CN107447120A - A kind of purifier of electrolytic manganese metal - Google Patents
A kind of purifier of electrolytic manganese metal Download PDFInfo
- Publication number
- CN107447120A CN107447120A CN201710913928.2A CN201710913928A CN107447120A CN 107447120 A CN107447120 A CN 107447120A CN 201710913928 A CN201710913928 A CN 201710913928A CN 107447120 A CN107447120 A CN 107447120A
- Authority
- CN
- China
- Prior art keywords
- container
- outer shaft
- purifier
- interior axle
- electrolytic manganese
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B47/00—Obtaining manganese
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/30—Electrolytic production, recovery or refining of metals by electrolysis of melts of manganese
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Removal Of Specific Substances (AREA)
Abstract
The present invention relates to a kind of purifier of electrolytic manganese metal, container including holding manganese sulfate solution, rotatable hollow interior axle is installed through its bottom in the container, the interior outer shaft sleeve is provided with the outer shaft in container that can be rotated with it, outer shaft perisporium is provided with the stirring rod of solution that can be in stirring container, by being lifted up outer shaft interior axle can be made to expose close to one section of container bottom, one section of interior axle that solution in container is exposed by this is filtered, and the filtrate after filtering flows into the clarifier-tank being arranged on the downside of the container.The present invention is filtered using the inside and outside axle for driving stirring rod to rotate to solution, reaction generation precipitation in container is retained in container, is achieved that stirring, filtering without other auxiliary equipments, substantially increases production efficiency.
Description
Technical field
The present invention relates to a kind of purifier of electrolytic manganese metal.
Background technology
Mainly include manganese oxide ore and manganese carbonate ore with industrial application value in natural manganese ore, according to the taste of manganese ore
It is internal and international at present that deep processing processing typically is carried out to it using two kinds of processes with the difference of impurity content：When pair
In objectionable impurities（Such as phosphorus, sulphur）Low high-grade ore can be directly using pyrometallurgical smelting process production Mn series alloy product or as battery
Manganese powder；Second, for most of manganese carbonate and partial oxidation manganese ore, the general serial salt using hydrometallurgical technology production manganese
Product.However, with the exploitation year by year to manganese resource, GOOD TASTE, the ANOMALY IN FINE QUALITY MANGANESE DEPOSITS increasingly depleted of low impurity, therefore, for
The research and development and utilization for the complicated manganese ore that manganese content is low, impurity content is high, which turn into, improves domestic manganese ore deep processing enterprise in the world
The key of the market competitiveness, also largely determine that can manganese ore processing industry sustainable development.Electricity is prepared existing
During solving manganese metal, impurity and purification need to be carried out to middle the product sulfur acid manganese solution, and current manganese sulfate electrolyte is net
Change time length, influence production efficiency.
The content of the invention
For above-mentioned technical problem, the present invention provides a kind of purifier for the electrolytic manganese metal for improving production efficiency.
Technical scheme is used by the present invention solves above-mentioned technical problem：A kind of purifier of electrolytic manganese metal, bag
The container for holding manganese sulfate solution is included, rotatable hollow interior axle is installed through its bottom in the container, the interior outer shaft sleeve
Provided with the outer shaft that can be rotated with it in container, outer shaft perisporium is provided with the stirring rod of solution that can be in stirring container, leads to
Cross and be lifted up outer shaft interior axle can be made to expose close to one section of container bottom, one section of interior axle that the solution in container is exposed by this
Filtered, the filtrate after filtering flows into the clarifier-tank being arranged on the downside of the container.
Preferably, offer the opening connected with its inner chamber in the one section of interior axle exposed, covered with filter screen in opening, by
Filtrate after the strainer filtering flows into the clarifier-tank from inner chamber,
Preferably, the inside and outside axle is connected by flat key.
Preferably, the interior axle is fixed with the flat key close to container bottom end, the outer shaft inwall is from its bottom end
Keyway is extended with upwardly, and the flat key can be embedded in keyway.
Preferably, the outer shaft top is provided with carrying handle.
Preferably, the stirring slurry rotated with the interior axle is provided with the clarifier-tank.
As can be known from the above technical solutions, the present invention is filtered using the inside and outside axle for driving stirring rod to rotate to solution, is made
Reaction generation precipitation is retained in container in container, is achieved that stirring, filtering without other auxiliary equipments, is substantially increased
Production efficiency.
Brief description of the drawings
Fig. 1 is the structural representation of the preferred embodiment of the present invention.
Embodiment
The present invention is discussed in detail with reference to Fig. 1, illustrative examples of the invention and explanation are used for explaining this herein
Invention, but it is not as a limitation of the invention.
A kind of purifier of electrolytic manganese metal, including the container 1 of manganese sulfate solution is held, its bottom is passed through in the container
Portion is provided with rotatable hollow interior axle 2, and the interior outer shaft sleeve is provided with the outer shaft 3 in container that can be rotated with it, outer shaft week
Wall is provided with the stirring rod 4 of solution that can be in stirring container, can make interior axle close to the one of container bottom by being lifted up outer shaft
Section is exposed, and one section of interior axle that the solution in container is exposed by this is filtered, and the filtrate after filtering flows into and is arranged on the appearance
Clarifier-tank 91 on the downside of device, one section of purification can be carried out in clarifier-tank.Thus, by inside and outside rotating shaft simultaneously realize stirring and
Filtering, is not only simple in structure, and can improve efficiency.
Specifically, the opening 5 connected with its inner chamber is offered in the one section of interior axle exposed, covered with filter screen 6 in opening,
Flowed out by the filtrate after the strainer filtering from inner chamber.The agitated reaction generation such as manganese sulfate leachate and barium sulphide is miscellaneous in container
Matter is precipitated, and solution can enter interior axle inner chamber by filter screen, and precipitation is then retained in container, realizes the purpose of purification.
In implementation process, the inside and outside axle is connected by flat key 7, and outer shaft rotates simultaneously in realization；Specifically described
Interior axle is fixed with the flat key close to container bottom end, and the outer shaft inwall has upwardly extended keyway 8, and institute from its bottom end face
State outer shaft top and be provided with carrying handle 9.When mounted, hold handle to be inserted in the outer shaft along internal axle axial, make flat key embedding
Enter in keyway；After the completion of stirring, to hold handle and be lifted up outer shaft so that flat key departs from keyway, while exposes opening, so as to
Realize filtering.In order to prevent precipitation from blocking filter screen, in filter process, interior axle can be rotated, make precipitation inside using centrifugal force
Thrown away on the outside of axle, avoid precipitation from being gathered near filter screen.
The stirring slurry 92 rotated with the interior axle is provided with implementation process, in the clarifier-tank, it is right in purification process
Mixed solution is stirred.From the above it can be seen that the present invention can be carried out continuously to the manganese sulfate solution in electrolytic manganese metal preparation process
Purification, production efficiency can be not only improved, and it is easy to operate simple, and cost is low.
Above-mentioned embodiment is used for illustrative purposes only, and is not limitation of the present invention, relevant technical field
Those of ordinary skill, can be so that various changes can be made and modification without departing from the spirit and scope of the present invention, therefore institute
There is equivalent technical scheme also to belong to scope of the invention.
Claims (6)
1. a kind of purifier of electrolytic manganese metal, including hold the container of manganese sulfate solution, it is characterised in that：In the container
Rotatable hollow interior axle is installed through its bottom, the interior outer shaft sleeve is provided with the outer shaft in container that can be rotated with it,
Outer shaft perisporium is provided with the stirring rod of solution that can be in stirring container, can make interior axle close to container bottom by being lifted up outer shaft
One section expose, one section of interior axle that the solution in container is exposed by this is filtered, and filtrate after filtering flows into and is arranged on institute
State the clarifier-tank on the downside of container.
2. the purifier of electrolytic manganese metal according to claim 1, it is characterised in that：Offered in the one section of interior axle exposed
The opening connected with its inner chamber, opening is upper covered with filter screen, by the filtrate after the strainer filtering from the inner chamber inflow clarifier-tank.
3. the purifier of electrolytic manganese metal according to claim 1, it is characterised in that：The inside and outside axle is connected by flat key
Connect.
4. the purifier of electrolytic manganese metal according to claim 3, it is characterised in that：The interior axle is close to container bottom end
The flat key is fixed with, the outer shaft inwall has upwardly extended keyway from its bottom end face, and the flat key can be embedded in keyway.
5. the purifier of electrolytic manganese metal according to claim 4, it is characterised in that：The outer shaft top is provided with lifting
Handle.
6. the purifier of electrolytic manganese metal according to claim 1, it is characterised in that：It is provided with the clarifier-tank with institute
State the stirring slurry of interior axle rotation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710913928.2A CN107447120A (en) | 2017-09-30 | 2017-09-30 | A kind of purifier of electrolytic manganese metal |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710913928.2A CN107447120A (en) | 2017-09-30 | 2017-09-30 | A kind of purifier of electrolytic manganese metal |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107447120A true CN107447120A (en) | 2017-12-08 |
Family
ID=60498624
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710913928.2A Withdrawn CN107447120A (en) | 2017-09-30 | 2017-09-30 | A kind of purifier of electrolytic manganese metal |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107447120A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109763147A (en) * | 2019-03-28 | 2019-05-17 | 杨俊芬 | A kind of Manganese alloy production equipment |
-
2017
- 2017-09-30 CN CN201710913928.2A patent/CN107447120A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109763147A (en) * | 2019-03-28 | 2019-05-17 | 杨俊芬 | A kind of Manganese alloy production equipment |
| CN109763147B (en) * | 2019-03-28 | 2020-11-06 | 乌海三美国际矿业有限公司 | Manganese alloy production equipment |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104911359B (en) | A kind of process that cobalt and nickel are extracted from manganese waste slag | |
| CN101323908B (en) | Method for reclaiming cobalt from manganese cobalt slag | |
| CN102226234B (en) | Integrated reactor suitable for purifying and impurity-removing of pyrolusite leachate | |
| JP2015206077A (en) | Method and apparatus for separating and recovering resource from waste dry cell and recovered substance | |
| CN106544511A (en) | A kind of method of synthetical recovery manganese, lead, silver and selenium from Manganese anode slime | |
| CN109593977B (en) | Method for removing iron ions in neodymium, praseodymium, dysprosium and iron-containing solution | |
| CN103710533B (en) | A kind of method of producing electrolytic metal Mn | |
| CN103695636A (en) | Preparation method of electrolytic manganese dioxide | |
| CN104229863A (en) | Production process of ammonia-method calcined zinc oxide | |
| CN108975406A (en) | A kind of method and device thereof of tungsten waste production APT | |
| JP2013057097A (en) | Sulfide precipitation method of metal | |
| CN107447120A (en) | A kind of purifier of electrolytic manganese metal | |
| CN108559842B (en) | A kind of method that low-concentration hcl Ore Leaching calcium strontium selects Weishan Lake rare earth ore concentrate | |
| CN107513626A (en) | A kind of knot screen of electrolytic manganese dioxide | |
| CN107513629A (en) | A kind of purifier of manganese sulfate electrolyte | |
| CN207468698U (en) | A kind of exclusion device of electrolytic manganese dioxide | |
| CN105483412B (en) | The method that high-purity tungsten-molybdenum alloy is prepared using low-grade tungsten bulk concentrate | |
| CN107675201A (en) | The preparation method of electrolytic manganese dioxide | |
| CN101376521A (en) | Method for removing high concentration iron impurity in copper-contained sludge copper sulfate leaching liquid | |
| CN206143278U (en) | A dissolving device for rare earth extraction usefulness | |
| CN202107753U (en) | Integrated reactor suitable for purifying and edulcorating pyrolusite lixivium | |
| CN107513615A (en) | A kind of purification method of electrolytic manganese metal | |
| JP5889603B2 (en) | Arsenic leaching method from non-ferrous smelting ash | |
| CN108149020A (en) | The technique for preparing bismuth using zinc anode sludge waste residue | |
| CN107447111A (en) | A kind of purification method of manganese sulfate electrolyte |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171208 |
|
| WW01 | Invention patent application withdrawn after publication |