、比重去石机除石等工艺,得到干净的500kg菜籽。(1) Select rapeseed with a moisture content of 7%, and obtain clean 500kg rapeseed through processes such as vibrating sieve to remove impurities and specific gravity stoner to remove stone.

(2)称取茶叶籽果皮1kg放置于浸提罐中在料液比1:4,浸提温度60℃,浸提时间2h的条件下浸提并收集滤液。(2) Weigh 1 kg of tea seed peel and place it in an extraction tank to extract and collect the filtrate under the conditions of a solid-to-liquid ratio of 1:4, an extraction temperature of 60°C, and an extraction time of 2 hours.

(3)采用雾化着水设备,对菜籽进行着茶叶籽果皮浸提水溶液,要求菜籽着水后水分控制在12%,着水后的菜籽放置于调质塔中,进行润菜籽处理,润菜籽时间:在温度30℃条件下,需要8h。(3) Use atomized watering equipment to extract the aqueous solution of tea seed peel on the rapeseed. It is required to control the water content of the rapeseed at 12% after watering, and place the watered rapeseed in the conditioning tower to moisten the vegetables Seed treatment, time for moistening rapeseed: 8 hours at a temperature of 30°C.

(4)将润菜籽后的原料输送到滚筒炒籽机,控制炒籽温度190℃,炒籽时间30min后用刮板输送机输送到螺旋榨油机进压榨处理后低温离心,得到浓香菜籽油,苯并芘含量2.5μg/kg。(4) Transport the raw materials after moistening the rapeseed to the drum seed frying machine, control the frying temperature at 190°C, and use the scraper conveyor to transport the seed to the screw oil press after 30 minutes of frying time, then press and centrifuge at low temperature to obtain a strong aroma Rapeseed oil, benzopyrene content 2.5μg/kg.

实施例9Example 9

实施例9提出了一种浓香菜籽油的制备方法,包括如下步骤:Embodiment 9 proposes a kind of preparation method of fragrant rapeseed oil, comprises the steps:

(1)选取菜籽水分含量8%,经过振动筛去杂、比重去石机除石等工艺,得到干净的500kg菜籽。(1) Select rapeseed with a moisture content of 8%, and obtain clean 500kg rapeseed through processes such as vibrating sieve to remove impurities and specific gravity stoner to remove stone.

(2)称取碣滩茶1kg放置于浸提罐中在料液比1:5,浸提温度60℃,浸提时间2h的条件下浸提并收集滤液。(2) Weigh 1 kg of Jietan tea and place it in an extraction tank for extraction under the conditions of a solid-to-liquid ratio of 1:5, an extraction temperature of 60°C, and an extraction time of 2 hours, and collect the filtrate.

(3)采用雾化着水设备,对菜籽进行着碣滩茶茶叶浸提水溶液,要求菜籽着水后水分控制在11%,着水后的菜籽放置于调质塔中,进行润菜籽处理,润菜籽时间:在温度30℃条件下,需要9h。(3) Using atomization watering equipment, the rapeseeds are soaked in the Jietan tea tea extraction aqueous solution, and the water content of the rapeseeds after watering is required to be controlled at 11%, and the watered rapeseeds are placed in the conditioning tower for moistening Rapeseed treatment, time to moisten rapeseed: 9 hours at a temperature of 30°C.

(4)将润菜籽后的原料输送到滚筒炒籽机,控制炒籽温度190℃,炒籽时间30min后用刮板输送机输送到螺旋榨油机进压榨处理后低温离心,得到浓香菜籽油,苯并芘含量2.0μg/kg。(4) Transport the raw materials after moistening the rapeseed to the drum seed frying machine, control the frying temperature at 190°C, and use the scraper conveyor to transport the seed to the screw oil press after 30 minutes of frying time, then press and centrifuge at low temperature to obtain a strong aroma Rapeseed oil, benzopyrene content 2.0μg/kg.

以下采用三种制取浓香菜籽油的方法进行对比:Adopt three kinds of methods of preparing fragrant rapeseed oil to compare below:

A方法:采用低温炒籽的方法进行制取取(不经过着水和润菜籽处理后),其中,菜籽含水量9%,采用炒籽温度160℃,炒籽时间30min的条件进行压榨处理。Method A: use the method of frying seeds at low temperature to produce (without watering and moistening the rapeseed), wherein the water content of the rapeseed is 9%, and the temperature of the seeds is 160°C, and the time for frying the seeds is 30 minutes. deal with.

B方法:采用传统的方法进行制取(不经过着水和润菜籽处理后),其中,菜籽含水量9%,采用炒籽温度190℃,炒籽时间30min的条件进行压榨处理。Method B: the traditional method is used for production (without watering and moistening the rapeseed), wherein the water content of the rapeseed is 9%, and the frying temperature is 190° C., and the frying time is 30 minutes for pressing.

C方法:采用实施例3的方法进行提取,其中,菜籽含水量9%,采用木姜叶柯甜茶茶叶浸提液进行着水和润菜籽处理后水分含量12%,炒籽温度190℃,炒籽时间30min的条件进行压榨处理。Method C: use the method in Example 3 to extract, wherein the rapeseed has a water content of 9%, and the water content of the rapeseed is 12% after the water and moistening of the rapeseed is carried out with the tea extract of Mujiangyeke sweet tea. The temperature of the fried seeds is 190°C. The pressing process was carried out under the condition of seed time 30min.

采用三种制油方法得到的浓香菜籽油理化指标如表1所示:The physical and chemical indicators of the strong fragrant rapeseed oil obtained by three kinds of oil production methods are shown in Table 1:

表1:三种处理方法得到的浓香菜籽油理化指标Table 1: Physicochemical indicators of fragrant rapeseed oil obtained by three processing methods

从表1可以得到C方法采用本专利制得的浓香菜籽油不仅苯并芘含量最低为1.5μg/kg,过氧化值为2mmol/kg,而且风味浓郁、醇厚,口感爽滑,品质最好;A方法的菜籽油由于采用低温炒籽工艺,油风味不浓郁,且苯并芘含量高4μg/kg;B方法采用传统浓香菜籽制油工艺高温炒籽,制得的浓香菜籽油虽然风味浓郁、醇厚,但其苯并芘含量最高达12μg/kg,超国标10μg/kg。From Table 1, it can be obtained that the fragrant rapeseed oil prepared by method C using this patent not only has a minimum benzopyrene content of 1.5 μg/kg, and a peroxide value of 2 mmol/kg, but also has a rich and mellow flavor, a smooth taste, and the best quality. Good; because the rapeseed oil of method A adopts the low-temperature frying process, the oil flavor is not strong, and the content of benzopyrene is 4 μg/kg; the method B adopts the traditional aroma rapeseed oil production process and high-temperature frying seeds, and the obtained aroma Although rapeseed oil has a rich and mellow flavor, its benzopyrene content is as high as 12 μg/kg, exceeding the national standard of 10 μg/kg.

随机选取18个正常成年人进行试验,平均分成6组,每天分别食用采用所述实施例1-6的浓香菜籽油烹饪的食物,每天采用30g的浓香菜籽油进行烹饪,一个月后,检测试验人员体内胆固醇(TC)和甘油三酯(TG)的含量。详见表2。Randomly select 18 normal adults for the test, divide them into 6 groups on average, eat the food cooked with the fragrant rapeseed oil of the embodiments 1-6 every day, and cook with the fragrant rapeseed oil of 30g every day, for one month Afterwards, the content of cholesterol (TC) and triglyceride (TG) in the test personnel's body was detected. See Table 2 for details.

表2:食用各实施例浓香菜籽油烹饪的食物前后的TC、TG含量Table 2: TC and TG contents before and after eating the food cooked with fragrant rapeseed oil in each embodiment

从表2可以看出,在食用本发明实施例1~6的浓香菜籽油烹饪食物后,试验人员体内的胆固醇(TC)和甘油三酯(TG)的含量都没有明显的增加,尤其是在食用实施例4-6的浓香菜籽油烹饪食物后,试验人员体内的胆固醇(TC)和甘油三酯(TG)的含量都有明显下降,说明实施例4~6采用加热浸提法制备的浓香菜籽油可以调节机体功能,降低胆固醇和血脂等。As can be seen from Table 2, after eating the fragrant rapeseed oil cooking food of Examples 1 to 6 of the present invention, the content of cholesterol (TC) and triglyceride (TG) in the tester's body does not increase significantly, especially It is after eating the fragrant rapeseed oil cooking food of embodiment 4-6, the content of cholesterol (TC) and triglyceride (TG) in the tester's body all have obvious decline, illustrate that embodiment 4-6 adopts heating extraction The fragrant rapeseed oil prepared by this method can regulate body functions, lower cholesterol and blood fat, etc.

本发明的浓香菜籽油的制备方法,利用废弃的茶叶籽果皮为茶浸提液的原料,对茶叶籽果皮进行回收利用,变废为宝,提升茶叶种植户的收入。由于茶叶和茶叶籽果皮具有多酚、黄酮等生理活性物质,能在高温条件下抑制苯并芘的生成,所以采用浓香制油工艺(高温炒籽)生产出的风味浓郁、口感爽滑的浓香菜籽油同时,又能使采用传统炒籽工艺生产的浓香菜籽油不含苯并芘或者含量不超国标,使浓香菜籽油天然、绿色、健康。The preparation method of the fragrant rapeseed oil of the present invention uses discarded tea seed peel as a raw material of tea extract, recycles the tea seed peel, turns waste into wealth, and increases the income of tea growers. Because tea leaves and tea seed peels contain physiologically active substances such as polyphenols and flavonoids, which can inhibit the formation of benzopyrene under high temperature conditions, the tea with strong flavor and smooth taste is produced by the Luzhou-flavored oil-making process (high-temperature fried seeds) At the same time, the fragrant rapeseed oil can make the fragrant rapeseed oil produced by the traditional frying process not contain benzopyrene or the content does not exceed the national standard, making the fragrant rapeseed oil natural, green and healthy.

在本说明书的描述中,参考术语“一个实施例”、“一些实施例”、“示例”、“具体示例”、或“一些示例”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或者特点包含于本发明的至少一个实施例或示例中。在本说明书中,对上述术语的示意性表述不必须针对的是相同的实施例或示例。而且,描述的具体特征、结构、材料或者特点可以在任一个或多个实施例或示例中以合适的方式结合。此外,在不相互矛盾的情况下,本领域的技术人员可以将本说明书中描述的不同实施例或示例以及不同实施例或示例的特征进行结合和组合。In the description of this specification, descriptions with reference to the terms "one embodiment", "some embodiments", "example", "specific examples", or "some examples" mean that specific features described in connection with the embodiment or example , structure, material or feature is included in at least one embodiment or example of the present invention. In this specification, the schematic representations of the above terms are not necessarily directed to the same embodiment or example. Furthermore, the described specific features, structures, materials or characteristics may be combined in any suitable manner in any one or more embodiments or examples. In addition, those skilled in the art can combine and combine different embodiments or examples and features of different embodiments or examples described in this specification without conflicting with each other.

尽管上面已经示出和描述了本发明的实施例,可以理解的是,上述实施例是示例性的,不能理解为对本发明的限制,本领域的普通技术人员在本发明的范围内可以对上述实施例进行变化、修改、替换和变型。Although the embodiments of the present invention have been shown and described above, it can be understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and those skilled in the art can make the above-mentioned The embodiments are subject to changes, modifications, substitutions and variations.

Claims (9)

1. a kind of preparation method of giving off a strong fragrance rapeseed oil, it is characterised in that comprise the following steps:
S101:Vegetable seed is subjected to removal of impurities processing first, obtains clean vegetable seed;
S102:Tealeaves and/or tea seeds pericarp are handled by ultramicro grinding, then sieves, is 1g according still further to solid-liquid ratio:(4mL ~8mL) add soft water after be ultrasonically treated, then filter and collect filtrate;
S103:The vegetable seed that the step S101 is obtained carries out the filtrate using atomizing-dampening system equipment to it;
S104:The obtained vegetable seed of the step S103 is positioned in tempering tower, carries out moistening vegetable seed processing;Wherein, vegetable seed temperature is moistened Spend for 28 DEG C~30 DEG C, the time is 8h~10h;
S105:The obtained products of the step S104 are put into roller seeds frying machine, the temperature for then adjusting the seeds frying machine is After 180 DEG C~200 DEG C, stir-fry seed is carried out;
S106:Centrifuged after the obtained products of the step S105 are carried out into squeezing processing, then filter and collect filtrate, obtain To giving off a strong fragrance rapeseed oil.
2. a kind of preparation method of giving off a strong fragrance rapeseed oil, it is characterised in that comprise the following steps:
S101:Vegetable seed is subjected to removal of impurities processing first, obtains clean vegetable seed;
S102:Tealeaves and/or tea seeds pericarp are placed in pot for solvent extraction, water is then added and carries out heating extraction, then filter simultaneously Collect filtrate;Wherein, solid-liquid ratio 1:(2~6), extraction temperature are 40 DEG C~60 DEG C, and extraction time is 2h~3h, is then filtered And collect filtrate;
S103:The vegetable seed that the step S101 is obtained carries out the filtrate using atomizing-dampening system equipment to it;
S104:The obtained vegetable seed of the step S103 is positioned in tempering tower, carries out moistening vegetable seed processing;Wherein, vegetable seed temperature is moistened Spend for 28 DEG C~30 DEG C, the time is 8h~10h;
S105:The obtained products of the step S104 are put into roller seeds frying machine, the temperature for then adjusting the seeds frying machine is After 180 DEG C~200 DEG C, stir-fry seed is carried out;
S106:Centrifuged after the obtained products of the step S105 are carried out into squeezing processing, then filter and collect filtrate, obtain To giving off a strong fragrance rapeseed oil.
3. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1 or 2, it is characterised in that in the step S106, Squeezing processing is carried out using screw oil expeller.
4. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1 or 2, it is characterised in that in the step S101, The removal of impurities processing comprises the following steps:Using vibratory sieve impurity elimination, then stone is removed with specific-gravity stoner.
5. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1 or 2, it is characterised in that in the step S105, The stir-fry seed time is 30min~60min.
6. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1 or 2, it is characterised in that the step S103 is obtained The vegetable seed moisture be 10%~12%.
7. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1, it is characterised in that in the step S102, surpass Sound temperature is 30 DEG C~50 DEG C, and ultrasonic time is 30min~60min, and ultrasonic power is 200W~250W.
8. the preparation method of giving off a strong fragrance rapeseed oil according to claim 1 or 2, it is characterised in that in the step S101 Vegetable seed is 500 with the tealeaves in the step S102 and/or the weight ratio of tea seeds pericarp:1.
9. giving off a strong fragrance rapeseed oil prepared by the method described in claim any one of 1-8.
CN201710805922.3A 2017-09-08 2017-09-08 Giving off a strong fragrance rapeseed oil and preparation method thereof Pending CN107460034A (en)

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CN104694243A (en) * 2015-02-13 2015-06-10 安徽嘉旗粮油工程技术有限公司 Method for preparing aromatic rapeseed oil
CN106554847A (en) * 2016-11-25 2017-04-05 威海恒基伟业信息科技发展有限公司 A kind of preparation method of tea-polyphenol-enrictea tea oil
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CN104694243A (en) * 2015-02-13 2015-06-10 安徽嘉旗粮油工程技术有限公司 Method for preparing aromatic rapeseed oil
CN106554847A (en) * 2016-11-25 2017-04-05 威海恒基伟业信息科技发展有限公司 A kind of preparation method of tea-polyphenol-enrictea tea oil
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Application publication date: 20171212