CN107446690A - A kind of squeezing of camellia oil and refinery practice - Google Patents
A kind of squeezing of camellia oil and refinery practice Download PDFInfo
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- CN107446690A CN107446690A CN201710507907.0A CN201710507907A CN107446690A CN 107446690 A CN107446690 A CN 107446690A CN 201710507907 A CN201710507907 A CN 201710507907A CN 107446690 A CN107446690 A CN 107446690A
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- camellia
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
Abstract
The invention provides a kind of squeezing of camellia oil and refinery practice, including shell, heat, squeezing, filtering, coldization, distillation, refining, secondary coldization.The present invention heats camellia seed by low pressure microwave, albumen and immobilized artificial membrane in kernel can preferably be destroyed, reduce the moisture content of tea seed, promote the dissolution of oil droplet, improve squeezing oil yield, and for microwave computer heating control at 100 130 DEG C, relatively low temperature can reduce free fatty acid content raising and oil peroxidation product produces, and reduce the difficulty of follow-up refinery practice；Squeezing is squeezed using lower temperature, squeezing is avoided to cause acid value and peroxide value too high, the present invention passes through the secondary coldization PROCESS FOR TREATMENT of coldization distillatory refining, the oyster shell whiting particularly used in refinement step contains micro calcium oxide and chitin, can effectively reduce the content of acid value in camellia oil, peroxide value and poisonous peroxide.
Description
Technical field
The invention belongs to squeezing and the refinery practice of the manufacture craft of edible oil, more particularly to a kind of camellia oil.
Background technology
Camellia oil, also known as camellia seed oil, it is from plant of theaceae oil tea (Camellia oleifera Abel) seeds
Middle acquisition, be one of most ancient traditional woody edible vegetable oil in China, its aliphatic acid composition is very much like with olive oil, again
It is referred to as " east olive oil ".Also contain tea polysaccharide, tsubakisaponin, flavones, Tea Polyphenols, vitamin and phytosterol in camellia oil
It is often edible that there is reduction cholesterol, improve HDL, reduce low-density lipoprotein, drop blood etc. various active material
Fat, cardiovascular and cerebrovascular disease is prevented, immunity, radioresistance is improved, removes free radical, pre- preventing tumor and other effects, international food and agricultural organization
It has been classified as the health-care edible oil of emphasis popularization.
Most of preparation method of existing camellia oil, which uses, dries, crushes, roll embryo and 110 DEG C of high temperature above steam the works such as stir-fry
Sequence, oil is then squeezed by high temperature hot pressing, manufacturing procedure is more complicated, equipment investment is larger, production cost is higher, oil colours is relatively deep,
Inferior quality, it is necessary to can turn into one-level expressed oil by the refinings such as depickling, dehydration, decolouring, deodorization, degreasing processing, refine
Oil cut rate is relatively low, and refined rear camellia oil loses natural flavour mountaineous.
The content of the invention
In order to solve the above technical problems, the invention provides a kind of squeezing of camellia oil and refinery practice, concrete technology is：
A kind of squeezing of camellia oil and refinery practice, comprise the following steps：
1）Shell, select the camellia fruit of maturation, ted, allow camellia fruit pericarp season crack, remove pericarp and obtain camellia seed, continue
The moisture content to camellia seed is tedded in 12-20%；
2）Heating, microwave heating, drying is carried out to above-mentioned camellia seed under environment under low pressure, heating-up temperature is 100-130 DEG C, to mountain
Tea seed water content is 2-4%, then naturally cools to normal temperature；
3）Squeezing, above-mentioned camellia seed cold press being squeezed out into camellia oil, press chamber temperature is 100~150 DEG C, oil outlet temperature is 80~
120℃；
4）Filtering, solid impurity is removed by above-mentioned camellia oil by plate and frame filter press；
5）Coldization, above-mentioned camellia oil is cooled to -5 DEG C~5 DEG C and preserves more than 30h, takes upper strata camellia edible vegetable oil；
6）Distillation, above-mentioned upper strata camellia edible vegetable oil is taken to distill, distillation pressure is 10-60kPa, and evaporating temperature is 130-150 DEG C, is kept
30-50min, it is then 20~25 DEG C in the drop of pressure as little as condensation temperature, takes camellia oil liquid；
7）Refining, is heated to 150-170 DEG C by above-mentioned camellia oil liquid and keeps 5-10min, then cool to 120-140 DEG C,
The 1-5% of camellia edible vegetable oil weight oyster shell whiting is added, stirring reaction 50-100min, is subsequently cooled to normal temperature at 130-150 DEG C,
Filter off and remove oyster shell whiting；
8）Secondary coldization, above-mentioned camellia oil is cooled to -5 DEG C~5 DEG C and preserves more than 30h, upper strata camellia edible vegetable oil is taken, obtains mountain
Tea essential oil.
Further, described oyster shell whiting passes through for fresh shell is polished into powder, 450-550 DEG C of temperature lower calcination 1-4h,
Obtained powder is cooled down, shell contains substantial amounts of calcium carbonate and a small amount of chitin, and the decomposition temperature of calcium carbonate is 898 DEG C,
By the calcining of 450-550 DEG C of temperature, can destroy shell surrounds and watches structure, discharges micro calcium oxide and chitin, makes
Obtaining oyster shell whiting has the effect such as purification, thickening, anti-oxidant.
Further, described step 2）Under the environment under low pressure, pressure 10-60kPa；The microwave heating, microwave
Power is 1000-2000 watts.
Further, described step 2）Camellia seed heating in add camellia seed weight 1-5% chaff shell；Chaff shell can
Camellia oil is decolourized, while contains a small amount of rice bran oil in chaff shell, camellia oil can be seasoned so that worth camellia
Essential oil taste is more sweet and dilitious.
The beneficial effects of the present invention are：The present invention heats camellia seed by low pressure microwave, can preferably destroy kernel
Middle albumen and immobilized artificial membrane, the moisture content of tea seed is reduced, promote the dissolution of oil droplet, improve squeezing oil yield, and microwave heats
At 100-130 DEG C, relatively low temperature can reduce free fatty acid content and improve and the generation of oil peroxidation product, reduction for control
The difficulty of follow-up refinery practice；Squeezing is squeezed using lower temperature, avoids squeezing from causing acid value and peroxide value too high, the present invention
Micro oxygen is contained by the oyster shell whiting used in coldization-distillation-refining-secondary coldization PROCESS FOR TREATMENT, particularly refinement step
Change calcium and chitin, can effectively reduce the content of acid value in camellia oil, peroxide value and poisonous peroxide；By inspection
Survey, the camellia essential oil acid value that makes of the present invention be less than 0.05 mg/g, and peroxide value is less than 1mg/kg, aoxidizes toxic products the third two
Aldehyde is less than 1ppb, and water content is less than 1ppm.
Embodiment
Be described further below technical scheme, but claimed scope be not limited to it is described.
Embodiment one
Squeezing and the refinery practice of a kind of camellia oil are present embodiments provided, is comprised the following steps：
1）Shell, select the camellia fruit of maturation, ted, allow camellia fruit pericarp season crack, remove pericarp and obtain camellia seed, continue
The moisture content to camellia seed is tedded in 12-20%；
2）Heating, microwave heating, drying is carried out to camellia seed under environment under low pressure, heating-up temperature is 100 DEG C, aqueous to camellia seed
Measure as 2%, then naturally cool to normal temperature；Pressure is 10kPa, microwave power 1000-2000w；
3）Squeezing, camellia seed cold press squeeze out camellia oil, and press chamber temperature is 100 DEG C, and oil outlet temperature is 80 DEG C；
4）Filtering, camellia oil remove solid impurity by plate and frame filter press；
5）Coldization, camellia oil is cooled to -5 DEG C and preserves more than 30h, take upper strata camellia edible vegetable oil；
6）Distillation, distillation pressure are 10kPa, and evaporating temperature is 130 DEG C, keeps 30min, is then as little as condensed in the drop of pressure
Temperature is 20 DEG C, takes camellia oil liquid；
7）Refining, is heated to 150 DEG C by camellia oil liquid and keeps 5min, then cools to 120- DEG C, adds camellia edible vegetable oil weight
1% oyster shell whiting of amount, stirring reaction 50min, is subsequently cooled to normal temperature at 130 DEG C, filters off except oyster shell whiting；Described shellfish
Shell powder passes through for fresh shell is polished into powder, and 450-550 DEG C of temperature lower calcination 1-4h cools down obtained powder, and shell contains greatly
The calcium carbonate of amount and a small amount of chitin, and the decomposition temperature of calcium carbonate is 898 DEG C, can by the calcining of 450-550 DEG C of temperature
Structure is surrounded and watched with destroy shell, discharges micro calcium oxide and chitin so that oyster shell whiting has purification, thickening, antioxygen
The effect such as change；
8）Secondary coldization, camellia oil is cooled to -5 DEG C and preserves more than 30h, taken upper strata camellia edible vegetable oil, obtain camellia essential oil.
Embodiment two
Squeezing and the refinery practice of a kind of camellia oil are present embodiments provided, is comprised the following steps：
1）Shell, select the camellia fruit of maturation, ted and allow camellia fruit pericarp season crack, remove pericarp and obtain camellia seed, continue
The moisture content to camellia seed is tedded in 12-20%；
2）Heating, microwave heating, drying is carried out to camellia seed under environment under low pressure, heating-up temperature is 130 DEG C, aqueous to camellia seed
Measure as 4%, then naturally cool to normal temperature；Pressure is 60kPa, and microwave power is 1000-2000 watts；
3）Squeezing, camellia seed cold press squeeze out camellia oil, and press chamber temperature is 150 DEG C, and oil outlet temperature is 120 DEG C；
4）Filtering, camellia oil remove solid impurity by plate and frame filter press；
5）Coldization, camellia oil is cooled to 5 DEG C and preserves more than 30h, take upper strata camellia edible vegetable oil；
6）Distillation, distillation pressure are 60kPa, and evaporating temperature is 150 DEG C, keeps 30-50min, then in the drop of pressure as little as
Condensation temperature is 25 DEG C, takes camellia oil liquid；
7）Refining, is heated to 170 DEG C by camellia oil liquid and keeps 10min, then cools to 140 DEG C, adds camellia edible vegetable oil weight
5% oyster shell whiting of amount, stirring reaction 100min, is subsequently cooled to normal temperature at 150 DEG C, filters off except oyster shell whiting；Described shellfish
Shell powder passes through for fresh shell is polished into powder, and 450-550 DEG C of temperature lower calcination 1-4h cools down obtained powder, and shell contains greatly
The calcium carbonate of amount and a small amount of chitin, and the decomposition temperature of calcium carbonate is 898 DEG C, can by the calcining of 450-550 DEG C of temperature
Structure is surrounded and watched with destroy shell, discharges micro calcium oxide and chitin so that oyster shell whiting has purification, thickening, antioxygen
The effect such as change；
8）Secondary coldization, camellia oil is cooled to -5 DEG C and preserves more than 30h, taken upper strata camellia edible vegetable oil, obtain camellia essential oil.
Embodiment three
Squeezing and the refinery practice of a kind of camellia oil are present embodiments provided, is comprised the following steps：
1）Shell, select the camellia fruit of maturation, ted, allow camellia fruit pericarp season crack, remove pericarp and obtain camellia seed, continue
The moisture content to camellia seed is tedded in 12-20%；
2）Heating, microwave heating, drying is carried out to camellia seed under environment under low pressure, heating-up temperature is 110 DEG C, aqueous to camellia seed
Measure as 3%, then naturally cool to normal temperature；Pressure is 50kPa, and microwave power is 1000-2000 watts；
3）Squeezing, camellia seed cold press squeeze out camellia oil, and press chamber temperature is 130 DEG C, and oil outlet temperature is 100 DEG C；
4）Filtering, camellia oil remove solid impurity by plate and frame filter press；
5）Coldization, camellia oil is cooled to -3 DEG C and preserves more than 30h, take upper strata camellia edible vegetable oil；
6）Distillation, distillation pressure are 30kPa, and evaporating temperature is 140 DEG C, keeps 40min, is then as little as condensed in the drop of pressure
Temperature is 22 DEG C, takes camellia oil liquid；
7）Refining, is heated to 160 DEG C by camellia oil liquid and keeps 7min, then cools to 130 DEG C, adds camellia edible vegetable oil weight
3% oyster shell whiting, stirring reaction 80min, is subsequently cooled to normal temperature at 140 DEG C, filters off except oyster shell whiting；Described shell
Powder passes through for fresh shell is polished into powder, and 450-550 DEG C of temperature lower calcination 1-4h cools down obtained powder, and shell contains largely
Calcium carbonate and a small amount of chitin, and the decomposition temperature of calcium carbonate is 898 DEG C, can be with by the calcining of 450-550 DEG C of temperature
That destroys shell surrounds and watches structure, discharges micro calcium oxide and chitin so that oyster shell whiting has purification, thickens, be anti-oxidant
Deng effect；
8）Secondary coldization, camellia oil is cooled to -3 DEG C and preserves more than 30h, taken upper strata camellia edible vegetable oil, obtain camellia essential oil.
Example IV
The present embodiment and embodiment three are essentially identical, and different places are：The step 2 of manufacture craft）Camellia seed heating in
Add camellia seed weight 1-5% chaff shell.Chaff shell can decolourize to camellia oil, while contain a small amount of rice bran oil in chaff shell,
Camellia oil can be seasoned so that worth camellia essential oil taste is more sweet and dilitious.
Claims (4)
1. squeezing and the refinery practice of a kind of camellia oil, it is characterised in that comprise the following steps：
1）Shell, select the camellia fruit of maturation, ted, allow camellia fruit pericarp season crack, remove pericarp and obtain camellia seed, continue
The moisture content to camellia seed is tedded in 12-20%；
2）Heating, microwave heating, drying is carried out to above-mentioned camellia seed under environment under low pressure, heating-up temperature is 100-130 DEG C, to mountain
Tea seed water content is 2-4%, then naturally cools to normal temperature；
3）Squeezing, above-mentioned camellia seed cold press being squeezed out into camellia oil, press chamber temperature is 100~150 DEG C, oil outlet temperature is 80~
120℃；
4）Filtering, solid impurity is removed by above-mentioned camellia oil by plate and frame filter press；
5）Coldization, above-mentioned camellia oil is cooled to -5 DEG C~5 DEG C and preserves more than 30h, takes upper strata camellia edible vegetable oil；
6）Distillation, above-mentioned upper strata camellia edible vegetable oil is taken to distill, distillation pressure is 10-60kPa, and evaporating temperature is 130-150 DEG C, is kept
30-50min, it is then 20~25 DEG C in the drop of pressure as little as condensation temperature, takes camellia oil liquid；
7）Refining, is heated to 150-170 DEG C by above-mentioned camellia oil liquid and keeps 5-10min, then cool to 120-140 DEG C,
The 1-5% of camellia edible vegetable oil weight oyster shell whiting is added, stirring reaction 50-100min, is subsequently cooled to normal temperature at 130-150 DEG C,
Filter off and remove oyster shell whiting；
8）Secondary coldization, above-mentioned camellia oil is cooled to -5 DEG C~5 DEG C and preserves more than 30h, upper strata camellia edible vegetable oil is taken, obtains mountain
Tea essential oil.
2. squeezing and the refinery practice of camellia oil as claimed in claim 1, it is characterised in that：Described oyster shell whiting is new scallop
Shell 450-550 DEG C of temperature lower calcination 1-4h, cools down obtained powder by being polished into powder.
3. squeezing and the refinery practice of camellia oil as claimed in claim 1, it is characterised in that：Described step 2）The low pressure
Under environment, pressure 10-60kPa；The microwave heating, microwave power are 1000-2000 watts.
4. squeezing and the refinery practice of camellia oil as claimed in claim 1, it is characterised in that：Described step 2）Camellia seed
Camellia seed weight 1-5% chaff shell is added in heating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710507907.0A CN107446690B (en) | 2017-06-28 | 2017-06-28 | Pressing and refining process of camellia oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710507907.0A CN107446690B (en) | 2017-06-28 | 2017-06-28 | Pressing and refining process of camellia oil |
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| CN107446690A true CN107446690A (en) | 2017-12-08 |
| CN107446690B CN107446690B (en) | 2020-09-15 |
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| CN201710507907.0A Expired - Fee Related CN107446690B (en) | 2017-06-28 | 2017-06-28 | Pressing and refining process of camellia oil |
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Citations (5)
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|---|---|---|---|---|
| JP2009183267A (en) * | 2008-02-07 | 2009-08-20 | Takaoka Yoshio | Method for reducing acid value, deodorizing and washing for cooking oil, and apparatus to be used for the same |
| CN102504938A (en) * | 2011-11-08 | 2012-06-20 | 浙江省林业科学研究院 | Cold pressing and physical refining process of camellia oil |
| CN104611125A (en) * | 2015-01-07 | 2015-05-13 | 安徽省华银茶油有限公司 | Method for producing tea seed oil by tea seed shelling and cold-pressing |
| CN105273826A (en) * | 2015-10-26 | 2016-01-27 | 全椒县尹氏油脂有限公司 | Pressing method of black pearl sunflower seed oil |
| CN105985863A (en) * | 2014-10-17 | 2016-10-05 | 郭少海 | Winterization method of oil-tea camellia seed oil |
-
2017
- 2017-06-28 CN CN201710507907.0A patent/CN107446690B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009183267A (en) * | 2008-02-07 | 2009-08-20 | Takaoka Yoshio | Method for reducing acid value, deodorizing and washing for cooking oil, and apparatus to be used for the same |
| CN102504938A (en) * | 2011-11-08 | 2012-06-20 | 浙江省林业科学研究院 | Cold pressing and physical refining process of camellia oil |
| CN105985863A (en) * | 2014-10-17 | 2016-10-05 | 郭少海 | Winterization method of oil-tea camellia seed oil |
| CN104611125A (en) * | 2015-01-07 | 2015-05-13 | 安徽省华银茶油有限公司 | Method for producing tea seed oil by tea seed shelling and cold-pressing |
| CN105273826A (en) * | 2015-10-26 | 2016-01-27 | 全椒县尹氏油脂有限公司 | Pressing method of black pearl sunflower seed oil |
Non-Patent Citations (1)
| Title |
|---|
| 刘金勇等: "注射用油茶籽油中杂质控制的研究现状", 《粮油食品科技》 * |
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Effective date of registration: 20200806 Address after: 554300 maopo Camellia experimental station, Yuping Dong Autonomous County, Tongren City, Guizhou Province Applicant after: Guizhou Qianyu Camellia oleifera Development Co.,Ltd. Address before: 554000, No. 224, Ping Zhen Town, Yuping Dong Autonomous County, Tongren, Guizhou, Zhongshan Road Applicant before: YUPING DONG AUTONOMOUS COUNTY CAMELLIA OLEIFERA INDUSTRIAL DEVELOPMENT LEADING Group OFFICE |
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