CN107454839A - 可摇动浓密化睫毛油 - Google Patents
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Abstract
本文公开的本发明实施方案包括可摇动凝胶睫毛油。所述可摇动凝胶睫毛油包含比其他凝胶睫毛油制剂中的蜡组分少约二十百分比的蜡组分。
Description
优先权要求
本专利申请要求于2015年2月5日提交的美国临时专利申请序列号62/112,461的优先权,其在此通过引用以其全部并入本文。
领域
本文公开的本发明实施方案涉及可摇动的浓密化睫毛油以及制备可摇动浓密化睫毛油的方法。
背景
古埃及人认为眼睛是心灵的窗口并且利用眼线和睫毛油对恶魔隐藏眼睛是重要的。最早的睫毛油由包括埃及妇女用的眼圈黑、鳄鱼粪、水和蜂蜜的成分制成。该睫毛油用骨头和象牙涂抹器施用。
在1913年,Eugene Rimmel创造了最早大量生产的无毒睫毛油,不是为了驱赶恶魔而是为了赋予睫毛长度和浓密。Rimmel睫毛油由石油和黑煤粉的混合物制成。
附图说明
图1A示出已经打开但未使用的包装中的可摇动睫毛油的横截面图。
图1B示出图1A的可摇动睫毛油的截面的俯视图。
图2A示出已经打开并使用十二周但是未摇动的包装中的可摇动睫毛油的横截面图。
图2B示出图2A的可摇动睫毛油的截面的俯视图。
图3A示出已经打开并使用十二周并且摇动了的包装中的可摇动睫毛油的横截面图。
图3B示出图3A的可摇动睫毛油的截面的俯视图。
图4A示出从未与睫毛油接触过的一缕人毛发的透视图。
图4B示出已经与常规的不可摇动睫毛油接触一次的图4A的毛发的透视图。
图5A示出从未与睫毛油接触过的一缕人毛发的透视图。
图5B示出已经与常规的不可摇动睫毛油接触十二周的图5A的毛发的透视图。
图6A示出从未与睫毛油接触过的一缕人毛发的透视图。
图6B示出已经与可摇动睫毛油实施方案接触一次的图6A的毛发的透视图。
图7A示出从未与睫毛油接触过的一缕人毛发的透视图。
图7B示出已经与可摇动睫毛油实施方案接触十二周的图7A的毛发的透视图。
概述
本文公开的本发明实施方案包括可摇动凝胶睫毛油制剂。所述制剂包括以下成分:
详述
以下详述包括对附图的参照,所述附图形成详述的一部分。通过举例说明,附图显示出其中可以实施本发明的具体实施方案。充分详细地描述在本文中也称作“实施例”的这些实施方案,以使得本领域技术人员能够实施本发明。所述实施方案可以组合,可以采用其他实施方案,或者可以在不脱离本发明的范围的条件下进行结构和逻辑的变化。因此,以下详述不被当作是限制意义的,并且本发明的范围通过所附权利要求及其等同方案限定。
在此文件中,术语“一个”或“一种”用于包括一个或种或多于一个或种,并且术语“或”用于指非独占性的“或”,除非另有说明。另外,应理解,本文中采用并且没有另外定义的短语或术语仅用于描述的目的而不是用于限制的目的。此外,本文件中引用的全部出版物、专利和专利文件都通过引用以其全部并入本文,如同单独地通过引用并入一样。在此文件和如此通过引用并入的那些文件之间的用法不一致的情况下,则应认为在并入的参考文件中的用法是对本文件的用法的补充;对于不相容的不一致,以本文件中的用法为准。
本文公开的本发明实施方案涉及当施用至睫毛时具有浓密化效果的可摇动的触变凝胶睫毛油制剂实施方案。“浓密化”意指睫毛由于睫毛油的施用而具有增加的直径和长度。本文公开的可摇动睫毛油制剂实施方案是防汗、防热和防湿的。可摇动制剂实施方案包含软蜡和硬蜡两者连同成膜复合物的组合,所述成膜复合物是环戊硅氧烷和三甲基甲硅烷氧基硅酸酯的组合;和失水山梨醇聚氧乙烯(20)醚月桂酸酯、水以及异丙醇和丙烯酸铵共聚物的组合;和氢化棕榈油甘油酯、鲸蜡基磷酸钾以及硅酸钠镁锂,所述硅酸钠镁锂是天然粘土;和铁氧化物。
本文公开的可摇动睫毛油制剂实施方案对于即时且可见地使睫毛卷曲、在睫毛上形成卷曲具有至少二十四小时的持续时间有效。特别地,卷曲归因于软蜡和硬蜡两者连同成膜复合物的组合。
本文公开的可摇动制剂实施方案由于软蜡和硬蜡两者连同尼龙共混物即Orgasol4000EXD Nat Cos Caresse/尼龙-6/12的组合表现出即时的睫毛体积增加,所述组合包括为每根睫毛增加即时体积的疏水/亲水性质两者。
可摇动制剂实施方案用容器摇动,所述容器在一个实施方案中是包含将触变睫毛油混合的可摇动不锈钢圆筒的塑料部件。对于其他实施方案,容器是玻璃。对于其他实施方案,不锈钢圆筒用聚合材料涂覆。对于其他实施方案,采用不同于圆筒的结构,如球体。熔体在特定重量范围内填充,使得可摇动重物持续地混合睫毛油以使其较长时间地新鲜施用并且持续较长时间。
对于常规的睫毛油制剂,消费者抱怨他们的睫毛油随时间变粘并且变干。这是由于他们的睫毛油中的许多被捕获在容器顶部处的擦拭物上,在这种情况下擦拭物不与在容器底部处的睫毛油混合。对于本发明的制剂实施方案,不锈钢重物使来自擦拭物周围的睫毛油与其余睫毛油混合使得其持续地变新鲜并且更浓密,因而其持续较长时间。
可摇动睫毛油制剂实施方案包括触变凝胶使得睫毛油的粘度在搅拌/摇动时液化并且在搅拌停止时快速硬化。可摇动制剂实施方案用胶质支撑以提供形体。触变凝胶对于该可摇动应用是关键的。
可摇动睫毛油制剂实施方案具有用于产生睫毛油的蜡的通常组合以增强美容益处,如使睫毛卷曲、浓密化、分离和变长,并且包含成膜剂以提供用于均匀施用的内聚力。例如,可摇动制剂实施方案包含中和剂以及任意数量的用于化妆品要求的植物提取物,如胶原蛋白和角蛋白以帮助增强眼睫毛。
可摇动睫毛油制剂实施方案是一般在组件中具有不锈钢重物的容器中摇动的触变凝胶体系。
一种可摇动睫毛油制剂实施方案表现出睫毛浓密化的增加。制剂被包装在促进摇动并且包括不锈钢重物的容器中。可摇动睫毛油制剂实施方案如下:
制剂1
表1中公开的可摇动睫毛油实施方案与其他凝胶睫毛油制剂不同,因为其包含少约20%的蜡,如表2中所示。制剂1是本发明的可摇动睫毛油制剂。制剂2是不可摇动的凝胶睫毛油。
表2
制剂1包含用于产生睫毛油的蜡的组合以增强美容益处,如使睫毛卷曲、浓密化、分离和变长,并且包含成膜剂以提供用于均匀施用的内聚力。
Trilon BD,由巴斯夫(BASF)制造,包含90%w/w浓度的乙二胺四乙酸(EDTA)的二钠盐和10%w/w浓度的水。
Laponite XLG是具有低重金属含量的合成层状硅酸盐。其不溶于水但是水合并且溶胀以给出在水或醇的水溶液中的透明且无色的胶态分散体。在水中2%以上的浓度,获得高触变凝胶。一旦形成凝胶,就将蜡连同着色剂添加到凝胶悬浮液中。其可能是双胶态分散体,并且最终产品是乳液。Laponite XLG由英国Widnes的BYK Additives Ltd.制造。
Tween 20,也称作失水山梨醇聚氧乙烯(20)醚月桂酸酯,是其稳定性和相对无毒性允许其被用作清洁剂和乳化剂的聚山梨醇酯表面活性剂。Tween 20的化学式为C58H114O26,分子量为1227.54g/mol,并且密度为1.10g/cm(3)。
Emulsiphos是鲸蜡基磷酸钾(和)氢化棕榈油甘油酯,由位于新泽西州Teterboro的Symrise AG制造。
氧化铁黑C33-5000和C33-6000都由俄亥俄州辛辛那提的Sun Chemical Corp.制造。其他氧化铁黑也是合适的。
Orgasol 4000EXD Nat Cos Caresse是共聚酰胺6/12,也称作尼龙-6/12。该材料由阿克玛法国(Arkema France)制造。
Paracera P蜡是由位于全球范围的百瑞美(Paramelt)制造的石蜡。
Euxyl PE 9010是苯氧乙醇和乙基己基甘油。该材料由Schulke Inc.制造并且典型地作为防腐剂。
道康宁(Dow Corning)(DC)749流体(Dow Corning(DC)749Fluid)是约50百分比的高分子量树脂和50百分比的挥发性低粘度环戊硅氧烷的共混物。
WorleeMicromer C50/25包含丙烯酸铵共聚物;水,CAS#7732-18-5;和异丙醇,CAS#67-63-0。WorleeMicromer C50/25由德国汉堡的Worlee-Chemie GmbH制造。
制剂中水含量的变化改变浓密化的程度。较大量的水使制剂变稀并且减少浓密化。在一些制剂实施方案中,省略以下成分中的一种或多种:Laponite(合成层状硅酸盐)、Orgasol 4000EXD Nat Cos Caresse(尼龙-6/12)、DC749、WorleeMicromer C50/25、氢氧化钠、Emulsiphos、连同阶段1中的蜡中的任一种。
另一实施方案包括睫毛油,所述睫毛油包含:
至少约45重量%浓度的水;
EDTA二钠;
失水山梨醇聚氧乙烯(20)醚月桂酸酯;
氧化铁黑;
15-20重量%浓度的选自由蜂蜡、巴西棕榈蜡和石蜡组成的组的一种或多种蜡;和
对用水形成胶态分散体有效的浓度的不溶于水的合成层状硅酸盐。
一种制备凝胶浓密睫毛油的方法,所述方法包括:
通过将乙二胺四乙酸(EDTA)二钠添加至去离子水制备去离子水和EDTA二钠的第一相;
将表面活性剂添加至所述第一相以产生第二相;
制备胶态分散体;
将粒状着色剂添加至所述胶态分散体以产生第三相,并且将所述第三相添加至所述第二相以产生第四相;和
制备包含硬脂酸、巴西棕榈蜡、石蜡、小烛树蜡或蜂蜡中的一种或多种的蜡相以产生蜡相,并且将所述蜡相添加至所述第三相以产生第五相;并且将苯氧乙醇和乙基己基甘油添加至所述第五相以产生所述凝胶浓密睫毛油。
对于一些实施方案,所述方法还包括将包含具有低重金属含量的合成层状硅酸盐的相添加至去离子水和EDTA二钠的所述第一相。
对于一些实施方案,所述方法还包括添加至所述第二相的鲸蜡基磷酸钾和氢化棕榈油甘油酯。
实施例1
本文公开的可摇动睫毛油保持其光滑性并且在施用至毛发延长的时间期时没有结块。图1A和1B示出在打开包装时的可摇动睫毛油。睫毛油是光滑的,没有结块。在使用十二周后,图1A和1B的可摇动睫毛油继续表现为光滑的睫毛油,没有结块,如图2A和2B中所示。图2A和2B中所示的睫毛油未被摇动。图3A和3B示出在摇动睫毛油后的图2A和2B的睫毛油。与表现为暗淡且不光滑的常规睫毛油相比,可摇动睫毛油的强度,即黑度和光泽尤其在摇动时随时间和使用保持在规格内。与其中粘度明显增加并且超出规格的常规睫毛油相比,可摇动睫毛油的粘度随使用保持在规格内。
图4A示出从未与睫毛油接触过的一缕毛发。图4B示出已经施用了常规的不可摇动睫毛油的图4A的毛发。可观察到睫毛油结块和不均匀分布。
图5A示出从未与睫毛油接触过的一缕毛发。图5B示出已经在十二周的时间内施用了常规的不可摇动睫毛油的图5A的毛发。可观察到睫毛油结块和不均匀分布。
图6A示出从未与睫毛油接触过的一缕毛发。图6B示出已经施用了可摇动睫毛油实施方案的图6A的毛发。没有观察到睫毛油结块和不均匀分布。
图7A示出从未与睫毛油接触过的一缕毛发。图7B示出已经在十二周的时间内施用了可摇动睫毛油实施方案的图7A的毛发。没有观察到睫毛油结块和不均匀分布。
本领域技术人员将容易理解,在不脱离所附权利要求中表达的本发明主题的原则和范围的条件下,可以进行为了解释本发明主题的本质已经描述和举例说明的细节、材料以及部分和方法阶段的排列的多种其他变化。
Claims (4)
1.一种可摇动凝胶睫毛油,所述可摇动凝胶睫毛油包含:
2.一种制备可摇动凝胶浓密睫毛油的方法,所述方法包括:
通过将乙二胺四乙酸(EDTA)二钠添加至去离子水制备去离子水和EDTA二钠的第一相;
将表面活性剂添加至所述第一相以产生第二相;
制备胶态分散体;
将粒状着色剂添加至所述胶态分散体以产生第三相,并且将所述第三相添加至所述第二相以产生第四相;和
制备包含硬脂酸、巴西棕榈蜡、石蜡、小烛树蜡或蜂蜡中的一种或多种的蜡相以产生蜡相,并且将所述蜡相添加至所述第三相以产生第五相;并且将苯氧乙醇和乙基己基甘油添加至所述第五相以产生所述凝胶浓密睫毛油。
3.权利要求2所述的方法,所述方法还包括将包含具有低重金属含量的合成层状硅酸盐的相添加至去离子水和EDTA二钠的所述第一相。
4.权利要求3所述的方法,还包括添加至所述第二相的鲸蜡基磷酸钾和氢化棕榈油甘油酯。
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US5800825A (en) * | 1996-11-08 | 1998-09-01 | Mcmullen; Alexandra | Mascara having enhanced drying capability |
US20120003171A1 (en) * | 2008-12-11 | 2012-01-05 | L'oreal S.A. | Volumizing smudge resistant mascara composition |
US20130164241A1 (en) * | 2011-12-23 | 2013-06-27 | Mary Kay Inc. | Mascara formulation |
US20140186282A1 (en) * | 2012-12-31 | 2014-07-03 | L'oreal | Clean volume mascara compositions comprising at least one film former and at least one silicone elastomer |
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CZ297086B6 (cs) * | 1996-11-27 | 2006-09-13 | The Procter & Gamble Company | Rasenkový prostredek emulsního typu zahrnující anorganické koloidní materiály |
US8333956B2 (en) | 2002-06-11 | 2012-12-18 | Color Access, Inc. | Stable cosmetic emulsion with polyamide gelling agent |
US9763872B2 (en) | 2015-02-05 | 2017-09-19 | Coty Inc. | Shakeable volumizing mascara |
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Publication number | Priority date | Publication date | Assignee | Title |
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US5800825A (en) * | 1996-11-08 | 1998-09-01 | Mcmullen; Alexandra | Mascara having enhanced drying capability |
US20120003171A1 (en) * | 2008-12-11 | 2012-01-05 | L'oreal S.A. | Volumizing smudge resistant mascara composition |
US20130164241A1 (en) * | 2011-12-23 | 2013-06-27 | Mary Kay Inc. | Mascara formulation |
US20140186282A1 (en) * | 2012-12-31 | 2014-07-03 | L'oreal | Clean volume mascara compositions comprising at least one film former and at least one silicone elastomer |
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