CN107442053A - A kind of intelligent response kettle - Google Patents
A kind of intelligent response kettle Download PDFInfo
- Publication number
- CN107442053A CN107442053A CN201710766952.8A CN201710766952A CN107442053A CN 107442053 A CN107442053 A CN 107442053A CN 201710766952 A CN201710766952 A CN 201710766952A CN 107442053 A CN107442053 A CN 107442053A
- Authority
- CN
- China
- Prior art keywords
- tank body
- chuck
- tank
- auxiliary material
- temperature control
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 230000004044 response Effects 0.000 title claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 56
- 230000036760 body temperature Effects 0.000 claims abstract description 19
- 238000009833 condensation Methods 0.000 claims abstract description 13
- 230000005494 condensation Effects 0.000 claims abstract description 13
- 238000010992 reflux Methods 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 9
- 239000002826 coolant Substances 0.000 claims abstract description 8
- 239000010865 sewage Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 239000000523 sample Substances 0.000 claims description 23
- 238000009826 distribution Methods 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 15
- 238000000576 coating method Methods 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 5
- 238000009434 installation Methods 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 230000008676 import Effects 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 abstract description 36
- 239000000498 cooling water Substances 0.000 abstract description 9
- 230000036632 reaction speed Effects 0.000 abstract description 4
- 230000006641 stabilisation Effects 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 description 11
- 210000003298 dental enamel Anatomy 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 230000001590 oxidative effect Effects 0.000 description 4
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 4
- 239000004810 polytetrafluoroethylene Substances 0.000 description 4
- 238000007086 side reaction Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- -1 conventional 304 Inorganic materials 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000003421 catalytic decomposition reaction Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 230000037452 priming Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 229910001200 Ferrotitanium Inorganic materials 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000009775 high-speed stirring Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000001546 nitrifying effect Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical compound FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/007—Aspects relating to the heat-exchange of the feed or outlet devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
- B01J2219/0006—Temperature measurement of the heat exchange medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
- B01J2219/00063—Temperature measurement of the reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0245—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of synthetic organic material
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
The invention discloses a kind of intelligent response kettle, agitating paddle is arranged on tank interior, variable-frequency motor is connected with agitating paddle, variable-frequency motor is also associated with frequency converter, sewage draining exit is arranged on tank base, condensation reflux unit connection is arranged on above tank body, chuck is arranged on the outside of tank body, cooling water inlet is connected to chuck bottom by magnetic valve, coolant outlet is arranged on chuck top, tank body temperature control system is connected with tank body, chuck temperature control system is connected with chuck, auxiliary material charging aperture is installed at the top of auxiliary material head tank, the bottom of auxiliary material head tank is connected by feed pipe with tank body, flowmeter is connected and installed with feed pipe.The present invention realizes that automatic stabilisation adds auxiliary material, meets that reaction system heats cooling demand, realizes that temperature of reaction system automatically controls, can effectively improve reaction speed, reduce material loss.
Description
Technical field
The present invention relates to chemical field, particularly a kind of intelligent response kettle.
Background technology
The broad understanding of reactor has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter
Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.Reactor be widely used in oil, chemical industry,
Rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying, hydrogenating, hydrocarbonylation, polymerization, the pressure of the technical process such as condensation
Force container.
Organic oxidizing reaction kettle using hydrogen peroxide as oxidant at present, structure is mainly by following characteristics：It is 1. usually used
Reactor material is enamel surfaces or the stainless steel material marked as 304,316L；What 2. enamel reaction still used is typically
Anchor Pattern agitating paddle, motor and agitating shaft are connected using the reductor of fixed rotating speed；3. the drain of reactor does not connect cold
Condenser；4. reactor charging uses delivery pump, interval is added in reactor from the conveying of auxiliary material storage tank during the course of the reaction；It is 5. anti-
It is conduction oil to answer the heat transfer medium in kettle chuck, without supporting cooling system.The shortcomings that said structure causes be mainly：（1）
The surfacing of enamel still is easily corroded in reaction system, causes reactor service life short, usually used less than 1 year,
Enamel shows the Durchgangshohle that will be corroded, and exposes baslled iron layer；（2）Enamel still or stainless steel（Including conventional 304,316L, titanium steel
Deng）Surfacing can not only be catalyzed the generation of side reaction, and be catalyzed the decomposition of major auxiliary burden, cause auxiliary material to be lost
The problems such as amount is big, the impurity of side reaction generation is more；（3）The stirring of enamel still is usually anchor formula stirring, and mixing speed compares
Slowly, it is poor to the two-phase dispersion mixing of reaction system；（4）Reactor drain does not have condensation reflux unit, part
Raw material meeting volatilization loss, not only causes the loss of raw material, and surrounding enviroment can be polluted；（5）Auxiliary material addition is not square
Just measure；（6）Add the poor continuity of auxiliary material and the bad control of flow；（7）Cause temperature of reaction system not because charging is unstable
It is stable, so as to influence reaction system stability；（8）Course of reaction system heat release elevates the temperature, it is difficult to which control is in technological requirement
In the range of.
So how reactor automatically and steadily adds auxiliary material, meets that reaction system heats cooling demand, can effectively carry
High reaction speed, reaction loss is reduced, turning into urgent problem in production process turns into what urgent need in production process solved
Problem.
The content of the invention
It is an object of the invention to provide a kind of reactor, realizes that automatic stabilisation adds auxiliary material, meets that reaction system heats
Cooling demand, realize that temperature of reaction system automatically controls, reaction speed can be effectively improved, reduce material loss.
To achieve the above object, kind intelligent response kettle of the invention, including tank body, agitating paddle, frequency converter, variable-frequency motor,
Sewage draining exit, condensation reflux unit, chuck, cooling water inlet, coolant outlet, magnetic valve, tank body temperature control system, chuck temperature control system
System, auxiliary material head tank, flowmeter and feed pipe, the agitating paddle are arranged on tank interior, and variable-frequency motor is connected with agitating paddle, become
Frequency motor is also associated with frequency converter, and sewage draining exit is arranged on tank base, and the condensation reflux unit connection is arranged on above tank body,
The chuck is arranged on the outside of tank body, and cooling water inlet is connected to chuck bottom by magnetic valve, and coolant outlet is arranged on folder
Top is covered, the tank body temperature control system is connected with tank body, and chuck temperature control system is connected with chuck, the top of the auxiliary material head tank
Auxiliary material charging aperture is installed, the bottom of auxiliary material head tank is connected by feed pipe with tank body, and flow is connected and installed with feed pipe
Meter.
Further, the condensation reflux unit includes steam pipe, condenser, drain tank, oil water separator and return duct,
The condenser is connected at the top of tank body by steam pipe, and condenser is connected by pipeline with drain tank, and drain tank passes through pipeline
It is connected with oil water separator, oil water separator is by return duct with being connected at the top of tank body.
Further, the tank body temperature control system include tank body digital display temperature-control distribution box, tank body temperature probe, magnetic valve,
Cooling water inlet and coolant outlet, tank body temperature probe are arranged on tank interior, the connection of tank body digital display temperature-control distribution box one end
Tank body temperature probe, other end connection magnetic valve.
Further, the chuck temperature control system includes chuck digital display temperature-control distribution box, chuck temperature probe and heating tube,
Chuck temperature probe and heating tube are arranged on inside chuck, chuck digital display temperature-control distribution box one end connection chuck temperature probe, another
One end connects heating tube.
Further, the tank inner surface spraying polytetrafluorethylecoatings coatings.
Further, the agitating paddle surface spraying polytetrafluorethylecoatings coatings.
Further, the oil water separator, which is also installed, is connected with drainpipe and blow-off pipe, and the return duct is connected to oil
Separator top, drainpipe are inserted into bottom, drain pipe port less than the backflow mouth of pipe, blow-off pipe connection by oil water separator top
In oil water separator bottom.
Further, it is provided with evacuation port at the top of the drain tank.
The substantive distinguishing features of the present invention and progress are：
The reactor of the application, available for the organic oxidizing reaction system using hydrogen peroxide as oxidant, there is advantages below：
（1）Agitating paddle is driven using the variable-frequency motor of adjustable speed, effectively improves reaction speed.Stirring at low speed, which feeds intake, is advantageous to maximum
Degree protects agitating paddle to be damaged caused by being collided from undissolved solid material, and course of reaction high-speed stirred makes in reaction system
The fully dispersed mixing of two phase materials, improve reaction rate.
（2）By the design of condensation reflux unit, the material loss in course of reaction is effectively reduced.Raw material in course of reaction
Volatilization can cause to be lost, the raw material for making volatilization by condenser is condensed, then by oil water separator by raw material and moisture
After being separated, raw material is again introduced into tank body reaction, moisture discharge.
（3）In tank inner surface, agitating paddle surface spraying polytetrafluorethylecoatings coatings, auxiliary material loss is reduced, improves target production
Thing conversion ratio, extend the service life of reactor.Polytetrafluoroethylene (PTFE) is to be currently known the extremely stable macromolecule material of chemical property
Material, will not be increased the service life in this reaction system by material corrosion.Applied in carbon steel reactor internal spray polytetrafluoroethylene (PTFE)
It layer, can not only reduce auxiliary material catalytic decomposition loss, and the impurity introduced by side reaction is greatly reduced, improve target production
The conversion ratio of thing, facilitate the separating-purifying in later stage.
（4）The auxiliary material charging aperture of auxiliary material head tank installation is connected with delivery pump, the charging that auxiliary material head tank is connected with tank body
Pipe is provided with flowmeter：1. it can accurately measure the addition total amount of auxiliary material, it is ensured that the stability of technique；2. can be auxiliary with default control
The addition flow of material, it is ensured that auxiliary material automatic stabilisation adds；3. the auxiliary material needed for a batch can be filled, it is not necessary to which repeated priming is auxiliary
Material conveying pump.
（5）By the design of chuck, tank body temperature control system and chuck temperature control system, reactant in reactor can be met simultaneously
System's heating, the demand of cooling.Realize that temperature of reaction system automatically controls, effectively improve reaction efficiency, reduce production cost, energy-conservation
Consumption reduction, reduce the impurity that side reaction is brought.
Brief description of the drawings
Fig. 1 is the main structure diagram of the present invention.
Component serial number and title in figure：
Auxiliary material charging aperture 1, auxiliary material head tank 2, coolant outlet 3, agitating paddle 4, tank body 5, tank body temperature probe 6, tank body digital display
Temperature control distribution box 7, sewage draining exit 8, cooling water inlet 9, magnetic valve 10, chuck 11, heating tube 12, chuck digital display temperature-control distribution box
13rd, chuck temperature probe 14, return duct 15, blow-off pipe 16, drainpipe 17, oil water separator 18, drain tank 19, evacuation port 20,
Condenser 21, steam pipe 22, variable-frequency motor 23, frequency converter 24, feed pipe 25, flowmeter 26.
Embodiment
Below in conjunction with the implementation structure ＆ working mechanism of the accompanying drawing description present invention.
Referring to shown in Fig. 1, reactor of the invention, agitating paddle 4 is arranged on inside tank body 5, variable-frequency motor 23 and agitating paddle 4
Connection, variable-frequency motor 23 are also associated with frequency converter 24.Speed governing can be carried out to variable-frequency motor 23 by frequency converter 24, stirring at low speed is thrown
Material is advantageous at utmost protect agitating paddle 4 to damage caused by colliding from undissolved solid material, course of reaction high-speed stirring
Mixing makes the fully dispersed mixing of two phase materials in reaction system, improves reaction rate.The inner surface of tank body 5, the surface spraying of agitating paddle 4 gather
Tetrafluoroethene coating, tank body 5 and agitating paddle 4 is set by material corrosion, not to reduce the catalytic decomposition loss of auxiliary material.
Condensation reflux unit connection is arranged on the top of tank body 5, and condensation reflux unit includes steam pipe 22, condenser 21, row
Slack tank 19, oil water separator 18 and return duct 15.Condenser 21 is connected to the top of tank body 5 by steam pipe 22, and condenser 21 is logical
Piping is connected with drain tank 19, and drain tank 19 is connected by pipeline with oil water separator 18, and oil water separator 18 passes through backflow
Pipe 15 is connected with the top of tank body 5.Return duct 15 is connected to the top of oil water separator 18, and drainpipe 17 is by the top of oil water separator 18
Be inserted into bottom, 17 mouthfuls of drainpipe is less than 15 mouthfuls of return duct, blow-off pipe 16 is connected to the bottom of oil water separator 18.Course of reaction
In, raw material has volatilization loss, is reduced and is lost by condensation reflux unit.After volatility of raw material, entered by steam pipe 22 and condensed
Device 21 carries out cooling and is condensed into liquid, and liquid is flowed into oil water separator 18 by pipeline, drain tank 19.Liquid is in water-oil separating
By density difference in device 18, raw material and moisture are separated, material density it is small in upper, moisture density greatly under, raw material leads to
The return duct 15 for crossing the top of oil water separator 18 is back to tank body 5 and continues to react, and moisture is discharged by the drainpipe 17 of bottom.It is cold
The design of solidifying reflux greatly reduces the loss of raw material in course of reaction.
The top of drain tank 19 is provided with evacuation port 20, reactor is communicated with air, allows the pressure of reactor whole system
Power is under atmospheric pressure, without malleation or negative pressure.
The bottom of tank body 5 is provided with sewage draining exit 8, and the bottom of oil water separator 18 is connected with blow-off pipe 16, be easy to tank body 5,
The cleaning of oil water separator 18, blowdown is carried out by sewage draining exit 8, blow-off pipe 16 after cleaning.
The top of auxiliary material head tank 2 is provided with auxiliary material charging aperture 1, and auxiliary material charging aperture 1 is connected with delivery pump.Auxiliary material head tank
2 bottom is connected by feed pipe 25 with tank body 5, and flowmeter 26 is connected and installed with feed pipe 25.Auxiliary material head tank 2 is by defeated
Pump is sent disposably to add the auxiliary material needed for a batch by auxiliary material charging aperture 1, it is no longer necessary to repeated priming auxiliary material delivery pump.It is logical
The addition total amount of auxiliary material can accurately be measured by crossing the graduation mark that auxiliary material head tank 2 carries, it is ensured that the stability of technique, while can be with
Pass through the addition flow of the default control auxiliary material of flowmeter 26, it is ensured that auxiliary material automatic stabilisation adds, and ensures the stability of reaction system.
Chuck 11 is arranged on the outside of tank body 5, and cooling water inlet 9 is connected to the bottom of chuck 11, cooling water by magnetic valve 10
Outlet 3 is arranged on the top of chuck 11, and tank body temperature control system is connected with tank body 5, and chuck temperature control system is connected with chuck 11.Tank body is surveyed
Temperature probe 6 is arranged on inside tank body 5, the one end of tank body digital display temperature-control distribution box 7 connection tank body temperature probe 6, other end connection electricity
Magnet valve 10.Tank body temperature probe 6 is arranged on inside tank body 5, monitors temperature of reaction system at any time.Tank body temperature probe 6 detects
Temperature raises, and when reaching setting value, tank body digital display temperature-control distribution box 7 can automatically control magnetic valve 10 and open, and water enters from cooling water
Mouth 9 flows into chucks 11, and tank body 5 is cooled.Tank body temperature probe 6 detects temperature reduction, during less than setting value, tank body number
Temperature display control distribution box 7 can automatically control magnetic valve 10 and close, and cooling water stops entering chuck 11.
Chuck temperature probe 14 and heating tube 11 are arranged on inside chuck 11, the connection of the one end of chuck digital display temperature-control distribution box 13
Chuck temperature probe 14, other end connection heating tube 11.Front half section is reacted, system requirement temperature is higher, it is necessary to be situated between in chuck 11
Matter temperature is higher than 10 DEG C -20 DEG C of liquid temperature in tank body 5, to ensure being normally carried out for reaction.Chuck temperature probe 14 detects chuck
When interior coolant-temperature gage is less than setting value, the control of chuck digital display temperature-control distribution box 13 starts heating tube 11 and the water in chuck 11 is carried out
Heating.The reaction second half section, chuck temperature probe 14 detected that the coolant-temperature gage in chuck 11 is high, it is necessary to cool to reaction system
When setting value, chuck digital display temperature-control distribution box 13 controls heating tube 11 to stop heating.
Claims (8)
- A kind of 1. intelligent response kettle, it is characterised in that：Including tank body（5）, agitating paddle（4）, frequency converter（24）, variable-frequency motor （23）, sewage draining exit（8）, condensation reflux unit, chuck（11）, cooling book import（9）, coolant outlet（3）, magnetic valve（10）、 Tank body temperature control system, chuck temperature control system, auxiliary material head tank（2）, flowmeter（26）And feed pipe（25）, the agitating paddle（4） Installed in tank body（5）Inside, variable-frequency motor（23）With agitating paddle（4）Connection, variable-frequency motor（23）It is also associated with frequency converter（24）, Sewage draining exit（8）Installed in tank body（5）Bottom, the condensation reflux unit connection are arranged on tank body（5）Top, the chuck（11） Installed in tank body（5）Outside, cool down book import（9）Pass through magnetic valve（10）It is connected to chuck（11）Bottom, coolant outlet（3） Installed in chuck（11）Top, the tank body temperature control system and tank body（5）Connection, chuck temperature control system and chuck（11）Connection, The auxiliary material head tank（2）Top auxiliary material charging aperture is installed（1）, auxiliary material head tank（2）Bottom pass through feed pipe（25） With tank body（5）Connection, feed pipe（25）On be connected and installed with flowmeter（26）.
- 2. intelligent response kettle according to claim 1, it is characterised in that：The condensation reflux unit includes steam pipe （22）, condenser（21）, drain tank（19）, oil water separator（18）And return duct（15）, the condenser（21）Pass through steam Pipe（22）It is connected to tank body（5）Top, condenser（21）Pass through pipeline and drain tank（19）Connection, drain tank（19）Pass through pipeline With oil water separator（18）Connection, oil water separator（18）Pass through return duct（15）With tank body（5）Top connects.
- 3. intelligent response kettle according to claim 1, it is characterised in that：The tank body temperature control system includes tank body digital display temperature Control distribution box（7）, tank body temperature probe（6）, magnetic valve（10）, cooling book import（9）And coolant outlet（3）, tank body thermometric Probe（6）Installed in tank body（5）Inside, tank body digital display temperature-control distribution box（7）One end connects tank body temperature probe（6）, the other end Connect magnetic valve（10）.
- 4. intelligent response kettle according to claim 1, it is characterised in that：The chuck temperature control system includes chuck digital display temperature Control distribution box（13）, chuck temperature probe（14）And heating tube（12）, chuck temperature probe（14）And heating tube（12）It is arranged on Chuck（11）Inside, chuck digital display temperature-control distribution box（13）One end connects chuck temperature probe（14）, the other end connection heating tube （12）.
- 5. intelligent response kettle according to claim 1, it is characterised in that：The tank body（5）Inner surface sprays polytetrafluoroethyl-ne Ene coatings.
- 6. intelligent response kettle according to claim 1, it is characterised in that：The agitating paddle（4）Surface spraying polytetrafluoroethyl-ne Ene coatings.
- 7. intelligent response kettle according to claim 2, it is characterised in that：The oil water separator（18）Also installation is connected with Drainpipe（17）And blow-off pipe（16）, the return duct（15）It is connected to oil water separator（18）Top, drainpipe（17）By oil Separator（18）Top is inserted into bottom, drainpipe（17）Mouth is less than return duct（15）Mouthful, blow-off pipe（16）It is connected to profit Separator（18）Bottom.
- 8. intelligent response kettle according to claim 2, it is characterised in that：The drain tank（19）Top be provided with emptying Mouthful（20）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710766952.8A CN107442053A (en) | 2017-08-31 | 2017-08-31 | A kind of intelligent response kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710766952.8A CN107442053A (en) | 2017-08-31 | 2017-08-31 | A kind of intelligent response kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107442053A true CN107442053A (en) | 2017-12-08 |
Family
ID=60494698
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710766952.8A Pending CN107442053A (en) | 2017-08-31 | 2017-08-31 | A kind of intelligent response kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107442053A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108261997A (en) * | 2018-03-28 | 2018-07-10 | 梧州黄埔化工药业有限公司 | A kind of temprature control method of camphor production and its isomery pot |
| CN114984898A (en) * | 2022-07-15 | 2022-09-02 | 常州市明珠干燥设备有限公司 | Temperature-controllable reaction kettle for lithium battery material |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050042155A1 (en) * | 2003-08-21 | 2005-02-24 | Duane Powell | Apparatus for synthesizing an oxidant |
| CN202369396U (en) * | 2011-12-15 | 2012-08-08 | 湖北泰盛化工有限公司 | Hydraulic phosphorus adding device |
| CN103045368A (en) * | 2012-09-08 | 2013-04-17 | 新疆新维制药厂 | Closed-type vacuum reflux extraction device |
| CN203695056U (en) * | 2014-02-17 | 2014-07-09 | 山东邹平大展新材料有限公司 | Wax emulsion production equipment |
| CN204338160U (en) * | 2014-12-26 | 2015-05-20 | 山东易达利化工有限公司 | Batch tank reactor |
| CN105233778A (en) * | 2015-10-23 | 2016-01-13 | 费正华 | Multifunctional reaction kettle |
| CN207204093U (en) * | 2017-08-31 | 2018-04-10 | 南宁辰康生物科技有限公司 | A kind of intelligent response kettle |
-
2017
- 2017-08-31 CN CN201710766952.8A patent/CN107442053A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050042155A1 (en) * | 2003-08-21 | 2005-02-24 | Duane Powell | Apparatus for synthesizing an oxidant |
| CN202369396U (en) * | 2011-12-15 | 2012-08-08 | 湖北泰盛化工有限公司 | Hydraulic phosphorus adding device |
| CN103045368A (en) * | 2012-09-08 | 2013-04-17 | 新疆新维制药厂 | Closed-type vacuum reflux extraction device |
| CN203695056U (en) * | 2014-02-17 | 2014-07-09 | 山东邹平大展新材料有限公司 | Wax emulsion production equipment |
| CN204338160U (en) * | 2014-12-26 | 2015-05-20 | 山东易达利化工有限公司 | Batch tank reactor |
| CN105233778A (en) * | 2015-10-23 | 2016-01-13 | 费正华 | Multifunctional reaction kettle |
| CN207204093U (en) * | 2017-08-31 | 2018-04-10 | 南宁辰康生物科技有限公司 | A kind of intelligent response kettle |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108261997A (en) * | 2018-03-28 | 2018-07-10 | 梧州黄埔化工药业有限公司 | A kind of temprature control method of camphor production and its isomery pot |
| CN114984898A (en) * | 2022-07-15 | 2022-09-02 | 常州市明珠干燥设备有限公司 | Temperature-controllable reaction kettle for lithium battery material |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN201470388U (en) | Reaction vessel with jacket | |
| CN203990582U (en) | A kind of controllable temperature heating reactor | |
| CN107442053A (en) | A kind of intelligent response kettle | |
| CN207204093U (en) | A kind of intelligent response kettle | |
| CN209005700U (en) | A kind of polytetramethylene ether diol specialty polymeric reaction kettle | |
| CN210382583U (en) | Molasses adding system of conditioner | |
| CN202876812U (en) | Reaction kettle for producing petrochemical products | |
| CN201921686U (en) | Reaction kettle | |
| CN206731104U (en) | Leather with temperature control equipment polyurethane resin agitator tank | |
| CN207872144U (en) | A kind of reaction unit being used to prepare big proportion and bulky grain crystal | |
| CN211411966U (en) | Reaction type film-forming auxiliary agent reaction tank | |
| CN105688789A (en) | Reaction kettle for synthesizing scale and corrosion inhibitor from allantoin production effluent | |
| CN209173872U (en) | Spiral diversion double-layered stirs lower bucket | |
| CN202921313U (en) | Reaction kettle | |
| CN207204094U (en) | A kind of energy-conservation reactor for being automatically added to auxiliary material | |
| CN213314999U (en) | Hydroxyl ether reaction kettle | |
| CN207210001U (en) | A kind of microbubble heater | |
| CN206996549U (en) | A kind of bitumen blowing reactor | |
| CN213590442U (en) | Chemical industry reation kettle's heat abstractor | |
| CN219186901U (en) | Oxalic ester synthesizing device | |
| CN201431882Y (en) | Spray polymerization kettle with regulating valve | |
| CN214716462U (en) | Reaction device | |
| CN217725559U (en) | Reaction unit is used in production of sulfur-resistant corrosion inhibitor | |
| CN207430278U (en) | The reaction kettle that a kind of reaction speed is fast, loss is small | |
| CN210846357U (en) | Constant-temperature waterborne polyurethane reaction kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171208 |
|
| WD01 | Invention patent application deemed withdrawn after publication |