CN107455632A - A kind of young coal degradation solution flavor beverage - Google Patents
A kind of young coal degradation solution flavor beverage Download PDFInfo
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- CN107455632A CN107455632A CN201710450040.XA CN201710450040A CN107455632A CN 107455632 A CN107455632 A CN 107455632A CN 201710450040 A CN201710450040 A CN 201710450040A CN 107455632 A CN107455632 A CN 107455632A
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- 230000015556 catabolic process Effects 0.000 title claims abstract description 86
- 238000006731 degradation reaction Methods 0.000 title claims abstract description 86
- 239000003245 coal Substances 0.000 title claims abstract description 71
- 235000013361 beverage Nutrition 0.000 title claims abstract description 61
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 47
- 235000019634 flavors Nutrition 0.000 title claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000002360 preparation method Methods 0.000 claims abstract description 12
- 239000012153 distilled water Substances 0.000 claims abstract description 11
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 7
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 7
- 239000008103 glucose Substances 0.000 claims abstract description 7
- 239000001814 pectin Substances 0.000 claims abstract description 7
- 235000010987 pectin Nutrition 0.000 claims abstract description 7
- 229920001277 pectin Polymers 0.000 claims abstract description 7
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims abstract description 7
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims abstract description 7
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000661 sodium alginate Substances 0.000 claims abstract description 6
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 6
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 6
- 238000006243 chemical reaction Methods 0.000 claims description 29
- 239000007788 liquid Substances 0.000 claims description 27
- 239000002817 coal dust Substances 0.000 claims description 12
- 239000006228 supernatant Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 9
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 238000001704 evaporation Methods 0.000 claims description 6
- 230000008020 evaporation Effects 0.000 claims description 6
- 239000012286 potassium permanganate Substances 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 abstract description 15
- 238000000034 method Methods 0.000 abstract description 11
- 235000012976 tarts Nutrition 0.000 abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 6
- 238000011049 filling Methods 0.000 abstract description 6
- 210000004907 gland Anatomy 0.000 abstract description 6
- 235000013305 food Nutrition 0.000 abstract description 3
- 235000009508 confectionery Nutrition 0.000 abstract description 2
- 238000007872 degassing Methods 0.000 abstract description 2
- 230000008447 perception Effects 0.000 abstract description 2
- 230000001954 sterilising effect Effects 0.000 abstract 1
- 238000004659 sterilization and disinfection Methods 0.000 abstract 1
- 239000003077 lignite Substances 0.000 description 15
- 238000012360 testing method Methods 0.000 description 14
- 239000007800 oxidant agent Substances 0.000 description 11
- 230000001590 oxidative effect Effects 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 230000036528 appetite Effects 0.000 description 7
- 235000019789 appetite Nutrition 0.000 description 7
- 230000003647 oxidation Effects 0.000 description 7
- 238000007254 oxidation reaction Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 238000000265 homogenisation Methods 0.000 description 5
- 238000002390 rotary evaporation Methods 0.000 description 5
- 238000004062 sedimentation Methods 0.000 description 5
- 238000000926 separation method Methods 0.000 description 5
- 239000003381 stabilizer Substances 0.000 description 5
- 235000021393 food security Nutrition 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 150000007524 organic acids Chemical class 0.000 description 3
- 241000894007 species Species 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 239000003415 peat Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 235000021419 vinegar Nutrition 0.000 description 2
- 239000000052 vinegar Substances 0.000 description 2
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 1
- 239000004342 Benzoyl peroxide Substances 0.000 description 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 1
- 230000010718 Oxidation Activity Effects 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 235000019400 benzoyl peroxide Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000013409 condiments Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 239000004021 humic acid Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 238000010525 oxidative degradation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000005648 plant growth regulator Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Tea And Coffee (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The present invention discloses a kind of young coal degradation solution flavor beverage, the flavor beverage component and percentage by weight are young coal degradation solution 30% 70%, glucose 3% 9%, pectin 0.01% 0.03%, sodium carboxymethylcellulose 0.02% 0.06%, sodium alginate 0.02% 0.04%, and surplus is distilled water；Homogeneous is carried out after each raw material is well mixed in proportion, filling while hot, degassing, gland, sterilization treatment, obtains flavor beverage product；Unlike the prior art, the degradation solution pH value produced is lower, tart flavour is more mellow, is more suitable for for preparing flavor beverage for the preparation method of young coal degradation solution；The beverage flavour is fragrant and sweet tasty and refreshing, tart flavour alcohol and thick and heavy, unique flavor；And water white transparency, perception are tempting；Young coal degradation solution is applied in field of food first, formula is simple, process, it is easy to accomplish industrialization, have a extensive future.
Description
Technical field
The present invention relates to a kind of young coal degradation solution flavor beverage, belong to field of food.
Background technology
Researcher prepares a kind of colourless when carrying out oxidative degradation to the young coal such as lignite, peat with oxidant
Bright distillate, its pH value have tart flavour between 2.0 to 2.6, are referred to as young coal degradation solution.The degraded liquid and preparation method thereof
And applied for national inventing patent as the application of plant growth regulator, and authorized（A kind of " life of young coal degradation solution
Production method and application thereof ", application number 201410006333.5）, it is stronger that the degradation solution tastes tart flavour, there is a kind of natural vegetation
Fragrance, unique flavor, and drink before the meal and have the function that significantly to whet the appetite, improve appetite.
Constituent analysis finds, containing substantial amounts of various small molecular organic acid classes in young coal degradation solution, makes the solution be in integrally
Faintly acid, also contain a small amount of small molecular alcohol and esters in addition；Although contained small molecule huge number, respective relative amount pole
Low, total content is also extremely low, and solution density is 1.01 to 1.05g/cm3Between, it is almost identical with pure water；Meanwhile chemical composition point
Analysis is also not detected by any toxicant（J. Chem. Pharm. Res., 2014, 6: 2456-2459）.Except with nothing
Color is transparent, single flash liquid, without heavy metal, without microorganism, natural tart flavour, the features such as appetite, same to vinegar, apple vinegar can be improved
Compared etc. the condiment or beverage that can whet the appetite, have plenty of mixed organic acid contained by the young coal degradation solution, acid ingredient species is rich
Richness, tart flavour alcohol and, suitable for directly drinking.
However, existing young coal degradation solution technology of preparing（Number of patent application：201410006333.5）Using to three kinds
Oxidant, their common feature is oxidation activity height, violent with the reaction of young coal, but oxidant is in itself or its reduzate tool
There is volatility, may be entered with vapor in degradation solution；To reduce the severe degree of reaction, ensure the peace of course of reaction
Entirely, anticatalyst and stabilizer need to be added into reaction system, these chemical substances may also influence the pure property of degradation solution, very
To mouthfeel is influenceed, its value used as raw-food material or additive is reduced.
The content of the invention
The young coal degraded liquid and preparation method thereof of the present invention compared with prior art, changes the species of oxidant, and use
Multi-level combined oxidation technology, does not add anticatalyst and stabilizer can be achieved with the safety and stability progress of course of reaction, completely
Volatile chemical reagent is not introduced, adds the security of product, while original oxidation effectiveness is ensured, makes degradation solution pH
Value reduces, and concentration effectively improves, tart flavour more alcohol and it is thick and heavy, do not stimulate, be more suitable for preparing flavor beverage.
It is an object of the invention to provide a kind of young coal degradation solution flavor beverage, the component and percentage by weight of the beverage are
Young coal degradation solution 30%-70%, glucose 3%-9%, pectin 0.01%-0.03%, sodium carboxymethylcellulose 0.02%-0.06%, sea
Mosanom 0.02%-0.04%, surplus are distilled water.
The preparation method of the young coal degradation solution flavor beverage, is comprised the concrete steps that：After various auxiliary materials are weighed, with distillation
Water dissolves, and stands, is added to after filtering in young coal degradation solution；Deployed liquid is subjected to homogeneous, homogenization pressure 20-25
MPa, 70-80 DEG C of temperature, homogeneous 2 times, each 5-6 min；Filling while hot after homogeneous, degassing, gland, under the conditions of 90-100 DEG C
Sterilize 30-40 min, and young coal degradation solution flavor beverage is made after cooling.
The preparation method of the young coal degradation solution, is comprised the following steps that：
By young coal（Lignite or peat）It is 5%-15% to be dried to moisture, and 200 mesh sieves are crossed after crushing, and coal dust is standby；By coal dust matter
The potassium permanganate of amount 9.6% is dissolved in the deionized water of 2 times of quality of pc, adds coal dust, 20 DEG C -30 DEG C are sufficiently stirred reaction
After 3h, the potassium bichromate of quality of pc 16.2% is added, 50 DEG C -60 DEG C are stirred for reacting 1h, are stored at room temperature reaction 12h, carry out liquid
Gu sedimentation separation；Upper strata stands liquid and centrifuges 10min under 5000r/min, supernatant is obtained, by supernatant vacuum filter, filtrate
In 65 DEG C of concentrated by rotary evaporations, the evaporation condensate for obtaining water white transparency is young coal degradation solution.
The preparation method and prior art of the young coal degradation solution（Number of patent application：201410006333.5）Difference,
The 2.0-2.6 of the pH value of degradation solution from the prior art can be reduced to 1.4-2.0, density is from 1.01-1.05g/cm3Improve
To 1.03-1.09g/cm3, it has following some innovation or different compared with prior art：
（1）Oxidant is influence factor most crucial in degradation solution production technology, and except hydrogen peroxide, prior art uses another
Two kinds of oxidants（Benzoyl peroxide, Peracetic acid）It is organic molecule oxidant, oxidant is in itself or its catabolite
It may be volatilized to enter into steam in degradation solution, degradation solution is polluted；Present invention process uses inorganic oxidizer completely, its
Itself or catabolite will not be volatilized to enter into degradation solution with steam, ensure that the purity of degradation solution.
（2）Three kinds of oxidizing performances that prior art uses are high, violent with the reaction of young coal, to reduce the play of reaction
Strong degree, ensure the safety of course of reaction, anticatalyst and stabilizer need to be added into reaction system, these chemical substances also can
Cause the pollution of degradation solution；The technique of the present invention uses multi-level combined oxidation technology, first using the condition and oxidant relaxed
Slowly aoxidized, then change oxidant and reaction condition gradually deepens degree of oxidation, make coal sample oxidation more thorough；The first step
After oxidation, the amount of acidic substances such as humic acid increase in solution, cause pH value of reaction system to reduce and be advantageous to improve second step oxygen
The oxidation susceptibility of agent potassium bichromate；Meanwhile because course of reaction need not gently add anticatalyst and stabilizer；The present invention's
Technique adds the content and species of organic acid in product, effectively reduces degradation solution pH value, improves mouthfeel, makes product more suitable
Preferably prepare beverage.
（3）Other technological parameters are optimized and standardized, makes the quality of degradation solution more stable, saves cost
And the time, to ensureing that the stay in grade of beverage is significant.
The innovation of the present invention and advantage：
（1）Innovate young coal degraded liquid preparing process and standardized；New technique can increase degradation solution small molecular thing
The content of matter, makes solution ph effectively reduce, and density rise, mouthfeel is improved, security increase, is more suitable for preparing flavor drink
Material.
（2）Young coal degradation solution is fabricated to flavor beverage product, takes full advantage of degradation solution water white transparency, single flash
Liquid, without heavy metal, without microorganism, have natural mellow tart flavour, the own characteristics such as appetite can be improved, only with the addition of in formula sugar and
Stabilizer, the natural character of raw material is greatly maintained, be its optimal edible way；Young coal degradation solution is in field of food
It is pioneering using category.
（3）Drink formula is simple, and quality is easily controlled, reliable preparation process；Tart flavour alcohol and it is thick and heavy, do not stimulate, flavour is fragrant
Sweet tea is tasty, unique flavor；And water white transparency, perception are tempting；There is increase gastric acidity simultaneously, the work(for appetite of whetting the appetite, improve
Effect；Without preservative, pigment, it is adapted to drink for a long time, has no side effect.
Embodiment
The present invention is described in further detail below by embodiment, but the scope of the present invention is not limited in described
Hold.
Embodiment 1
The component and percentage by weight of the young coal degradation solution flavor beverage of the present embodiment be young coal degradation solution 30%, glucose 3%,
Pectin 0.01%, sodium carboxymethylcellulose 0.02%, sodium alginate 0.02%, surplus are distilled water.
Using Zhaotong County, Yunnan lignite as raw material, by patent " a kind of production method of young coal degradation solution and application thereof "（Application
Number：201410006333.5）The method of middle embodiment 1 prepares young coal degradation solution, is designated as sample 1-1, after testing the degradation solution
PH value is 2.3, density 1.03g/cm3。
So that with a collection of Zhaotong County, Yunnan lignite, as raw material, it is 15% that lignite is dried into moisture, and 200 mesh sieves, coal dust are crossed after crushing
It is standby；The potassium permanganate of quality of pc 9.6% is dissolved in the deionized water of 2 times of quality of pc, adds coal dust, 20 DEG C fully
After stirring reaction 3h, the potassium bichromate of quality of pc 16.2% is added, 60 DEG C of stirring reaction 1h, reaction 12h is stored at room temperature, carries out
The solid sedimentation separation of liquid；Upper strata stands liquid and centrifuges 10min under 5000r/min, obtains supernatant, by supernatant vacuum filter, filter
For liquid in 65 DEG C of concentrated by rotary evaporations, the evaporation condensate for obtaining water white transparency is young coal degradation solution, is designated as sample 1-2, after testing should
Degradation solution pH value is 1.5, density 1.05g/cm3。
Flavor beverage is prepared using young coal degradation solution sample 1-1 and sample 1-2 respectively, labeled as beverage 1-1 and beverage
1-2；During preparation, carry out as follows：
In proportion by various auxiliary materials weigh after, dissolved with distilled water, stand, filter after be added in young coal degradation solution；It will adjust
The liquid prepared carries out homogeneous, homogenization pressure 20MPa, 80 DEG C of temperature, homogeneous 2 times, each 5min；It is filling while hot after homogeneous, de-
Gas, gland, sterilize 30min under the conditions of 100 DEG C, and young coal degradation solution flavor beverage is made after cooling.
After testing, the beverage 1-1 and beverage 1-2 products prepared meets GB 7101-2015《Food security country mark
Quasi- beverage》Technical requirements.
Embodiment 2
The component and percentage by weight of the young coal degradation solution flavor beverage of the present embodiment be young coal degradation solution 40%, glucose 5%,
Pectin 0.01%, sodium carboxymethylcellulose 0.06%, sodium alginate 0.02%, surplus are distilled water.
Using Xundian Area, Yunnan lignite as raw material, by patent " a kind of production method of young coal degradation solution and application thereof "（Application
Number：201410006333.5）The method of middle embodiment 1 prepares young coal degradation solution, is designated as sample 2-1, after testing the degradation solution
PH value is 2.5, density 1.01g/cm3。
So that with a collection of Xundian Area, Yunnan lignite, as raw material, it is 8% that lignite is dried into moisture, and 200 mesh sieves, coal dust are crossed after crushing
It is standby；The potassium permanganate of quality of pc 9.6% is dissolved in the deionized water of 2 times of quality of pc, adds coal dust, 25 DEG C fully
After stirring reaction 3h, the potassium bichromate of quality of pc 16.2% is added, 50 DEG C of stirring reaction 1h, reaction 12h is stored at room temperature, carries out
The solid sedimentation separation of liquid；Upper strata stands liquid and centrifuges 10min under 5000r/min, obtains supernatant, by supernatant vacuum filter, filter
For liquid in 65 DEG C of concentrated by rotary evaporations, the evaporation condensate for obtaining water white transparency is young coal degradation solution, is designated as sample 2-2, after testing should
Degradation solution pH value is 2.0, density 1.04g/cm3。
Flavor beverage is prepared using young coal degradation solution sample 2-1 and sample 2-2 respectively, labeled as beverage 2-1 and beverage
2-2；During preparation, carry out as follows：
In proportion by various auxiliary materials weigh after, dissolved with distilled water, stand, filter after be added in young coal degradation solution；It will adjust
The liquid prepared carries out homogeneous, homogenization pressure 25MPa, temperature 70 C, homogeneous 2 times, each 6min；It is filling while hot after homogeneous, de-
Gas, gland, sterilize 40min under the conditions of 90 DEG C, and young coal degradation solution flavor beverage is made after cooling.
After testing, the beverage 2-1 and beverage 2-2 products prepared meets GB 7101-2015《Food security country mark
Quasi- beverage》Technical requirements.
Embodiment 3
The component and percentage by weight of the young coal degradation solution flavor beverage of the present embodiment be young coal degradation solution 50%, glucose 7%,
Pectin 0.02%, sodium carboxymethylcellulose 0.04%, sodium alginate 0.03%, surplus are distilled water.
Using Yunnan E Shan lignite as raw material, by patent " a kind of production method of young coal degradation solution and application thereof "（Application
Number CN201410006333.5）The method of middle embodiment 1 prepares young coal degradation solution, is designated as sample 3-1, after testing the degradation solution
PH value is 2.1, density 1.03g/cm3。
So that with a collection of Yunnan E Shan lignite, as raw material, it is 10% that lignite is dried into moisture, and 200 mesh sieves, coal dust are crossed after crushing
It is standby；The potassium permanganate of quality of pc 9.6% is dissolved in the deionized water of 2 times of quality of pc, adds coal dust, 30 DEG C fully
After stirring reaction 3h, the potassium bichromate of quality of pc 16.2% is added, 55 DEG C of stirring reaction 1h, reaction 12h is stored at room temperature, carries out
The solid sedimentation separation of liquid；Upper strata stands liquid and centrifuges 10min under 5000r/min, obtains supernatant, by supernatant vacuum filter, filter
For liquid in 65 DEG C of concentrated by rotary evaporations, the evaporation condensate for obtaining water white transparency is young coal degradation solution, is designated as sample 3-2, after testing should
Degradation solution pH value is 1.5, density 1.06g/cm3。
Flavor beverage is prepared using young coal degradation solution sample 3-1 and sample 3-2 respectively, labeled as beverage 3-1 and beverage
3-2；During preparation, carry out as follows：
In proportion by various auxiliary materials weigh after, dissolved with distilled water, stand, filter after be added in young coal degradation solution；It will adjust
The liquid prepared carries out homogeneous, homogenization pressure 22MPa, 78 DEG C of temperature, homogeneous 2 times, each 5min；It is filling while hot after homogeneous, de-
Gas, gland, sterilize 35min under the conditions of 95 DEG C, and young coal degradation solution flavor beverage is made after cooling.
After testing, the beverage 3-1 and beverage 3-2 products prepared meets GB 7101-2015《Food security country mark
Quasi- beverage》Technical requirements.
Embodiment 4
The component and percentage by weight of the young coal degradation solution flavor beverage of the present embodiment be young coal degradation solution 70%, glucose 9%,
Pectin 0.03%, sodium carboxymethylcellulose 0.05%, sodium alginate 0.04%, surplus are distilled water.
Using Heilungkiang Baoqing lignite as raw material, by patent " a kind of production method of young coal degradation solution and application thereof "（Shen
Please number：201410006333.5）The method of middle embodiment 1 prepares young coal degradation solution, is designated as sample 4-1, after testing the degraded
Liquid pH value is 2.0, density 1.04g/cm3。
So that with a collection of Heilungkiang Baoqing lignite, as raw material, it is 5% that lignite is dried into moisture, and 200 mesh sieves, coal are crossed after crushing
Powder is standby；The potassium permanganate of quality of pc 9.6% is dissolved in the deionized water of 2 times of quality of pc, adds coal dust, 30 DEG C are filled
After dividing stirring reaction 3h, the potassium bichromate of quality of pc 16.2% is added, 55 DEG C of stirring reaction 1h, reaction 12h is stored at room temperature, enters
The solid sedimentation separation of row liquid；Upper strata stands liquid and centrifuges 10min under 5000r/min, obtains supernatant, by supernatant vacuum filter,
For filtrate in 65 DEG C of concentrated by rotary evaporations, the evaporation condensate for obtaining water white transparency is young coal degradation solution, is designated as sample 4-2, after testing
The degradation solution pH value is 1.4, density 1.09g/cm3。
Flavor beverage is prepared using young coal degradation solution sample 4-1 and sample 4-2 respectively, labeled as beverage 4-1 and beverage
4-2；During preparation, carry out as follows：
In proportion by various auxiliary materials weigh after, dissolved with distilled water, stand, filter after be added in young coal degradation solution；It will adjust
The liquid prepared carries out homogeneous, homogenization pressure 24MPa, 76 DEG C of temperature, homogeneous 2 times, each 6min；It is filling while hot after homogeneous, de-
Gas, gland, sterilize 38min under the conditions of 92 DEG C, and young coal degradation solution flavor beverage is made after cooling.
After testing, the beverage 4-1 and beverage 4-2 products prepared meets GB 7101-2015《Food security country mark
Quasi- beverage》Technical requirements.
The quality of beverage product made of different ratios of raw materials is evaluated, specific experiment is as follows：
The beverage prepared using embodiment 1-4 selects experienced person 20 as sample（10 males and 10 women, age
For 20-40 year）, by beverage organoleptic indicator's standards of grading（It is shown in Table 1）Scored, finally averaged, total score is 100 points, knot
Fruit is shown in Table 2；After 8 batches of prepared beverages are drunk, all testing crews there are no any uncomfortable generation.
Result of the test shows, with prior art（Patent " a kind of production method of young coal degradation solution and application thereof ", application
Numbers 201410006333.5）The degradation solution of production is that flavor beverage sensory evaluation overall score prepared by raw material is below 80；With this
The young coal degradation solution of the innovative technology production of invention is flavor beverage prepared by raw material, and its quality is greatly improved, general comment
Point be above 80, particularly improve in smell and the aspect of flavour two it is more significant, tart flavour more alcohol and it is thick and heavy, do not stimulate, wherein right
Beverage quality lifting of the raw material from Zhaotong Brown Coal is maximum, illustrate young coal degradation solution that the inventive method produces be more suitable for for
Prepare flavor beverage；In addition, the beverage sensory evaluation in different material source also has larger difference, wherein being degraded with Heilungkiang Baoqing
Liquid is flavor beverage performance optimal prepared by raw material.
Claims (2)
1. a kind of young coal degradation solution flavor beverage, it is characterised in that the component and percentage by weight are young coal degradation solution
30%-70%, glucose 3%-9%, pectin 0.01%-0.03%, sodium carboxymethylcellulose 0.02%-0.06%, sodium alginate 0.02%-
0.04%, surplus is distilled water.
2. young coal degradation solution flavor beverage according to claim 1, it is characterised in that the system of the young coal degradation solution
Preparation Method is as follows：It is 5%-15% that young coal is dried into moisture, and 200 mesh sieves are crossed after crushing, and coal dust is standby；By quality of pc 9.6%
Potassium permanganate be dissolved in the deionized water of 2 times of quality of pc, add coal dust, after 20 DEG C -30 DEG C are sufficiently stirred reaction 3h, add
Enter the potassium bichromate of quality of pc 16.2%, 50 DEG C of -60 DEG C of stirring reaction 1h, be stored at room temperature reaction 12h, carry out liquid and settle admittedly point
From；Upper strata stands liquid and centrifuges 10min under 5000r/min, obtains supernatant, and by supernatant vacuum filter, filtrate is in 65 DEG C of rotations
Inspissation contracts, and the evaporation condensate for obtaining water white transparency is young coal degradation solution.
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