CN107442189B - Easy rotten coal detects sample storage integrated unit - Google Patents
Easy rotten coal detects sample storage integrated unit Download PDFInfo
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- CN107442189B CN107442189B CN201710770715.9A CN201710770715A CN107442189B CN 107442189 B CN107442189 B CN 107442189B CN 201710770715 A CN201710770715 A CN 201710770715A CN 107442189 B CN107442189 B CN 107442189B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L3/00—Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
- B01L3/50—Containers for the purpose of retaining a material to be analysed, e.g. test tubes
- B01L3/508—Containers for the purpose of retaining a material to be analysed, e.g. test tubes rigid containers not provided for above
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
- B01L2200/06—Fluid handling related problems
- B01L2200/0689—Sealing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2200/00—Solutions for specific problems relating to chemical or physical laboratory apparatus
- B01L2200/16—Reagents, handling or storing thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L2300/00—Additional constructional details
- B01L2300/10—Means to control humidity and/or other gases
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W90/00—Enabling technologies or technologies with a potential or indirect contribution to greenhouse gas [GHG] emissions mitigation
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Abstract
The invention discloses a storage combination device for a perishable coal detection sample, which comprises: the device comprises an inflatable protective cylinder, a built-in sample storage barrel and an inert gas source; the inflatable protection cylinder comprises a shell, and an inner cavity is arranged in the shell; the bottom surface and the side wall of the inner cavity are uniformly provided with gas dispersion holes; a preset distance is reserved between the bottom surface and the side wall of the inner cavity and the inner surface of the shell; the top edge of the inner cavity is welded with the inner surface of the shell; the top of the shell is hermetically provided with a diffusing cover; the built-in sample storage barrel is arranged in the inner cavity; a gap is reserved between the built-in sample storage barrel and the inner cavity; the built-in sample storage barrel comprises a sample barrel body and a cover plate; the inert gas source is connected with the lower part of the shell through a gas transmission pipeline and is communicated with the cavity between the inner cavity and the shell; the gas transmission pipeline is provided with a gas regulating valve and a gas transmission pressure gauge. The device breaks through the bottleneck of scientific and effective preservation of the easily-deteriorated coal samples such as weak caking property and the like, and has wide use value and higher social benefit.
Description
Technical Field
The invention relates to the technical field of inspection and analysis, in particular to a coal deterioration easily detecting sample storage combined device.
Background
The relevant data show that the coke productivity and the coke yield in China all account for about 70 percent of the global proportion. However, from the general situation of the global and Chinese coking coal resources, the global coking coal resources only account for less than 30 percent, and the Chinese coking coal accounts for 26.3 percent of the resources/reserves. The proportion of coal for coking in resources/reserves in China is less, only accounts for 1/4, and half of the coal is gas coal, while the strongly bonded fat coal and coking coal only account for 1/3 of the coal for coking, the coal for coking is also influenced by harmful components such as ash, sulfur, phosphorus and the like and selectivity, and the coal for coking can really serve as coking coal blending in resources/reserves which is less than 1/2. In the process of using precious disposable and non-renewable energy for a long time in the industry, the ratio of the high-quality main coking coal and the rich coal of the metallurgical coke is over 60 percent for a long time under the constraint of a coking and coal blending theory and the pressure of stable operation of a blast furnace. 1 ton of coke is smelted, and about 1.4 tons of fine coking coal are needed. And at least 2 tons of raw coal with better washing performance are needed for 1 ton of coking clean coal. Face the pressure of exhaustion of resource consumption. Related experts point out that the reserve and the use speed of the coking coal source coking coal, fat coal and the like in 2014 can be supported for about 50 years. But the reserves of the weak caking coal in China are rich, the research of strengthening the comprehensive utilization of the weak caking coal is important and urgent, the weak caking coal with rich reserves and low price is fully utilized, the comprehensive coal blending cost of the coking coal is reduced, the disposable resource is protected, and the method has great economic value and far-reaching social benefit.
The research and application of the coal blending coking test on the weak caking coal are continuously strengthened from the world to China in recent years, the weak caking coal is easy to oxidize due to the characteristics of deterioration times and coal formation processes in the coal blending coking test process, the sample retention time has large influence on the properties of the coal, and important adverse effects are generated on the research of the coal blending test, so that the objectivity, reality and accuracy of test detection data are restricted, the properties of the weak caking coal and the effect of the weak caking coal in the coal blending coking are difficult to scientifically and accurately judge, the serious influence is caused on the whole coal blending of a coking plant, and the coke quality and the coking comprehensive cost are directly influenced. The scientific and effective preservation of the coal sample which is easy to deteriorate, such as weak caking property and the like, becomes the biggest bottleneck restricting the coal blending coking test, and the coking test has the significance and the effect of guiding the actual production only if the truth and the objectivity of the sample coal sample are ensured.
Disclosure of Invention
In order to solve the technical problems, the invention provides a storage combination device for easy-to-deteriorate coal detection samples.
The invention provides a perishable coal detection sample storage combination device, which comprises: the device comprises an inflatable protective cylinder, a built-in sample storage barrel and an inert gas source; wherein, the first and the second end of the pipe are connected with each other,
the inflatable protection cylinder comprises a shell, wherein an inner cavity is arranged in the shell; the bottom surface and the side wall of the inner cavity are uniformly provided with gas dispersion holes; a preset distance is reserved between the bottom surface and the side wall of the inner cavity and the inner surface of the shell; the top end edge of the inner cavity is welded with the inner surface of the shell; the top of the shell is hermetically provided with a diffusing cover;
the built-in sample storage barrel is arranged in the inner cavity; a gap is reserved between the built-in sample storage barrel and the inner cavity; the built-in sample storage barrel comprises a sample barrel body and a cover plate; the cover plate is arranged at the top of the sample cylinder body in a sealing manner;
the inert gas source is connected with the lower part of the shell through a gas transmission pipeline and is communicated with the cavity between the inner cavity and the shell; and the gas transmission pipeline is provided with a gas regulating valve and a gas transmission pressure gauge.
Furthermore, a first sealing clamping groove is formed in the outer edge of the top of the shell, and a first sealing strip matched with the first sealing clamping groove is arranged at the buckling edge of the diffusing cover; and a gas safety relief valve is arranged on the gas-filled protection cylinder relief cover.
Furthermore, a second sealing clamping groove is formed in the outer edge of the top of the sample cylinder body, and a second sealing strip matched with the second sealing clamping groove is arranged at the edge of the cover plate buckle.
Furthermore, a gap of 5-10 mm is reserved between the built-in sample storage barrel and the inner cavity.
Furthermore, the bottom of the shell that the inflatable protection barrel body includes is provided with universal gyro wheel.
Furthermore, a left taking and placing lifting lug and a right lifting and placing lug are arranged on the sample cylinder body with the built-in sample storage barrel; and a flexible connecting piece is connected between the left taking and placing lifting lug and the right lifting and placing lug.
Further, the device also comprises a manual hydraulic fetching and placing device; the manual hydraulic power taking and placing device comprises:
the bottom of the supporting base is provided with a movable universal wheel, and the top surface of the supporting base is fixed with a balance beam;
the hydraulic mechanism is arranged on the supporting base; the hydraulic mechanism includes: the hydraulic device comprises a hydraulic cylinder, a hydraulic rod which is sealed in the hydraulic cylinder in a sliding mode along the vertical direction, and an operation handrail connected with the bottom of the hydraulic cylinder; the control armrest is provided with a manual hydraulic oil filling valve and a pressure release valve;
a pick and place mechanism comprising: the taking and placing telescopic rod is arranged along the horizontal direction, and the telescopic chain is arranged along the vertical direction; one end of the taking and placing telescopic rod is connected with the tail end of the hydraulic rod through a connecting hinge, the other end of the taking and placing telescopic rod is connected with one end of a telescopic chain, and a hook for hooking the flexible connecting piece is arranged at the other end of the telescopic chain;
the counterweight mechanism is arranged on the supporting base and is positioned on the opposite side of the taking and placing telescopic rod; the counterweight mechanism includes: a balancing weight supporting rod arranged on the supporting base and a movable balancing weight arranged on the balancing weight supporting rod.
The invention provides a storage combination device for a coal sample easy to deteriorate, which is characterized in that an inner cavity is arranged in an inflatable protection cylinder, gas dispersion holes are uniformly distributed on the surface of the inner cavity, the inflatable protection cylinder keeps an inert gas environment with continuous and stable pressure, and a storage sample barrel is arranged in the inflatable protection cylinder, so that a coal sample easy to deteriorate, such as weak caking and the like, is arranged in the inert gas protection environment.
The storage combination device for the easy-to-deteriorate coal detection sample provided by the invention completely solves the problems that the property of the easy-to-deteriorate coal sample such as weak caking property is unstable and is easy to chemically change in an air environment so as to influence a coal blending coking test, and can scientifically and accurately judge the property of the easy-to-deteriorate coal such as weak caking property and the effect of the easy-to-deteriorate coal in coal blending coking, so that the real, objective, scientific and accurate coking coal blending experimental data are ensured, the coking production of a coking plant is powerfully guided, the basic conditions of scientific and accurate experimental data are provided for the scientific and effective easy-to-deteriorate coal such as weak caking property and the like, the bottleneck of scientific and effective storage of the easy-to-deteriorate coal sample such as weak caking property and the like is broken, the use value is wide, and positive social benefits are generated.
Drawings
FIG. 1 is a schematic structural diagram of a perishable coal detection sample storage combination device provided by the invention.
Fig. 2 is a schematic structural diagram of a manual hydraulic dispenser in the storage combination device for the easily rotten coal detection sample provided by the invention.
Description of the reference numerals:
1-inflating protection cylinder;
1-2-inner cavity;
1-3-gas diffusion holes;
1-4-a first sealed card slot;
1-5-a diffusing cover;
1-6-a first seal bar;
1-7-gas safety relief valve;
1-8-fastener of the diffusing cover;
1-9-a sample storage barrel is arranged in the sample storage barrel;
1-10-cover plate;
1-11-buckling of cover plate;
1-12 — a second seal bar;
1-13-second sealing neck;
1-14-picking and placing lifting lugs on the right;
1-15, taking and placing the lifting lug on the left;
1-16-gas line;
1-17-gas delivery pressure gauge;
1-18-gas regulating valve;
1-19-inert gas source;
1-20-universal rollers;
2-1-a support base;
2-operating the handrail;
2-3-manual hydraulic oil filling valve;
2-4-relief valve;
2-5-hydraulic cylinder;
2-6-hydraulic rod;
2-7-connecting hinges;
2-8, taking and placing the telescopic rod;
2-9-a telescopic chain;
2-10-hook;
2-11-balance beam;
2-12-movable counterweight block;
2-13-counterweight support rod;
2-14-moving universal wheel.
Detailed Description
In order that those skilled in the art will better understand the disclosure, the invention will be described in further detail with reference to the accompanying drawings and specific embodiments.
In a specific embodiment, the invention provides a storage integrated unit for a perishable coal detection sample. Referring to fig. 1, a schematic diagram of a storage complex for a perishable coal detection sample according to an embodiment of the present invention is shown.
The embodiment of the invention provides a storage combination device for a perishable coal detection sample, which comprises: the device comprises an air inflation protection cylinder body 1-1, a built-in sample storage barrel 1-9 and an inert gas source 1-19; wherein the content of the first and second substances,
the inflatable protection cylinder body 1-1 comprises a shell, and an inner cavity 1-2 is arranged in the shell; the bottom surface and the side wall of the inner cavity 1-2 are uniformly provided with gas dispersion holes 1-3; a preset distance is reserved between the bottom surface and the side wall of the inner cavity 1-2 and the inner surface of the shell so as to facilitate the uniform and continuous discharge of inert gas; the top end edge of the inner cavity 1-2 is welded with the inner surface of the shell; the top of the shell is hermetically provided with a diffusion cover 1-5 so as to form a closed cabin filled with inert gas in the inflatable protection cylinder 1-1;
the built-in sample storage barrel 1-9 is arranged in the inner cavity 1-2; a gap is reserved between the built-in sample storage barrel 1-9 and the inner cavity 1-2; the built-in sample storage barrel 1-9 comprises a sample barrel body and a cover plate 1-10; the cover plate 1-10 is hermetically arranged at the top of the sample cylinder body;
the inert gas source 1-19 is connected with the lower part of the shell through a gas pipeline 1-16 and is communicated with the cavity between the inner cavity 1-2 and the shell; and the gas transmission pipeline is provided with gas regulating valves 1-18 and gas transmission pressure gauges 1-17.
Furthermore, a first sealing clamping groove 1-4 is formed in the outer edge of the top of the shell, and a first sealing strip 1-6 matched with the first sealing clamping groove 1-4 is arranged at the edge of a buckle 1-8 of the diffusing cover; and a gas safety relief valve 1-7 is arranged on the relief cover 1-5 of the inflation protection cylinder body 1-1. When the gas pressure in the gas-filled protection cylinder body 1-1 exceeds a specified safety value, the gas safety relief valve 1-7 is automatically opened to release gas, and after the safety pressure is restored, the gas safety relief valve 1-7 is automatically closed.
Preferably, a second sealing clamping groove 1-13 is formed in the outer edge of the top of the sample cylinder body, and a second sealing strip 1-12 matched with the second sealing clamping groove 1-13 is arranged at the edge of a buckle 1-11 of the cover plate.
Furthermore, a gap of 5-10 mm is reserved between the built-in sample storage barrel 1-9 and the inner cavity 1-2.
For moving convenience, the bottom of the shell of the inflatable protection cylinder body 1-1 is preferably provided with universal rollers 1-20.
As the preferred scheme of the invention, a sample cylinder body of the built-in storage sample barrel 1-9 is provided with a left picking and placing lifting lug 1-15 and a right picking and placing lifting lug 1-14; and a flexible connecting piece is connected between the left taking and placing lifting lug 1-15 and the right lifting and placing lug 1-14.
Furthermore, the storage sample barrel 1-9 is arranged in the storage combination device for conveniently and quickly taking and placing the easy-to-deteriorate coal, and the easy-to-deteriorate coal detection sample storage combination device preferably further comprises a manual hydraulic taking and placing device; the manual hydraulic power taking and placing device comprises:
the bottom of the supporting base 2-1 is provided with a movable universal wheel 2-14, and the top surface of the supporting base is fixed with a balance beam 2-11;
the hydraulic mechanism is arranged on the supporting base 2-1; the hydraulic mechanism includes: the hydraulic device comprises a hydraulic cylinder 2-5, a hydraulic rod 2-6 sealed in the hydraulic cylinder 2-5 in a sliding mode in the vertical direction, and a control armrest 2-2 connected with the bottom of the hydraulic cylinder 2-5; the control armrest 2-2 is provided with a manual hydraulic oil filling valve 2-3 and a pressure release valve 2-4; the hydraulic cylinder 2-5 is arranged on the supporting base 2-1;
pick and place mechanism, it includes: the taking and placing telescopic rods 2-8 are arranged along the horizontal direction, and the telescopic chains 2-9 are arranged along the vertical direction; one end of the taking and placing telescopic rod 2-8 is connected with the tail end of the hydraulic rod 2-6 through a connecting hinge 2-7, the other end of the taking and placing telescopic rod is connected with one end of a telescopic chain 2-9, and a hook 2-10 for hooking the flexible connecting piece is arranged at the other end of the telescopic chain 2-9;
the counterweight mechanism is arranged on the supporting base 2-1 and is positioned at the opposite side of the taking and placing telescopic rod 2-8; the counterweight mechanism includes: a balancing weight support rod 2-13 arranged on the support base 2-1, and a movable balancing weight 2-12 arranged on the balancing weight support rod 2-13.
The invention further provides a storage combination device for a test sample of the easy-to-deteriorate coal, which is provided by the invention, by taking an example of storage and sample reservation of the easy-to-deteriorate coal sample with weak caking property and the like in a coal blending coking test.
The method comprises the steps of putting easily-deteriorated coal samples with weak caking property and the like to be reserved into a built-in storage sample barrel 1-9 according to the requirements of sample reserving operation rules, operating a manual hydraulic taking and placing device after a cover plate 1-10 is covered, moving to a proper position, holding a control handle 2-2 tightly, treading a manual hydraulic pressurizing valve 2-3, moving a hydraulic rod 2-6 to a proper position, putting down a telescopic chain 2-9, hooking a hook 2-10 on a right taking and placing lifting lug 1-14 and a left taking and placing lifting lug 1-15 on the built-in storage sample barrel 1-9 through a flexible connecting piece such as a binding rope, putting the flexible connecting piece into an air-filled protection barrel 1-1, covering a releasing cover 1-5, carefully checking devices such as an opening valve and a pressure gauge of a gas safety releasing valve 1-7, and ensuring the safe use of the gas safety releasing valve 1-7. And the manual hydraulic fetching and placing device is controlled to restore the original state and is placed at a fixed position.
Opening an inert gas source 1-19 to enter, opening a gas regulating valve 1-18, observing a gas transmission pressure gauge 1-17, entering an inner cavity 1-2 in the gas-filled protective cylinder 1-1 through a gas transmission pipeline 1-16, uniformly arranging and distributing gas dispersion holes 1-3 on the surface to fill inert gas in a cabin body, ensuring that the easy-to-deteriorate coal samples with weak caking property and the like to be stored are placed in an inert gas environment, preventing the easy-to-deteriorate coal samples with weak caking property and the like from being in contact with air to generate chemical change and influencing the properties of the easy-to-deteriorate coal samples with weak caking property and the like, and further causing serious deviation on the reality, objectivity, science and accuracy of coal blending coking test data.
The invention provides a storage combination device for a coal sample easy to deteriorate, which is characterized in that an inner cavity is arranged in an inflatable protection cylinder, gas dispersion holes are uniformly distributed on the surface of the inner cavity, the inflatable protection cylinder keeps an inert gas environment with continuous and stable pressure, and a storage sample barrel is arranged in the inflatable protection cylinder, so that a coal sample easy to deteriorate, such as weak caking and the like, is arranged in the inert gas protection environment.
The storage combination device for the easy-to-deteriorate coal detection sample provided by the invention completely solves the problems that the property of the easy-to-deteriorate coal sample such as weak caking property is unstable and is easy to chemically change in an air environment so as to influence a coal blending coking test, and can scientifically and accurately judge the property of the easy-to-deteriorate coal such as weak caking property and the effect of the easy-to-deteriorate coal in coal blending coking, so that the real, objective, scientific and accurate coking coal blending experimental data are ensured, the coking production of a coking plant is powerfully guided, the basic conditions of scientific and accurate experimental data are provided for the scientific and effective easy-to-deteriorate coal such as weak caking property and the like, the bottleneck of scientific and effective storage of the easy-to-deteriorate coal sample such as weak caking property and the like is broken, the use value is wide, and positive social benefits are generated.
The invention provides a storage combination device for a coal detection sample easy to deteriorate. The principles and embodiments of the present invention are explained herein using specific examples, which are presented only to assist in understanding the method and its core concepts. It should be noted that, for those skilled in the art, without departing from the principle of the present invention, it is possible to make various improvements and modifications to the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
Claims (3)
1. The utility model provides a yielding coal detects sample storage integrated unit which characterized in that includes: the device comprises an inflatable protective cylinder, a built-in sample storage barrel and an inert gas source; wherein the content of the first and second substances,
the inflatable protection cylinder comprises a shell, wherein an inner cavity is arranged in the shell; the bottom surface and the side wall of the inner cavity are uniformly provided with gas dispersion holes; a preset distance is reserved between the bottom surface and the side wall of the inner cavity and the inner surface of the shell; the top end edge of the inner cavity is welded with the inner surface of the shell; the top of the shell is hermetically provided with a diffusing cover;
the built-in sample storage barrel is arranged in the inner cavity; a gap is reserved between the built-in sample storage barrel and the inner cavity; the built-in sample storage barrel comprises a barrel body and a cover plate; the cover plate is arranged at the top of the barrel body in a sealing manner;
the inert gas source is connected with the lower part of the shell through a gas pipeline and is communicated with the cavity between the inner cavity and the shell; the gas transmission pipeline is provided with a gas regulating valve and a gas transmission pressure gauge;
a left taking and placing lifting lug and a right lifting and placing lug are arranged on the barrel body with the built-in sample storage barrel; a flexible connecting piece is connected between the left taking and placing lifting lug and the right lifting and placing lug;
the easy-to-deteriorate coal detection sample storage combined device further comprises a manual hydraulic taking and placing device; the manual hydraulic power taking and placing device comprises:
the bottom of the supporting base is provided with a movable universal wheel, and the top surface of the supporting base is fixed with a balance beam;
the hydraulic mechanism is arranged on the supporting base; the hydraulic mechanism includes: the hydraulic device comprises a hydraulic cylinder, a hydraulic rod which is sealed in the hydraulic cylinder in a sliding manner along the vertical direction, and an operation handrail which is connected with the bottom of the hydraulic cylinder; a manual hydraulic oil filling valve and a pressure release valve are arranged on the control handrail;
pick and place mechanism, it includes: the taking and placing telescopic rod is arranged along the horizontal direction, and the telescopic chain is arranged along the vertical direction; one end of the taking and placing telescopic rod is connected with the tail end of the hydraulic rod through a connecting hinge, the other end of the taking and placing telescopic rod is connected with one end of the telescopic chain, and the other end of the telescopic chain is provided with a hook for hooking the flexible connecting piece;
the counterweight mechanism is arranged on the supporting base and is positioned on the opposite side of the taking and placing telescopic rod; the counterweight mechanism includes: a balancing weight support rod arranged on the support base, and a movable balancing weight arranged on the balancing weight support rod;
a first sealing clamping groove is formed in the outer edge of the top of the shell, and a first sealing strip matched with the first sealing clamping groove is arranged at the edge of a buckle of the diffusing cover; a gas safety relief valve is arranged on a relief cover of the inflation protection cylinder;
the top outer edge of the barrel body is provided with a second sealing clamping groove, and the edge of the cover plate buckle is provided with a second sealing strip matched with the second sealing clamping groove.
2. The coal deterioration detection sample storage combination device as claimed in claim 1, wherein a gap of 5-10 mm is reserved between the internal storage sample barrel and the inner cavity.
3. The coal deterioration detecting sample storage combination device as claimed in claim 1, wherein the casing of the gas filled protection cylinder is provided with universal rollers at the bottom.
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