CN107446667A - A kind of antifreezing oil - Google Patents

A kind of antifreezing oil Download PDF

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Publication number
CN107446667A
CN107446667A CN201710779247.1A CN201710779247A CN107446667A CN 107446667 A CN107446667 A CN 107446667A CN 201710779247 A CN201710779247 A CN 201710779247A CN 107446667 A CN107446667 A CN 107446667A
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CN
China
Prior art keywords
parts
oil
antifreezing
antifreezing oil
atoleine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710779247.1A
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Chinese (zh)
Inventor
徐加树
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NANTONG RUNDE MECHANICAL TECHNOLOGY Co Ltd
Original Assignee
NANTONG RUNDE MECHANICAL TECHNOLOGY Co Ltd
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Filing date
Publication date
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Priority to CN201710779247.1A priority Critical patent/CN107446667A/en
Publication of CN107446667A publication Critical patent/CN107446667A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085—Phosphorus oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/102—Silicates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022—Ethene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/024—Propene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C10M2215/064—Di- and triaryl amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
    • C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/36—Seal compatibility, e.g. with rubber

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The present invention relates to a kind of antifreezing oil, it is characterised in that：The antifreezing oil is made up of each component of following mass fraction：70 75 parts of machine oil, 23 parts of sorbierite, 23 parts of atoleine, 58 parts of alkyl phosphate, 0.2 0.3 parts of sulfide isobutene, 0.2 0.3 parts of BTA, 0.5 0.8 parts of di-iso-octyldiphenylamine；59 parts of sodium phosphite, 23 parts of tackifier, 47 parts of talcum powder, 0 13 parts of phosphatase 11,0.2 0.8 parts of oxidation and corrosion inhibitor；The antifreezing oil of the present invention can solve the problems, such as that existing antifreezing oil viscosity index (VI) is low, and antifreezing oil of the invention has good cooling, sealing, anti-corrosion, antifreeze, insulating effect to machinery equipment.Cooling, high lubricating effect, frictional force is small during use.

Description

A kind of antifreezing oil
Technical field
The present invention relates to mechanical lubrication field, more particularly to a kind of antifreezing oil.
Background technology
Antifreezing oil is used in automobile, in plant equipment to reduce friction, the liquid of protection machinery and workpiece or half Kollag, it is main to play lubrication, cooling, antifreeze, cleaning, sealing and buffering etc..Antifreezing oil is by base oil and adds Agent two parts are added to form, base oil is the main component of antifreezing oil, decides the fundamental property of antifreezing oil, additive The deficiency of base oil aspect of performance can be then made up and improved, assigns some new performances, is the important composition portion of antifreezing oil Point.
Viscosity index (VI) refers to the degree that oil viscosity varies with temperature, and viscosity index (VI) is higher, represents oil viscosity by temperature Influence it is smaller, its viscosity temperature characteristic is better, otherwise poorer；Viscosity index (VI) is the important indicator of antifreezing oil performance, therefore, such as What improves the viscosity index (VI) of antifreezing oil as the focus of current antifreezing oil research field.
Antifreezing oil is typically made up of base oil and additive two parts.Base oil be antifreezing oil it is main into Divide, decide the fundamental property of antifreezing oil, additive can then make up and improve the deficiency of base oil aspect of performance, assign certain A little new performances, it is the important component of antifreezing oil.Antifreezing oil is used in all kinds automobile, in plant equipment To reduce friction, mechanical and workpiece liquid or semisolid lubricants are protected, it is main to play lubrication, cool down, be antifreeze, clean, be close The effect such as envelope and buffering.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of antifreezing oil, solves existing antifreezing oil viscosity index (VI) The problem of low, cooling, high lubricating effect, frictional force is small during use.
In order to solve the above technical problems, the technical scheme is that：A kind of antifreezing oil, its innovative point are：Institute Antifreezing oil is stated to be made up of each component of following mass fraction：Machine oil 70-75 parts, sorbierite 2-3 parts, atoleine 2-3 parts, alkyl phosphate 5-8 parts, sulfide isobutene 0.2-0.3 parts, BTA 0.2-0.3 parts, diisooctyl Diphenylamines 0.5-0.8 parts；Sodium phosphite 5-9 parts, tackifier 2-3 parts, talcum powder 4-7 parts, phosphatase 11 0-13 parts, Oxidation and corrosion inhibitor 0.2-0.8 parts.
Further, the machine oil is I, II, III class base oil of the high viscosity index (HVI) that viscosity index (VI) is more than 100.
Further, the tackifier are polymethacrylates, polyacrylate, random polypropylene, ethylene-propylene copolymer In one kind or mixture.
Further, the preparation method of the antifreezing oil is specific as follows：
（1）The machine oil of formula ratio, sorbierite, atoleine, alkyl phosphate, sulfide isobutene are mixed, are heated to 50-55 DEG C, stir 30-35min；
（2）Remaining component of formula ratio is added, 15-20min is stirred, is cooled to room temperature, filters and produce.
The advantage of the invention is that：
1）The antifreezing oil of the present invention can solve the problems, such as that existing antifreezing oil viscosity index (VI) is low, antifreeze profit of the invention Lubricating oil has good cooling, sealing, anti-corrosion, antifreeze, insulating effect to machinery equipment.Cooling, high lubricating effect, rub during use It is small to wipe power.
Embodiment
The following examples can make professional and technical personnel that the present invention be more fully understood, but therefore not send out this It is bright to be limited among described scope of embodiments.
Embodiment 1：
Machine oil 70kg, sorbierite 2kg, the kg of atoleine 2, the kg of alkyl phosphate 5, the kg of sulfide isobutene 0.2, benzo The kg of triazole 0.2, the kg of di-iso-octyldiphenylamine 0.5；The kg of sodium phosphite 5, the kg of tackifier 2, the kg of talcum powder 4, phosphorus Acid 10 kg, the kg of oxidation and corrosion inhibitor 0.2；
The antifreezing oil preparation method of the present invention is as follows：
Machine oil 70kg, sorbierite 2kg, the kg of atoleine 2, the kg of alkyl phosphate 5, the kg of sulfide isobutene 0.2 are mixed Close, be heated to 50 DEG C；Stir 30min；
Add the kg of BTA 0.2, the kg of di-iso-octyldiphenylamine 0.5；The kg of sodium phosphite 5, the kg of tackifier 2 are sliding The kg of stone flour 4, the kg of phosphatase 11 0, the kg of oxidation and corrosion inhibitor 0.2；15min is stirred, room temperature is cooled to, filters and produce.
Embodiment 2：
Machine oil 72kg, sorbierite 2.5kg, atoleine 2.5kg, alkyl phosphate 7kg, sulfide isobutene 0.25kg, benzene And triazole 0.25kg, di-iso-octyldiphenylamine 0.7kg；Sodium phosphite 7kg, tackifier 2.5kg, talcum powder 6kg, phosphoric acid 12kg, oxidation and corrosion inhibitor 0.5kg.
The antifreezing oil preparation method of the present invention is as follows：
By machine oil 72kg, sorbierite 2.5kg, atoleine 2.5kg, alkyl phosphate 7kg, sulfide isobutene 0.25kg Mixing, is heated to 50 DEG C；Stir 30min；
Add BTA 0.25kg, di-iso-octyldiphenylamine 0.7kg；Sodium phosphite 7kg, tackifier 2.5kg, talcum Powder 6kg, phosphatase 11 2kg, oxidation and corrosion inhibitor 0.5kg；15min is stirred, room temperature is cooled to, filters and produce.
Embodiment 3：
Machine oil 75kg, sorbierite 3kg, atoleine 3kg, alkyl phosphate 8kg, sulfide isobutene 0.3kg, benzo three Nitrogen azoles 0.3kg, di-iso-octyldiphenylamine 0.8kg；Sodium phosphite 9kg, tackifier 3kg, talcum powder 7kg, phosphatase 11 3kg, resist Oxygen anti-corrosion additive 0.8kg.
The antifreezing oil preparation method of the present invention is as follows：
Machine oil 75kg, sorbierite 3kg, atoleine 3kg, alkyl phosphate 8kg, sulfide isobutene 0.3kg mixing, add Heat is to 55 DEG C；Stir 35min；
Add BTA 0.3kg, di-iso-octyldiphenylamine 0.8kg；Sodium phosphite 9kg, tackifier 3kg, talcum powder 7kg, phosphatase 11 3kg, oxidation and corrosion inhibitor 0.8kg；20min is stirred, room temperature is cooled to, filters and produce.
It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, above-described embodiment and explanation Merely illustrating the principles of the invention described in book, without departing from the spirit and scope of the present invention, the present invention also have Various changes and modifications, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention By appended claims and its equivalent thereof.

Claims (4)

  1. A kind of 1. antifreezing oil, it is characterised in that：The antifreezing oil is made up of each component of following mass fraction：Machine Oily 70-75 parts, sorbierite 2-3 parts, atoleine 2-3 parts, alkyl phosphate 5-8 parts, sulfide isobutene 0.2- 0.3 part, BTA 0.2-0.3 parts, di-iso-octyldiphenylamine 0.5-0.8 parts；Sodium phosphite 5-9 parts, tackifier 2-3 parts, talcum powder 4-7 parts, phosphatase 11 0-13 parts, oxidation and corrosion inhibitor 0.2-0.8 parts.
  2. A kind of 2. antifreezing oil according to claim 1, it is characterised in that：The machine oil be viscosity index (VI) for 100 with On high viscosity index (HVI) I, II, III class base oil.
  3. A kind of 3. antifreezing oil according to claim 1, it is characterised in that：The tackifier are polymethylacrylic acid One kind or mixture in ester, polyacrylate, random polypropylene, ethylene-propylene copolymer.
  4. A kind of 4. antifreezing oil according to claim 1, it is characterised in that：The preparation method of the antifreezing oil is specific It is as follows：
    （1）The machine oil of formula ratio, sorbierite, atoleine, alkyl phosphate, sulfide isobutene are mixed, are heated to 50-55 DEG C, stir 30-35min；
    （2）Remaining component of formula ratio is added, 15-20min is stirred, is cooled to room temperature, filters and produce.
CN201710779247.1A 2017-09-01 2017-09-01 A kind of antifreezing oil Pending CN107446667A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710779247.1A CN107446667A (en) 2017-09-01 2017-09-01 A kind of antifreezing oil

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Application Number Priority Date Filing Date Title
CN201710779247.1A CN107446667A (en) 2017-09-01 2017-09-01 A kind of antifreezing oil

Publications (1)

Publication Number Publication Date
CN107446667A true CN107446667A (en) 2017-12-08

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1904002A (en) * 2006-07-21 2007-01-31 宁波宁兴国贸实业有限公司 Antifreezing and lubricating injection agent
CN104830483A (en) * 2015-04-30 2015-08-12 柳州玲通科技有限责任公司 Fast-cooling lubricating oil and preparation method thereof
CN106811268A (en) * 2016-11-30 2017-06-09 河池市技术开发中心 A kind of lubricating oil for delaying mechanical wear

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1904002A (en) * 2006-07-21 2007-01-31 宁波宁兴国贸实业有限公司 Antifreezing and lubricating injection agent
CN104830483A (en) * 2015-04-30 2015-08-12 柳州玲通科技有限责任公司 Fast-cooling lubricating oil and preparation method thereof
CN106811268A (en) * 2016-11-30 2017-06-09 河池市技术开发中心 A kind of lubricating oil for delaying mechanical wear

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